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102\ul0\nosupersub\cf11\f12\fs22 HO\ul0\nosupersub\cf10\f11\fs24 \u-3961?\u-3960
?\u-3960?\ul0\nosupersub\cf11\f12\fs22 CO{\par}}}}\pard\sb0\sl-240{\bkmkstart P
g1}{\bkmkend Pg1}\par\pard\ql \li8311\sb0\sl-220\slmult0 \par\pard\ql\li8311\ri1
004\sb139\sl-220\slmult0\tx8795 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf
1\f2\fs20 Rolando Oyola Martnez, Ph. D. \line\tab \up0 \expndtw-3\charscalex100 D
epartamento de Qumica \par\pard\ql \li9580\sb12\sl-230\slmult0 \up0 \expndtw-3\ch
arscalex100 100 Carretera 908 \par\pard\ql \li8824\ri1006\sb2\sl-240\slmult0\tx9
105 \up0 \expndtw-3\charscalex100 Humacao, PR 00791-4300 \line\tab \up0 \expndtw
-3\charscalex100 rolando.oyola@upr.edu \par\pard\ql \li1170\sb167\sl-184\slmult0
\up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf4\f5\fs16 Derechos Reservados@2
012-13 \par\pard\ql \li3083\sb240\sl-276\slmult0 \up0 \expndtw0\charscalex102 \u
l0\nosupersub\cf6\f7\fs24 Espectrofotometra: Determinacin de manganeso en acero\pa
r\pard\sect\sectd\sbknone\cols2\colno1\colw6176\colsr160\colno2\colw5764\colsr16
0\ql \li1169\sb0\sl-230\slmult0 \par\pard\ql \li1170\sb2\sl-230\slmult0 \up0 \ex
pndtw0\charscalex106 \ul0\nosupersub\cf5\f6\fs20 Introduccin\par\pard\qj \li1170\
ri220\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex102 El acero es una aleacin de
metales donde el manganeso \line \up0 \expndtw0\charscalex106 (Mn, PA 54.938) se
encuentra en cantidades pequeas \line \up0 \expndtw-1\charscalex100 (aproximadam
ente 0.5% w/w). La cantidad de manganeso \line \up0 \expndtw0\charscalex106 depe
nde de la compaa comercial que lo produce y la \line \up0 \expndtw0\charscalex103
aplicacin del acero. En trminos generales, en el acero \line \up0 \expndtw-2\chars
calex100 tambin se puede encontrar presente otros metales como el \line \up0 \exp
ndtw-1\charscalex100 hierro, cromo y nquel. La presencia de una diversidad de \l
ine \up0 \expndtw-2\charscalex100 metales y en diferentes concentraciones hacen
que el acero \line \up0 \expndtw0\charscalex107 posea ciertas cualidades fsicas.
El manganeso, por su \line \up0 \expndtw0\charscalex103 parte, le aumenta la
fortaleza, dureza, durabilidad y \line \up0 \expndtw0\charscalex108 resisten
cia al uso del acero. Otra forma molecular del \line \up0 \expndtw-1\charscalex1
00 manganeso, el bixido de manganeso, se puede usar como \line \up0 \expndtw0\cha
rscalex102 depolarizador. El manganeso es el responsable del color \line \up0 \e
xpndtw-2\charscalex100 amatista en piedras y vidrios.\par\pard\qj \li1169\ri223\
sb0\sl-229\slmult0\fi180 \up0 \expndtw0\charscalex112 El mtodo ms usado en
la determinacin \line \up0 \expndtw-1\charscalex100 espectrofotomtrica de man
ganeso se basa en la oxidacin \line \up0 \expndtw0\charscalex101 del in de mangane
so, Mn\ul0\super\cf7\f8\fs19 2+\ul0\nosupersub\cf5\f6\fs20 al permanganato, MnO
\ul0\sub\cf7\f8\fs19 4-\ul0\nosupersub\cf5\f6\fs20 . El \line \up0 \expndtw0\cha
rscalex103 in de permanganato absorbe luz visible en la regin de \line \up0 \expnd
tw-1\charscalex100 los 525 nm lo que le imparte un color violeta a la solucin \li
ne \up0 \expndtw0\charscalex109 acuosa de este in. El agente oxidante es el iodat
o de \line \up0 \expndtw-3\charscalex100 potasio (KIO\ul0\sub\cf7\f8\fs19 4\ul0\
nosupersub\cf5\f6\fs20 , PM 230.000) el cual oxida a Mn\ul0\super\cf7\f8\fs19 2+
\ul0\nosupersub\cf5\f6\fs20 mediante \line \up0 \expndtw-3\charscalex100 la ec
uacin (1):\par\pard\ql \li1169\sb0\sl-161\slmult0 \par\pard\ql \li1520\sb7\sl-161
\slmult0\tx2114\tx3927\tx4700\tx5444 \up0 \expndtw-2\charscalex100 \ul0\nosupers
ub\cf9\f10\fs13 2 \up0 \expndtw-6\charscalex80 \u-4053? \tab \up0 \expndtw-6\cha
rscalex80 \u-4051? \tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf8\f9\fs1
1 \u-4051? \tab \up0 \expndtw-6\charscalex80 \ul0\nosupersub\cf9\f10\fs13 \u-405
1? \tab \up0 \expndtw-6\charscalex80 \u-4053?\par\pard\column \ql \li20\sb229\sl
-230\slmult0 \up0 \expndtw0\charscalex110 \ul0\nosupersub\cf5\f6\fs20 espectrofo
tomtricas las llevar a cabo en un\par\pard\ql \li20\sb0\sl-230\slmult0
\up0 \expndtw-3\charscalex100 espectrofotmetro Hewlett Packard modelo 8453.\par\
pard\ql \li1169\sb0\sl-230\slmult0 \par\pard\ql \li20\sb3\sl-230\slmult0 \up0 \e
xpndtw0\charscalex103 Objetivo\par\pard\qj \li20\ri967\sb0\sl-229\slmult0 \up0 \
expndtw-2\charscalex100 Determinar la concentracin de manganeso en una muestra \u
p0 \expndtw0\charscalex107 de acero por medidas espectrofotomtricas y curva de \u
p0 \expndtw-3\charscalex100 calibracin.\par\pard\ql \li1169\sb0\sl-230\slmult0 \p

