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Table Of Contents Safety Glasses Gloves Laboratory Coats
1.1.2Material Safety Data Sheets
1.1.3Never Taste Chemicals
1.2.1Anhydrous Solvents
1.2.3Preparation and Titration of Grignard Reagents
1.2.5Generation of Zinc Reagent
1.2.6Preparation of Diazomethane
1.2.7Preparation of the Dess−Martin Reagent
1.3.2Recipes of Common Thin Layer Chromatography Stains
1.3.3Flash Chromatography
1.4 Crystallization
1.5Residual Solvent Peaks in Nuclear Magnetic Resonance Alcohol to Alkyl Bromide Alcohol to Alkyl Chloride Alcohol to Alkyl Iodide Alcohol to Azide Alcohol (Halohydrin) to Epoxide to Olefin via Burgess Dehydrating Reagent to Olefin via Martin’s Sulfurane Reaction Traditional Vinylogous Mannich Hartwig-Buchwald Aromatic Amination Hartwig-Buchwald Ether Formation Aromatic Substitution (SNAr) Reaction Michael Addition
2.2.1Alkyne Hydrolysis Ring Opening Reactions, SN1 Ketal Formation Enamine Formation Imine Formation Oxime Formation Formation Formation Chloride Formation by Oxalyl Chloride Chloride Formation by Phosphorous Oxychloride Chloride Formation by Thionyl Chloride Carbonyldiimidazole Activation EDCI Activation EEDQ Activation Isobutylchloroformate Activation Mukaiyama Esterification Yamada Coupling Yamaguchi Esterification Fischer Esterification TMSCHN2 Esterification Schotten–Baumann Reaction Dehydration to Nitrile to Acid Promoted Promoted Promoted Hydrolysis to Acid Promoted Hydrolysis to Acid Promoted Hydrolysis to Amide
3.1.1 Activated Manganese Dioxide Oxidation Pyridinium Chlorochromate Pyridinium Dichromate Collins Oxidation Oxalyl Chloride (Swern) Dicyclohexylcarbodiimide (Moffatt) SO3.Pyridine (Parikh–Doering Oxidation) Trifluoracetic Anhydride Acetic Anhydride With P2O5 With N-Chlorosuccinimide (Corey–Kim)
3.1.5 Fleming Oxidation Standard Schreiber–Meyer Modification 1-Hydroxy-1,2,benziodoxol-3(1H)-one Oxidation
3.1.8Pummerer Rearrangement
3.1.10 Tetrapropylammonium Perruthenate oxidation
3.1.11Wacker Oxidation
3.2.1Jones Oxidation
3.2.2 Permanganate Oxidation
3.3.1Dimethyl Dioxirane
3.3.2 Halogenation with N-bromosuccinimide
3.3.3Jacobsen–Katsuki Epoxidation
3.3.4Oxidation of Olefin with meta-Chloroperbenzoic Acid
3.3.5 Osmium Tetroxide Dihydroxylation
3.3.6 Sharpless Asymmetric Dihydroxylation
3.3.7Sharpless Asymmetric Aminohydroxylation
3.3.8 Katsuki–Sharpless Asymmetric Epoxidation
3.3.9 Shi Epoxidation
3.3.10VO(acac)2, t-BuOOH Oxidation of Allylic Alcohols
3.4.1Baeyer–Villiger Oxidation
3.4.2 Sodium Chlorite Oxidation
3.5.1Amine to Nitrone
3.5.2Sulfide to Sulfoxide Oxidation
3.5.3Sulfide to Sulfone Oxidation
3.5.4Kagan Asymmetric Sulfur Oxidation
4.1Alcohols to Alkanes
4.2.1Reductive Amination with Sodium Triacetoxyborohydride
4.2.2Lithium Aluminum Hydride Reduction of an Amide
4.2.3Lithium Aluminum Hydride Reduction of a Nitrile
4.3.1 Lithium Aluminum Hydride
4.3.3Borane of a Carboxylic Acid of a Lactone
4.3.5Sodium Borohydride/Boron Trifluoride Etherate of an Ester of a Weinreb Amide of a Lactone of a Nitrile
4.4.2Triethylsilane and Pd/C (Fukuyama Reduction)
4.5.1 Lithium Aluminum Hydride
4.5.2 Sodium Borohydride
4.5.3Sodium Borohydride/Cerium Trichloride (Luche Reduction)
4.5.4Zinc Borohydride
4.5.5 Diisobutylaluminum Hydride
4.5.6 Lithium tri-tert-Butoxyaluminohydride
4.5.7 L-Selectride
4.5.8 Samarium Iodide/Isopropanol (Meerwein–Pondorf–Verlag)
4.5.9 Tetramethylammonium Triacetoxyborane
4.5.10Corey–Bakshi–Shibata Reduction
4.5.11 R-Alpine Borane (Midland Reduction)
