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OBSERVATION TABLE

titrate disc
reading( diamete Bi(gmeq Bf(gmeq
No rps rpm ml) r(cm) /lit) /lit) a1(m2) a2(m2)

1 6 360 30 4.53 0.19 0.15 0 0

2 8.75 525 34 4.52 0.19 0.11 0 0

3 11.67 700 35.5 4.51 0.19 0.1 0 0

4 14.43 866 37.8 4.5 0.19 0.07 0 0

5 16.83 1010 39 4.5 0.19 0.06 0 0


ksl Ksl
calculated predicted
A(m2) a_(m2/m3) (m/s) Re Sc Sh (m/s)

0 6.19 0 11037.19 1175.86 1187.01 0

0 6.17 0 16003.71 1175.86 1429.33 0

0 6.16 0 21262.82 1175.86 1647.53 0

0 6.15 0 26165.41 1175.86 1827.63 0

0 6.15 0 30516.24 1175.86 1973.74 0


Height
of dp(orific
No H1(cm) H2(cm) dh(cm) H3(cm) H4(cm) dh(cm) bed(cm) e)
1 36 36 0 31.5 31.5 0 12.8 0
2 36 36.25 0.25 31.3 31.6 0.3 12.8 2.62
3 36 36.5 0.5 31.2 31.7 0.5 12.8 5.24
4 36 36.5 0.5 31 31.9 0.9 12.8 5.24
5 36 36.5 0.5 30.9 32.1 1.2 12.8 5.24
6 35.8 36.5 0.7 30.5 32.5 2 12.8 7.34
7 35.5 36.75 1.25 30.1 32.8 2.7 12.8 13.11
8 35.4 36.8 1.4 30 33.1 3.1 12.8 14.68
9 35 37.2 2.2 29.5 33.5 4 12.8 23.07
10 34.8 37.5 2.7 29.1 33.8 4.7 12.8 28.31
11 34.2 38 3.8 28.5 34.5 6 12.8 39.85

Height
of dp(orific
No H1(cm) H2(cm) dh(cm) H3(cm) H4(cm) dh(cm) bed(cm) e)
1 33 39.2 6.2 28.1 34.8 6.7 13.3 65.01
2 32 40.2 8.2 28 35 7 14.2 85.99
3 31.5 40.8 9.3 28 35 7 15 97.52
4 30.5 41 10.5 28 35.1 7.1 16.1 110.1
5 30 42.2 12.2 28 35.1 7.1 16.75 127.93
6 29.5 43.2 13.7 28 35.2 7.2 17.38 143.66
7 29 43.5 14.5 28 35.2 7.2 17.42 152.05
8 28.5 44 15.5 27.9 35.3 7.4 18.2 162.53
9 28 44.5 16.5 27.9 35.3 7.4 18.75 173.02
10 28 45 17 27.9 35.3 7.4 19 178.26

Height
of dp(orific
No H1(cm) H2(cm) dh(cm) H3(cm) H4(cm) dh(cm) bed(cm) e)
1 28 45 17 27.9 35.3 7.4 19 178.26
2 28 44.5 16.5 27.8 35.5 7.7 18.5 173.02
3 28.5 44.5 16 27.7 35.4 7.7 17.8 167.78
4 29 44.5 15.5 27.8 35.3 7.5 17.7 162.53
5 29 44 15 27.8 35.3 7.5 17.4 157.29
6 29.5 43 13.5 27.9 35.2 7.3 17 141.56
7 30 42.5 12.5 27.9 35.2 7.3 16.38 131.08
8 31 41.2 10.2 27.9 35.2 7.3 15.63 106.96
9 32 39.75 7.75 28 35.1 7.1 14.1 81.27
10 33 38.75 5.75 28 35 7 13.4 60.29

Height
of dp(orific
No H1(cm) H2(cm) dh(cm) H3(cm) H4(cm) dh(cm) bed(cm) e)
1 35 37 2 29.5 33.5 4 13.3 20.97
2 35.4 37 1.6 29.7 33.3 3.6 13.3 16.78
3 35.6 36.75 1.15 30.4 33 2.6 13.3 12.06
4 35.8 36.8 1 30.5 32.5 2 13.3 10.49
5 36 36.5 0.5 31 32 1 13.3 5.24
6 36 36.2 0.2 31.1 31.9 0.8 13.3 2.1
7 36 36.1 0.1 31.3 31.7 0.4 13.3 1.05
8 36 36 0 31.5 31.5 0 13.3 0

