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TP ON DU KH QUC GIA VIT NAM

VIN DU KH VIT NAM

S LC V CNG NGH
NH MY LC DU DUNG QUT

Thc hin: Phng Cng ngh Lc du


Trnh by: L Dng Hi
12/22/2013

TRUNG TM NGHIN CU V PHT TRIN CH BIN DU KH


www.pvpro.com.vn

NI DUNG
Vietnam Petroleum Institute

B tr mt bng
Phn xng cng ngh

H thng ph tr
Cht lng sn phm

TRUNG
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V PHT
CH BIN
DU KH 22
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PROCESSING

B tr mt bng nh my
Vietnam Petroleum Institute

Din tch: 338ha

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B tr mt bng nh my
Vietnam Petroleum Institute

Khu nh hnh
chnh

Khu b cha sn
phm trung gian

Cc phn xng
cng ngh

Khu b cha
du th

Khu cc phn
xng ph tr
M rng

Nc-Kh nn-in

HDT-LCO

CDU, KTU
Flare
SWS, ARU,
NHT, CCR,
RFCC, LTU,
X l cht thi
PRU,
SRU
ISOM
NTU,
PRU
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PROCESSING

SPM v kho cha du th


Vietnam Petroleum Institute

SPM

Tu Aframax (80.000 tn du th)


2 ng ng 50
Gia nhit ng ng n 50oC

B cha du th
6 b dung tch 59.000 m3
15 ngy vn hnh nh my
TRUNG
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V PHT
CH BIN
DU KH 55
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& TM
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PETROLEUM
PROCESSING

Phn xng cng ngh chnh


Vietnam Petroleum Institute

Unit

K hiu

011
CDU
012
NHT
013
CCR
014
KTU
015
RFCC
016
LTU
017
NTU
018
SWS
019
ARU
020
CNU
021
PRU
022
SRU
023
ISOM
024 HDT-LCO

Vai tr

Chng ct du th
X l naphtha
Reforming
X l Kerosene
Cracking cn
X l LPG
X l naphtha RFCC
X l nc chua
Ti sinh amin
Trung ho cn thi
Thu hi propylene
Thu hi lu hunh
Isomer ho
X l light cycle oil

Cng sut thit


k
148.000
BPSD
23.500
BPSD
21.100
BPSD
10.000
BPSD
69.700
BPSD
21.000
BPSD
45.000
BPSD
82,91
m3/h
102,5
m3/h
1,5
m3/h
19.535
kg/h
5
TPD
6.500
BPSD
28.826
BPSD

Nh bn
quyn

UOP
UOP
Merichem
Axens/IFP
Merichem
Merichem
-

Merichem
-

UOP
Axens

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PROCESSING

S cng ngh
Vietnam Petroleum Institute

Xng 95/92

Xng 90

Du th Bch
H hoc Dubai
(ti a 15%)

TRUNG
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V PHT
CH BIN
DU KH 77
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CM PHN XNG CDU


Vietnam Petroleum Institute

X l 100% du chua Dubai (0,35%wt S)

Linh hot thay i im ct


Cm thit b chnh
Tch mui
Thit b gia nhit du th
Thp chng ct chnh

Thp n nh sn phm nh
Thp lm kh tch nc
TRUNG
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DU KH 88
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CM PHN XNG CDU


