You are on page 1of 15

Cc phng php phn tch Ha l (Instrumental Analysis)

M mn hc: 602002

M u

Instrumental Analysis
3 tn ch (2 l thuyt v 1 th nghim) Mn tin quyt: Ha Phn tch
Ging vin: Trn Th Kiu Anh Phng TN Ha Phn tch, 207 B2 B mn K thut Ha l E-mail: ttkanh@hcmut.edu.vn

Mn k tip: Phn tch K thut


M u
2

Gii thiu mn hc
Ha phn tch (Analytical Chemistry)
nh tnh (Qualitative), nh lng (Quantitative)

Ha phn tch (Analytical Chemistry 1)


Cc hng s cn bng, hng s cn bng iu kin Phng php phn tch ha hc (Classical Analysis)
Phng php phn tch khi lng (Gravimetric Analysis) Phng php phn tch th tch (Titrimetric Analysis)

Phng php phn tch dng c (Instrumental Analysis)


PP quang ph hp thu t ngoi v thy c (UV-Vis) PP chun in th (Potentiometric)

M u

Cc phng php phn tch ha l (Instrumental Analysis) (Analytical Chemistry 2)

Phng php ha hc
Chun Axit - baz

M u

Phng php ha hc
Chun oxy ha kh

M u

Pp ptch dng c
Pp quang ph hp thu thy c (Vis)
nh lng Fe trong mu nc
1

7 2 3

M u

Phng php phn tch dng c


Chun t ng

M u

1. Define the Problem 2. Select a Method

Cc giai on ca 1 phng php phn tch (The Analytical Process)


What is the problem (Qualitative and/or quantitative?), Sample type, sample size, analytes, concentrations (large amounts or small amounts), how much tools or instrument available, cost, speed, sensitivity,) Sample type/homogeneity/size

4. Prepare the Sample for Analysis

3. Obtain a Representative Sample

5. Perform the Measurement

Sample type (gas, solid, liquid), dissolve (pH, reagent), concentration, derivatize Distillation, precipitation, solvent extraction, solid phase extraction

- Titrations, chromatography

6. Calculation the Results and Report


8

or electrophoresis

M u

Ni dung
2

Nhm pp ph nghim
Ph t ngoi kh kin (UV/VIS) Ph hng ngoi (IR) Khi ph (MS) Ph cng hng t ht nhn (NMR)
M u

Ph nguyn t
1

Nhm pp in
3

Nhm pp tch
4 Sc k n

PP in khi lng PP pt da vo o th PP VoltAmpere

gin

5 6 7

Sc k kh (GC) Sc k lng (HPLC)

Ni dung

Chng 1: i cng v cc phng php phn tch quang Chng 2: Ph t ngoi kh kin (UV-VIS) Chng 3: Ph hng ngoi (IR) Chng 4: Ph nguyn t Chng 5: Khi ph (MS) Chng 6: Ph cng hng t (NMR) Chng 7: i cng v cc phng php phn tch in ha Chng 8: Phng php in khi lng Chng 9: Phng php phn tch da vo vic o th
10

M u

Ni dung (tt)
Chng 10: Phng php Volt-Ampere Chng 11: i cng v phng php sc k Chng 12: Sc k n gin Chng 13: Sc k kh Chung 14: Sc k lng

M u

11

Ni dung (tm tt)


Tun 1 7 Pp UV-VIS, Ph nguyn t, pp in, pp sc k n gin Tun 10 -16 Pp sc k kh (GC), pp sc k lng (HPLC), pp hng ngoi (IR), pp khi kh (MS) v pp cng hng t ht nhn (NMR) Tun 8,9
/////////////

Tun 17,18
/////////////

M u

12

Ti liu tham kho


Phn tch nh lng, Nguyn Th Thu Vn, HQG TP. HCM Th nghim Phn tch nh lng, Nguyn Th Thu Vn, Trn Th Minh Hiu, Nguyn Duy Khim, L Xun Mai, Nguyn Bch Tuyt, HQG TP. HCM Bi tp v S tay Phn tch nh lng, Nguyn Th Thu Vn, HQG TP. HCM Analytical chemistry, Gary D. Christian, 6th edition, John Wiley & Sons, 2004.

M u

13

Ti liu tham kho


Modern Analytical Chemistry, David Harvey, The McGraw-Hill Companies, Inc., 2000. Introduction to Spectroscopy, third edition, Donald L. Pavia, Gary M. Lampman and George S. Kriz, Thomson learning, Inc., 2001.

M u

14

Cc phng php phn tch Ha l


Mc tiu
Phng php phn tch dng c (nh tnh v nh lng) Xy dng phng php phn tch thch hp cho tng i tng phn tch

Yu cu i vi sinh vin
c trc bi ging, sch tham kho v lm bi tp sau mi chng

Ni dung nh gi

T luan va trac nghiem

Kim tra gia hc k (45): 30% Kim tra cui k (90): 70%
M u
15