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“Process in which a liquid or vapour mixture
of two or more substances is separated into
its component fractions of desired purity, by
the application and removal of heat”
CHOICE BETWEEN PLATE AND
PACKED COLUMN
The choice between use of tray column or a
packed column for a given mass transfer
operation should, theoretically, be based on a
detail cost analysis for the two types of
contactors. However, the decision can be made
on the basis of a qualitative analysis of relative
advantages and disadvantages, eliminating the
need for a detailed cost comparison.
Which are as follows
Liquid dispersion difficulties
Capable of handling wide ranges
liquid rates
Cleaning.
Nonfoaming systems
Periodic cleaning
weight of the column
Design information
Inter stage cooling
Temperature change
Diameters
As my system is non foaming and
diameter calculated is larger than 0.67 m
so I am going to use Tray column.
Also as average temperature calculated
for my distillation column is higher that is
approximately equal to 98
o
c. So I prefer
Tray column.
PLATE CONTACTORS:
Cross flow plate are the most commonly
used plate contactor in distillation. In which
liquid flows downward and vapours flow
upward. The liquid move from plate to plate
via down comer. A certain level of liquid is
maintained on the plates by weir.
Three basic types of cross flow
trays used are
Sieve Plate (Perforated Plate)
Bubble Cap Plates
Valve plates (floating cap plates)
Selection of Trays:
I prefer Sieve Plate because:
Pressure drop is low as compared to bubble
cap trays
Their fundamentals are well established,
entailing low risk.
The trays are low in cost relative to many other
types of trays.
They can easily handle wide variations in flow
rates.
They are lighter in weight. It is easier and
cheaper to install.
Maintenance cost is reduced due to the ease of
cleaning.
Sieve Tray
Label Diagram (sieve tray)
Major Beam
Plate Support
Ring
Downcomer
And
Weir
Calming
Zone
Man
Way
FACTORS AFFECTING DISTILLATION
COLUMN OPERATION
Adverse vapour flow conditions can cause:
Blowing
Coning
Dumping
Raining
Weeping
Flooding
FEED
REFLUX
DRUM
(1) Methyl Iodide = 0.074
(2) Acetic Acid = 0.65
(3)Methyl Acetate = 0.215
(4) Water = 0.065
(1) Methyl Iodide
= 0.212
(2) Acetic Acid =
0.0005
(3)Methyl
Acetate = 0.62
(4) Water = 0.167
Condenser
Pump
Reboiler
FEED
(1) Methyl Iodide = 0.07
(2) Acetic Acid = 0.65
(3)MethylAcetate=0.22
(4) Water = 0.065
REFLUX DRUM
(1) Methyl Iodide = 0.21
(2) Acetic Acid = 0.0005
(3)Methyl Acetate = 0.62
(4) Water = 0.17
(1)Acetic Acid = 0.99
(2)Water = 0.01
FLOW SHEET
From Material Balance:
Heavy Key Component = Acetic Acid
Light Key Component = Water
Component Feed
Fraction
x
f
Bottom
Fraction
x
b
Top
Fraction
x
d
(1) Methyl
Iodide
0.07
0
0.21
(2) Acetic
Acid
0.65
0.99 0.0005
(3) Methyl
Acetate
0.22
0
0.62
(4) Water
0.07
0.01
0.17
DESIGNING STEPS OF
DISTILLATION COLUMN
Calculation of Minimum number of stages.N
min
Calculation of Minimum Reflux Ratio R
m
.
Calculation of Actual Reflux Ratio.
Calculation of theoretical number of stages.
Calculation of actual number of stages.
Calculation of diameter of the column.
Calculation of weeping point, entrainment.
Calculation of pressure drop.
Calculation of the height of the column.
Calculation of Minimum no. of Plates:
The minimum no. of stages N
min
is obtained
from Fenske equation which is,
N
min
= LN[(x
LK
/x
HK
)
D
(x
HK
/x
LK
)
B
]
LN (α
LK
/
HK
)
average
Average geometric relative volatility = 1.53
So,
N
min
= 24
Calculation of Minimum Reflux
Ratio R
m
:
Using Underwood equations
As feed is entering as saturated vapors so,
q = 0
By trial, u = 1.68
Using equation of minimum reflux ratio,
Putting all values we get,
R
m
= 4.154
1 R
θ α
α
θ α
α
m
B
DB B
A
DA A
+ =
÷
+
÷
x x
q 1
θ α
α
θ α
α
B
fB B
A
fA A
÷ =
÷
+
÷
x x
Actual Reflux Ratio:
The rule of thumb is:
R = (1.2  1.5) R
min
R = 1.5 R
min
R = 6.23
Theoretical no. of Plates:
Gilliland related the number of
equilibrium stages and the minimum
reflux ratio and the no. of
equilibrium stages with a plot that
was transformed by Eduljee into the
relation;
From which the theoretical no. of stages
to be,
N= 39
(
¸
(
¸