Vietnam Petroleum Institute

Corrosion inhibitor injection


Neutraliser injection
OFFGAS TO RFCC
WCC
OFFGAS TO WCC ON RFCC
1
E1122

D 1104

T 1107

4
1

E1112

LPG TO RFCC GAS


RECOVERY SYSTEM

11

15

T 1102

12

FULL RANGE NAPHTHA TO NHT

22
23

KEROSENE TO BLENDING

Du th

26

Demulsifer Injector

T 1103

Antiflouant Injector

34
35

OFFGAS TO H1101

T 1005

38

D 1106

42

HYDROCABON TO SLOP

T1104

48
43

LGO TO BLENDING
E1116

T 1006

H 1101
Antifoulant Injector

T 1101
HGO TO STORAGE
E1117

SUPERHEAD LP STEAM
RESIDUE TO STORAGE. RFCC

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Cm NHT-ISOM-CCR
Fuel Gas

Vietnam Petroleum Institute

Light Naphtha

Isomerate

ISOMER

To LCO-HDT

SPLITTER

Untreated
Naphtha

NHT

Fuel Gas

LPG

Heavy Naphtha

Reformate

CCR

Hydrogen
Spent Cat

Regen
Cat

REGEN

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10
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NHT
Vietnam Petroleum Institute

Recycle gas

Sour gas
Compressor

Receiver

Fuel
gas

Charge
Heater

Stripper

Reactor

Full Range
Naphtha

Cooling
water

Stripper
Heater

Separator

Feed Surge
Drum

Xc tc Co,Mo/Al2O3

Splitte
r

Receiver

Light Naphtha
MP Steam

Heavy Naphtha
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11
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ISOM
Vietnam Petroleum Institute

To Fuel gas

Reactors
Condenser
Net Gas Scruber
Clo
injection

Dryers

Surge
Drum

Heater

Feed
Dryers

Deisohexanizer

Stabilizer

Methanator

Isomerate

Makeup Gas

Light naphtha
nC6, methyl C5 reprocessing

DIH process

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12
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CCR
Vietnam Petroleum Institute

Continuous Catalytic Reforming process

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13
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S cng ngh
Vietnam Petroleum Institute

Xng 95/92

Xng 90

Du th Bch
H hoc Dubai
(ti a 15%)

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DU KH 14
14
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RFCC
Vietnam Petroleum Institute

Chuyn ho cn nng t CDU,


cng ngh RFCC hin i ca
IFP/StoneWebber (Axens) &
x l kh
Vn hnh ch max
distillate/max gasoline (max
propylene?)
Cm thit b chnh

Reactor/Regeneration
Flue Gas Treatment
Fractionation
Gas Recovery Section
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15
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RFCC (tt)
Vietnam Petroleum Institute

Nguyn liu vo phn xng: cn chng ct kh quyn


(sch, paraffinic) v kh, LPG (vo gas plant)
Sn phm:

Kh: off-gas;
LPG c cha propylene;
RFCC Naphtha giu olefin (RON: 91)
LCO (light cycle oil)
DCO (decant oil)

Xc tc: RE-USY (c Sn) vi lng b sung hng ngy


5,5/15,2 tn
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16
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KTU
Vietnam Petroleum Institute

X l kerosene: axit naphthenic, lu hunh , nc v


tp cht khc t tiu chun Kero/JetA1
Cng ngh Merichem vi cc cm thit b chnh

NAPFININGSM trung ho axit naphthenic

MERICAT IISM x l lu hunh v loi b mui

AQUAFINING loi b cc mui sodium cn st li

SALT DRIER kh lng nc t do v gim lng nc bo ho

CLAY FILTER loi b cc ht rn cn li, hi m, mui hu c, nh


tng, cht hot ng b mt

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17
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LTU-NTU
Vietnam Petroleum Institute

LTU: X l LPG
Loi b H2S, RSH, COS
Cng ngh tch loi Thiolex ca Merichem
Xc tc MEA

NTU: X l RFCC naphtha


Tch loi H2S v RSH RSSH
Cng ngh Mericat ca Merichem
TRUNG
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DU KH 18
18
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HDT-LCO
Vietnam Petroleum Institute

X l tch loi lu hunh khi LCO, GO


(LGO,HGO)
Hm lng S trong sn phm
Bch H: 20 50 ppm
Chua: 150 - 350 ppm

Hot ng lin tc, ti sinh xc tc sau 2 nm


Tui th xc tc: 5 nm
TRUNG
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DU KH 19
19
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& TM
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PROCESSING

