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Icon NMR Manual

Icon NMR Manual

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Published by sahaj
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Published by: sahaj on Apr 03, 2013
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12/03/2014

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NOTE: Routine Spectroscopy is designed to help users perform NMR experiments by
following a step by step menu.

1. Type iconnmr

2. Click on ‘Routine Spectroscopy’

3. Click on ‘Identify User’

4. Select user

5. Click on ‘OK’

6. Enter the password

134

Journey through ICON-NMR Setup

DONE

INDEX

INDEX

7. Click on ‘Inject/Eject’

7.6 Routine Spectroscopy

135

DONE

INDEX

INDEX

8. Click on ‘Insert Sample’ and wait until the ”Insert Sample” window appears

9. Insert your sample

10. Click on ‘OK’

136

Journey through ICON-NMR Setup

DONE

INDEX

INDEX

11. Type sample for Data Set Filename

12. Type 10 for Experiment No.

13. Click on ‘OK’

14. Click on ‘Continue’

7.6 Routine Spectroscopy

137

DONE

INDEX

INDEX

15. Select solvent e.g. CDCl3

16. Click on ‘Continue’

NOTE: If the data set name ”sample 10” already exists, a Data Set Report window
appears which gives the option to overwrite the existing data set or to increment the
experiment number to the next available one.

138

Journey through ICON-NMR Setup

DONE

INDEX

INDEX

17. Select the experiment PROTON

18. Click on ‘Set Plot Title’

7.6 Routine Spectroscopy

139

DONE

INDEX

INDEX

19. Click in the ”Plot Title Setup” window and enter a plot title

20. Click on ‘Save’

21. Click on ‘OK’

22. Click on ‘START’

NOTE: At this point an ”Online Control” window and the acquisition status icons
appear on the screen.

140

Journey through ICON-NMR Setup

DONE

INDEX

INDEX

Online Control function keys:

FID

display the acquisition window

(active after the acquisition has started

Lock

view the lock window

Spectrum

view the spectrum window

Halt

stop the acquisition after the next scan

is completed then start the processing

Plot

plot data or additional expansions

EXIT

to exit back to ICON-NMR/Routine window

Stop

stop all processes and do not continue

7.6 Routine Spectroscopy

141

DONE

INDEX

INDEX

Search

open the Portfolio Editor

23. Click on ‘EXIT’ after all processing status icons stop flashing

24. Click on ‘Eject + Terminate’

25. Remove your sample and insert another other sample if desired.

NOTE: It is generally better to keep a sample in the magnet if the instrument will not
be used for a long periods of time.

142

Journey through ICON-NMR Setup

DONE

INDEX

INDEX

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