.

\

+
÷
÷ =
+
÷
566 . 0
min min
1
1 75 . 0
1 R
R R
N
N N
Calculation of actual number of
stages:
Overall Tray Efficiency:
(
¸
(
¸


.

\

÷ =
avg avg o
E o µ . log 5 . 32 51
α
avg
=average relative volatility of light key component
=1.75
μ
avg
= molar average liquid viscosity of feed evaluated at
average temperature of column
Average temperature of column =(118+71)/2
= 95
o
C
Feed viscosity at average temperature = µ
avg
= 0.39 mNs/m
2
So,
E
o
= 56.60%
So,
No. of actual trays = 39/0.566 = 68
Location of feed Plate:
The Kirk bride method is used to determine the
ratio of trays above and below the feed point.
From which,
Number of Plates above the feed tray = ND = 47
Number of Plates below the feed tray = NB = 21
( )
( )
( )
(
¸
(
¸

.

\


.

\

=

.

\

2
log 206 . log
D HK
B LK
LK
HK
B
D
x
x
x
x
D
B
N
N
Determination of the
Column Diameter:
Flow Parameter:
F
LV
= Liquid Vapor Factor = 0.056
0.5
L
v
n
n
LV
ρ
ρ
V
L
F


.

\



.

\

=
Capacity Parameter:
Assumed tray spacing = 18 inch (0.5 m)
From Fig (155) Plant Design and Economics for
Chemical Engineering, sieve tray flooding capacity,
C
sb
= 0.0760 m/Sec
Surface tension of Mixture = σ = 18.35 dynes/Cm
V
nf
=1.67 m/sec
Assume 90% of flooding then
V
n
=0.9V
nf
So, actual vapor velocity,
V
n
=1.51 m/sec
5 . 0
2 . 0
20


.

\
 ÷

.

