ADVANCED CLEANING RODUCT FORMULATIONS

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ADVANCED CLEANING PRODUCT FOR MULATlONS
Volume 5

Ernest W. Flick

NOYES PUBLICATIONS WILLIAM ANDREW PUBLISHING, LLC
Nomich, New York, U.S.A.

Copyright 0 1999 by Ernest W. Flick No part of this book may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying, recording or by any information storage and retrieval system, without permission in writing from the Publisher. Library of Congress Catalog Card Number: 89-30274 ISBN: 0-8155-1431-X Printed in the United States Published in the United States of America by Noyes Publications/William Andrew Publishing, LLC 13 Faton Avenue, Norwich, New York 13815

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Library of Congress Cataloging-in-Publication Data (Revised for vol. 5) Flick, Ernest W. Advanced cleaning product formulations Includes bibliographical references and index. 1. Cleaning compounds. I. Title TP990.F56 1989 668'1 89-30274 ISBN 0-8155-1186-8 (v. 1) ISBN 0-8155-1346-1 (v. 2) ISBN 0-8155-1382-1 (v. 3) ISBN 0-8155-1396-8 (v. 4) ISBN 0-8155-1431-X (v. 5)

To the late Ernie and Jeanne and Allyn and Barbara and Chris and Rachel V .

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Upholstery Shampoos and Cleaners (33) 14. Only the most recent formulas have been included. Floor. Polishes. All formulations are completely different than those contained in Volumes 1. manufacturers have been able to control costs but still enhance performance. Metal Cleaners and Polishes (72) 10. Oven. By changing formulations to improve cost/performance characteristics. Raw materials costs have risen and manufacturers have been reluctant to pass along these increases. Laundry Products (55) 9. Bathroom Cleaners (9) 2. The data represent selections made at no cost to. 3 and 4 published earlier. Rinse Aids (2) 13. with the number of formulations indicated in ( ): H. industrial and automotive applications. Rug. This book presents manufacturers' suggested formulations which might meet new performance criteria. o The formulations in this book are divided into the following sections and chapters. Food and General Industrial Cleaners (27) 3. Miscellaneous (33) vii . Carpet. Dairy. Dishwashing Detergents (34) 5. the makers or distributors of these materials. nor influence from. Household and Industrial Cleaners and Polishes 1. Degreasers (9) 4. Environmental considerations have also played a part. Grill and Hot Plate Cleaners (9) 11. Coatings and Finishes (6) 12. ~ ~ in the cleaning product industry has gradually been~undergoing ~ ~ ~ a ~ significant change during the past years. Glass CleanersPoiishes (12) ard Surface Cleaners (21) 8. 2. General Purpose Cleaners (31) 6. It is the result of information received from numerous industrial companies and other organizations.reface ohme 5) presents more than 423 up-to-date advanced cleaning product formulations for household.

A formula number is included. The table of contents is organized in such a way as to serve as a subject index. Miscellaneous (12) Each formula is located in the chapter which is most applicable. as available. who furnished information describing their trademarked raw materials. Massachusetts July 1999 Ernest W. there are two other sections which will be helpful to the reader. Flick . A chemical trademark section where each tradenamed raw material included in the book is listed with a chemical description rand the supplier's name. if applicable. The specifications which each raw material meets are included. The secondary source may be the originating company andlor the primary source's publication title. in the manufacturer's own words: Description of end use and most outstanding properties. Preface Transportation Cleaners and Polishes 15. which is the company or organization that supplied the formula. Key properties of the formula. IV. Whitewall Tire Cleaners (3) 18. Main office addresses of the suppliers of trademarked raw materials. Auto Cleaners and Polishes (6) 16. The percent by weight or volume of each raw material included i the n formula. should check each chapter which could possibly apply. Car and Truck Wash Compounds (49) 17. seeking a formula for a specific end use. if applicable. or both. My fullest appreciation is expressed to the companies and organizations who supplied the original starting formulations included in this book. which are the features that the source considers to be more outstanding than other formulations of the same type. I also thank the suppliers of the raw materials included in these formulations. The reader.viii 11. Each formulation in the book lists the following information. In addition to the above. Newburyport. rounded to a decimal figure. 111. The formula source.

