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Table Of Contents

1. Introduction
1.1 Scope of the Present Guide
1.2 The Nature of Porous Solids
1.3 Important Characteristics
2. Porous and Highly Dispersed Solids
2.1 General Definitions and Terminology
2.1.1 Physical Adsorption (physisorption)
2.1.2 Sorption
2.1.3 Desorption
2.1.4 Multilayer Adsorption
2.1.5 Monolayer Capacity
2.2 Qualitative Description of a Porous Solid
2.2.1 Pore Types
2.2.2 Pore Classes
2.3.1 Specific Surface Area
2.4 The Fractal Character of Porous Structures
3. Pore Analysis Instruments
4.1.1 Cone and Quartering
4.1.2 Table Sampling
4.2 Steps in a Sampling Procedure
4.3 Special Preparation Steps
4.3.1 Gas Adsorption Method
4.3.2 Mercury Intrusion Method
5. Specific Surface Area and Pore Analysis by Gas Adsorption
5.1 Principle of Measurement
5.2 Determination of Surface Area
5.3 Mesoporosity and the Kelvin Equation
5.4.1 Micropore Volume from the Langmuir Isotherm
Figure 5.2.Linear isotherm plot of Ar on zeolite at 87.3 K
5.4.2 Dubinin-Radushkevich Method
Table 5.2.Adsorbent Parameters (according to DIN 66135-4)
Table 5.3.Adsorbent Parameters (according to DIN 66135-4)
6.1 Principle of Measurement
6.2 Calculation of the Pore Size Distribution
6.3 Calculation of the Specific Surface Area
7. Conclusion
8. References
Appendix 1: SRM/CRMs Worldwide
Table A1.2.Certified reference materials for porosity properties
Appendix 2: Additional Illustrative Case Study Results
Appendix 2.1 CRM BAM-P107 (a microporous CRM)
Figure A2.1.1.The nitrogen (N2) Isotherm for CRM BAM-P107
Appendix 2.3 CRM BAM-P123 (a macroporous CRM)
Appendix 2.4 CRM BAM-PM-122 (Hg Porosimetry)
Appendix 3: Relevant Measurement Standards
Appendix 4: Glossary
A5.2 Scientific items
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Porosity & Specific Surface Area Measurements

Porosity & Specific Surface Area Measurements

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Published by: tjleong on Jun 07, 2014
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