DAFTAR ISI

HALAMAN JUDUL .......................................................

HALAMAN PERSETUJUAN ........................................
HALAMAN PENGESAHAN .........................................
ABSTRAK ......................................................................
KATA PENGANTAR .....................................................
DAFTAR ISI ...................................................................
DAFTAR TABEL ...........................................................
DAFTAR GAMBAR .......................................................
DAFTAR LAMPIRAN ...................................................
BAB I. PENDAHULUAN

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A. Latar Belakang Masalah ................................

B. Rumusan Masalah ..........................................
C. Tujuan Penelitian ...........................................
D. Manfaat Penelitian .........................................
E. Definisi Oprasional ........................................
F. Asumsi dan Pembatasan Penelitian ................
BAB II. TINJAUAN PUSTAKA
A. Minyak Biji Kapuk.........................................
B. Gliserol ..........................................................
C. Destilasi Vakum .............................................
D. Ekstraksi ........................................................
E. Gas Chromatography (GC)..............................
F. Hasil Penelitian yang Relevan.........................
G. Kerangka Konseptual ...............................
BAB III. METODE PENELITIAN
A. Jenis Penelitian ..............................................
B. Tempat dan Waktu Penelitian.........................

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C. Populasi dan Sampel.......................................

D. Rancangan Penelitian .....................................
E. Variabel Penelitian .........................................
F. Prosedur Penelitian..........................................
G. Instrumen Penelitian ......................................
H. Teknik Analisis Data ....................................
BAB IV. HASIL PENELITIAN DAN PEMBAHASAN
A. Pembuatan Gliserol.........................................
1. Tahap Pengepresan Biji Kapuk..................
2. Tahap Degumming.....................................
3. Tahap Esterifikasi......................................
4. Tahap Transesterifikas...............................
B. Penentuan Kadar Gliserol...............................
C. Analisis Gas Chromatography Gliserol..........
BAB V. SIMPULAN DAN SARAN
A. Simpulan ........................................................
B. Saran ..............................................................
DAFTAR PUSTAKA ......................................................
LAMPIRAN ....................................................................

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DAFTAR TABEL
Nomor Tabel
Halaman
2.1 Komposisi Biji Kapuk............................................... 8
2.2 Karakteristik Minyak Biji Kapuk............................... 8
2.3 Komposisi Asam Lemak Minyak Biji Kapuk............ 9
2.3 Komposisi Asam Lemak Minyak Biji Kapuk............ 9
2.4 Komposisi Minyak Biji Kapuk.................................. 11
2.5 Sifat Gliserol.............................................................. 42
4.1 Hasil Analisa Kadar Gliserol..................................... 47

DAFTAR GAMBAR
Nomor Gambar
Halaman
2.1 Pohon dan Buah Tanaman Kapuk.............................. 8
2.2 Struktur Asam Oleat.................................................. 9
2.3 Struktur Asam Siklopropenoid.................................. 10
2.4 Struktur Umum Gliserol/Trigliserida......................... 11
2.5 Reaksi Hidrolisis....................................................... 12
2.6 Reaksi Saponifikasi................................................... 13
2.7 Reaksi Transesterifikasi............................................. 14
2.8 Seperangkat Alat Destilasi Vakum ........................... 18
2.9 Alat Instrumen GC..................................................... 28
3.1 Rancangan Penelitian................................................ 31
4.1 Proses Pemisahan Gum dari Minyak......................... 40
4.2 Proses Pemisahan Metanol dari Minyak.................... 41
4.3 Proses Pemisahan Gliserol dari Minyak.................... 42
4.4 Hasil Pemurnian Gliserol........................................... 44

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DAFTAR LAMPIRAN
Nomor
Lampiran
Halaman
1 Pernyataan Keaslian Tulisan........................................ 54
2 Surat Ijin Penelitian..................................................... 55
3 Diagram Alur Kerja Penelitian.................................... 56
4 Perhitungan Rendemen Minyak Kapuk....................... 61
5 Perhitungan Kadar Asam lemak Bebas........................ 63
6 Perhitungan Kebutuhan Methanol............................... 66
7 Spektroskopi Gas Chromatography............................. 67
8 Dokumentasi................................................................ 73

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