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13C NMR Spectroscopy Power Point Presentation

13C NMR Spectroscopy Power Point Presentation

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Published by BASKAR.L

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Published by: BASKAR.L on May 28, 2009
Copyright:Attribution Non-commercial

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09/24/2010

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1313
C NMR SpectroscopyC NMR Spectroscopy
 
11
H and H and 
1313
C NMR compared:C NMR compared:
both give us information about the number of both give us information about the number of chemically nonequivalent nucleichemically nonequivalent nuclei(nonequivalent hydrogens or nonequivalent(nonequivalent hydrogens or nonequivalentcarbons)carbons)both give us information about theboth give us information about theenvironment of the nuclei (hybridization state,environment of the nuclei (hybridization state,attached atoms, etc.)attached atoms, etc.)it is convenient to use FT-NMR techniques for it is convenient to use FT-NMR techniques for 
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H; it is standard practice for H; it is standard practice for 
1313
C NMRC NMR
 
11
H and H and 
1313
C NMR compared:C NMR compared:
1313
C requires FT-NMR because the signal for aC requires FT-NMR because the signal for acarbon atom is 10carbon atom is 10
-4-4
times weaker than thetimes weaker than thesignal for a hydrogen atomsignal for a hydrogen atoma signal for aa signal for a
1313
C nucleus is only about 1% asC nucleus is only about 1% asintense as that for intense as that for 
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H because of the magneticH because of the magneticproperties of the nuclei, andproperties of the nuclei, andat the "natural abundance" level only 1.1% of at the "natural abundance" level only 1.1% of all the C atoms in a sample areall the C atoms in a sample are
1313
C (most areC (most are
1212
C)C)

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