Name: Eldee R. Balolong Student Number: 2007-58545 Class-Section: Chem 28.

1-1 Date Performed: July 17, 2008 Date Submitted: July 17, 2008
I. TITLE. Precipitation Titration: Determination of the Chloride in the Sample

II.

RESULTS.

A. Standardization of Silver Nitrate Solution Primary Standard used: Formula mass of 1O standard: % Purity of 1O standard: Trials Mass of NaCl (g) Final Reading AgNO3 Initial Reading AgNO3 Volume AgNO3 used (ml) (ml) (ml) 1 0.1003 49.5 20.0 29.5 0.00005817 0.1039 33.7 0.0 33.7 0.00005275 0.00005492 NaCl 58.44 g/mol 99.5% 2 0.1004 31.9 0.0 31.9 0.00005385 3

Corrected Volume of AgNO3, mL Molarity of AgNO3 Average Molarity of AgNO3

Titer NaCl (mg/mL) Average Titer NaCl (mg/mL) B. Indicator Blank

3.441 x 10-7 3.441 x 10-7

3.441 x 10-7

3.441 x 10-7

Trials Final volume AgNO3 (ml) Initial volume AgNO3 (ml) Net Volume AgNO3 (ml) Average volume of AgNO3, (ml)

6.1 5.0 1.1 1.2

7.4 6.1 1.3

8.6 7.4 1.2

C. Analysis of Unknown

Trials Mass of the sample (g) Final volume AgNO3 (ml) Initial volume AgNO3 (ml) Net Volume AgNO3 (ml) Corrected volume of AgNO3, (ml) mg Cl- of unknown % Cl- of unknown Average % Cl- of unknown

1 0.2321 62.3 0

62.3 0.021 9.235

0.2027 53.4 0 53.4 0.018 9.064 8.325

0.2402 46.6 0 46.6 0.016 6.675