4.5.12Baker’s Yeast Traditional Myers’ Modification
4.6.2Desulfurization with Raney Nickel
4.6.3Reduction of Tosylhydrazones with Sodium Cyanoborohydride
4.6.4Zinc Amalgam (Clemmensen Reduction)
4.6.5Ionic Hydrogenation with Triethyl Silane and Boron Trifluoride
4.6.6Shapiro Reaction
4.7.1Tributyltin Hydride
4.7.2 Trialkylsilanes
4.8.1 Pd/C, H2
4.8.2Lindlar’s Catalyst
4.8.4 Sodium Bis(2-methoxyethoxy(aluminum hydride))
4.8.5 Lithium/Ammonia (Birch Reduction)
4.9.1Reduction of a Nitro Group to an Amine Using Ammonium Formate
4.9.2 Sodium Borohydride/Nickel Dichloride
4.9.3 Staudinger Reaction Aldol (With Two Oxazolidinone Chiral Auxillaries) Masamune Aldol Standard Asymmetric Mukaiyama’ Asymmetric Aldol (Thione Chiral Auxillary)
5.1.2Asymmetric Deprotonation
5.1.3Baylis–Hillman Reaction
5.1.4Benzoin Condensation
5.1.5Brown Asymmetric Crotylation
5.1.6Claisen Condensation Order Cuprates
5.1.8Dieckmann Condensation Norephedrine-Derived Oxazolidinone Valinol-Derived Oxazolidinone Myers’ Asymmetric Alkylation
5.1.10Friedel–Crafts Reaction
5.1.11Grignard Reaction (Organomagnesium Reagents)’s Ligandless Conditions Reactions of Aryl Chlorides (Fu Modification)
5.1.13Henry Reaction (Nitro Aldol) Standard Hiyama Modification Modification (Room Temperature Coupling)
5.1.15Keck Stereoselective Allylation a Palladium Catalyst a Nickel Catalyst Standard Fu Modification
5.1.18Nozaki–Hiyama–Kishi Reaction (Organochromium Reagents)
5.1.19Organocerium Reagent Addition to a Carbonyl With n-BuLi With t-BuLi Alkynes Ortho-metallations
5.1.21Reformatsky Reaction (Organozinc)
5.1.22Roush Crotylation Traditional’s Version Using a Chiral Bis-phosphoramide
5.1.24Schwartz’s Reagent
5.1.25Shapiro Reaction
5.1.26Sonogashira Coupling
5.1.27Stille Reaction
5.1.28Stille–Kelly Reaction of the Boronic Acid Suzuki Modification of a Boronic Ester: Halogen–Lithium Exchange Standard Suzuki–Miyaura Formation of an Organotrifluoroborate Standard Suzuki
5.1.30Tsuji–Trost Reaction of a Dibromoalkene of a Methylalkyne
5.2.2 Corey–Peterson Olefination Horner–Wadsworth–Emmons–Roush Modification of the Horner–Wadsworth–Emmons Reaction–Gennari Modification of the Horner–Wadsworth–Emmons Reaction Modification of the Horner–Wadsworth–Emmons Reaction
5.2.4Julia Coupling
5.2.5 Knoevenagel Condensation
5.2.6 McMurry Coupling Lombardo–Takai Petasis Reagent Tebbe Reagent Wittig’s Catalyst for Ring Closing Metathesis Generation Grubbs’catalyst Generation Grubbs’ Catalyst: Diene Formation from an Enyne–Grubbs’ Catalyst (Intermolecular Reaction)
5.2.9Peterson Olefination
5.2.10Takai Olefination Unstabilized Ylides Stabilized Ylides
5.3.1Diels–Alder Reaction Using Danishefsky’s Diene
5.3.2Hetero-Diels-Alder Reaction Using Rawal’s Diene
5.3.3Simmons−Smith Reaction
6.1.1 Acetate
6.1.2 Acetonide
6.1.3Benzyl ether
6.1.4 para-Methoxybenzyl
6.1.5 Methyl ether
6.1.6 Methoxymethylene ether
6.1.7 tert-Butyldiphenylsilyl ether
6.2.4 Carbobenzyloxy
6.2.5 9-Fluorenylmethyl carbamate
6.2.7 Sulfonamide
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Modern Organic Synthesis in the Laboratory

Modern Organic Synthesis in the Laboratory

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Published by Farooq Muhammad
Modern Organic Synthesis in the Laboratory
Modern Organic Synthesis in the Laboratory

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Published by: Farooq Muhammad on Mar 17, 2013
Copyright:Attribution Non-commercial


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