ar\pard\ql \li20\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex102 Mtodo\par\pard\q
j \li20\ri969\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex118 En el experime
nto se usar la tcnica de \line \up0 \expndtw0\charscalex101 espectrofoto
metra. La tcnica se basa en la absorcin de \line \up0 \expndtw0\charscalex101 luz p
or parte de un cromforo (especie qumica capaz de \line \up0 \expndtw0\charscalex10
6 absorber luz). La determinacin cuantitativa del \line \up0 \expndtw0\
charscalex109 manganeso se basa en la ley de Beer-Lambert la cual \line \up0 \ex
pndtw0\charscalex108 establece que la absorbencia es proporcional a la \l
ine \up0 \expndtw0\charscalex101 concentracin del cromforo. Se construir una curva
de \line \up0 \expndtw0\charscalex100 calibracin con soluciones de concentracin co
nocida del \line \up0 \expndtw-2\charscalex100 in de permanganato y se determinar
los parmetros de la \line \up0 \expndtw0\charscalex105 pendiente e intercepto
por el mtodo de cuadrados \line \up0 \expndtw0\charscalex108 mnimos. La co
ncentracin del desconocido se \line \up0 \expndtw0\charscalex114 determinar
en base a los valores de la pendiente e \line \up0 \expndtw-3\charscalex100 inte
rcepto obtenidos por el mtodo de cuadrados mnimos.\par\pard\ql \li1169\sb0\sl-230\
slmult0 \par\pard\ql \li20\sb2\sl-230\slmult0 \up0 \expndtw0\charscalex104 React
ivos y su preparacin:\par\pard\sect\sectd\sbknone\cols2\colno1\colw6176\colsr160\
colno2\colw5764\colsr160\ql \li1196\sb0\sl-213\slmult0\tx1720\tx5672 \up0 \expnd
tw-3\charscalex100 \ul0\nosupersub\cf6\f7\fs24 2 \up0 \expndtw-11\charscalex82 M
n\tab \up0 \expndtw-11\charscalex80 \u-4053? \up0 \expndtw-3\charscalex100 5 \up
0 \expndtw-11\charscalex95 IO \up0 \expndtw-3\charscalex100 ( \up0 \expndtw-11\c
harscalex94 ac \up0 \expndtw-3\charscalex100 ) \up0 \expndtw0\charscalex61 \u-40
53? 3 \up0 \expndtw-3\charscalex100 H \up0 \expndtw-3\charscalex100 O \up0 \expn
dtw0\charscalex130 \ul0\nosupersub\cf10\f11\fs24 \u-3961?\u-3960?\u-3960? \up0 \
expndtw-3\charscalex100 \ul0\nosupersub\cf6\f7\fs24 2 \up0 \expndtw-11\charscale
x82 MnO \up0 \expndtw-3\charscalex100 ( \up0 \expndtw-11\charscalex94 ac \up0 \e
xpndtw-3\charscalex100 ) \up0 \expndtw-11\charscalex80 \u-4053? \up0 \expndtw-3\
charscalex100 5 \up0 \expndtw-11\charscalex95 IO \up0 \expndtw-3\charscalex100 (
\up0 \expndtw-11\charscalex94 ac \up0 \expndtw-3\charscalex100 ) \up0 \expndtw11\charscalex80 \u-4053? \up0 \expndtw-3\charscalex100 6 \up0 \expndtw-3\charsca
lex100 H\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf5\f6\fs20 (1)\par\p
ard\column \ql \li20\sb0\sl-160\slmult0 \up0 \expndtw0\charscalex109 1)\ul0\nosu
persub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Solucin valorada de KMnO\ul0\s
ub\cf7\f8\fs19 4\ul0\nosupersub\cf5\f6\fs20 (~0.02 M) = ya se\par\pard\sect\s
ectd\sbknone\cols2\colno1\colw6175\colsr160\colno2\colw5765\colsr160\ql \li1509\
sb0\sl-126\slmult0\tx2099\tx2835\tx3911\tx4682\tx5427 \up0 \expndtw-2\charscalex
100 \ul0\nosupersub\cf9\f10\fs13 ( \up0 \expndtw-6\charscalex75 ac )\tab \up0 \e
xpndtw-2\charscalex100 4\tab \up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw-2
\charscalex100 \ul0\nosupersub\cf8\f9\fs11 4\tab \up0 \expndtw-2\charscalex100 \
ul0\nosupersub\cf9\f10\fs13 3\tab \up0 \expndtw-2\charscalex100 ( \up0 \expndtw6\charscalex94 ac \up0 \expndtw-2\charscalex100 )\par\pard\qj \li1169\ri221\sb0\
sl-229\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf5\f6\fs20 El anlisi
s espectrofotomtrico de manganeso en el acero \line \up0 \expndtw-1\charscalex100
presenta una posible interferencia de parte del hierro. Esto \line \up0 \expndt
w-1\charscalex100 se debe a que el hierro en el acero se encuentra en grandes \l
ine \up0 \expndtw-2\charscalex100 cantidades y al disolver el acero este pasa al
in frrico. La \line \up0 \expndtw0\charscalex101 interferencia del in frrico se pue
de minimizar al aadir \line \up0 \expndtw-1\charscalex100 cido fosfrico donde el in
de fosfato forma un complejo \line \up0 \expndtw0\charscalex111 incoloro con el
in de hierro. Por ltimo, el carbono \line \up0 \expndtw0\charscalex108 presente en
la muestra se puede eliminar mediante su \line \up0 \expndtw0\charscalex101 oxi
dacin con peroxidisulfato de amonio de acuerdo a la \line \up0 \expndtw-3\charsca
lex100 reaccin (2).\par\pard\ql \li2083\sb0\sl-108\slmult0\tx4630\tx5485 \up0 \ex
pndtw-1\charscalex100 \ul0\nosupersub\cf8\f9\fs11 2 \up0 \expndtw-1\charscalex10
0 \u-4051? \tab \up0 \expndtw-1\charscalex100 2 \up0 \expndtw-1\charscalex100 \u
-4051? \tab \up0 \expndtw-1\charscalex100 \u-4053?\par\pard\column \ql \li380\sb
0\sl-180\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf5\f6\fs20 encue
ntra preparada en el extractor.\par\pard\ql \li20\sb1\sl-192\slmult0 \up0 \expnd
tw0\charscalex105 2)\ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20

