Welcome to Scribd, the world's digital library. Read, publish, and share books and documents. See more ➡
Download
Standard view
Full view
of .
Add note
Save to My Library
Sync to mobile
Look up keyword
Like this
2Activity
×
0 of .
Results for:
No results containing your search query
P. 1
Thermal Methods in the Study of Polymorphs

Thermal Methods in the Study of Polymorphs

Ratings: (0)|Views: 658|Likes:
Published by Nandhan

More info:

Published by: Nandhan on Mar 11, 2010
Copyright:Attribution Non-commercial

Availability:

Read on Scribd mobile: iPhone, iPad and Android.
download as PDF, PPT, TXT or read online from Scribd
See More
See less

09/05/2011

pdf

text

original

 
 
Thermal Methods in the Study of Polymorphsand Solvates
 
Susan M. Reutzel-Edens, Ph.D.Research AdvisorLilly Research LaboratoriesEli Lilly & CompanyIndianapolis, IN 46285
 Presented at:
“Diversity Amidst Similarity:A Multidisciplinary Approach to Polymorphs, Solvates and Phase Relationships”(The 35
th
Crystallographic Course at the Ettore Majorana Centre)Erice, SicilyJune 9-20, 2004
 
 
Thermal Analysis Techniques
Differential Thermal Analysis (DTA)
the temperature difference between a sample and an inert reference material,
=
S
-
R
, is measured as both are subjected to identical heat treatments
Differential Scanning Calorimetry (DSC)
the sample and reference are maintained at the same temperature, even during athermal event (in the sample)the energy required to maintain zero temperature differential between the sampleand the reference, d
/d
, is measured
Thermogravimetric Analysis (TGA)
the change in mass of a sample on heating is measured
A group of techniques in which a physical property is measured as a function oftemperature, while the sample is subjected to a predefined heating or coolingprogram.
 
 
Basic Principles of Thermal Analysis
Modern instrumentation used for thermal analysis usually consists of four parts:1)sample/sample holder2)sensors to detect/measure a property of the sample and the temperature3)an enclosure within which the experimental parameters may be controlled4)a computer to control data collection and processingDTApower compensated DSCheat flux DSC

You're Reading a Free Preview

Download
/*********** DO NOT ALTER ANYTHING BELOW THIS LINE ! ************/ var s_code=s.t();if(s_code)document.write(s_code)//-->