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Table Of Contents

1 Introduction
2 Literature Review
2.1 Hydrocarbon Components
2.2 Analytical Methods for the Determination of Petroleum
2.2.1 Spectroscopic Methods
2.2.2 Chromatographic Methods
2.2.3 Methods for Petroleum Hydrocarbon Analysis
2.2.3.1 Standard Method 5520
2.2.3.2 Partition-Infrared Method (Standard Method 5520 C)
2.2.3.4 Ultraviolet Fluorescence Spectroscopy and the SiteLAB UVF-3100A
3 Materials and Methods
3.1 Supplies, Reagents & Solutions
3.2 Sample collection, Preservation and Storage:
3.3 Preparation of Artificial Samples
3.4 Analytical Methods
3.4.1 EPA Method 1664, Revision A
3.4.1.1 Quality Control
3.4.2 UVF-3100A and TPH Analysis
4 Quality Control Study
4.1 Initial Precision and Recovery (IPR) Study
4.1.1 IPR Experiment 1
Table 4.1 Initial Precision and Recovery (IPR) study for EPA 1664A
4.1.2 IPR Experiment 2
Table 4.2 Results for the IPR Study: 2
4.1.3 IPR Experiment 3
4.1.4 IPR Experiment 4
4.1.5 IPR Experiment 5
4.1.5.1 Qualitative Test
Figure 4.1 Observation of the evaporation step of the qualitative test
4.1.5.2 Quantitative test
Figure 4.2 Observation of the qualitative test using smooth walled aluminum pan
4.1.6 IPR Experiment 6
4.2 Determination of Method Detection Limit (MDL)
4.4 Ongoing Precision and Recovery Study (OPR)
4.5 Quality Assurance for UVF Method
5.1 Experimental results for Surface Water samples:
5.2 Experimental results of o-terphenyl and stearic acid samples:
5.3 Experimental results of o-terphenyl samples:
Table 5.1 Results for the analysis of o-terphenyl using UVF Method
5.4 Experiments using Formula Shell 10W-30 Motor Oil
Table 5.2 Results for the analysis of Motor oil
5.5 Experiments results of No.6 Fuel Oil:
Table 5.3 Results for the analysis of No.6 Fuel oil
5.6 Experimental results of p-terphenyl samples:
Table 5.4 Results for the analysis of p-terphenyl using EPA Method
Table 5.5 Results of the analysis of p-terphenyl in n-hexane using UVF Method
Table 5.6 Results of the analysis of p-terphenyl in cyclohexane using UVF Method
6 Conclusions
References
Acknowledgement
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Published by: Daniel Franklin on Feb 22, 2012
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01/29/2013

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