Solucin de HNO\ul0\sub\cf7\f8\fs19 3\ul0\nosupersub\cf5\f6\fs20 concentrado \up0
\expndtw0\charscalex106 = ya se encuentra\par\pard\ql \li380\sb7\sl-230\slmult0
\up0 \expndtw-3\charscalex100 preparada en el extractor.\par\pard\ql \li20\sb0\
sl-229\slmult0 \up0 \expndtw0\charscalex103 3)\ul0\nosupersub\cf12\f13\fs20 \ul
0\nosupersub\cf5\f6\fs20 Slido de peroxidisulfato de amonio (NH\ul0\sub\cf7\f8\f
s19 4\ul0\nosupersub\cf5\f6\fs20 )\ul0\sub\cf7\f8\fs19 2\ul0\nosupersub\cf5\f6\f
s20 S\ul0\sub\cf7\f8\fs19 2\ul0\nosupersub\cf5\f6\fs20 O\ul0\sub\cf7\f8\fs19 8 \
up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf5\f6\fs20 =\par\pard\ql \li21\ri9
70\sb2\sl-229\slmult0\fi359\tx390 \up0 \expndtw-3\charscalex100 slido que debe es
tar disponible en el extractor. \line \up0 \expndtw0\charscalex102 4)\ul0\nosupe
rsub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Solucin de H\ul0\sub\cf7\f8\fs19
3\ul0\nosupersub\cf5\f6\fs20 PO\ul0\sub\cf7\f8\fs19 4\ul0\nosupersub\cf5\f6\fs2
0 85% = ya se encuentra preparada \line\tab \up0 \expndtw-3\charscalex100 en el
extractor.\par\pard\qj \li20\ri972\sb2\sl-230\slmult0\tx391 \up0 \expndtw-1\cha
rscalex100 5)\ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Slido de
periodato de potasio KIO\ul0\sub\cf7\f8\fs19 4\ul0\nosupersub\cf5\f6\fs20 = sli
do que debe \line\tab \up0 \expndtw-3\charscalex100 estar disponible en el extra
ctor.\par\pard\qj \li21\ri970\sb0\sl-230\slmult0\tx391 \up0 \expndtw0\charscalex
101 6)\ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Slido NaHSO\ul0
\sub\cf7\f8\fs19 3\ul0\nosupersub\cf5\f6\fs20 = slido que debe estar disponible
en \line\tab \up0 \expndtw-3\charscalex100 el extractor.\par\pard\sect\sectd\sbk
none\cols4\colno1\colw3250\colsr160\colno2\colw276\colsr160\colno3\colw2350\cols
r160\colno4\colw5764\colsr160\ql \li1195\sb0\sl-176\slmult0\tx2057\tx2917 \up0 \
expndtw-2\charscalex100 \ul0\nosupersub\cf11\f12\fs22 C \up0 \expndtw-7\charscal
ex100 (s) \up0 \expndtw-9\charscalex90 \u-4053?2 \up0 \expndtw0\charscalex50 SO
\ul0\nosupersub\cf8\f9\fs11 2\tab \up0 \expndtw-2\charscalex100 8 \up0 \expndtw2\charscalex100 \ul0\nosupersub\cf11\f12\fs22 ( \up0 \expndtw-6\charscalex100 ac
\up0 \expndtw-2\charscalex100 ) \up0 \expndtw-9\charscalex80 \u-4053? \up0 \exp
ndtw-2\charscalex100 2\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf8\f9\
fs11 2\par\pard\column \ql \li20\sb0\sl-216\slmult0 \up0 \expndtw0\charscalex120
\ul0\nosupersub\cf10\f11\fs24 \u-3960?\par\pard\column \ql \li20\sb0\sl-152\slm
ult0\tx957 \up0 \expndtw0\charscalex107 \ul0\nosupersub\cf8\f9\fs11 2\ul0\nosupe
rsub\cf11\f12\fs22 ( \up0 \expndtw-2\charscalex100 g \up0 \expndtw-2\charscalex1
00 ) \up0 \expndtw-8\charscalex80 \u-4053? \up0 \expndtw-2\charscalex100 4 \up0
\expndtw-8\charscalex93 SO \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf8\f9\
fs11 4\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf11\f12\fs22 ( \up0 \e
xpndtw-5\charscalex100 ac \up0 \expndtw-2\charscalex100 ) \up0 \expndtw-8\charsc
alex80 \u-4053? \up0 \expndtw-2\charscalex100 4 \up0 \expndtw-2\charscalex100 H
\up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf8\f9\fs11 ( \up0 \expndtw-3\char
scalex100 ac) \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf5\f6\fs20 (2)\par\
pard\column \ql \li20\sb0\sl-160\slmult0 \up0 \expndtw0\charscalex100 7)\ul0\nos
upersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Solucin de H\ul0\sub\cf7\f8\f
s19 2\ul0\nosupersub\cf5\f6\fs20 SO\ul0\sub\cf7\f8\fs19 4\ul0\nosupersub\cf5\f6\
fs20 1.0 M = ya se encuentra preparada\par\pard\sect\sectd\sbknone\cols2\colno1
\colw6175\colsr160\colno2\colw5765\colsr160\ql \li1170\sb1\sl-180\slmult0 \up0 \
expndtw-2\charscalex100 En este experimento usted determinar la concentracin de\pa
r\pard\qj \li1170\ri220\sb9\sl-229\slmult0 \up0 \expndtw0\charscalex108 manganes
o en acero por espectrofotometra. El \line \up0 \expndtw0\charscalex100
experimento consiste principalmente en cuatro partes. En \line \up0 \expndtw0\c
harscalex103 la primera parte preparar una solucin valorada de \line \up0 \
expndtw0\charscalex103 permanganato de potasio (KMnO4, PM 158.034). En la \line
\up0 \expndtw-2\charscalex100 segunda parte preparar cinco soluciones por el mtodo
de \line \up0 \expndtw0\charscalex104 dilucin. En la tercera parte, preparar una
solucin del \line \up0 \expndtw0\charscalex108 desconocido y su blanco de re
accin. Finalmente, \line \up0 \expndtw0\charscalex106 determinar la absorbencia
de todas las soluciones \line \up0 \expndtw0\charscalex103 preparadas. Con
estos datos preparar una curva de \line \up0 \expndtw-2\charscalex100 cali
bracin de absorbencia como funcin de concentracin \line \up0 \expndtw0\charscalex10
4 conocida de manganeso y con la absorbencia de la \line \up0 \expndtw0\
charscalex111 solucin del desconocido podr determinar la \line \up0 \exp

