Characterisationof Polymers
T.R. Crompton
Volume
2
i1. Pyrolysis – Gas Chromatography ....................................................................11.1 Discussion of Technique and Equipment ................................................1Combustion Furnace Pyrolyser ..............................................................4Filament Pyrolyser .................................................................................5Curie Point Pyrolyser .............................................................................5Laser Pyrolysis .......................................................................................9Random Scission .................................................................................11Depolymerisation ................................................................................14Side Group Elimination .......................................................................151.2 Applications, Homopolymers ..............................................................171.2.1 Polypropylene .........................................................................171.2.2 Determination of Degree of Cure of Rubber ...........................171.2.3 Polybutadiene .........................................................................191.2.4 Polyacrylates and Polymethacrylates .......................................191.2.5 Polyethylene Oxide .................................................................211.2.6 Polysulfides .............................................................................211.2.7 Silicon Containing Polymers ...................................................301.2.8 Miscellaneous Polymers ..........................................................301.3 Copolymer Applications ......................................................................301.3.1 Determination of Unsaturation in Ethylene-Propylene-Diene Terpolymers ..................................................................301.3.2 Acrylate and Methacrylate Based Copolymers ........................321.3.3 Styrene-based Copolymers ......................................................381.3.4 Vinyl Chloride-Vinylidene Chloride Copolymers.....................45
C
ontents
ii
Characterisation of Polymers – Volume 2
1.3.5 Comonomer Units in Polyhexafluoropropylene-Vinylidiene Chloride Copolymers ............................................461.3.6 Acrylonitrile-butadiene ...........................................................461.3.7 Miscellaneous Copolymers ......................................................56References .....................................................................................................562. Complementary Pyrolysis-Gas Chromatography-FT-IR .................................632.1 Theory .................................................................................................632.2 Instrumentation ...................................................................................672.3 Applications ........................................................................................672.3.1 Copolymers .............................................................................67References .....................................................................................................743. Complementary Pyrolysis – Mass Spectrometry ............................................773.1 Applications ........................................................................................773.1.1 Polyurethane ...........................................................................783.1.2 Polyacrylamide ........................................................................813.1.3 Miscellaneous Polymers ..........................................................91References .....................................................................................................944. Complementary Pyrolysis Gas Chromatography-Mass Spectrometry ............994.1 Homopolymers ....................................................................................994.1.1 Polyacrylates ...........................................................................994.1.2 Chlorinated Polyethylene ......................................................1044.1.3 Polyimide Synthesised from (4,4
′
-Hexafluoroisopropylidene)diphthalic Dianhydride (DTG) and an UnfluorinatedPolyamide 4,4
′
-diamino diphenyl Methane (PIF
1
) .................1084.1.4 Polypyrrol .............................................................................1124.1.5 Miscellaneous Homopolymers ..............................................1164.2 Copolymers .......................................................................................1164.2.1 Ethylene – Carbon Monoxide ...............................................1164.2.2 Ethylene-vinyl Cyclohexane ..................................................116
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3.1.2 Polyacrylamide for Characterisation of Polymers – Volume 2
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