Neraca massa zona 1

Citronell
al
Hexane
NiZrS

Citronell
al
Hexane
NiZrS

Mixer

Massa Masuk (kg)

Massa Keluar (kg)

Citronellal

1.259,5589

Citronellal

1.259,5589

Hexane

52.591,1609

Hexane

52.591,1609

NiZrS

40,8948

NiZrS

40,8948

Total

53.891,6146

Total

53.891,6146

Neraca massa zona 2

Citronellal
Hexane
NiZrS

Menthol
Hexane
NiZrS

Reaktor

Hidrogen

Massa Masuk
(kg)
Citronella
l

1.259,558 Menthol
9
52.591,16 Hexane
09

1.275,916
8

NiZrS

40,8948

40,8948

Hidrogen

16,3579

Total

53.907,9
Total
725

Hexane

C10 H18O (l) +

Citronellal

H2 (g)

Hidrogen

C10H20O (l)

Massa Keluar
(kg)

Menthol

NiZrS

52.591,16
09

53.907,9
725

Neraca massa zona 3

Menthol
Hexane
NiZrS
<1>

Akumulator

Menthol
Hexane
NiZrS

Menthol
Hexane

Centrifuge

Crystallizer

Menthol
NiZrS
<3>

Massa Masuk
(kg)

Massa Keluar
(kg)

<1>

<3>

Menthol

1.275,9168

Menthol

63,7958

Hexane

52.591,1609

NiZrS

40,8948

NiZrS

40,8948

Total

53.907,9725

<2>
Menthol

1.121.1212

Hexane

52.591,1609

Total

53.907,9725

Menthol
Hexane
<2>

Nermas zona 4
Menthol
Hexane
<1>

Air
<2>
Belt Vacuum
Washing Filter
Air
Hexan
e
<3>

Menthol
Air

Belt Vacuum
Filter
Air
Hexan
e
<4>

Menthol
Air

Udara
Kering
<5>
Menthol
Belt Drying
<6>
Filter
Udara Kering
Air
<7>

Massa Masuk (kg)

Massa Keluar (kg)

<1>

<3>

Menthol

1.121.1212

Air

52.393.078,4165

Hexane

52.591,1609

Hexane

52.591,1609

<2>
Air

52.498.074,5657
<4>

Udara Kering

Total

<5>
Udara Kering

206.205,9000

Air

209,9923

206.205,9000

52.551.887,8746

<6>
Menthol

1.121.1212

Total

52.551.887,8746

Neraca Panas
Heat capacity komponen :
Cpcitronellal
cpHexane
cpNiZrS solid

= 3,0266 kJ/kg. K
= 3,7465 kJ/kg. K
= 0,4100 kJ/kg. K

cp air pada suhu 364.15 K = 4,210

kJ/kg K
cp air pada suhu 303.15 K = 4,181
kJ/kg K

cp, Menthol liquid = 3,2186 kJ/kg. K

cp air pada suhu 296,15 K = 4,183

cp, Menthol solid = 1,8186 kJ/kg. K

kJ/kg K
cp air pada suhu 288.15 K = 4,190
kJ/kg K
cp air pada suhu 283.15 K = 4,195
kJ/kg K

Neraca panas zona 1

Citronell
al
Hexane
NiZrS

Mixer

Citronell
al
Hexane
NiZrS

0 = Hin Hout
Hin = hout
Suhu reference ( Tref ) = 25oC = 293,15
K
H = m cp T

Panas Masuk (kJ)

Panas Keluar (kJ)

Citronellal

2.2873,2631

Citronellal

2.2873,2631

Hexane

1.182.200,3755

Hexane

1.182.200,3755

NiZrS

100,6107

NiZrS

100,6107

Total

1.205.174,24
92

Total

1.205.174,24
92

Neraca Panas Zona 2

Citronellal
Hexane
NiZrS

Menthol
Hexane
NiZrS

Reaktor

Hidrogen

C10 H18O (l) +

Citronellal

H2 (g)

Hidrogen

C10H20O (l)
Menthol

Persamaan :
akumulasi = masuk keluar
steadystatesehingga tidak terjadi akumulasi, akumulasi = 0
terjadi reaksi,sehingga terdapat nilai HR
menggunakan steamsehingga terdapat Qair
0

= Hin (Hout + HR + Qair)

Panas Masuk (kJ)

Citronellal
2.2873,2631

Panas Keluar (kJ)

Menthol
14.777.504,69
35

Hexane

1.182.200,3755 Hexane

307.998,9496

NiZrS

100,6107

NiZrS

1.267,6232

Hidrogen

774,1265

Qloss

120.594,8376

HR

11.848.833,55
50

Qsteam

2.152.574,198
2

Total

15.207.356,1
289

Total

15.207.356,1
289

Neraca massa zona 3

Menthol
Hexane
NiZrS
<1>

Akumulator

Menthol
Hexane
NiZrS

Akumulator dan
Centrifuge

0 = Hin Hout
Hin = hout

Centrifuge

Menthol
Hexane

Crystallizer

Menthol
NiZrS
<3>

Menthol
Hexane
<2>

Crystallizer

menggunakan air pendingin sehingga

terdapat Qc
0 = Hin (Hout + QC)

Massa Masuk
(kg)

Massa Keluar
(kg)

<1>

<3>

Menthol

24.639,9172

Menthol

1.231,9959

Hexane

1.182.200,3758

NiZrS

100,6107

NiZrS

100,6107

Total

1.206.940,9033

<2>
Menthol

22.043,5082

Hexane

1.970.333,9591

Qc

-786.769,17053

Total

1.206.940,9033

Neraca Panas
Menthol
Hexane
<1>

Air
<2>
Belt Vacuum
Washing Filter
Air
Hexan
e
<3>

Menthol
Air

Belt Vacuum
Filter
Air
Hexan
e
<4>

Belt Vacuum Washing

Filter & Belt Vacuum
Filter :
0 = Hin Hout
Hin = hout

Menthol
Air

Udara
Kering
<5>
Menthol
Belt Drying
<6>
Filter
Udara Kering
Air
<7>

Belt Drying Filter :

G 1 + DHS1 = G 2 +
DHS2

Panas Masuk (kJ)

Panas Keluar (kJ)

<1>

<3>

Menthol

-22.042,5082

Hexane

-1.970.333,9591

Hexane

-1.970.333,9591

Air

2.197.240.319,6
119

<2>
Air

2.199.669.324,3
014

<4>
Air

<5>
G 1

18.346.180,19
9

<6>
DHS2

DHS1
DHS1

Total

-30.842,297

-4.398.458,7809

- 6.165,220
<7>

G 2

Total

18.321.503,42
1