ndtw0\charscalex115 concentracin del in de MnO4-. Las medidas\par\pard\colum
n \ql \li381\sb0\sl-180\slmult0 \up0 \expndtw-3\charscalex100 en el extractor.\p
ar\pard\qj \li21\ri970\sb0\sl-229\slmult0\tx391 \up0 \expndtw0\charscalex104 8)\
ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Solucin de la muestra
desconocida = NO tiene que \line\tab \up0 \expndtw-3\charscalex100 secar el acer
o.\par\pard\ql \li21\sb205\sl-230\slmult0 \up0 \expndtw0\charscalex103 Procedimi
ento\par\pard\qj \li21\ri970\sb0\sl-230\slmult0\tx2746 \up0 \expndtw-1\charscale
x100 Nota importante: El proceso de disolucin y oxidacin del \up0 \expndtw0\charsc
alex106 manganeso TIENE que llevarlo a cabo en el extractor. \up0 \expndtw0\char
scalex100 Puede regresar a la mesa de trabajo tan pronto no observe \line \up0 \
expndtw0\charscalex111 emanacin de gas marrn \tab \up0 \expndtw0\charscalex108
(xido nitroso, N\ul0\sub\cf7\f8\fs19 2\ul0\nosupersub\cf5\f6\fs20 O).\par\pard\
qj \li20\ri970\sb0\sl-229\slmult0 \up0 \expndtw-1\charscalex100 Importante: Tien
e que preparar un blanco de reaccin que \up0 \expndtw0\charscalex101 a su vez ser
el blanco del desconocido en las lecturas de \up0 \expndtw-3\charscalex100 absor
cin.\par\pard\qj \li20\ri971\sb0\sl-230\slmult0\tx390 \up0 \expndtw0\charscalex10
7 1)\ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20 Preparacin de la
muestra (SE TIENE que llevar a \line\tab \up0 \expndtw-3\charscalex100 cabo en e
l extractor) \par\pard\sect\sectd\sbknone \ql \li1289\sb0\sl-130\slmult0 \par\pa
rd\ql\li1289\ri1194\sb117\sl-130\slmult0\fi46\tx5869 \up0 \expndtw-1\charscalex1
00 \ul0\nosupersub\cf3\f4\fs12 LA UNIVERSIDAD DE PUERTO RICO EN HUMACAO NO DISCR
IMINA POR EDAD, SEXO, ORIENTACIN SEXUAL, RAZA, COLOR, NACIONALIDAD, ORIGEN O COND
ICIN \line \up0 \expndtw-1\charscalex100 SOCIAL, NI POR IDEAS POLTICAS, RELIGIOSAS
E IMPEDIMENTOS FSICOS O POR CONDICIN DE VETERANOS \u9632? PATRONO CON IGUALDAD D
E OPORTUNIDADES DE \line\tab \up0 \expndtw-1\charscalex100 EMPLEO \par\pard\sect
\sectd\fs24\paperw12240\paperh15840\pard\sb0\sl-240{\bkmkstart Pg2}{\bkmkend Pg2
}\par\pard\ql \li10970\sb0\sl-230\slmult0 \par\pard\ql\li10970\sb100\sl-230\slmu
lt0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf13\f14\fs20 2\par\pard\sect\
sectd\sbknone\cols2\colno1\colw6175\colsr160\colno2\colw5765\colsr160\ql \li1530
\sb203\sl-230\slmult0\tx1885 \up0 \expndtw-3\charscalex100 a)\tab \up0 \expndtw0
\charscalex111 Pese una muestra de \up0 \expndtw0\charscalex112 0.25 gramos de
acero\par\pard\ql \li1890\sb0\sl-230\slmult0 \up0 \expndtw0\charscalex107 (balan
za analtica). Disuelva la muestra en 10\par\pard\column \ql \li20\sb203\sl-230\sl
mult0 \up0 \expndtw-3\charscalex100 Tabla 1: Preparacin de soluciones estndares de
KMnO\ul0\sub\cf16\f17\fs19 4\par\pard\sect\sectd\sbknone\cols2\colno1\colw6175\
colsr160\colno2\colw5765\colsr160\ql \li1890\sb0\sl-230\slmult0 \up0 \expndtw0\c
harscalex109 \ul0\nosupersub\cf13\f14\fs20 mL de cido ntrico (HNO\ul0\sub\cf16\f17
\fs19 3\ul0\nosupersub\cf13\f14\fs20 ) 6 M. Caliente la\par\pard\ql \li1889\sb0\
sl-230\slmult0 \up0 \expndtw-3\charscalex100 muestra por ~ 5 minutos la mezcla.\
par\pard\ql \li1529\sb0\sl-230\slmult0\tx1884 \up0 \expndtw-2\charscalex100 b)\t
ab \up0 \expndtw-1\charscalex100 Aada 0.25 gramos de peroxidisulfato de amonio\pa
r\pard\ql \li1889\sb1\sl-229\slmult0 \up0 \expndtw0\charscalex108 ((NH\ul0\sub\c
f16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 )\ul0\sub\cf16\f17\fs19 2\ul0\nosupe
rsub\cf13\f14\fs20 S\ul0\sub\cf16\f17\fs19 2\ul0\nosupersub\cf13\f14\fs20 O\ul0\
sub\cf16\f17\fs19 8\ul0\nosupersub\cf13\f14\fs20 ) y ponga a hervir ligeramente
la\par\pard\ql \li1889\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex110 muestra d
e 10 a 15 minutos. Tiene que tener\par\pard\ql \li1889\sb0\sl-230\slmult0 \up0 \
expndtw-1\charscalex100 cuidado durante la adicin del peroxidisulfato. S\par\pard\
ql \li1889\sb1\sl-229\slmult0 \up0 \expndtw0\charscalex103 la solucin es rosad
a o contiene bixido de\par\pard\ql \li1889\sb1\sl-230\slmult0 \up0 \expndtw-2
\charscalex100 manganeso (MnO\ul0\sub\cf16\f17\fs19 2\ul0\nosupersub\cf13\f14\fs
20 ) que muestra un color marrn,\par\pard\ql \li1890\sb0\sl-230\slmult0 \up0 \exp
ndtw0\charscalex106 aada 0.1 gramos de NaHSO\ul0\sub\cf16\f17\fs19 3\ul0\nosupers
ub\cf13\f14\fs20 y caliente por 5\par\pard\ql \li1889\sb1\sl-229\slmult0 \up0 \
expndtw-3\charscalex100 minutos adicionales.\par\pard\ql \li1529\sb1\sl-230\slmu
lt0\tx1885 \up0 \expndtw-3\charscalex100 c)\tab \up0 \expndtw0\charscalex109 Enf
re un poco la solucin y aada 25 mL de\par\pard\ql \li1890\sb0\sl-229\slmult0 \up0 \
expndtw-3\charscalex100 agua deionizada en el envase.\par\pard\ql \li1530\sb2\sl
-230\slmult0\tx1885 \up0 \expndtw-2\charscalex100 d)\tab \up0 \expndtw-3\charsca
lex100 Aada 3 mL de H\ul0\sub\cf16\f17\fs19 3\ul0\nosupersub\cf13\f14\fs20 PO\ul0