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such information.NOTICE To the best of our knowledge the information in this publication is accurate. X . however. or consequences arising from. the Publisher does not assume any responsibility or liability for the accuracy or completeness of. and that he can meet all applicable safety and health standards. Final determination of the suitability of any information or product for use contemplated by any user. Mention of trade names or commercial products does not constitute endorsement or recommendation for use by the Publisher. This book is intended for informational purposes only. We recommend that anyone intending to rely on any recommendation of materials QB procedures mentioned in this publication should satisfy himself as to such suitability.

. . . . . . . . . . . 9 Cleaners for Industrial Application 10 Desinfecting Cleaner. . . . .. . .. . . . . . . . . . Acid . . . . . . . . . . . . . . . . . . 2 3 4 4 5 5 6 6 6 7 2. . . . . . . . . . . . . . . . . . . . . . . Heavy Duty Cleaners BBll Purpose-Food Process Plant . . . . . . . . . . . . . . . . . . . . . . .. . . . . . ... . . . Powder) . . . . . ... . . . . .. .. . FOOD AND GENERAL INDUSTRIAL CLEANERS . . . . . .. .. . . . .. . 12 12 13 13 xi . powder . . . . . . . . . . .. . . . . . . . . . . . . ... . Hard Surface Spray Cleaner . . . . . . . . . . . . 9 ust Removal Jelly .. . . . . . . .. .. . . . .. . . . . . . . . . . . . . . . . . . . . . . athroom Cleaner with Disinfectant . .. . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . .. .. Baking Pan Cleaner phosphate. . . . . . .. . . . . . . . . . . . . . . . . . . . ~ o w ~ ~ ~ Cleaner . . .. . .. . .. . . . . ... . . . .. . . . Heavy Duty Acid Bathroom Cleaner . .. . . . . . .. . . ... . . . . . . . . . . . . l d e w Tile Porcelain and Bathroom Cleaner. . . . . . . Acid .. .ntents and Subject Index SECTION I OUSEHOLD AND INDUSTRIAL CLEANERS AND POLISHES B OM CLEANERS: Toilet Bowl Cleaner . . . . . . . . . . .. . . . . . . . . . . . . 11 Zero phosphate. . . . . . . Hypochlorite Tub and Tile Cleaner and Mildew Stain Remover . . . . . . 11 uced Phosphate. . . . . . . 10 Spray Cleaner . . . . . . . . . .. . . . .. . . . . . . Powder) .. . . . . . . . . . ... . Mildew Remover .. . .. . .. . . . . . . . . . 10 Destainer sphate. . . . . . .. . . . . . . . . . . . . . . .. . . . Toilet Bowl Cleaner with Bleach . . . . . . . . . . . . . . . . . . . . . . . . . . . Dipping Cleaner . .. . . . . . . . . . . . . 8 Acid Industrial and Household Cleaners Oxalic Acid Gel . . .. . . . . . . . . . . . . . . Tub and Tile Cleaner . . . . . ... . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . ... . . . . powder) . . . . . . .

