BCF train (hydrogen carrier

)

C1 C3+ N2 CO2 C2 Vent

Causes peak generation

.00

15.00

30.00

60.00

90.00

Seconds

Typical settings (individual analyzers may vary) Cycle time Sort order Sample size Target component Target retention time Inject time 90 seconds 84 40 ul C2 60 seconds 6 seconds Inject time variance Carrier pressure Carrier pressure variance Flow rate Flow rate variance Oven temperature ± 10% 30 psig ± 15% 20 ml/min ± 15% 60° C

Range (mol%) Component number Separated component Maximum

%RSD Minimum detectable limit (mol%) Peak detection method Minimum peak area Peak retention time Peak direction Baseline segment start 0 0 0 0 0 0 Baseline segment end 0 0 0 0 0 0 Front height ratio 0.95 0.95 0.75 0.75 0.75 0.75 Slope (rise) 3 3 3 3 3 3 Slope (run) 9 5 5 5 5 5

Minimum

1 2 3 4 5 6

Propane plus Nitrogen Methane Carbon dioxide Ethylene Ethane

0.1 0.1 0.1 0.2 0.2 0.2

100 100 100 100 100 100

2 2 2 2 2 2

0.02 0.02 0.02 0.02 0.02 0.02

7.2 10.4 10.4 21.75 28 52

8.8 11.07 14 24 44 57.4

10.4 21.75 21.75 26 52 64

Gate off

Gate on

3000 3000 3000 3000 3000 3000

Auto Auto Auto Auto Auto Auto

Positive Positive Positive Positive Positive Positive

Interfering component Water Acetylene

Symbol H2O C2*

Max. tolerance 0.02 0.01

Notes Elutes with H2S Elutes with C2=

64 BCF | PGC1000 analytical offerings

Backflush mode In column A. they change the amount of energy necessary to maintain the temperature level of the bead. This change in energy is what causes the peak generation for each of the gasses. The lighter gasses will continue through column B. the lighter gasses have already moved through column A and into column B.BCF train Inject mode 15 (±2) seconds The provided illustration shows that during the inject mode. C3 and heavier gasses are combined into a group named C3+. Simplified view Sample & Carrier Column A Column B To Detector & Vent Simplified view To Detector & Vent Column A Column B Carrier GC Valve 1 Col 1A Detector GC Valve 1 Col 1A Detector Col 1B Sample Vent Vent EPC Sample Vent Col 1B Vent EPC Stream Input 3-15 psig Carrier In Stream Input 3-15 psig Carrier In PGC1000 analytical offerings | BCF 65 . When the gasses cross the detector bead. The heavier gasses are retained on column A. pass through column A again and cross the detector bead.

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