\sub\cf16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 concentrado (al 85%).\par\par
d\ql \li1529\sb0\sl-230\slmult0\tx1885 \up0 \expndtw-3\charscalex100 e)\tab \up0
\expndtw0\charscalex104 ESTE PASO NO LO TIENE QUE HACER SI\par\pard\ql \li1890\
sb0\sl-229\slmult0 \up0 \expndtw0\charscalex103 SE EST PREPARANDO EL BLANCO DEL\p
ar\pard\ql \li1890\sb2\sl-230\slmult0 \up0 \expndtw0\charscalex101 DESCONOCIDO.
Aada aproximadamente 0.1\par\pard\ql \li1890\sb0\sl-230\slmult0 \up0 \expndtw0\ch
arscalex107 gramos de periodato de potasio (KIO\ul0\sub\cf16\f17\fs19 4\ul0\nosu
persub\cf13\f14\fs20 ) y deje\par\pard\ql \li1889\sb0\sl-229\slmult0 \up0 \expnd
tw0\charscalex105 hervir suavemente por aproximadamente \up0 \expndtw-3\chars
calex100 3\par\pard\ql \li1889\sb2\sl-230\slmult0 \up0 \expndtw0\charscalex100 m
inutos. Luego de los 3 minutos, espere a que la\par\pard\ql \li1889\sb0\sl-230\s
lmult0 \up0 \expndtw0\charscalex107 temperatura disminuya un poco y aada otros\pa
r\pard\ql \li1889\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex117 0.10 gramos
de KIO\ul0\sub\cf16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 . Vuelva a hervi
r\par\pard\ql \li1889\sb2\sl-230\slmult0 \up0 \expndtw-3\charscalex100 suavement
e la solucin de 1 o 2 minutos.\par\pard\ql \li1529\sb0\sl-230\slmult0\tx1884 \up0
\expndtw-3\charscalex100 f)\tab \up0 \expndtw0\charscalex109 Deje enfriar la so
lucin hasta temperatura de\par\pard\ql \li1889\sb0\sl-229\slmult0 \up0 \expndtw0\
charscalex105 saln. Luego, transfiera cuantitativamente a\par\pard\ql \li1889
\sb2\sl-230\slmult0 \up0 \expndtw0\charscalex107 matraz volumtrico de 100.0 mL. E
sta ser la\par\pard\ql \li1889\sb0\sl-230\slmult0 \up0 \expndtw-3\charscalex100 s
olucin de su desconocido.\par\pard\ql \li1170\sb0\sl-229\slmult0\tx1524 \up0 \exp
ndtw-2\charscalex100 2)\tab \up0 \expndtw0\charscalex100 Preparacin del blanco de
la muestra (SE TIENE que\par\pard\ql \li1529\sb2\sl-230\slmult0 \up0 \expndtw-3
\charscalex100 llevar a cabo en el extractor)\par\pard\ql \li1529\sb0\sl-230\slm
ult0 \up0 \expndtw0\charscalex110 a)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupers
ub\cf13\f14\fs20 La preparacin del blanco ser igual a la\par\pard\ql \li18
90\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex102 preparacin de la solucin del de
sconocido solo\par\pard\ql \li1890\sb2\sl-230\slmult0 \up0 \expndtw-2\charscalex
100 que NO llevar a cabo el paso de aadir periodato\par\pard\ql \li1890\sb0\sl-229
\slmult0 \up0 \expndtw0\charscalex100 de potasio (KIO\ul0\sub\cf16\f17\fs19 4\ul
0\nosupersub\cf13\f14\fs20 ), es decir NO hacer la parte (e)\par\pard\ql \li1889
\sb1\sl-230\slmult0 \up0 \expndtw-3\charscalex100 del mtodo en la parte (1).\par\
pard\ql \li1169\sb1\sl-230\slmult0\tx1524 \up0 \expndtw-2\charscalex100 3)\tab \
up0 \expndtw-1\charscalex100 Preparacin de soluciones estndares de KMnO\ul0\sub\cf
16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 para\par\pard\ql \li1530\sb0\sl-229\
slmult0 \up0 \expndtw-3\charscalex100 construir curva de calibracin.\par\pard\ql
\li1530\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex101 a)\ul0\nosupersub\cf15\f
16\fs20 \ul0\nosupersub\cf13\f14\fs20 Prepare las soluciones por el mtodo de di
lucin.\par\pard\ql \li1890\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex103 Debe s
er muy cuidadoso con la preparacin del\par\pard\ql \li1890\sb0\sl-229\slmult0 \up
0 \expndtw0\charscalex105 equipo y transferencia de los reactivos. Un\par\
pard\ql \li1890\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex103 ejemplo para pre
parar una solucin, digamos la\par\pard\ql \li1890\sb1\sl-230\slmult0 \up0 \expndt
w-2\charscalex100 solucin I de la Tabla 1. Para preparar la solucin\par\pard\ql \l
i1890\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex108 I, usted transferir con pip
eta \up0 \expndtw0\charscalex114 2.00 mL de la\par\pard\ql \li1890\sb1\sl-230\sl
mult0 \up0 \expndtw0\charscalex108 solucin valorada de KMnO\ul0\sub\cf16\f17\f
s19 4\ul0\nosupersub\cf13\f14\fs20 a un matraz\par\pard\ql \li1889\sb1\sl-23
0\slmult0 \up0 \expndtw0\charscalex102 volumtrico de \up0 \expndtw0\charscalex10
8 100.00 mL. Luego lleva a\par\pard\ql \li1889\sb0\sl-229\slmult0 \up0 \expn
dtw0\charscalex104 volumen con agua deionizada y homogeniza la\par\pard\ql \li18
89\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex103 solucin. Otro ejemplo, digamos
la solucin II,\par\pard\ql \li1889\sb1\sl-230\slmult0 \up0 \expndtw0\charscalex1
01 usted transferir con pipeta \up0 \expndtw0\charscalex104 15.00 mL de la\
par\pard\ql \li1889\sb0\sl-229\slmult0 \up0 \expndtw0\charscalex100 solucin I a u
n matraz volumtrico de 25.00 mL.\par\pard\ql \li1889\sb1\sl-230\slmult0 \up0 \exp
ndtw0\charscalex106 Luego lleva a volumen con agua deionizada y\par\pard\ql \li1
889\sb1\sl-230\slmult0 \up0 \expndtw-3\charscalex100 homogeniza la solucin.\par\p
ard\column \ql \li20\sb0\sl-180\slmult0\tx1239\tx2549\tx3790 \up0 \expndtw-2\cha