\

=
v
v l
C V
sb nf
µ
µ µ o
Net column area used in separation is
A
n
= m
v
/V
n
Volumetric flow rate of vapors = m
v
m
v
= (mass vapor flow rate /(3600)
vapor density)
m
v
= 2.1184m
3
/sec
Now, net area A
n
= m
v
/V
n
= 1.41m
2
Assume that downcommer occupies 15% of
cross sectional Area (A
c
) of column thus:
A
c
= A
n
+ A
d
Where, A
d
= downcommer area
A
c
= A
n
+ 0.15(A
c
)
A
c
= A
n
/ 0.85
A
c
=1.65 m
2
So Diameter of Column Is
A
c
=(π/4)D
2
D = (4A
c
/π)
D = 1.45 meter = 5ft
(based upon bottom conditions)
Liquid flow arrangement:
In order to find liquid flow arrangement first
find maximum liquid volumetric flow rate
So liquid flow rate =
(Liquid mass rate)/ (3600) (Liquid density)
Max Liquid Rate Is At the bottom of column
so using "L
m
" values
So Maximum liquid flow rate = 0.005 m
3
/sec
So from fig11.28 Coulson & Richardson 6th
volume 3rd edition cross flow single pass
plate is selected
Provisional Plate Design:
Column Diameter D
c
= 1.4513 m
Column Crosssectional Area(A
c
)= 1.65 m
2
Down comer area Ad = 0.15A
c
= 0.25 m
2
Net Area (A
n
) = A
c
 A
d
=1.41 m
2
Active area A
a
=A
c
2A
d
= 1.16 m
2
Hole area A
h
take 10% A
a
= 0.1 × 1.16
=0.0462 m
2
Weir length
Ad / Ac = 0.248 / 1.654 = 0.15
From figure 11.31 Coulson &
Richardson 6th volume 3rd
edition
L
w
/ dc = 0.80
L
w
= 1.452*0.80
= 0.733 m
Weir length should be 60 to 85% of
column diameter which is satisfactory
Take weir height, h
w
= 50 mm
Hole diameter, d
h
= 5 mm
Plate thickness = 5 mm
Check Weeping:
where U
min
is the minimum design vapor
velocity.
The vapor velocity at weeping point is
the minimum velocity for the stable
operation.
In order to have K
2
value from fig11.30
Coulson & Richardson 6th volume 3rd edition we
have to 1st find h
ow
(depth of the crest
of liquid over the weir)
where h
ow
is calculated by following
formula:
( )
( )
( )
2 / 1
2
min
4 . 25 9 . 0
v
d K
U
h
µ
÷ ÷
=
h
ow
=750[(L
m
/l
w
*ρ)
2/3
]
Maximum liquid rate “L
m
”= 4.7 kg/sec
Minimum Liquid Rate At 70% turn down ratio
= 3.3Kg/sec
At Maximum rate ( h
ow
)= 20 mm Liquid
At Minimum rate (h
ow
) = 16 mm Liquid
h
w
+ h
ow
= 50 + 16 = 66 mm Liquid
from fig 11.30, Coulson and Richardson Vol.6
K
2
= 30.50
So,
U
(min)
= 9 m/sec
Now maximum volumetric flow rate
(vapors)
Base = 2.12 m
3
/sec
Top = 1.14 m
3
/sec
At 70% turn down ratio
Actual minimum vapor velocity
=minimum vapor rate / A
h
= 12.81 m/sec
So minimum vapor rate will be well
above the weep point.
Plate Pressure Drop (P.D):
Consist of dry plate P.D (orifice loss), P.D
due to static head of liquid and residual
P.D (bubbles formation result in energy
loss)
Dry Plate Drop:
Max. Vapor velocity through holes (Uh) =
Maximum Volumetric Flow Rate / Hole
Area = 18.30 m/sec
Perforated area Ap (active area) =1.16 m
2
Ah/Ap = 0.100
From fig. 11.34 (Coulson & Richardson
6th volume 3rd edition) for
plate thickness/hole diameter = 1.00
We get, C
o
= 0.84
This equation is derived for orifice
meter pressure drop.
h
d
= 48 mm Liquid
Residual Head (h
r
):
hr = (12.5*10
3
/ ρ
L
)
= 13.3 mm Liquid
L
V
o
h
d
C
U
h
µ
µ
2
ˆ
51
(
(
¸
(
¸
=
So,
Total pressure drop
=48+(50+20)+13.32
h
t
= 131.35 mm liquid
Total column pressure drop Pa, (N/m
2
)
= (9.81*10
3
) h
t
ρ
L
N
= 82771.6 Pa = 82 kPa
r ow w d t
h h h h h + + + = ) (
Down comer Liquid Backup:
Caused by Pressure Drop over the plate and resistance to
flow in the downcomer it self.
h
b
= (h
w
+ h
ow
) + h
t
+ h
dc
The main resistance to flow in downcomer will be
caused by constriction in the downcomer outlet, and
head loss in the down comer can be estimated using the