HDT-LCO
Vietnam Petroleum Institute

To FG

Reactor Heater

Lean Amine
Amine Abs

Recycle
Compressor

Reactor

Rich
Amine

Quench streams

HEX
H2 recycle
To SWS

Stripper T-2401

HP
Separator

Wild
Naph. To
RFCC/CD
U
MPS
Dryer
18

H2 Make-up

Washing
Water

Treated LCO

Feed

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20
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PROCESSING

PRU
Vietnam Petroleum Institute

Tch LPG thnh hn hp C4/propane v propylen v lm


sch propylene sn xut nha PP
Thit b chnh
Thp tch C3/C4
Thp tch C2Thp tch
propane/propylene
(190 a)

TRUNG
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DU KH 21
21
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Phn xng cng ngh khc


Vietnam Petroleum Institute

------ CNU
FROM CDU

------ ARU

SRU

------

FROM NHT

SOUR
WATER

SWS
FROM RFCC

DESALTER

------

SOUR WATER
TREATMENT

------

FROM CCR
(NNF)
FROM

SOUR FLARE
(NNF)

TANK

------

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22
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Cc phn xng cng ngh


Vietnam Petroleum Institute

+ SRU,
SWS,
CNU,
ARU

Xng 95/92

Xng 90

Du th Bch
H hoc Dubai
(ti a 15%)

TRUNG
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V PHT
CH BIN
DU KH 23
23
RESEARCH
& TM
DEVELOPMENT
CENTER
FORTRIN
PETROLEUM
PROCESSING

Cm phn xng ph tr, tin ch


Vietnam Petroleum Institute

Sn xut in, hi nc
Sn xut nit
Cung cp nc ngt
Cung cp nc bin
Kho cha sn phm trung gian
H thng phi trn
Kho cha sn phm
Cng xut sn phm ,
TRUNG
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24
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B cha trung gian


Vietnam Petroleum Institute

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DU KH 25
25
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PROCESSING

H thng phi trn


Vietnam Petroleum Institute

Fuel gas

C4s
Isomerate
Reformate
RFCC
naphtha
BLENDING
Kero
LGO
HGO
LCO
DCO
BLENDING

TRUNG
NGHIN CU
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CH BIN
DU KH 26
26
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ng ng dn sn phm
Vietnam Petroleum Institute

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DU KH 27
27
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Khu b cha sn phm


Vietnam Petroleum Institute

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28
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Cng xut sn phm


Vietnam Petroleum Institute

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29
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CHT LNG SN PHM XNG V


DIESEL
Vietnam Petroleum Institute

Tiu chun cht lng sn phm ca nh my


Cht lng sn phm nh my

Tiu chun cht lng Vit Nam


Xu hng cht lng sn phm nhin liu

TRUNG
NGHIN CU
V PHT
CH BIN
DU KH 30
30
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& TM
DEVELOPMENT
CENTER
FORTRIN
PETROLEUM
PROCESSING

EURO SPECIFICATION IN GASOLINE


Vietnam Petroleum Institute

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31
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EURO SPECIFICATION IN DIESEL


Vietnam Petroleum Institute

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DU KH 32
32
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PETROLEUM
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XNG
Vietnam Petroleum Institute

Tnh cht
RON
MON
Sulfur, ppm
Benzen, %vol
Aromatic, %vol

Olefin, %vol

Bch H

Mixed

>= 90.2/92.2/95.2
81.2/83.2/85.2
< 10
<1
<35 (tr mogas 95 ch MG )

<38

So snh vi TCVN: p ng v tt hn (MON)

So vi tiu chun Euro: EURO II and EURO III (tr olefin)


TRUNG
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33
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DIESEL
Vietnam Petroleum Institute