5-cm 10cm 15-cm 20-cm time(min) B'/t B'/t B'/t


1 1.9 4.3 6.4 9.3 1 0.04 0.03 0.03
2 1.9 4.4 6.3 9.4 2 0.04 0.03 0.03
3 5.9 7.8 9.9 12.3 3 0.01 0.02 0.02
4 3.1 5.8 7.8 9.3 4 0.02 0.02 0.03
5 3.4 6.1 7.9 9.2 5 0.02 0.02 0.03
6 2.9 4.9 6.9 9.4 6 0.02 0.03 0.03
7 2.4 4.5 6.7 8.9 8 0.03 0.03 0.03
8 2.3 5.1 6.9 8.9 12 0.03 0.03 0.03
9 2.1 4.5 6.8 9.1 13 0.03 0.03 0.03
10 2.4 4.8 7.5 10.5 15 0.03 0.03 0.03
11 1.9 4.5 7.3 10.1 17 0.04 0.03 0.03
12 3 6 8 10.5 20 0.02 0.02 0.03
13 2.9 6.4 9 11.5 25 0.02 0.02 0.02
14 3 6.8 9.4 12.3 30 0.02 0.02 0.02
15 3.3 7.8 10.1 14.2 35 0.02 0.02 0.02
16 3.5 7.7 11.1 15.2 40 0.02 0.02 0.02
17 3.6 6.9 10.8 15.4 45 0.02 0.02 0.02
18 3.7 7.8 11.8 15.9 50 0.02 0.02 0.02
19 3.9 8.2 12 15 55 0.02 0.02 0.02
dp(bed) vom u (dp/l)bed € log u log
0 0 0
14.32 1.26 0.03 111.86 0.82 -1.55 -0.09
23.86 1.78 0.04 186.43 0.82 -1.4 -0.09
42.95 1.78 0.04 335.57 0.82 -1.4 -0.09
57.27 1.78 0.04 447.43 0.82 -1.4 -0.09
95.45 2.11 0.05 745.72 0.82 -1.33 -0.09
128.86 2.82 0.06 1006.72 0.82 -1.2 -0.09
147.95 2.99 0.07 1155.86 0.82 -1.17 -0.09
190.9 3.74 0.08 1491.44 0.82 -1.08 -0.09
224.31 4.15 0.09 1752.44 0.82 -1.03 -0.09
286.36 4.92 0.11 2237.16 0.82 -0.96 -0.09

dp(bed) vom u (dp/l)bed € log u log


319.76 6.28 0.14 2404.24 0.82 -0.85 -0.08
334.08 7.23 0.16 2352.69 0.84 -0.79 -0.08
334.08 7.69 0.17 2227.21 0.84 -0.76 -0.07
338.85 8.18 0.18 2104.69 0.85 -0.74 -0.07
338.85 8.81 0.2 2023.01 0.86 -0.7 -0.07
343.63 9.34 0.21 1977.71 0.87 -0.68 -0.06
343.63 9.61 0.22 1972.6 0.87 -0.67 -0.06
353.17 9.93 0.22 1940.51 0.87 -0.65 -0.06
353.17 10.25 0.23 1883.59 0.88 -0.64 -0.06
353.17 10.4 0.23 1858.8 0.88 -0.63 -0.06

dp(bed) vom u (dp/l)bed € log u log


353.17 10.4 0.23 1858.8 0.88 -0.63 -0.06
367.49 10.25 0.23 1986.43 0.87 -0.64 -0.06
367.49 10.09 0.23 2064.55 0.87 -0.65 -0.06
357.95 9.93 0.22 2022.29 0.87 -0.65 -0.06
357.95 9.77 0.22 2057.16 0.87 -0.66 -0.06
348.4 9.27 0.21 2049.41 0.86 -0.68 -0.06
348.4 8.92 0.2 2127.63 0.86 -0.7 -0.07
348.4 8.06 0.18 2229.76 0.85 -0.74 -0.07
338.85 7.02 0.16 2403.22 0.83 -0.8 -0.08
334.08 6.05 0.14 2493.15 0.83 -0.87 -0.08

dp(bed) vom u (dp/l)bed € log u log


190.9 3.57 0.08 1435.37 0.82 -1.1 -0.08
171.81 3.19 0.07 1291.83 0.82 -1.15 -0.08
124.09 2.71 0.06 932.99 0.82 -1.22 -0.08
95.45 2.52 0.06 717.68 0.82 -1.25 -0.08
47.73 1.78 0.04 358.84 0.82 -1.4 -0.08
38.18 1.13 0.03 287.07 0.82 -1.6 -0.08
19.09 0.8 0.02 143.54 0.82 -1.75 -0.08
0 0 0 0 0.82 -0.08