equation given as,
where L
wd
is the liquid flow rate in downcomer, kg/sec
and Aap is the clearance area under the downcomer, m
2
A
ap
=h
ap
L
w
2
166
(
(
¸
(
¸
=
ap L
wd
dc
A
l
h
µ
Where h
ap
the height of bottom edge of
apron above the plate.
h
ap
= h
w
– (5 to 10 mm)
h
ap
= 40 mm
so,
Area under apron “A
ap
” = 0.05 m
2
As this is less than area of downcomer A
d
so
using A
ap
values in above formula.
So,
h
dc
= 1.95 mm
As a result,
h
b
= 203.24 mm
= 0.203 m
h
b
< ½ (Tray spacing + weir height)
0.20 < 0.25
So tray spacing is acceptable
Check Residence Time:
Sufficient residence time should be allowed
in the downcomer for the entrained vapors
to disengage from liquid stream to prevent
aerated liquid being carried under the
downcomer.
t
r
=A
d
h
bc
ρ
L
/L
(max)
t
r
= 10 sec
It should be > 3 sec. so, result is satisfactory
Check Entrainment:
(u
n
) actual velocity = (maximum volumetric
flow rate at base V
m
/ net area A
n
)
(u
n
) actual velocity = 1.51 m/sec
Velocity at flooding condition U
f
= 1.67 m/sec
So Percent flooding =u
n
/ u
f
= 0.90 = 90%
Liquid flow factor F
LV
= 0.056
From fig. 11.29 Coulson &
Richardson 6th volume 3rd edition
fractional entrainment ψ can be found
out.
Fractional entrainment (ψ) =
0.0750
Well below the upper limit of (ψ) which
is 0.1. Below this the effect of
entrainment on efficiency is small.
No of Holes:
Area of 1 Hole = (π/4) D
hole
2
= 0.00002 m
2
Area of N Holes = 0.1158 m
2
So,
Number OF Holes = 5900
Height of Distillation Column
Height of column H
c
= (N
act
1) H
s
+ ∆H+ plates
thickness
No. of plates = 68
Tray spacing H
s
= 0.50 m
∆H= 0.5 meter each for liquid hold up and
vapor disengagement
∆H=1 m
Total thickness of trays = 0.005*68 = 0.34 m
So,
Height of column = (681)*0.50+ 1+0.34
= 35 meters
1.45m height=35m
Hole
diameter=5mm
No. of
holes=5900
h
ap
=40 mm
h
W
=50 mm
h
ow
=Weir crust
Plate Specifications
Specification Sheet Of Distillation Column:
Identification:
Item Distillation column
No. required 1
Tray type Sieve tray
Function: Separation of Acetic Acid from iodo methane
and Reaction by products.
Operation: Continuous
Feed
Top
Bottom
Amount
4755 Kg/hr
1968 Kg/hr
2786 Kg/hr
Composition
of
Acetic Acid
0.64
0.005
0.99
Temp.
119
o
C
71
o
C
118
o
C
Material handled:
Design data:
No. of tray= 68
Pressure = 101.325 Kpa
Height of column = 35 m
Diameter of column=1.45m
Hole size = 5 mm
Pressure drop per
tray=1.2 Kpa
Tray thickness = 5 mm
Active holes = 5900
Weir height = 50 mm
Weir length = 1 m
Reflux ratio = 6.23
Tray spacing =0.5 m
Active area = 1.16 m
2
Percent Flooding =90%
Entrainment = 0.075
References
Coulson & Richardson 6th volume 3rd
edition
Plant Design and Economics for
Chemical Engineering
Coulson & Richardson 2th volume 5th
edition
Perry’s Chemical engineer’s hand book
The End
Distillation:
“Process in which a liquid or vapour mixture of two or more substances is separated into its component fractions of desired purity, by the application and removal of heat”
CHOICE BETWEEN PLATE AND PACKED COLUMN
The choice between use of tray column or a packed column for a given mass transfer operation should, theoretically, be based on a detail cost analysis for the two types of contactors. However, the decision can be made on the basis of a qualitative analysis of relative advantages and disadvantages, eliminating the need for a detailed cost comparison.
Which are as follows
Liquid dispersion difficulties Capable of handling wide ranges liquid rates Cleaning. Nonfoaming systems Periodic cleaning weight of the column Design information Inter stage cooling Temperature change Diameters
