No Order Date Acceptance No Sertificate Name Company Address Loc Calibration Themperature Humudity Reference SMM-WI-I-03 C %

Analisa Data Instrumentasi pH Meter

Unit Under Test Merk Type Serial Number Capacity Resolution

RESULT CALIBRATION

Themperature Liquid C

Nominal Standar ( ) X1

Unit Under Test Indication ( X2 X3

) Xmean

Use Calibrator
Name Standard Standard pH Thermometer Date Calibration Merk Hanna Instrument Gizmo Calibration By Correction By Witness Type Serial Number U95% : Uncertainty k:

FR-SMM-I-03

No Order Date Acceptance No Sertificate Date Isue Name Company Address Loc Calibration Themperature Humudity Reference

400.13.19-16 November 30 , 2013 5740.EPE.12.13 November 28, 2013 PT. Uniliver Indonesia NSD Liquid Factory , JL. Jababeka Raya In Lab. Mini pH 2 23 60 2 5 C %

Analisa Data Instrumentasi pH Meter

Unit Under Test Merk Type Serial Number Capacity Resolution RESULT CALIBRATION

pH Meter mettler Toledo IMTE-LP-296 4~10 0.01 pH pH

Blok O Jababeka Industrial Estate Cikarang - Bekasi

SMM-WI-I-03

Themperature Liquid C 23 23 23

Nominal Standar pH 5000 8000 12000 X1 5002 8003 12003 X2

Unit Under Test Indication ( s ) X3 5002 8007 12003 Xmean 5002.0 8005.0 12003.0 Stdev 0.0 2.0 0.0

Stedev Maximum

5002 8005 12003

2.0

Use Calibrator
Name Standard Standard Conductivity Thermometer Date Calibration November 30, 2013 Merk Hanna Instrument Gizmo Calibration By Rangga Gumilar Type /D78/R Correction By RNG Serial Number /9812 Treceability Hanna Instrument LK-112-IDN Uncer 0.1 0.2 % C

TABEL BUDGET KETIDAKPASTIAN BIDANG INSTRUMENTASI

1 Besaran yang diukur

Nama Alat Standard yang digunakan Kapasitas Accuracy Uncertainty Kemampuan Baca Alat
Componen
Ketidakpastian Baku Standard Ketidakpastian Baku Drift Standard Ketidakpastian Baku Suhu Cairan Ketidakpastian Baku Daya Baca Alat Ketidakpastian Baku Pengulangan Pembacaan Jumlah Ketidakpastian Baku Gabungan , Uc Derajat Kebebasan , v eff

: : : : : : :
Unit pH pH
C

Kelistrikan pH Meter pH Buffer Standrad pH 4 1 % pH 0.004 pH 1.00

Distribution
normal rect. rect. Rect. t-student

U
0.004 0.0004 0.5 0.5000 0.008

Divisor
2 1.73205 1.73205 1.732051 1.73205

vi
60 60 60 60 2

ui
0.002 0.00023094 0.288675135 0.288675135 0.007598357

ci
1 1 1 1 1

uici
0.002 0.00023094 0.288675135 0.288675135 0.007598357

(uici )2
0.000004 5.33333E-08 0.083333333 0.083333333 5.7735E-05

( uici )4/vi

2.66667E-13 4.74074E-17 0.000115741 0.000115741 1.66667E-09

pH pH

Factor Cakupan , k=student's for v eff and CL 95 % Ketidakpastian Bentangan , U = k Uc

0.166728455 0.000231483 0.408323958 120.088127 1.979930405 pH 0.8085

2 Besaran yang diukur

Nama Alat Standard yang digunakan Kapasitas Accuracy Uncertainty Kemampuan Baca Alat
Componen
Ketidakpastian Baku Standard Ketidakpastian Baku Drift Standard Ketidakpastian Baku Suhu Cairan Ketidakpastian Baku Daya Baca Alat Ketidakpastian Baku Pengulangan Pembacaan Jumlah Ketidakpastian Baku Gabungan , Uc Derajat Kebebasan , v eff

