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A-10-1-17-9b6d246

A-10-1-17-9b6d246

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Published by Flavio Bernardotti

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Published by: Flavio Bernardotti on Sep 01, 2012
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09/01/2012

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J. of Nuclear Sci. and Tech.
 5067-631388 
No. 50, pp. 63-67, 2010
Short Paper
-99 -
m
99 
...
*
 
ﮋﭘ
 
 ﮕ ﮋﭘ
 
 ﭘ
 :3486-11365- 
 ﭼ
:
 -99- )
4
MoO
2
Na
:
2
ZrO
/
2
SiO
(. -
m
99 
 ﮔ 
 . -
m
99 
 ﭘ 
 . -99  .-
m
99 9
/
0% 
 
 ﮔ 
. .
 
 m
99 99 
 ﮔ  
 
Silica-Gel Modified with Zirconium Oxide as a Novel
99
Mo Adsorbentin
99m
Tc Generators
H. Salehi*, E. Mollarazi, H. Abbasi
 
Nuclear Science Research School, Nuclear Science and Technology Research Institute, AEOI, P.O. Box: 11365-3486, Tehran-Iran
Abstract:
 
A new
99
Mo adsorbent has been prepared with modified silica gel with zirconium oxide(SiO
2
 /ZrO
2
:Na
2
MoO
4
) and used in technetium-99m generator. The adsorption behaviors of 
99
Mo in theform of molybdate and
99m
Tc in the form of pertechnetate on the new adsorbent was investigated showedthat the adsorption capacity of molybdate on this generator was considerably higher than the usualgenerator with alumina column. Coating zirconium oxide on the surface of silica gel resulted in higher
99
Mo adsorption of this compound.
99m
Tc is eluted with 0.9% NaCl, and the radionuclidic, radiochemicaland chemical purities of the eluate were checked. This generator has a great potential as compared to thetraditional alumina generators.
 Keywords:
Technetium-99m Generator, Molybdenium-99, Chromatography, Zirconium Oxides
:6/6/87
 ﭘ 
 :19/9/88 
hsalehi@aeoi.org.ir*email:
 
 
 . . . 
1- 
 ﭘ 
 - 
ﮋ 
 
 ﭘ 
 
]
1
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. 
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)1(
 
]
2 3
[
. - 
 ﮔ 
 
 ﮔ 
 
 ﮔ 
 
 ﮔ 
 
 ﭘ  ﮔ 
 100 
keV
300. - 
 ﮔ 
 
 ﮔ  ﭘ 
.-- .-
 ﭘ 
 
 ﮔ 
 
 ﮔ 
. 
 ﭙ 
 
 ﮔ 
 
 ﮔ 
 )
h
0
/
13(
I
123
,
)
h
0
/
6(
m
Tc
99
,
)
s
0
 / 
13(
m
Kr
81
,
)
d
0
/
8(
I
131
 
)
h
3
/
78(
Ga
67
,
)
h
0
/
73(
Tl
201
,
)
h
9
/
68(
In
111
,
)
h
0
/
57(
Br
77
 
]
4
[
.-
m
99 
ﮋ 
 
 ﭼ
- )6 (
 ﮔ  ﭘ  ﮔ 
 
 ﭘ 
)
keV
140(
 ﮔ 
 -99 
 
 ﭘ 
 . -99/-
m
99 -
m
99
 ﭘ 
 
 ﭘ 
 . 
 ﭼ
 -99  - 
 ﮔ 
 .-99  . 4  :
 ﭼ
 
7
O
2
Tc
 
 ﮔ 
 
 ﮔ 
 
 ﮔ 
 
 ﭘ 
 
 ﮔ 
 . 
 ﮔ 
 
 ﭼ
 
]
5
[]
6
[
 ﮕ 
]
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Tc
99
 
)2(
 
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]
8
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. 
)3(
 
 ﭘ 
 
 ﮕ 
 
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]
9
[
. 
 ﮕ 
 
 
 501388 
-
m
99. 
 ﭼ
-
m
99 
 ﭼ
 -99 
 ﭼ
 -
m
99)
 ﭼ
 ( . 
 ﭘ 
 -
m
99 .  . . -99 -
m
99 . 
2- 
1 
)35-40( 
 ﭘ 
30% )
III
( -99 
IRE
. 
 
]
10
[
 6 100 
 ﮔ 
 
 ﮔ 
 .
 ﭙ 
5
 ﮔ 
 63
/
1 
 ﮔ 
 
O (IV)
2
H
8
.
2
ZrOCl
30 . 6 
 ﭘ 
 
 ﮔ 
 50 )25
×
2 ( 100 
 ﮔ 
. 
 99  
 /ZrO
SiO
(   
2
/
0 
 ﭘ 
 
 ﮕ 
 1
/
0 )( 
pH
 5
/
4. 
 ﭙ 
 
 ﮔ 
 )1.( 
 ﮔ 
 
 ﮔ 
 -99 )  6 6
/
0 ( 
 ﭘ 
 1 
 ﮔ 
 
 ﮔ 
 . 7  9
/
0%)( )  24 ( -
m
99 -99 
 ﮕ 
 
Capintec ARC-120
 ﮔ 
. 
3- 
 ﮔ 
]
11
[
 
2SiOH + ZrOCl
2
+ H
2
O (SiO)
2
Zr (OH)
2
+ 2HCl
1-
 -
m
99 
(SZCG)
 
(ACG)
. 
m
Tc
99
 ) 
 ﮕ ﮔ 
( -99 (%)
**
 (%)
**
 
m
Tc
99
 )(
*SZCG
 
ACG
 
SZCG
 
ACG
 
SZCGACG
5
/
9 08
/
4 )5
/
110( 55
/
3 )2
/
96( 44
/
4 )2
/
120( 
4-
10×1
/
1 
3-
10×1 92 80  5
/
33 86
/
4 )2
/
82( 21
/
4 )3
/
69( 47
/
5 )4
/
89( 
4-
10×5
/
0 
3-
10×1 89 77  5
/
57 95
/
3 )5
/
22( 3
/
3 )8
/
18( 25
/
4 )6
/
25( 
4-
10×5
/
0 
3-
10×5
/
1 93 77  5
/
81 03
/
3 )7
/
13( 56
/
2 )6
/
11( 3
/
3 )3
/
15( 
4-
10×1 
3-
10×3 92 77  5
/
177 )11
/
1( )5
/
110( )98
/
0( )2
/
96( )2
/
1( )2
/
120( 
4-
10×1 
3-
10×2 93 81  5
/
201 )82
/
0( )107(  )7
/
0( )3
/
89( )94
/
0( )115( 
4-
10×1 
3-
10×1 87 74  5
/
225 65
/
0 )3
/
30( 53
/
0 )5
/
26( 72
/
0 )6
/
32( 
4-
10×1
/
1 
4-
10×5 91 73  5
/
249 5
/
0 )9
/
17( 42
/
0 )5
/
14( 56
/
0 )7
/
19( 
4-
10×7
/
0 
3-
10×2 90 76  5
/
273 4
/
0 )7
/
10( 32
/
0 )83
/
8( 44
/
0 )9
/
11( 
4-
10×1 
3-
10×1 90 74 
*
 ﮔ 
 -99 
GBq
5
/
4. 
**
 -99 15
/
0 -
m
99. 
***
 -
m
99 -
m
99 . 

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