67 m so I am going to use Tray column.As my system is non foaming and diameter calculated is larger than 0. So I prefer Tray column. . Also as average temperature calculated for my distillation column is higher that is approximately equal to 98oc.
The liquid move from plate to plate via down comer.PLATE CONTACTORS: Cross flow plate are the most commonly used plate contactor in distillation. In which liquid flows downward and vapours flow upward. . A certain level of liquid is maintained on the plates by weir.
Three basic types of cross flow trays used are Sieve Plate (Perforated Plate) Bubble Cap Plates Valve plates (floating cap plates) .
Selection of Trays: .
entailing low risk. They are lighter in weight.I prefer Sieve Plate because: Pressure drop is low as compared to bubble cap trays Their fundamentals are well established. . The trays are low in cost relative to many other types of trays. It is easier and cheaper to install. Maintenance cost is reduced due to the ease of cleaning. They can easily handle wide variations in flow rates.
Sieve Tray .
Label Diagram (sieve tray) Downcomer And Weir Man Way Calming Zone Major Beam Plate Support Ring .
FACTORS AFFECTING DISTILLATION COLUMN OPERATION Adverse vapour flow conditions can cause: Blowing Coning Dumping Raining Weeping Flooding .
65 (3)Methyl Acetate = (3)MethylAcetate=0.62 (4) Water = 0.065 Pump Reboiler (1)Acetic Acid = 0.167 FEED FEED (1) Methyl Iodide = 0.17 (4) Water = 0.07 (2) Acetic = 0.22 0.01 .21 (2) Acetic Acid =(2) Acetic Acid = 0.074 (1) Methyl Iodide = 0.99 (2)Water = 0.FLOW SHEET Condenser REFLUX DRUM REFLUX DRUM (1) Methyl Iodide = 0.065 (4) Water = 0.212 (1) Methyl Iodide = 0.0005 0.0005 (3)Methyl Acetate = 0.215 (4) Water = 0.62 (3)Methyl Acetate = 0.65 (2) Acetic AcidAcid = 0.
07 0.01 0.22 0.62 0.99 0 0.From Material Balance: Component Feed Fraction xf Bottom Fraction xb Top Fraction xd (1) (2) (3) (4) Methyl Iodide Acetic Acid Methyl Acetate Water 0.0005 0.65 0.07 0 0.21 0.17 Heavy Key Component = Acetic Acid Light Key Component = Water .
Nmin Minimum Reflux Ratio Rm. entrainment.DESIGNING STEPS OF DISTILLATION COLUMN Calculation Calculation Calculation Calculation Calculation Calculation Calculation Calculation Calculation of of of of of of of of of Minimum number of stages. Actual Reflux Ratio. the height of the column. actual number of stages. weeping point. diameter of the column. theoretical number of stages. . pressure drop.
53 So. Nmin = 24 . of Plates: The minimum no. of stages Nmin is obtained from Fenske equation which is. Nmin = LN[(xLK/xHK)D(xHK /xLK)B] LN (αLK/HK) average Average geometric relative volatility = 1.Calculation of Minimum no.
Rm = 4.154 . q=0 By trial.68 Using equation of minimum reflux ratio. = 1. α A xfA α x B fB 1 q αA θ αB θ Putting all values we get.Calculation of Minimum Reflux Ratio Rm: Using Underwood equations α A xDA α B xDB Rm 1 αA θ αB θ As feed is entering as saturated vapors so.
Actual Reflux Ratio: The rule of thumb is: R = (1.5) R R = 1.23 min .2 .5 R min R = 6.1.
Theoretical no.566 R Rmin 0. N N min 0. N= 39 .751 N 1 R 1 From which the theoretical no. of Plates: Gilliland related the number of equilibrium stages and the minimum reflux ratio and the no. of equilibrium stages with a plot that was transformed by Eduljee into the relation. of stages to be.
avg α avg =average relative volatility of light key component =1.75 μ avg = molar average liquid viscosity of feed evaluated at average temperature of column .5log avg .Calculation of actual number of stages: Overall Tray Efficiency: Eo 51 32.