rscalex100 Solucin\tab \up0 \expndtw-3\charscalex100 Volumen\tab \up0 \expndtw-2\
charscalex100 Solucin\tab \up0 \expndtw-3\charscalex100 Volumen\par\pard\ql \li10
31\sb117\sl-230\slmult0\tx2643\tx3690 \up0 \expndtw-3\charscalex100 Alcuota (mL)\
tab \up0 \expndtw-2\charscalex100 Patrn\tab \up0 \expndtw-3\charscalex100 Matraz,
mL\par\pard\ql \li343\sb182\sl-230\slmult0\tx1435\tx2562\tx3937 \up0 \expndtw-2
\charscalex100 I\tab \up0 \expndtw-2\charscalex100 2.00\tab \up0 \expndtw-3\char
scalex100 ~0.02 M\tab \up0 \expndtw-3\charscalex100 100.0\par\pard\ql \li310\sb1
66\sl-230\slmult0\tx1386\tx2491\tx3938 \up0 \expndtw-3\charscalex100 II\tab \up0
\expndtw-3\charscalex100 15.00\tab \up0 \expndtw-3\charscalex100 Solucin I\tab \
up0 \expndtw-3\charscalex100 25.00\par\pard\ql \li276\sb166\sl-230\slmult0\tx138
6\tx2491\tx3938 \up0 \expndtw-3\charscalex100 III\tab \up0 \expndtw-3\charscalex
100 10.00\tab \up0 \expndtw-3\charscalex100 Solucin I\tab \up0 \expndtw-3\charsca
lex100 25.00\par\pard\ql \li270\sb166\sl-230\slmult0\tx1435\tx2491\tx3938 \up0 \
expndtw-3\charscalex100 IV\tab \up0 \expndtw-3\charscalex100 5.00\tab \up0 \expn
dtw-3\charscalex100 Solucin I\tab \up0 \expndtw-3\charscalex100 25.00\par\pard\ql
\li304\sb166\sl-230\slmult0\tx1435\tx2491\tx3938 \up0 \expndtw-3\charscalex100
V\tab \up0 \expndtw-3\charscalex100 1.00\tab \up0 \expndtw-3\charscalex100 Soluc
in I\tab \up0 \expndtw-3\charscalex100 25.00\par\pard\ql \li6335\sb0\sl-230\slmul
t0 \par\pard\ql \li20\sb65\sl-230\slmult0 \up0 \expndtw0\charscalex101 4)\ul0\no
supersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\fs20 Lecturas de absorcin\par\p
ard\qj \li380\ri971\sb0\sl-230\slmult0 \up0 \expndtw0\charscalex106 Las instruc
ciones de uso del instrumento se le \line \up0 \expndtw0\charscalex110 bri
ndarn el da del laboratorio. En trminos \line \up0 \expndtw-1\charscalex100 g
enerales, le tiene que medir el espectro de absorcin\par\pard\ql \li380\ri967\sb0
\sl-230\slmult0 \up0 \expndtw0\charscalex106 a todas las soluciones preparadas e
n la Tabla 1. El \up0 \expndtw-3\charscalex100 blanco de estas medidas es agua d
eionizada. \line \up0 \expndtw-2\charscalex100 La lectura del espectro de absorc
in de la solucin del \up0 \expndtw0\charscalex101 desconocido tendr como blanco
la solucin que \up0 \expndtw0\charscalex107 prepar en la parte 2. Determine la
absorbencia al \up0 \expndtw0\charscalex104 largo de onda mximo de todas la
s soluciones. \up0 \expndtw-2\charscalex100 Recuerde que este largo de onda mxim
o tiene que ser \up0 \expndtw-3\charscalex100 igual para todas las soluciones.\p
ar\pard\ql \li20\ri971\sb0\sl-230\slmult0\tx390\tx390 \up0 \expndtw0\charscalex1
02 5)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\fs20 Calcule la co
ncentracin de soluciones estndares de \line\tab \up0 \expndtw-2\charscalex100 KMnO
\ul0\sub\cf16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 preparadas por dilucin y a
ntelas en la Tabla \line \tab \up0 \expndtw-3\charscalex100 2.\par\pard\ql \li20\
sb229\sl-230\slmult0 \up0 \expndtw0\charscalex103 Datos Experimentales\par\pard\
qj \li20\ri1234\sb220\sl-239\slmult0\tx318 \up0 \expndtw-3\charscalex100 Tabla 2
: Medidas de absorbancia soluciones estndares. \line\tab \up0 \expndtw0\charscale
x105 Solucin Molaridad Absorbancia\par\pard\ql \li309\sb9\sl-230\slmult0 \up0
\expndtw-2\charscalex100 I\par\pard\ql \li309\sb1\sl-230\slmult0 \up0 \expndtw3\charscalex100 II\par\pard\ql \li309\sb0\sl-230\slmult0 \up0 \expndtw-3\charsca
lex100 III\par\pard\ql \li309\sb0\sl-229\slmult0 \up0 \expndtw-3\charscalex100 I
V\par\pard\ql \li309\sb1\sl-230\slmult0 \up0 \expndtw-3\charscalex100 V\par\pard
\qj \li20\ri2017\sb234\sl-239\slmult0\tx318\tx1958 \up0 \expndtw-3\charscalex100
Tabla 3: Dato de absorbencia del desconocido \line\tab \up0 \expndtw-3\charscal
ex100 Muestra \tab \up0 \expndtw-3\charscalex100 Absorbancia\par\pard\ql \li309\
sb9\sl-230\slmult0 \up0 \expndtw-3\charscalex100 1\par\pard\ql \li309\sb0\sl-229
\slmult0 \up0 \expndtw-3\charscalex100 2\par\pard\ql \li6335\sb0\sl-230\slmult0
\par\pard\ql \li20\sb14\sl-230\slmult0 \up0 \expndtw0\charscalex102 Clculos\par\p
ard\ql \li20\ri971\sb0\sl-229\slmult0\tx390\tx390\tx390 \up0 \expndtw0\charscale
x112 1)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\fs20 Lleve a grfi
ca los valores de absorbencia como \line\tab \up0 \expndtw-1\charscalex100 funcin
de concentracin de KMnO\ul0\sub\cf16\f17\fs19 4\ul0\nosupersub\cf13\f14\fs20 qu
e aparecen en \line \tab \up0 \expndtw0\charscalex106 la Tabla 2. Adems, tiene qu
e incluir el dato de su \line \tab \up0 \expndtw-3\charscalex100 desconocido ya
sea en otra serie o manual.\par\pard\qj \li21\ri970\sb0\sl-230\slmult0\tx390 \up
0 \expndtw0\charscalex101 2)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\
f14\fs20 Determine la pendiente de la recta y su incertidumbre \line\tab \up0 \

