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  • Shimadzu 50-50

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    Wira Atmaja
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    shimadzu 50-50

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    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
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    12 views4 pages

    Shimadzu 50-50

    Uploaded by

    Wira Atmaja

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 4

    7/30/2011 11:16:03 1 / 4

    ==== Shimadzu LCsolution Analysis Report ====


    Acquired by
    Sample Name
    Sample ID
    Injection Volume
    Data File Name
    Method File Name
    Report File Name
    Data Acquired
    Data Processed

    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd


    : Admin
    : campuran barbiturat
    : campuran barbiturat
    : 20 uL
    : campuran barbiturat3.lcd
    : MeOH-Bufer fosfat 3.5 (50-50)
    : Default.lcr
    : 6/13/2011 3:04:23 PM
    : 6/15/2011 5:55:22 PM

    <Chromatogram>
    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd

    30

    8.946 / fenitoin

    40

    8.066 / butalbital

    3.129 / barbital

    50

    4.983 / fenobarbital

    4.518 / alobarbital

    mAU
    PDA Multi 1

    0.0

    2.5

    10.276 /

    6.328 /

    3.925 /
    4.065 /

    3.424 /

    2.161 /
    2.283 /
    2.389 /
    2.553 /

    1.603 /
    1.723 /

    10

    1.824 /

    20

    5.0

    7.5

    10.0
    min

    1 PDA Multi 1/216nm 4nm

    Quantitative Results
    PDA
    Name
    barbital
    alobarbital
    fenobarbital
    butalbital
    fenitoin
    Width at 50% Height
    0.095
    0.124
    0.137
    0.205
    0.231

    Ret. Time
    3.129
    4.518
    4.983
    8.066
    8.946

    Area
    Peak Start Peak End
    194447
    2.816
    3.349
    363789
    4.288
    4.757
    377417
    4.757
    5.355
    397732
    7.648
    8.523
    779138
    8.523
    9.472

    Tailing Factor
    1.217
    1.120
    1.104
    1.047
    1.041

    USP Width
    0.181
    0.227
    0.248
    0.360
    0.403

    HETP
    31.399
    23.759
    23.206
    18.637
    18.997

    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd

    7/30/2011 11:16:03 2 / 4

    Spectrum
    Retention Time
    Compound Name

    : 3.129
    : barbital

    mAU
    55 198.10
    50
    45
    40
    35
    30
    25
    20
    15
    10
    5
    0

    304.66

    200

    382.82

    300
    nm

    Retention Time
    Compound Name

    : 4.518
    : alobarbital

    mAU
    80

    198.22

    70
    60
    50
    40
    30
    20
    283.99

    10

    382.78

    0
    200

    300
    nm

    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd

    7/30/2011 11:16:03 3 / 4

    Retention Time
    Compound Name

    : 4.983
    : fenobarbital

    mAU
    100 198.29
    90
    80
    70
    60
    50
    40
    30
    20
    10
    0

    382.70

    200

    300
    nm

    Retention Time
    Compound Name

    : 8.066
    : butalbital

    mAU
    55 198.38
    50
    45
    40
    35
    30
    25
    20
    15
    10
    5
    0
    200

    302.27

    378.82

    300
    nm

    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd

    7/30/2011 11:16:03 4 / 4

    Retention Time
    Compound Name

    : 8.946
    : fenitoin

    mAU
    150 198.56

    100 193.43

    50
    331.06

    398.92
    382.74

    0
    200

    300
    nm

    C:\Drugs Abuse\Barbiturate\fosfat3.5 MeOH 5050 (13juni)\campuran barbiturat3.lcd

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