Frances Diane Gelle Romelyn Mae Fortuno Justin Albert A. Garcia De La Salle University-Dasmarias Dasmarias, Cavite, Philippines ABSTRACT The experiment was focused on classifying the unknown compounds based on its solubility in different solvents. Five unknown organic compounds were dissolved in solvents H 2O (Distilled water), NaOH (Sodium hydroxide), NaHCO 3 (Sodium bicarbonate) and HCl (Hydrochloride). Each 6 drops or 6mg of the compounds were mixed to the solvents to test their solubility. A soluble compound will be miscible with the solvent, while an insoluble compound will rather settle down thus being immiscible. Solubility is a factor in the possible identity of each compound. The unknown compounds were determined based on the results of its solubility in different solvents and were classified based on the characteristics of each group. The Polarity and pH of compounds are some factors, which affect the solubility of organic compounds.