. . . . Chlorine Free. . . . . . . . . . . . . . . . . . . . . . . . . . . 15 Cleaner. . 21 Aqueous Degreaser d-Limonene Microemulsion . . . 23 Solvent Based Degreaser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Milk Can Cleaner (Phosphate. . . . . . . . . . . . . . . . Powder) . . . . . . . . . 25 Automatic Dishwash Detergent-Consumer (Zero Phosphate. Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 Aqueous Degreaser . . . . . 19 3 DEGREASERS . . Strongly Alkaline . . . . . . . . . . . . 26 Automatic Dishwash Detergent-Industrial & Institutional (Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 Metal Cleaner (Liquid) . . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Weakly Alkaline . . 22 Solvent Degreaser . 44 Steam Cleaner . . . . 24 Engine Cleaner and Degreaser . 18 Enzyme Prespotter for Oily/Smutty Soils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Strongly Alkaline (Phosphate-Free) . . . . 16 Food Industry Cleaner (Liquid) . . . . . . . . . . . . . . . . Chlorine Free. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Metal De-Oiling Liquid Concentrate (Liquid) . . . . . . . . . . . . . 1 9 Sanitizing Agent (Phosphate. . . . . . . . . . . . . . . . . . . . . . . 18 Premium Presoak . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 Automatic Dishwashing Detergent-Industrial & Institutional (Liquid~7 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . . Powder) . IS Sanitizing Cleaner (Phosphate. . . . . . . . . . . . . . . . . . . Solid Block . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 Automatic Dishwash Detergent-Consumer (Phosphate. . . . . . . . . 24 . . 21 Water Based Degreaser . . . . . . . . . . . . . . . . .xii Contents and Subject Index High Foaming Alkaline Cleaner . . . . Weakly Alkaline (Phosphate-Free) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 Degreaser Concentrate (Liquid) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 Cleaner. . . . . . . . . . . . . . . . 14 Industrial and High Pressure Cleaners Cleaner. . . . . . . . . . . . . . 14 Heavy Duty Alkaline Degreaser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 Powdered Enzyme Presoaks Economy Presoak . . . . . . . . . . 15 Cleaner. . . Powder) . . . . . . . . . . . DISHWASHING DETERGENTS . 4. . . . . . . 17 (Zero Phosphate. . . . . . . . . . . . . . . .

. . . . . . . . . . . . . Premium Hand Dishwash . . . 34 90% Premium Formulation . . . . . . . . . Powder . . . . . . . . . . . . . . All Purpose Cleaner . . . . . . . . . . . . . . . . . . .Phosphate. . . . . . . . . . . . . . . . . . . . . . . . 42 Premium Hand Dishwashing Detergent . . . . . . . . . . . . . . . . . . . . . . . . . . Chlorine Free. . . . . . . . . . . . . . . . . . . . . . 1 . . . . . . 30 Dish Washing Agents . . . 31 sh w/Amine Oxide/LABS/SLES . . . . . . . . . . . . . . . . . . . . . . . . 33 Hand Dishwashing Liquid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 Dish Washing Agents for Manual Use . . . rasive Cleaner Without Bleach . . . . . . . . . . . . . . . . . . . . . 39 Manual Dishwashing Gel . .Contents and Subject Index xiii Automatic Dishwash Detergent-Industrial & Institutional (Zero. . . . . . . . . . . . . . .No Rinse . . . . . . . . . Colorless Manual Dish Wash . . . . 40 Manual Dishwashing Liquid . . . . . . . . . . 42 Chlorinated Machine Dishwashing Compound. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 Dish Wash w l h i n e Oxide/LABS/ALES . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 Low Alkaline Warewashing Block . . . . . . . . . . . . . . . . . . . 35 Hand Dishwashing Liquid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 Rand Dishwashing Paste . . . . . Purpose Cleaner . Powder . . . . . . . . . . . . . Standard Formulation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 Now-Chlorinated Machine Dishwashing Compound. . . . . . . . . . A Purpose Cleaner . . . . . . . . . . . . . . . 33 Foam Booster: E-14-5 in Hand Dishwashing Liquids 34 Economy Formulation . . . . . . . . . . . . . . . . . 43 5 GEN LEANERS . 30 Powder Stainless Silverware Pre-Soak . . . 29 Clear. 38 Light Duty Liquid Low Cost Hand Dishwash . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 Light Duty Liquid. . . . . &alp Purpose Cleaner w/Amide/€’hosphate Ester . . . . . . . . . 34 Rernium Formulation . . . . . . . . . . Chlorine Free. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . All Purpose Cleaner . . . . . . . . . . . . . . . . . . . . . . . 38 Liquid Automatic Dishwasher Detergent . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . AB1-Purpose Disinfectant Cleaner . . . . . . . . . . . . . . . . . . . . . . . . 35 Pearlescent Dishwash . . . . . . 44 45 46 47 48 49 49 50 50 . . 34 Hand Dish Detergent Formulations Clear Dishwash . . . . . . . . . . . . . . . . . . . . . . . . Liquid . . . . . . . . . . . . Abrasive Cleaner with Bleach . 28 Automatic Dishwash Detergent-Industrial & Institutional (Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . 42 Non-Chlorinated Machine Dishwashing Compound. . . . . . . . . . . . . . . . . . . . . . . . . 28 Automatic Dishwashing Gel with Chlorine Bleach . . . . . . . . . . . . . . . . . . . . . . . .