expndtw-3\charscalex100 absoluta.\par\pard\ql \li21\sb1\sl-229\slmult0 \up0 \exp
ndtw-1\charscalex100 3)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\f
s20 Determine el intercepto y su incertidumbre absoluta\par\pard\qj \li20\ri181
0\sb1\sl-229\slmult0\fi0\tx3164 \up0 \expndtw-1\charscalex100 4)\ul0\nosupersub\
cf15\f16\fs20 \ul0\nosupersub\cf13\f14\fs20 Determine el coeficiente de correl
acin (R\ul0\super\cf16\f17\fs19 2\ul0\nosupersub\cf13\f14\fs20 ) \line \up0 \expn
dtw-3\charscalex100 Tabla 4: Datos obtenidos para curva calibracin: \line \up0 \e
xpndtw-3\charscalex100 Pendiente (m) \tab \up0 \expndtw-3\charscalex100 \par\pard
\ql \li20\sb11\sl-230\slmult0\tx3168 \up0 \expndtw-3\charscalex100 Intercepto (b
)\tab \up0 \expndtw-3\charscalex100 \par\pard\ql \li20\sb10\sl-230\slmult0 \up0 \
expndtw-2\charscalex100 R\ul0\super\cf16\f17\fs19 2 \par\pard\sect\sectd\sbknone
\ql \li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard
\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\ri1193\sb4\sl-130\slmult0\fi46
\tx5869 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf14\f15\fs12 LA UNIVERSID
AD DE PUERTO RICO EN HUMACAO NO DISCRIMINA POR EDAD, SEXO, ORIENTACIN SEXUAL, RAZ
A, COLOR, NACIONALIDAD, ORIGEN O CONDICIN \line \up0 \expndtw-1\charscalex100 SOC
IAL, NI POR IDEAS POLTICAS, RELIGIOSAS E IMPEDIMENTOS FSICOS O POR CONDICIN DE VETE
RANOS \u9632? PATRONO CON IGUALDAD DE OPORTUNIDADES DE \line\tab \up0 \expndtw1\charscalex100 EMPLEO
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}}\par\pard\sect\sectd\fs24\paperw12240\paperh15840\pard\sb0\sl-240{\bkmkstart P
g3}{\bkmkend Pg3}\par\pard\ql \li10970\sb0\sl-230\slmult0 \par\pard\ql\li10970\s
b100\sl-230\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf13\f14\fs20
3 \par\pard\ql \li1170\ri3329\sb188\sl-233\slmult0\tx1529\tx1529\tx1529 \up0 \ex
pndtw-1\charscalex100 5)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\
fs20 Calcule la concentracin de Mn (M\ul0\sub\cf16\f17\fs19 desc\ul0\nosupersub\
cf13\f14\fs20 ) en el acero \line\tab \up0 \expndtw-3\charscalex100 con el valor
promedio de la absorbencia de su \line \tab \up0 \expndtw-3\charscalex100 desco
nocido (Tabla 3), la pendiente (m) y el \line \tab \up0 \expndtw-3\charscalex100
intercepto (b) de la Tabla 4 y la ecuacin (3). \par\pard\li1170\sb45\sl-276\slmu
lt0\fi1343\tx2969\tx3151\tx3870\tx4159\tx4276\tx5677 \up0 \expndtw-11\charscalex
86 \ul0\nosupersub\cf20\f21\fs24 A\t \dn2 \expndtw-4\charscalex100 \ul0\nosupers
ub\cf19\f20\fs14 desc\tab \up0 \expndtw-11\charscalex80 \ul0\nosupersub\cf20\f21
\fs24 \u-4035?\tab \dn3 \expndtw-8\charscalex100 \ul0\nosupersub\cf18\f19\fs27 \
u-4056?\t \up0 \expndtw-11\charscalex94 \ul0\nosupersub\cf20\f21\fs24 m\t \dn3 \
expndtw0\charscalex50 \ul0\nosupersub\cf18\f19\fs27 \u-4055?\u-4056?\t \up0 \exp
ndtw-11\charscalex95 \ul0\nosupersub\cf20\f21\fs24 M\tab \dn2 \expndtw-4\charsca
lex100 \ul0\nosupersub\cf19\f20\fs14 desc\tab \dn3 \expndtw-8\charscalex100 \ul0
\nosupersub\cf18\f19\fs27 \u-4055?\tab \up0 \expndtw-7\charscalex100 \ul0\nosupe
rsub\cf20\f21\fs24 \u-4053?b\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\c
f13\f14\fs20 (3)\par\pard\li1170\sb87\sl-230\slmult0\fi0 \up0 \expndtw-5\charsca
lex100 6)\ul0\nosupersub\cf15\f16\fs20 \ul0\nosupersub\cf13\f14\fs20 Determine
el % w/w de Mn en la muestra de acero por\par\pard\li1170\sb0\sl-230\slmult0\fi
359 \up0 \expndtw-5\charscalex100 la ecuacin (4)\par\pard\sect\sectd\sbknone\cols
4\colno1\colw1836\colsr40\colno2\colw119\colsr40\colno3\colw848\colsr20\colno4\c
olw9217\colsr160\ql \li1621\sb256\sl-276\slmult0 \up0 \expndtw-5\charscalex100 \
ul0\nosupersub\cf23\f24\fs23 %\par\pard\column \ql \li1876\sb0\sl-161\slmult0 \p
ar\pard\ql \li20\sb105\sl-161\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosuper
sub\cf24\f25\fs13 w\par\pard\ql \li20\sb0\sl-151\slmult0 \up0 \expndtw-2\charsca
lex100 w\par\pard\column \ql \li549\sb44\sl-310\slmult0 \up0 \expndtw0\charscale
x80 \ul0\nosupersub\cf21\f22\fs27 \u-4056? \up0 \expndtw-11\charscalex96 \ul0\no
supersub\cf23\f24\fs23 M\par\pard\ql \li20\sb0\sl-201\slmult0 \up0 \expndtw-7\ch
arscalex100 Mn \up0 \expndtw-11\charscalex80 \u-4035?\par\pard\column \ql \li680
\sb42\sl-161\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf24\f25\fs13
Desc\par\pard\ql \li308\sb0\sl-208\slmult0\tx1062 \up0 \expndtw0\charscalex50 \
ul0\nosupersub\cf21\f22\fs27 \u-4055?\ul0\nosupersub\cf22\f23\fs29 \u-4056? \up0
\expndtw-11\charscalex88 \ul0\nosupersub\cf23\f24\fs23 V\tab \up0 \expndtw0\cha
rscalex50 \ul0\nosupersub\cf22\f23\fs29 \u-4055?\ul0\nosupersub\cf21\f22\fs27 \u
-4056? \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf23\f24\fs23 PAMn \up0 \ex
pndtw0\charscalex50 \ul0\nosupersub\cf21\f22\fs27 \u-4055?\u-4056? \up0 \expndtw
-3\charscalex100 \ul0\nosupersub\cf23\f24\fs23 100 \up0 \expndtw0\charscalex80 \
ul0\nosupersub\cf21\f22\fs27 \u-4055?\par\pard\ql \li20\sb0\sl-126\slmult0\tx631
\up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf24\f25\fs13 desc\tab \up0 \expn
dtw0\charscalex100 matraz\par\pard\ql \li2814\sb0\sl-160\slmult0 \up0 \expndtw-3
\charscalex100 \ul0\nosupersub\cf13\f14\fs20 (4)\par\pard\ql \li362\sb0\sl-208\s
lmult0 \up0 \expndtw0\charscalex80 \ul0\nosupersub\cf21\f22\fs27 \u-4056? \up0 \
expndtw0\charscalex103 \ul0\nosupersub\cf23\f24\fs23 masamuestra \up0 \expndtw0\
charscalex80 \ul0\nosupersub\cf21\f22\fs27 \u-4055? \par\pard\sect\sectd\sbknone
\ql \li1170\sb119\sl-230\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\
cf13\f14\fs20 Conclusiones \par\pard\qj \li1170\ri6171\sb0\sl-230\slmult0 \up0 \
expndtw0\charscalex100 Presente los resultados obtenidos. Identifique posible
s \line \up0 \expndtw0\charscalex104 fuentes de error y discuta como el error af
ecta el valor \line \up0 \expndtw-1\charscalex100 reportado en sus resultados. I
dentifique en qu direccin, \line \up0 \expndtw-3\charscalex100 mayor o menor relat
ivo al valor esperado, el error descrito \line \up0 \expndtw-3\charscalex100 afe
cta sus resultados. \par\pard\ql \li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\
sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb
0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\
sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl
-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-1
30\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130