Tnh cht

Bach Ho MG

Bach Ho MD

Mixed MG

55

53

53

50

Sulfur, ppm

154

147

1020

1482

ASTM D86
90%vol, oC

348

368

350

368

Cetane Index

Mixed MD

p ng hu ht cc ch tiu TCVN ngoi tr im 90%


chng ct
p ng EURO III i vi du Bch H v EURO II vi
du Mixed

TRUNG
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DU KH 34
34
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Kt lun
Vietnam Petroleum Institute

NMLD Dung Qut c thit k vi cc phn xng


cng ngh hin i, ch bin du ngt, parafinic v
khng c VDU, HDS gasoline FCC
Nh my cn c nhng vn cn gii quyt
Ngun nguyn liu du th Bch H ang gim dn (thp hn
cng sut nh my)
Cht lng sn phm (tng lai)
S thiu ht cng sut ca phn xng CCR
Cng sut hin ti ca SRU v cht lng kh thi khi chy du
hn hp (mixed)
Mt s ti nghin cu ca PVPro phc v cho DQR
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DU KH 35
35
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Ti liu tham kho


Vietnam Petroleum Institute

Ti liu FEED 2004, EPCC 2006, OM 2007 ca DQR


Ti liu ging dy ca DQR
Raze Shadeghbeigi, Fluid Catalytic Cracking Handbook
Robert Meyer, Handbook of Petroleum Refining
Processes, 3rd Edition, 2003

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36
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Vietnam Petroleum Institute

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37
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Q&A
Vietnam Petroleum Institute

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38
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S dng KTU
Vietnam Petroleum Institute

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39
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S dng KTU (tt)


Vietnam Petroleum Institute

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40
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SWS
Vietnam Petroleum Institute
H2S

TO SRU

POLYSULPHIDE

TO INCENERATOR

NH3
1.2
6.0

COLD CONDENSATE

90

90

E-1802

FROM LCO-HDT

FROM NHT

P-1803

T-1801
FROM CDU

T-1802

E-1804

FROM RFCC

1.7
6.3

130

165
FROM SOUR
FLARE PUMP OUT
FROM CCR

E-1803

E-1805
TO CDU
DESALTER
D-1801

EFFLUENT
TREAMENT

P-1804
E-1801
KEROSENE

LIGHT SLOPS

P-1801

P-1802

ANTI-FOAM

TK-1801
P-1805

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41
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ARU
Vietnam Petroleum Institute

Corrosion
Inhibitor
Lean Amine

Lean Amine Cooler


E-1904

Condenser
E-1902

1. 2
121

Filter

Rich Amine

De-mineral
Water

T-1901

Flash Drum
D-1901

1. 35

26

Reboiler

Boiler Feed Water


LP Steam

126.5

To Light Slops

Reflux
Drum
D-1902

1
3

To Fuel Gas

To Sour Flare

E-1903A/B

Lean/Rich Amine
Ex E-1901

Condensate

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42
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SRU
Vietnam Petroleum Institute

Sn xut lu hunh t dng kh giu H2S i t cc phn


xng SWS v ARU, t dng kh t ARU v CNU
Qu trnh Clauss
H2S + O2 SO2 + H2O
H2S + SO2 S + H2O

Cc b phn chnh

Thu hi lu hunh
Cha v tch kh lu hunh lng
L thiu hu
Che chn lu hunh

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DU KH 43
43
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CNU
Vietnam Petroleum Institute

Trung ho kim v x l nc thi t cc phn


xng KTU, LTU, CNU, NHT, LCO-HDT, nh
my x l nc thi
S dng cng ngh trung ho trit MIRICON
ca Merichem

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44
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Phn xng sn xut in


Vietnam Petroleum Institute

Sn xut v cung cp in, hi nc


Nhin liu t l: FO hoc Fuel gas (C4 d)
in: 4 turbin hi cng sut 27 MW, cung cp 81
MW
4 l hi: 196 T/h, 107 kg/cm3, 505oC cung cp hi
nc HHP, HP, MP v LP
S dng thit b lm lnh bng nc bin
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45
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Cung cp nc ngt
Vietnam Petroleum Institute

