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Peroxide Acid Method

Peroxide Acid Method

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Published by AFLAC ............
Peroxide Acid Method.doc
Peroxide Acid Method.doc

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Published by: AFLAC ............ on Mar 27, 2010
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04/25/2013

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on Thu Apr 26, 2007 7:16 pmThe ratio I start with is 2 HCl:1 Peroxide.I use the 3% peroxide. The higher concentration stuff will work faster. I've found that if I keep the color aclear to dark emerald green it tends to react quicker.Here's how my stock vessel looks right now:Here's the strainer I made to keep the scrap (fingers usually) separated from the gold foil/flake:I typically agitate the bath twice a day by pulling the strainer out, waiting a moment or two, then slowlyletting it back down into the bath. This causes the gold foils to go into the solution thru the bottom of thestrainer and separates them from the finger boards.
 
Heat helps of course. If I want to hurry it along I'll add a little peroxide every so often to keep the solutionwarm (it heats and bubbles when you add more peroxide). Once the copper chloride concentration getsright (see the copper chloride document on my website) the solution works really good with an occasionalkick start of peroxide. If the solution darkens or precipitates copper chloride ( greenish white crystals ) thenadd some more muratic to dissolve the precipitates. The solution will slowly dissolve gold if you get it tooreactive (excessive peroxide). I'm not in any real hurry, so I typically set up a three gallon bucket (lowes)and let the scrap soak for a few days. I agitate it occasionally to keep the gold foil that has loosened from blocking the remaining copper plate. You can reuse the stuff forever if you keep it filtered and primed withHCl and Peroxide occasionally.Here's the dirty foil before the rinses: Notice the copper chloride (greyish white) powder in the mash.
 
Here's the 'gold mash' produced after washing and rinsing:And finally here's the foils from the batch:I hope this helps... any questions .Steve

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