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BI 5: XC INH CNG TRONG NC ................................................................. 4
1. L thuyt ................................................................................................................... 4
2. Dng c v thit b ................................................................................................... 4
3. Ha cht .................................................................................................................... 4
4. Tin hnh .................................................................................................................. 4
4.1. Pha dung dch ......................................................................................................... 4
4.2. Xc nh cng tm thi ...................................................................................... 5
4.3. Xc nh cng tng cng ................................................................................... 5
5. Cu hi chun b ........................................................................................................ 5
BI 4: XC NH HM LNG CANXI BNG PP KT TA OXALAT ...................... 6
1. Gii thiu .................................................................................................................. 6
2. Cc phng php xc nh canxi ............................................................................... 6
BI 6: NH LNG HM LNG NaCl TRONG NC MM ................................... 9
1. Nguyn tc phng php ........................................................................................... 9
2. Nhng iu kin chnh............................................................................................... 9
3. Dng c v ha cht ................................................................................................ 10
4. Qu trnh xc nh ................................................................................................... 10
BI 3. XC NH AXIT TRONG SA...................................................................... 12
1. Phm vi p dng ...................................................................................................... 12
2. Dng c ................................................................................................................... 12
3. Ho cht .................................................................................................................. 12
4.Tin hnh ................................................................................................................. 12
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BI 1: NH TNH MT S ION
1. Th nghim 1: nh tnh ion NH4+ bng thuc th Nestler
-
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Tr li cu hi:
1. Vit phn ng xy ra cho tng th nghim?
2. Gii thch hin tng xy ra?
3. Nu nh hng ca cc cht trong tng th nghim n sc khe con ngi?
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2. Dng c v thit b
3 becher 250mL
3 erlen 250mL
1 buret 25mL
1 phu, ng nh git
1 a thy tinh
1 cn phn tch
1 bp in, li amiang
1 pipet 25mL
1 pipet 10mL
1 bnh nh mc 100mL
3. Ha cht
Dung dch chun HCl 0.05N
Dung dch chun HCl 0.01N
Ch th MO 1% trong cn.
1,179 g EDTA.2H2O
7.8g MgSO4.7H2O
16.9 g NH4Cl
143mL NH3
4. Tin hnh
4.1. Pha dung dch
Dung dch tiu chun EDTA 0.05N
Dung dch m pH 10 gm:
1,179 g EDTA.2H2O + 7.8g MgSO4.7H2O + 50mL H2O + 16.9 g NH4Cl + 143mL
NH3 . nh mc bng nc ct n 1000mL.
Ch th ETOO: Cn 1g Eriochrom black T + 100g NaCl, nghin v trn u.
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5. Cu hi chun b
Trnh by tc ng ca Mg2 v Ca2+ i vi thc phm?
Vit cc phng trnh phn ng xy ra?
ngha ca cc phng php kim nghim trn trong thc t?
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Vdm 100
.
Vxd mbd
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Mu mui n
Ch th K2CrO4 5%
3.2.
-
Dng c
a thy tinh
- 3 erlen 250 ml
- 3 cc 250 ml
-
Buret 25 ml
Bp cao su
- 2 Pipet 10 ml
4. Qu trnh xc nh
1. Thit lp nng cho dung dch AgNO3 0,05N
Sinh vin tnh cn chnh xc mt lng cn KCl pha 250 ml KCl 0,05N
dng thit lp nng cho dung dch AgNO3 0,05N
Ht chnh xc 10-25 ml dung dch KCl va pha, chuyn vo bnh nn 250ml,
thm 4 5 git ch th K2CrO4 5%, un si ri chun dung dch bng AgNO3 0,05N
ti khi xut hin kt ta gch Ag2CrO4
Cn th nghim 3 ln, sai lch gia ba ln chun 0,1ml
NAgNO3
( NV ) KCl
VAgNO3
2. Qu trnh xc nh
Cn chnh xc 1,0 0,0002g mu mui n ( uc sy k 105 0C khong 2
gi, lun bo qun trong bnh ht m, c nghin mn). Ha tan bng nc ct
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nng, lc qua giy lc dy (loi tp cht khng tan), dng nc ct trng ra sch
giy lc, ngui v nh mc thnh 250ml dung dch. Lc trn u.
Ht chnh xc 10-25 ml dung dch, chuyn vo bnh nn 150 250ml, thm 4
5 git ch th K2CrO4 5%, un si ri chun dung dch bng AgNO3 0,05N ti khi xut
hin kt ta gch Ag2CrO4
Cn th nghim 3 ln, sai lch gia ba ln chun 0,1ml. Kt qu c tnh
nh cng thc ghi
5. Cu hi
1.
2.
3.
4.
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BI 3. XC NH AXIT TRONG SA
1. Phm vi p dng
p dng kim tra sa ti nguyn liu v thnh phm
2. Dng c
Pipet 10 mL c vch chia 0,1 mL.
Pipet hay Buret 10 25 mL c vch chia 0,1 mL.
Cc thu tinh 250 mL
3. Ho cht
Dung dch Phenolphtalin 1%.
Dung dch NaOH 0,1 N
4.Tin hnh
Xc nh theo n v % acid lactic:
Trn u mu, dng Pipet chuyn 17,6 mL sa ti vo cc thu tinh. Thm vo 3 5 git
dung dch Phenolphtalein, lc u. nh phn vi dung dch NaOH 0,1 N cho n khi dung
dch xut hin mu hng nht bn trong 30 giy. c th tch dung dch NaOH 0,1N tiu tn,
mL
Hm lng acid trong sa ti (% acid lactid) c tnh thheo cng thc: % Acid = V/20
Xc nh theo n v T:
Trn u mu, dng Pipet chuyn 10 mL sa ti vo cc thu tinh. Thm vo 3 5 git
dung dch Phenolphtalein, lc u. nh phn vi dung dch NaOH 0,1N cho n khi dung
dch xut hin mu hng nht bn trong 30 giy. c th tch dung dch NaOH 0,1N tiu tn,
mL
Hm lng acid trong sa ti ( T) c tnh theo cng thc: 0T = 10.V
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