. . . . . 65 Windows/Glass Glass Cleaner (Concentrate) . . . . . . . . . . . . . . . . . . 58 All Purpose Cleaner . . . . . . . . . . . . . . . . Anti-Static Glass Cleaner . . . . . . . . . . . . 64 Household Window Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Alkaline Hard Surface Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Hard Surface Cleaner-Spray . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65 Premium Household Window Cleaner . . . . . 57 Pump Spray All Purpose Cleaner . . . 65 Glass Cleaner . . . . . . . . . . . 53 General Purpose Cleaner (Consumer Low Alkaline. . . . . . 59 Disinfecting Cleaner. . . . . . . . . . . . . . . . . . . 5% Calcium Carbonate Abrasive Cleaner Without Bleach . . . . . . . . . . . . . . . . . . . . . . . 62 Glass Cleaner Concentrate (Non-Ammoniated) . . . . Alkaline . . . . . . . . . . . . . . . . . . . . . . . . . . 51 All Purpose Concentrate (Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66 Windshield Washer Concentrate (Low VOC) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 1 Anti. . . . 58 Pine Oil Cleaner Concentrate . . . . . . . . . . . . . . . Non-Phosphate Powder) . . . . . . . . . . 63 Glass and Window Cleaner . . . . . . . . . Liquid. . . . . . . . . . . . . . . . . . . Non-Phosphated Powder) . . . . . . . . . . . . . . . . . . 63 Glass Cleaner Concentrate . Ready to Use . . . . . . . . . . . . . Concentrated Hard Surface Cleaner . . . Hard Surface Cleaner Concentrate (All Purpose Type) . . . . Hard Surface Cleaner . . . . . . . . . . . . 56 All Purpose Cleaner . . . . . . . . . 66 7 HARD SURFACE CLEANERS . . . . . .Fogging. . . . . . . . . . . . . . . . . . . . . . . . 59 Sodium Bicarbonate Abrasive Cleaner Without Bleach . . . . . . . . . . . . . .xiv Contents and Subject Index (Phosphate. . . . . . . . . . . 57 Liquid Cleanser with Bleach . . . . . . . . . 62 Glass Cleaner. 52 Citric Acid Cleaner . . 55 General Purpose Spray & Wipe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54 General Purpose Cleaner (Consumer High Alkaline. . . . . . . . . . Pine Cleaner . . . . 54 General Purpose Spray & Wipe Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60 All Purpose Cleaner Concentrate 6 GLASS CLEANERS/POLISHES . 63 Ammoniated Glass Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid) . . 56 Hypochlorite Vertical Surface Cleaner . . . . . . . . . . . . . . . . . . . . . Foam . . . . . . 67 58 68 69 69 69 70 . . . . . . . . . . . . . . . . . . . . . . 66 Windshield Washer Concentrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. . Laundry Detergent-Consumer (Zeolite Built.. . Liquid Abrasive Cleaner . . Detergent for Fine Fabrics-2 . . . . . .. .. . . .. . . . . . . . . . . . . . .. .. . . . Industrial Laundry Detergents High Caustic Formulation . .. . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . .. . . . . . .. . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . Powder for Automatic Dishwashing Machines . . . .. . . . . . . .. . . . . . . . . . Powder) . . . . . dustrial Heavy Duty Laundry Liquid . . . . . . . . . . . . . .. . Liquid Hard Surface Cleaner . . . . . . . .. . . . . . . . . .. . . . . . . . . Tile and Sanitary Cleaners . . . . . . . . . . . . . . . .. . .. . . . .Contents and Subject Index Bard Surface Cleaner w/Amphoteric . . . Hard Surface Cleaner Concentrate wmipentene . Bard Surface Cleaner Concentrate (Phosphate. . . .. . . . . . . Laundry Detergent-Industrial & Institutional (Phosphate. . . . . . . . . .. .. . . . . . . Laundry Detergent-Consumer (Liquid) . ... . . . . . . . . . . . . . . . . . . . . .. . . .. . . . . . . . . . . . . . . . . . .. . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . Liquid) . . . . . . . . Powder) . . . . . . .. . . . . . . . . . . . . . . . .. . . . Powder) . . . . . . .. . . . . . . . . .. . ... . . .. . Laundry Detergent-Industrial & Institutional (Sodium Carbonate. . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . bundry Break-Industrial & Institutional (Liquid. . 1 h 1 Liquid Laundry Detergent with Enzyme & Optical . . . . . . . . . . . . . . . . . . . . . Washing Paste with Bleaching Agent . . . . . . . . . . Surfactant Rich Detergent for Nursing Homes . . . . . . . . . . . . .. . . . ... . . . . . . . Mixed Builder Formulation . . . . . .. . . . . . . . . .. .. . .. . . . . . . . . old and Mildew Remover . . . . . . . . . . . . . . . . Phosphate) . .. . Powder) . . . . ... . 84 85 85 86 86 87 87 . . Zero Phosphate. . . . Laundry Detergent-Consumer phosphate. . . . . . . .. . Liquid) . . Heavy Duty Laundry . . . Hard Surface Cleaner Concentrate w/d’Limonene . . . . . . . . . . . . . .. . .. . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . Alkaline Hard Surface Cleaner . . . . . . . . . . . . . Laundry Detergent-Industrial & Institutional (NTAJZeolite. . . . . . . . Hard Surface Cleaner-All Purpose .. .. . . Laundry Break-Industrial & Institutional (Liquid) . Hard Surface Spray Cleaner (Phosphate. . . . . . . . . . . . . . Liquid) . . .. Powder) . . .. . .. . . . . Laundry Break-Industrial & Institutional (Zero Phosphate. xv 71 71 72 72 73 73 74 74 74 75 76 77 78 78 79 80 80 80 81 82 82 82 83 83 84 PRODUCTS gent for Fine Fabrics-1 . . . . ... . .. . . . . . .. . . . . . . . . . . . . . . . . . . Laundry Detergent-Consumer (Zero Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . .

. . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . Laundry Detergent-Industrial & Institutional (Zeolite Built. . . . . . . . 96 Calsoft LAS-99 Based . . . . . . . Powder. . . . . . . . . . . . . . . Powder) . . . . . . 91 1 Laundry Detergent-Industrial & Institutional (Phosphate Built. . . . . . . . . . 98 Dry Cleaner: Pre Spot-Water Soluble . . . . . . . Powder) . 91 Laundry Detergent-Industrial and Institutional (Zero Phosphate. . 100 Detergent Additive . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100 Ultra Liquid Laundry Detergent . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .m i Contents and Subject Index Laundry Break-Industrial & Institutional phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Powder) . . . . . Aluminum CleanerBrightener . . . . . . . . . . . . . . . . . . . . . . . 99 99 Wool Wash . . . . . . . . . . . . . . . . . . . . . . . . . . . 802 p03 103 104 104 1104 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . 88 Laundry Detergent-Industrial & Institutional (Reduced Phosphate. . Liquid) . . . . . . . . . . . . . . . . . Solid Block) . . . . . . . . . . . . . . . . . . . . . . 92 Laundry Detergent-Industrial & Institutional (Liquid) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101 Fine Fabric Wash . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94 6 Laundry Detergent-Industrial and Institutional (Zero Phosphate. . . . . . . . . . . . . . . . 92 Laundry Builder-Industrial & Institutional 93 (Liquid) . . . . . . . . . . . . . . . . . . . . . . . . 90 Laundry Detergant-Industrial & Institutional (Phosphate. . . . . High Alkalinity) . . . . High Alkalinity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93 Laundry Prespotter Sprayable Gel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 0 10 Mixed Builder Break . . . . . Powdered Metal Cleaning Concentrate . . . . . . . . . . . . . . . . . . . . . . . . . Two Part Industrial Laundry Detergents Break Formulations Highly Alkaline Break . . . 89 Laundry Detergent-Industrial & Institutional (Sodium Carbonate with Flow Aid. . . . . Zero Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Acid Metal Cleaner . . . . . . . Aluminum Cleaner . . . . . . . . . . Dipping Cleaner for Silver . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95 Light Duty Liquid Detergent . . . . . . Liquid) . 94 Laundry Prespotter Sprayable Liquid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 61 9 METAL CLEANERS AND POLISHES . . . . . . . . . . . . . . . . . . . . . 88 Laundry Break-Industrial & Institutional (Zero Phosphate Powder. . . . . . . . . . . . . . . . . . . . . . . 89 Laundry Detergent-Industrial & Institutional (NTA. . . . .