: : : : : : :
Unit pH pH
C

Kelistrikan pH Meter pH Buffer Standrad pH 7 1 % 0.007 pH pH 1.00

Distribution
normal rect. rect. Rect. t-student

U
0.007 0.0007 0.5 0.5000 0

Divisor
2 1.73205 1.73205 1.732051 2.23607

vi
60 60 60 60 2

ui
0.0035 0.000404145 0.288675135 0.288675135 0

ci
1 1 1 1 1

uici
0.0035 0.000404145 0.288675135 0.288675135 0

(uici )2
0.00001225 1.63333E-07 0.083333333 0.083333333 0

( uici )4/vi

2.50104E-12 4.4463E-16 0.000115741 0.000115741 0

pH pH

Factor Cakupan , k=student's for v eff and CL 95 % Ketidakpastian Bentangan , U = k Uc

0.16667908 0.000231481 0.408263493 120.0178746 1.979930405 pH 0.8083

3 Besaran yang diukur

Nama Alat Standard yang digunakan Kapasitas Accuracy Uncertainty Kemampuan Baca Alat
Componen
Ketidakpastian Baku Standard Ketidakpastian Baku Drift Standard Ketidakpastian Baku Suhu Cairan Ketidakpastian Baku Daya Baca Alat Ketidakpastian Baku Pengulangan Pembacaan Jumlah Ketidakpastian Baku Gabungan , Uc Derajat Kebebasan , v eff

: : : : : : :
Unit pH pH
C

Kelistrikan Conductivity Meter Conductivity Standrad 10 pH 1 % 0.01 pH pH 1.00

Distribution
normal rect. rect. Rect. t-student

U
0.010 0.001 0.5 0.5000 0

Divisor
2 1.73205 1.73205 1.732051 2.23607

vi
60 60 60 60 2

ui
0.005 0.00057735 0.288675135 0.288675135 0

ci
1 1 1 1 1

uici
0.005 0.00057735 0.288675135 0.288675135 0

(uici )2
0.000025 3.33333E-07 0.083333333 0.083333333 0

( uici )4/vi

1.04167E-11 1.85185E-15 0.000115741 0.000115741 0

pH pH

Factor Cakupan , k=student's for v eff and CL 95 % Ketidakpastian Bentangan , U = k Uc

0.166692 0.000231481 0.408279316 120.0364774 1.979930405 pH 0.8084 Uncertainty Maximum (4,7,10) 0.8085 pH

Number Date Page Order Number : 400.13.19-16

: 5740.EPE.12.13 : November 28, 2013 1 of 2

UNIT UNDER TEST (UUT) 1. Name 2. Type/Model 3. Manufacture OWNER 1 Name 2 Address STANDARD Name Standard Conductivity Thermometer Date of acceptance Manufacture/Type/SN Hanna Instrument /9812 Gizmo /D78/R : November 30 , 2013 Traceable SI unit through Hanna Instrument LK-112-IDN : November 30, 2013 : PT. Uniliver Indonesia : NSD Liquid Factory , JL. Jababeka Raya Blok O Jababeka Industrial Estate Cikarang - Bekasi : pH Meter :: mettler Toledo 4. Serial Number 5. Capacity 6. Resolution : IMTE-LP-296 : 4~10 : 0.01 pH pH

Date of calibration

Environment condition of calibration Temperature Humidity Location of calibration In Lab. Mini pH 2 Refference Result of Calibration : SMM-WI-I-03 : Attached : : 23 60 2 5 C %

Director

Ir.Sukiswanto

Number Date Page

: 5740.EPE.12.13 : November 28, 2013 2 of 2

Unit Under Test Serial Number/ID Capacity Resolution

: pH Meter : IMTE-LP-296 : 4~10 : 0.01 pH pH

Result of calibration
Themp Liquid C 23 23 23 Nominal Standard pH 4 7 10 UUT Indication pH 4.19 7.06 9.84 Correction pH -0.19 -0.06 0.16 0.81 Uncertainty pH

- The Uncertainty is taken at a Convidence Level 95% and Coverage Factor ( k ) = 2

Technician

Rangga Gumilar