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Progress Report of Anamica T3

Progress Report of Anamica T3

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Published by Jonathan Hicks

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Published by: Jonathan Hicks on Dec 07, 2009
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12/07/2009

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Progress report of I semester (2009-2010)Anamica Tripathi (2006CYZ8240
)
1)
In
I
st
 
semester of 
2009-2010
, for the synthesis of anion- templated rotaxane based on bile acidfollowing sequence of reactions has been done. All these compounds were characterized by IR and NMR spectroscopy.
Scheme 1
OHOOHH1.CH
3
OH/H
2
SO
4
2.BrCH
2
COBR/K
2
CO
3
OCH
3
OOHCH
2
Br O
12
NHNOCH
3
OOHONN
3
Reflux
OH
3
COOHOOCH
3
OOHONN
5
Br 
-
CH
3
CNOCH
3
OOHCH
2
Br O
2
OCH
3
OOHONN
4
+
OH
3
COOHOOCH
3
OOHONN
6
CHCl
3
/H2ONH
4
ClCl
-
Scheme 2
OHOOHH1.CH
3
OH/H
2
SO
4
2.BrCH
2
COBR/K
2
CO
3
OCH
3
OOHCH
2
Br O
78
OHOOBr DMFOHOH/K
2
CO3

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