. . . . . . Synthetic Machining Fluid . . . . . . . . . . . . . . . Metal De-Oiling Liquid Concentrate (Liquid) . . . . . . . . . . . . . . . . . . . Metal Cleaner (Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Water Soluble Stamping Fluid . . . . . . . . . . . . . . . . Synthetic . . . . . Semi-synthetic Cutting Oil . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Non-Phosphorous Aluminum Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Soluble Oil . Synthetic Formula . . . . . . . . . Alkaline Aluminum Cleaner . . . . Copper Machining Fluid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Burnishing Compound . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Cutting Oil Concentrate . . . . . . . . . . . . . . . Silver and Metal Polish . . Synthetic DrawindStamping Fluid . . . . . . . . . . Oil Based DrawindStamping Fluid . General Purpose Machine Cleaner . . . . . . . . . . . . . . . . . . . . . (Zero Phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Contents and Subject Index Aluminum Cleaner Concentrate F-498 . . . . . Soluble Oil Machining Fluid . . . . . . . . . . . . . . . . . . eta1 Cleaner phosphate. . . . . . . . . . . . . . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . General Purpose Synthetic Fluid (C) . . . . . . . . . . . . . . . . . . . . Aluminum Wash F-499 . . . . . . . . . . . . . . . . . . Semi Synthetic . . . . . . . . . . Powder) . . . . . . . . Powder) . . . . . . . Penetrating Oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Aluminum Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . Synthetic Formulation . . . . . . . . . . . . . . . . Universal Scouring Paste . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Cutting Oil . . . . . . . . . . . . . . . . . . . . . t Alkaline Paint Stripper Concentrate . . . . . General Purpose Synthetic Fluid (€3) . . . . . . . . . . . General Purpose Synthetic Fluid @) . . . . . Aluminum Cleaner phosphate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . xvii 105 105 106 106 106 107 109 109 110 110 111 111 111 112 112 113 113 114 115 116 116 117 119 120 122 122 123 124 124 124 125 130 133 133 134 134 134 134 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . -40 Type Lubricant Concentrate . . . . . . . . . . . . . Spray Metal Cleaning Concentrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ffing Compound Remover . . . Aircraft Cleaner Type I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . V General Purpose Synthetic Fluid (A) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. . . . Carpet Cleaner . High Gloss. . . . . . . . . . . . . . 1 Furniture Polish . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid Floor Cleaner . . . . . . . . . . . Floor Cleaner . . . . . . . . . . . . . . GRILL AND HOT PLATE CLEANERS . . . .xviii 10 Contents and Subject Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 RUG. . . . . . Household Carpet Freshenedhtistat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 147 147 Rinse Aid. Rug Steam Cleaner . . . . OVEN. . . . . . . . . . . . . . . . . UPHOLSTERY SHAMPOOS AND CLEANERS . . . . . . . . . . . . (Phosphate. . . . . . . . Marble Polish . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . n48 19 4 149 149 149 150 150 15 11 151 152 15 12 153 153 154 154 155 155 155 156 . . . . . . . . . . . . . . . . . . . . . . . Carpet Cleaners for the Spray-Extraction Process . . . . . . . . . . . . . . 