246 m3/h

4 m3/h

99 m3/h

120 m3/h

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46
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Cung cp nc bin
Vietnam Petroleum Institute

12.000 m3/h

34.500 m3/h

22.500 m3/h

50.000 m3/h

22.500 m3/h
34.500 m3/h
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47
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Sn xut Nit
Vietnam Petroleum Institute

Sn xut, tn cha v cung cp nit di dng


lng, kh
Thit b lm lnh
Bn cha nit lng
Thit b bay hi nit lng

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48
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Sn xut nit
Vietnam Petroleum Institute

347 m3/h

647 m3/h

10 ngy
vn hnh
95 m3/h

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DU KH 49
49
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Fuel gas system


Vietnam Petroleum Institute

Thu fuel gas


Ho hi off-spec LPG/Propylene v C4s d

Cung cp fuel gas cho l t gia nhit trong


cc phn xng cng ngh

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DU KH 51
51
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Vietnam Petroleum Institute

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DU KH 52
52
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Vietnam Petroleum Institute

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Flare
Vietnam Petroleum Institute

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PETROLEUM
PROCESSING

B cha sn phm trung gian


Vietnam Petroleum Institute

S lng v Dung tch (m3)


TT

K hiu

B cha
Working

Gross

TK-5201 A/B/C

B cha Xng Mogas 92/95 xut cho tu (Mi


ni)

03 x 22.970

03 x 30.085

TK-5203 A/B/C

B cha Xng Mogas 90 xut cho tu (Mi


ni)

03 x 30.012

03 x 38.867

TK-5205 A/B/C

B cha JET A1/Kerosen xut cho tu (Mi


ni trong)

03 x 9.558

03 x 13.644

TK-5207 A/B/C

B cha Diezen t xut cho tu (Mi chp)

03 x 48.391

03 x 54.723

TK-5211 A/B

B cha FO xut cho tu v xe bn (Mi chp)

02 x 8.299

02 x 9.649

TK-5212
A/B/C/D/E

B cha LPG xut cho tu (B cu)

05 x 4.510

05 x 4.949

TK-5213 A/B/C

B cha Propylen xut cho tu v ng ng


(B cu)

03 x 3.340

03 x 3.710

381.961

467.130

1
2
3

Tng cng: 22 b

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B cha
Vietnam Petroleum Institute

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SPM
Vietnam Petroleum Institute

Tham kho thm


SPM
Flushing oil

SPM data
Item
Vessel size
Unloading rate
Cargo volume
Unloading time
Mooring work
Total loading time
Shiff draft
Required min Depth
Preferable Depht
Operation day/year
Vessel lenght
Bouy type
Hose size
Misc
Flushing
Pig??

unit
DWT
m3/hr
m3/ship
hrs
hrs
hrs
m
m
m
days
m
SALM
CALM
Inch x 2

Existing
111.000
6.000
120.000
20
<16
28
15
17
20
260
270
selected
30 U/sea
Yes
Yes

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Vietnam Petroleum Institute

S CNG NGH RFCC


..\Operating manual\8474L-015-ML001-1.pdf

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FLUE GAS TREATMENT


Vietnam Petroleum Institute

59
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FRACTIONATION
Vietnam Petroleum Institute

60
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GAS RECOVERY
Vietnam Petroleum Institute

61
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TCVN LPG 6548-1999

Vietnam Petroleum Institute

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TCNM Gasoline
Vietnam Petroleum Institute

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TCVN 6776 : 2005


Vietnam Petroleum Institute

TT

Tn ch tiu
90

1 Tr s octan, min
- theo phng php nghin cu (RON)
- theo phng php mt (MON)
2 Hm lng ch, g/l, max
3 Thnh phn ct phn on:
- im si u, oC
- 10% th tch, max
- 50% th tch, max
- 90% th tch, max
- im si cui, oC, max
- Cn cui, % th tch, max
4 n mn ming ng 50oC/3 gi, max

90
79

Xng khng ch
92
95
92
81
0,013

95
84

Bo co
70
120
190
215
2.0

22/12/2013
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TCVN 6776 : 2005


Vietnam Petroleum Institute

Tn ch tiu

TT

Xng khng ch
90
92
95

5 Hm lng nha thc t ( ra dung mi), mg/


100ml, max.
6 n nh xy ha, pht, min.