39 mNs/m2 So. No.566 = 68 . of actual trays = 39/0.Average temperature of column =(118+71)/2 = 95 oC Feed viscosity at average temperature = avg = 0. Eo = 56.60% So.
206 log B log D x HK D NB x LK From which.Location of feed Plate: The Kirk bride method is used to determine the ratio of trays above and below the feed point. 2 ND x HK x LK B . Number of Plates above the feed tray = ND = 47 Number of Plates below the feed tray = NB = 21 .
Determination of the Column Diameter: Flow Parameter: Ln F LV V n ρ v ρ L 0.5 FLV = Liquid Vapor Factor = 0.056 .
67 m/sec Assume 90% of flooding then Vn=0.Capacity Parameter: Assumed tray spacing = 18 inch (0.2 l v v 0. sieve tray flooding capacity.0760 m/Sec Surface tension of Mixture = σ = 18. Vn=1.35 dynes/Cm Vnf Csb 20 0.5 m) From Fig (155) Plant Design and Economics for Chemical Engineering.51 m/sec .5 Vnf=1. Csb = 0. actual vapor velocity.9Vnf So.
41m2 Assume that downcommer occupies 15% of cross sectional Area (Ac) of column thus: Ac = An + Ad Where. Ad = downcommer area . net area An = mv/Vn = 1.Net column area used in separation is An = mv/Vn Volumetric flow rate of vapors = mv mv = (mass vapor flow rate /(3600) vapor density) mv = 2.1184m3/sec Now.
Ac = An + 0.45 meter = 5ft (based upon bottom conditions) .15(Ac) Ac = An / 0.65 m2 So Diameter of Column Is Ac =(π/4)D2 D = (4Ac/π) D = 1.85 Ac=1.
005 m3/sec So from fig11.Liquid flow arrangement: In order to find liquid flow arrangement first find maximum liquid volumetric flow rate So liquid flow rate = (Liquid mass rate)/ (3600) (Liquid density) Max Liquid Rate Is At the bottom of column so using "Lm" values So Maximum liquid flow rate = 0.28 Coulson & Richardson 6th volume 3rd edition cross flow single pass plate is selected .
1 × 1.Provisional Plate Design: Column Diameter Dc= 1.16 =0.0462 m2 Weir length Ad / Ac = 0.16 m2 Hole area Ah take 10% Aa = 0.248 / 1.Ad =1.15 .41 m2 Active area Aa=Ac2Ad = 1.654 = 0.15Ac = 0.25 m2 Net Area (An) = Ac .4513 m Column Crosssectional Area(Ac)= 1.65 m2 Down comer area Ad = 0.
452*0.From figure 11.80 = 0. hw= 50 mm Hole diameter.80 Lw = 1.31 Coulson & Richardson 6th volume 3rd edition Lw / dc = 0. dh = 5 mm Plate thickness = 5 mm .733 m Weir length should be 60 to 85% of column diameter which is satisfactory Take weir height.
In order to have K2 value from fig11.Check Weeping: K 2 0.30 Coulson & Richardson 6th volume 3rd edition we have to 1st find how(depth of the crest of liquid over the weir) where how is calculated by following formula: .925. The vapor velocity at weeping point is the minimum velocity for the stable operation.4 d h U min v1 / 2 where Umin is the minimum design vapor velocity.
30.50 So.7 kg/sec Minimum Liquid Rate At 70% turn down ratio = 3.6 K2 = 30.3Kg/sec At Maximum rate ( how)= 20 mm Liquid At Minimum rate (how) = 16 mm Liquid hw + how = 50 + 16 = 66 mm Liquid from fig 11.how=750[(Lm/lw*ρ)2/3] Maximum liquid rate “Lm”= 4. Coulson and Richardson Vol. U (min) = 9 m/sec .
81 m/sec So minimum vapor rate will be well above the weep point. .14 m3/sec At 70% turn down ratio Actual minimum vapor velocity =minimum vapor rate / Ah = 12.Now maximum volumetric flow rate (vapors) Base = 2.12 m3/sec Top = 1.
16 m2 Ah/Ap = 0.Plate Pressure Drop (P. Vapor velocity through holes (Uh) = Maximum Volumetric Flow Rate / Hole Area = 18.100 .D (bubbles formation result in energy loss) Dry Plate Drop: Max.D (orifice loss).D): Consist of dry plate P.D due to static head of liquid and residual P. P.30 m/sec Perforated area Ap (active area) =1.