B'/t B B B B A A A A
0.03 0.26 0.03 0.03 0.03 1069.47 1069.7 1069.7 1069.7
0.03 0.05 0.54 0.06 0.05 1069.67 1069.19 1069.67 1069.67
0.02 0.08 0.08 0.09 0.08 1069.65 1069.65 1069.64 1069.65
0.03 0.1 0.11 0.12 0.1 1069.62 1069.62 1069.61 1069.62
0.03 0.13 0.14 0.15 0.13 1069.6 1069.59 1069.58 1069.6
0.03 0.16 0.16 0.17 0.15 1069.57 1069.57 1069.55 1069.57
0.03 0.21 0.22 0.23 0.2 1069.52 1069.51 1069.5 1069.52
0.03 0.31 0.32 0.35 0.29 1069.41 1069.4 1069.38 1069.43
0.03 0.34 0.35 0.38 0.31 1069.39 1069.38 1069.35 1069.41
0.03 0.39 0.4 0.43 0.35 1069.34 1069.32 1069.29 1069.38
0.03 0.44 0.46 0.49 0.38 1069.28 1069.27 1069.24 1069.34
0.03 0.52 0.53 0.58 0.42 1069.21 1069.19 1069.15 1069.3
0.02 0.64 0.66 0.72 0.45 1069.08 1069.06 1069.01 1069.27
0.02 0.76 0.79 0.86 0.43 1068.96 1068.93 1068.87 1069.3
0.02 0.88 0.92 1 0.33 1068.85 1068.81 1068.73 1069.39
0.02 0.98 1.04 1.14 0.14 1068.75 1068.69 1068.59 1069.58
0.02 1.08 1.15 1.27 -0.15 1068.65 1068.57 1068.45 1069.88
0.02 1.17 1.27 1.41 -0.58 1068.56 1068.46 1068.32 1070.3
0.02 1.24 1.37 1.54 -1.15 1068.48 1068.35 1068.19 1070.87
v v v v Cc Cc dc/dt dc/dt*v
99.98 100 100 100 0 0
100 99.96 99.99 100 0 0 0 0
99.99 99.99 99.99 99.99 0 0 0 0
99.99 99.99 99.99 99.99 0 0 0 0
99.99 99.99 99.99 99.99 0 0 0 0
99.99 99.99 99.98 99.99 0 0 0 0
99.98 99.98 99.98 99.98 0 0 0 0
99.98 99.98 99.97 99.97 0 0 0 0
99.97 99.97 99.97 99.97 0 0 0 0
99.97 99.97 99.96 99.97 0 0 0 0
99.97 99.97 99.95 99.96 0 0 0 0
99.96 99.96 99.95 99.96 0 0 0 0
99.95 99.95 99.93 99.96 0 0 0 0
99.94 99.94 99.92 99.96 0 0 0 0
99.93 99.93 99.91 99.97 0 0 0 0
99.93 99.92 99.89 99.99 0 0 0 0
99.92 99.91 99.88 100.01 0 0 0 0
99.91 99.9 99.87 100.05 0 0 0 0
99.91 99.9 99.86 100.11 0 0 0 0
Cc dc/dt dc/dt*v Cc cd/dt Ca ln ca Ca
0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.7
0 0 0 0 10.7 2.37 10.69
0 0 0 0 10.69 2.37 10.69
ln ca Ca ln ca Ca ln ca da/dt da/dt da/dt da/dt
2.37 10.7 2.37 10.7 2.37
2.37 10.7 2.37 10.7 2.37 #DIV/0! -0.01 0 0
2.37 10.7 2.37 10.7 2.37 -0.01 0 0 0
2.37 10.7 2.37 10.7 2.37 0.01 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.09 0 0 0
2.37 10.7 2.37 10.7 2.37 0.05 0 0 0
2.37 10.7 2.37 10.7 2.37 0.11 0 0 0
2.37 10.7 2.37 10.7 2.37 1.04 0 0 #DIV/0!
2.37 10.7 2.37 10.7 2.37 0.13 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.17 0 0 0
2.37 10.7 2.37 10.7 2.37 0.1 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.07 0 0 0
2.37 10.7 2.37 10.7 2.37 1.24 0 0 0
2.37 10.7 2.37 10.7 2.37 -1.2 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.38 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.53 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.97 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.89 0 0 0
2.37 10.7 2.37 10.7 2.37 -0.38 0 0 0
da/dt/v da/dt/v da/dt/v da/dt/v ln ln ln ln

#DIV/0! 0 0.11 0 -9.22 -2.24 -15.1


0 0 0.11 0 -9.64 -2.24 -18.5
0 0 0.11 0 -2.24
0 0 0.11 0 -7.04 -13.27 -2.24
0 0 0.11 0 -2.24 -15.83
0 0 0.11 0 -2.23
-0.01 0 0.11 #DIV/0! -12.58 -2.23
0 0 0.11 0 -2.23 -16
0 0 0.11 0 -6.36 -12.61 -2.23 -17.35
0 0 0.11 0 -2.23
0 0 0.11 0 -7.28 -13.8 -2.23 -16.05
-0.01 0 0.11 0 -11.98 -2.23 -17.25
0.01 0 0.11 0 -4.42 -12 -2.23
0 0 0.11 0 -5.58 -12.94 -2.23
0.01 0 0.11 0 -5.24 -2.23
0.01 0 0.11 0 -4.63 -2.23
0.01 0 0.11 0 -4.72 -12.94 -2.23
0 0 0.11 0 -5.57 -12.16 -2.23 -14.2
wt of Radius(c clearance wt in speed(rp
resin(gm) Impellar m) (cm) pan(gm) m) P(watts)