480

7 Hm lng lu hunh, mg/kg, max

500

8 p sut hi (Reid) 37,8 oC, kPa

43 - 75

9 Hm lng benzen, %th tch, max

2,5

10 Hydrocacbon thm, %th tch, max

40

11 Olefin, %th tch, max

38

12 Hm lng xy, % khi lng, max

2,7

13 Hm lng kim loi, mg/l


14 Khi lng ring ( 15oC), kg/m3
15 Ngoi quan

5
Bo co

Trong, khng c tp cht l


Tp. H Ch Minh
lng
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KEROSENE
Vietnam Petroleum Institute

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TCVN JET 6426-2007

Vietnam Petroleum Institute

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TCVN DO 5689-2005
Vietnam Petroleum Institute

Tn ch tiu

TT

Mc

Hm lng lu hunh, mg/kg, max.

Ch s xtan, min.

46

Nhit ct, oC, 90% th tch, max.

360

im chp chy cc kn, oC, min.

55

nht ng hc 40oC, mm2/ s

2 - 4,5

Cn cc bon ca 10% cn chng ct, %kl, max.

0,3

im ng c, oC, max.

+6

Hm lng tro, %khi lng, max.

0,01

Hm lng nc, mg/kg, max.

10

Tp cht dng ht, mg/l, max.

200
10

11

n mn mnh ng 50oC, 3 gi, max.

12

Khi lng ring 15oC, kg/m3

13

bi trn, m, max.

14

Ngoi quan

500

2500

Loi 1
820 - 860
460
Sch, trong

Tp. H Ch Minh

68
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Tiu chun nh my
Vietnam Petroleum Institute

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FO
Vietnam Petroleum Institute

MAX GAS

MAX DIS

BCH H 395

339

CHUA

3756

5330

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TCVN FO 6239-2002

Vietnam Petroleum Institute

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Din tch nh my
Vietnam Petroleum Institute

Khu ch bin, khu ph tr v nh iu hnh

110

Khu bn cha du th v h thng Flare

42

Khu bn cha sn phm

36

Khu ly nc bin, x l nc thi, ng ng


cng ngh, ng

44

Din tch cng xut sn phm

Tng cng (ha)

106

338

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Phn xng cng ngh


Vietnam Petroleum Institute

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NTU
Vietnam Petroleum Institute

X l RFCC naphtha: tch loi H2S v RSH RSSH


Cng ngh Mericat ca Merichem

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B cha sn phm
Vietnam Petroleum Institute

S lng v Dung tch (m3)


TT

K hiu

B cha
Working

Gross

TK-5201 A/B/C

B cha Xng Mogas 92/95 xut cho tu (Mi


ni)

03 x 22.970

03 x 30.085

TK-5203 A/B/C

B cha Xng Mogas 90 xut cho tu (Mi


ni)

03 x 30.012

03 x 38.867

TK-5205 A/B/C

B cha JET A1/Kerosen xut cho tu (Mi ni


trong)

03 x 9.558

03 x 13.644

TK-5207 A/B/C

B cha Diezen t xut cho tu (Mi chp)

03 x 48.391

03 x 54.723

TK-5211 A/B

B cha FO xut cho tu v xe bn (Mi chp)

02 x 8.299

02 x 9.649

TK-5212
A/B/C/D/E

B cha LPG xut cho tu (B cu)

05 x 4.510

05 x 4.949

TK-5213 A/B/C

B cha Propylen xut cho tu v ng ng


(B cu)

03 x 3.340

03 x 3.710

381.961

467.130

1
2
3

Tng cng: 22 b

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