00 We get. 11.84 ˆ U h V hd 51 Co L 2 This equation is derived for orifice meter pressure drop.5*103 / ρL) = 13. Co = 0.3 mm Liquid .34 (Coulson & Richardson 6th volume 3rd edition) for plate thickness/hole diameter = 1.From fig. hd= 48 mm Liquid Residual Head (hr): hr = (12.
So.35 mm liquid Total column pressure drop Pa. (N/m2) = (9.32 ht = 131.6 Pa = 82 kPa . ht hd (hw how ) hr Total pressure drop =48+(50+20)+13.81*103) htρLN = 82771.
m2 Aap =hapLw . kg/sec and Aap is the clearance area under the downcomer. and head loss in the down comer can be estimated using the equation given as.Down comer Liquid Backup: Caused by Pressure Drop over the plate and resistance to flow in the downcomer it self. hb = (hw+ how) + ht + hdc The main resistance to flow in downcomer will be caused by constriction in the downcomer outlet. hdc l wd 166 L Aap 2 where Lwd is the liquid flow rate in downcomer.
05 m2 As this is less than area of downcomer Ad so using Aap values in above formula.Where hap the height of bottom edge of apron above the plate. So. hdc = 1. so. hap = hw – (5 to 10 mm) hap = 40 mm Area under apron “Aap” = 0.95 mm .
203 m hb < ½ (Tray spacing + weir height) 0.As a result. hb = 203.24 mm = 0.25 So tray spacing is acceptable .20 < 0.
result is satisfactory . tr =Ad hbc ρL/L(max) tr = 10 sec It should be > 3 sec.Check Residence Time: Sufficient residence time should be allowed in the downcomer for the entrained vapors to disengage from liquid stream to prevent aerated liquid being carried under the downcomer. so.
67 m/sec So Percent flooding =un/ uf = 0.51 m/sec Velocity at flooding condition Uf = 1.Check Entrainment: (un) actual velocity = (maximum volumetric flow rate at base Vm / net area An) (un) actual velocity = 1.90 = 90% .
11. .0750 Well below the upper limit of (ψ) which is 0.1.29 Coulson & Richardson 6th volume 3rd edition fractional entrainment ψ can be found out. Fractional entrainment (ψ) = 0.056 From fig.Liquid flow factor FLV = 0. Below this the effect of entrainment on efficiency is small.
Number OF Holes = 5900 .1158 m2 So.00002 m2 Area of N Holes = 0.No of Holes: Area of 1 Hole = (π/4) Dhole2 = 0.
Height of Distillation Column Height of column Hc= (Nact1) Hs+ ∆H+ plates thickness No.34 m So.50+ 1+0.005*68 = 0.34 = 35 meters .50 m ∆H= 0. Height of column = (681)*0. of plates = 68 Tray spacing Hs = 0.5 meter each for liquid hold up and vapor disengagement ∆H=1 m Total thickness of trays = 0.
of holes=5900 h W=50 mm .45m height=35m Hole diameter=5mm hap=40 mm No.Plate Specifications how=Weir crust 1.
Operation: Continuous . required 1 Tray type Sieve tray Function: Separation of Acetic Acid from iodo methane and Reaction by products.Specification Sheet Of Distillation Column: Identification: Item Distillation column No.
119oC 71oC 118oC .Material handled: Feed Amount Composition of Acetic Acid 4755 Kg/hr Top 1968 Kg/hr Bottom 2786 Kg/hr 0.64 0.99 Temp.005 0.
45m Hole size = 5 mm Pressure drop per tray=1.Design data: No. of tray= 68 Pressure = 101.23 Tray spacing =0.5 m Active area = 1.16 m2 Percent Flooding =90% Entrainment = 0.2 Kpa Tray thickness = 5 mm Active holes = 5900 Weir height = 50 mm Weir length = 1 m Reflux ratio = 6.325 Kpa Height of column = 35 m Diameter of column=1.075 .
References Coulson & Richardson 6th volume 3rd edition Plant Design and Economics for Chemical Engineering Coulson & Richardson 2th volume 5th edition Perry’s Chemical engineer’s hand book .
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