\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\s
lmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slm
ult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmul
t0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0
\par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \
par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \pa
r\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\
pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pa
rd\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard
\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\q
l\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\
li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li
1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li12
90\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290
\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\s
b0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0
\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\s
l-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-13
0\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\
slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\sl
mult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmu
lt0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult
0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0
\par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \p
ar\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par
\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\p
ard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\par
d\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\
ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql
\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\ri1193\sb63\sl-130\slmult0\fi46\t
x5869 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf14\f15\fs12 LA UNIVERSIDAD
DE PUERTO RICO EN HUMACAO NO DISCRIMINA POR EDAD, SEXO, ORIENTACIN SEXUAL, RAZA,
COLOR, NACIONALIDAD, ORIGEN O CONDICIN \line \up0 \expndtw-1\charscalex100 SOCIA
L, NI POR IDEAS POLTICAS, RELIGIOSAS E IMPEDIMENTOS FSICOS O POR CONDICIN DE VETERA
NOS \u9632? PATRONO CON IGUALDAD DE OPORTUNIDADES DE \line\tab \up0 \expndtw-1\
charscalex100 EMPLEO
shpbxpage\shpbypage\shpwr3\shpwrk0\shpfblwtxt1\shpz55\shplid0{\sp{\sn shapeType}
{\sv 20}}{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv 0}}{\sp{\sn li
neWidth}{\sv 16035}}
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bxpage\shpbypage\shpwr3\shpwrk0\shpfblwtxt1\shpz155\shplid1{\sp{\sn shapeType}{\
sv 20}}{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv 0}}{\sp{\sn line
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bxpage\shpbypage\shpwr3\shpwrk0\shpfblwtxt1\shpz176\shplid2{\sp{\sn shapeType}{\
sv 20}}{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv 0}}{\sp{\sn line
Width}{\sv 9476}}
}}\par\pard\sect\sectd\fs24}

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{\rtf1{\fonttbl

{\f2 Imprint MT Shadow;}

p0 \expndtw-3\charscalex100 calibracin.\par\pard\ql \li1169\sb0\sl-230\slmult0 \p

tw0\charscalex105 2)\ul0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf5\f6\fs20

charscalex111 solucin del desconocido podr determinar la \line \up0 \exp

lex100 Aada 3 mL de H\ul0\sub\cf16\f17\fs19 3\ul0\nosupersub\cf13\f14\fs20 PO\ul0

ard\column \ql \li20\sb0\sl-180\slmult0\tx1239\tx2549\tx3790 \up0 \expndtw-2\cha

f14\fs20 Determine la pendiente de la recta y su incertidumbre \line\tab \up0 \

30\slmult0 \par\pard\ql\li1290\sb0\sl-130\slmult0 \par\pard\ql\li1290\sb0\sl-130

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