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Table Of Contents

Preface to the sixth edition
Preface to the first edition
Glossary of symbols
1.1Analytical problems
1.2Errors in quantitative analysis
1.3Types of error
1.4Random and systematic errors in titrimetric analysis
1.5Handling systematic errors
1.6Planning and design of experiments
1.7Calculators and computers in statistical calculations
Bibliography and resources
2.1Mean and standard deviation
Statistics of repeated measurements
2.2The distribution of repeated measurements
2.3Log-normal distribution
2.4Definition of a ‘sample’
2.5The sampling distribution of the mean
2.6Confidence limits of the mean for large samples
2.7Confidence limits of the mean for small samples
2.8Presentation of results
2.9Other uses of confidence limits
2.10Confidence limits of the geometric mean for a log-normal distribution
2.11Propagation of random errors
2.12Propagation of systematic errors
Significance tests
3.2Comparison of an experimental mean with a known value
3.3Comparison of two experimental means
3.4Paired t-test
3.5One-sided and two-sided tests
3.6F-test for the comparison of standard deviations
3.8Analysis of variance
3.9Comparison of several means
3.10The arithmetic of ANOVA calculations
3.11The chi-squared test
3.12Testing for normality of distribution
3.13Conclusions from significance tests
3.14Bayesian statistics
The quality of analytical measurements
4.3Separation and estimation of variances using ANOVA
4.7Shewhart charts for ranges
4.8Establishing the process capability
4.9Average run length: CUSUM charts
4.10Zone control charts (J-charts)
4.11Proficiency testing schemes
4.12Method performance studies (collaborative trials)
4.14Acceptance sampling
4.15Method validation
5.1Introduction: instrumental analysis
Calibration methods in instrumental analysis: regression and correlation
5.2Calibration graphs in instrumental analysis
5.3The product–moment correlation coefficient
5.4The line of regression of yon x
5.5Errors in the slope and intercept of the regression line
5.6Calculation of a concentration and its random error
5.8The method of standard additions
5.9Use of regression lines for comparing analytical methods
5.10Weighted regression lines
5.11Intersection of two straight lines
5.12ANOVA and regression calculations
5.13Introduction to curvilinear regression methods
5.14Curve fitting
5.15Outliers in regression
Non-parametric and robust methods
6.2The median: initial data analysis
6.3The sign test
6.4The Wald–Wolfowitz runs test
6.5The Wilcoxon signed rank test
6.7Non-parametric tests for more than two samples
6.8Rank correlation
6.9Non-parametric regression methods
6.10Introduction to robust methods
6.11Simple robust methods: trimming and winsorisation
6.12Further robust estimates of location and spread
6.13Robust ANOVA
6.14Robust regression methods
6.15Re-sampling statistics
Experimental design and optimisation
7.2Randomisation and blocking
7.3Two-way ANOVA
7.4Latin squares and other designs
7.6Identifying the important factors: factorial designs
7.7Fractional factorial designs
7.8Optimisation: basic principles and univariate methods
7.9Optimisation using the alternating variable search method
7.10The method of steepest ascent
7.11Simplex optimisation
7.12Simulated annealing
Multivariate analysis
8.2Initial analysis
8.3Principal component analysis
8.4Cluster analysis
8.5Discriminant analysis
8.6 K-nearest neighbour method
8.7Disjoint class modelling
8.8Regression methods
8.9Multiple linear regression
8.10Principal component regression
8.11Partial least-squares regression
8.12Natural computation methods: artificial neural networks
Solutions to exercises
Appendix 1: Commonly used statistical significance tests
Appendix 2: Statistical tables
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Statistics and Chemometrics for Analitical Chemistry

Statistics and Chemometrics for Analitical Chemistry

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Published by Leandregg

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Published by: Leandregg on Sep 18, 2013
Copyright:Attribution Non-commercial


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