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Amphetamine Sulphate Synthesis - Scribd.pdf

Amphetamine Sulphate Synthesis - Scribd.pdf

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Published by Joost Will

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Published by: Joost Will on Jun 12, 2013
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12/01/2013

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 Amphetamine sulphate synthesis
What we are need is:5g P2NP50ml Isopropanol7,5-8,5g of Aliuminium foil (better to use thick foil)50ml 98% acetic acid (can also use 70%, than don’t need water)50g NaOH1ml H2SO4Firstly, you will make mix with acetic acid and water.Water we need, because we areusing 98% of acetic.If will be 70%, than we will not need.Pour (50ml GAA + 25mldH2O) in to 250ml erlenmeyer flask.
 
 Prepar solution of 5g P2NP and IPA.Disolve 5g in to 50ml of warm IPA.Let to cool.While IPA solutions is cooling, need to make aliuminium amalgam.Cut the squares1x1.Than put in to 200ml dH2O, add 50mg of Hg(no3) or other Hg salts and stir.After5-10 minutes you will see grey dregs in the jar.That mean, the amalgamation isstarted.Wait about 10 minutes more and wash aliuminium with water 3 times.Than alldregs and Hg(no3) wash out.Becouse Hg salts are very dangerous!
 
  You are ready to start reaction.Add aliuminium amalgam in to acetic acid with watermix.Wait for about 3-5 minutes, while solution will be grey.You can stir it. Than add P2NP solution and stir a little bit.After adition in the 5-10 minutes will startstormy reaction.So let the flask to stay quietly, for about 20-25 minutes.

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