25 disc 10 3 0 440 5.99


25 disc 5 5 2 510 0.29
25 disc 10 3 30 120 0.12
25 disc 5 5 50 150 0.01
25 pitch 10 3 0 390 13.87
25 pitch 5 5 0 510 0.97
25 pitch 10 3 20 210 2.17
25 pitch 5 5 25 230 0.09
50 disc 10 3 5 500 8.8
50 disc 5 5 7 620 0.52
50 disc 10 3 55 160 0.29
50 disc 5 5 85 220 0.02
50 pitch 10 3 0 500 29.22
50 pitch 5 5 5 540 1.15
50 pitch 10 3 25 230 2.84
50 pitch 5 5 55 260 0.13
60 disc 10 3 5 550 11.71
60 disc 5 5 10 650 0.6
60 disc 10 3 60 170 0.35
60 disc 5 5 100 240 0.03
60 pitch 10 3 0 540 36.81
60 pitch 5 5 5 670 2.2
60 pitch 10 3 30 240 3.23
60 pitch 5 5 30 300 0.2

volume volume
volume of of warer
of acetic toluene( added(ml
No acid(ml) ml) )

1 0 100 0
2 10 90 0.2
3 30 70 0.8
4 45 55 3.7
5 65 35 9.5
bottle1 bottle2
volume wt wt fraction volume
acetic acid 10 10.49 0.06 acetic acid 20
toluene 95 82.27 0.44 toluene 90
water 95 95 0.51 water 90

bottle3 bottle3
volume wt wt fraction volume
acetic acid 30 31.47 0.17 acetic acid 40
toluene 85 73.61 0.39 toluene 80
water 85 85 0.45 water 80

Aqueous phase

titration burette wt
volume( volume( reading( fraction(a
bottle ml) ml) ml) normality wt )

1 105 5 4.5 1.8 11.34 0.11


2 110 5 8.5 3.4 22.44 0.2
3 115 5 13 5.2 35.88 0.31
4 120 5 16.9 6.76 48.67 0.41

organic phase

titration burette wt
volume( volume( reading( fraction(b wt
bottle ml) ml) ml) normality wt ) fraction(a)

1 95 5 0.6 0.24 1.37 0.02 0.11


2 90 5 0.8 0.32 1.73 0.02 0.2
3 85 5 1.2 0.48 2.45 0.03 0.31
4 80 5 1.7 0.68 3.26 0.05 0.41
Torque w p(watts) ln(resin) ln(speed) D/T P*Nc

0 46.05 0 3.22 6.09 1.9 2637.55


0 53.38 0.12 3.22 6.23 3.8 148.77
0.03 12.56 0.42 3.22 4.79 1.9 14.59
0.06 15.7 0.88 3.22 5.01 3.8 1.11
0 40.82 0 3.22 5.97 1.9 5408.74
0 53.38 0 3.22 6.23 3.8 494.27
0.02 21.98 0.5 3.22 5.35 1.9 454.69
0.03 24.07 0.68 3.22 5.44 3.8 20.45
0.01 52.33 0.29 3.91 6.21 1.9 4398.15
0.01 64.89 0.51 3.91 6.43 3.8 324.94
0.06 16.75 1.04 3.91 5.08 1.9 46.12
0.1 23.03 2.21 3.91 5.39 3.8 5.15
0 52.33 0 3.91 6.21 1.9 14612.27
0.01 56.52 0.32 3.91 6.29 3.8 621.24
0.03 24.07 0.68 3.91 5.44 1.9 654.26
0.06 27.21 1.69 3.91 5.56 3.8 33.39
0.01 57.57 0.32 4.09 6.31 1.9 6439.33
0.01 68.03 0.77 4.09 6.48 3.8 392.55
0.07 17.79 1.2 4.09 5.14 1.9 58.77
0.11 25.12 2.83 4.09 5.48 3.8 7.3
0 56.52 0 4.09 6.29 1.9 19879.83
0.01 70.13 0.4 4.09 6.51 3.8 1472.27
0.03 25.12 0.85 4.09 5.48 1.9 775.68
0.03 31.4 1.06 4.09 5.7 3.8 59.18
wt wt fraction
20.98 0.11
77.94 0.41
90 0.48

wt wt fraction
41.96 0.22
69.28 0.36
80 0.42

distribution
coefficient

0.16
0.11
0.11
0.12
12

10

1
1 1 1 1 1