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Table Of Contents

2.2 Sample Preparation
2.3 Sample Status and Tracking
3.0Spectrometer Operation
3.1 Preparation for Operation and Shutdown
3.2 Gain and Baseline Adjustment
3.3 Run Options
4.0Data Analysis and Reporting
4.1 Field Data Entry
4.2 Least Squares Analysis
4.3 Detection Limits
4.4 Data Reporting
4.5 Data Archiving
5.0Calibration
5.1 Source and Description of Calibration Standards
5.2 Gain and Baseline Adjustments
5.3 Background Measurement
5.4 Shape Standards
5.5 Determine Fraction of Measured K Lines to Total K Lines
5.6 Measure Calibration Standards
5.7 Calculate Sensitivities
5.8 Overlap Coefficients
6.0Quality Control
6.1 Description of QC Standards
6.2 Run-time Quality Control
6.3 Quality Control with Standard Reference Materials
6.4 Acceptance Criteria and Procedures for Corrective Action
6.5 Field Data Entry Checking
6.6 Control Charts
6.7 Self Consistency Checks
6.8 Goodness-of-Fit Measurements
6.9 Audit Reports
7.0Preventive Maintenance
7.1 Liquid Nitrogen Filling Procedure
7.2 Argon Bag Filling Procedure
7.3 Preparation for Power Outage
7.4 Lab Environment
8.0References
9.0Appendix
9.1 Definitions
9.2 Derivation of -Effective Mass from NIST Certified Values
9.3 Results of SRM Analysis on 4/29/1992
9.4 Computer Menu
9.5 Data Report on a Sample from a VAPS Sampler
9.6 Example SEM Format Data Report
9.7 Detection Limits (1ó) for Teflo and Nuclepore Blank Filters
9.8 Typical Run-time QC Results
9.9 Assignment of XRFIDs Form
9.10XRF Run Status Log Form
9.11Sample Check-Out Form
9.12Calibration Standards and Concentrations
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Environmental Protection Agency: atmspher

Environmental Protection Agency: atmspher

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Published by: Environmental Documents on Jan 28, 2008
Copyright:Attribution Non-commercial

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