11 4 142 143 144 144 145 145 12 . . . . Heavy Duty Oven Cleaner . . . . . . . . . . . . . . . . . . . . . Oven Cleaner wphosphate . . . . . . . . . . . . . . . . . . . . . . Liquid) . . . . . . . . . . 135 136 B6 3 137 138 138 139 139 10 4 140 1 POLISHES. . . . . . . . . . . . . . . . . . . . LeatherPlastic Polish . . . . . . . . . . . . . . . . . . . . . . . COATINGS AND FINISHES . . . . . . Vinyl Dressing (B) . . Oven Cleaner w/Amphoteric . . . . . . . . . . . Non-Caustic Oven Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Detergent Resistant Polish . . . . . . . . . . . . . . . 14 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Aerosol Oven Cleaner . . . . . . . . . . . . Carpet Shampoo . . . . . . . . . . . . . . . Low Foam Carpet Shampoo . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . High Caustic Oven Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Carpet & Upholstery Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Rust Removing Polish . . . . . Caustic Oven Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Oven Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . RINSE AIDS . . . . . . . . . . . Carpet Shampoo. . . . . . . High Foam . . . . . . . . . . . . . Scratched Wood Polish . . Steam Rug Cleaner-A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Carpet & Upholstery Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Heavy-Duty Floor Scrubber . . . . . . . . . CARPET. . . . . . . . . . . . . . . . . . . . . . . . . . . Oven Cleaner . . . . . . . . . . . . . . . . Acid . . FLOOR. . . . . . . . . . . . . . . . . Steam Rug Cleaner-B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid Steam Carpet Cleaner For Hard Water Systems . Rinse Aid . . . . . . . . Carpet Spot Remover . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . .. . . . . . . .. . . . . . . . . . Concentrated Formula . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . Isopar M Formulations . .. . . Bottle Wash Formulations w Foam . . . . . . . . . . . and Plastic Cleaner . . . oderate Foam . . . . . . . .. . . . . . . . . .. .. Low Cost Extraction Carpet Cleaner . .. . . . . White Wall Cleaner . . . . .. . . . . . . iao-Emulsions with d-Limonene . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . Concrete Cleaner . . . .. . . . . . . . . . . . . . . . . . . Plastic Bottle Wash .. . . . .. . . . . . . . . . . . .. . . . .. . . . . . . . .. . . . . . . . . . . . . .. . . . . . . .. . . . . . ... . . . . . ... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Wax Emulsion Using Pemulen Resins . .. aming Carpet Extractor Detergent . . . . Hospital Disinfectant . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . Pea Shampoo . . . . h w Viscosity Silicone Emulsion Using Pemulen Resins . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Micro-Emulsions with Pine Oil . . . . . . . . . . . acteriostatic Concentrate w/Pine Oil . .. . Dipentene Microemulsion Formulations -alkaline Formulations . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . .. . .. . . . . . No Rinse Floor Cleaner . .Contents and Subject Index Pump Spray Carpet Antistat . . . .. . . . . . . . .. . . Cutting Oil Concentrate . . Liquid Leather.. Liquid Leather.. . . . .. . . . . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . Medium Duty Steam Extraction Carpet Cleaner . . . . . m Cleaner (Liquid) .. . . . . . . . . . . . . . . . . . . . .. . . . . .. .. . . line Formulations . . . . . . .. . . . . . . . . . .. . ax Stripper (B) . . . . . . . . . . . No-Rinse Floor Cleaner Degreaser .. . . . . . . . . . . . . . . uty Steam Extraction Carpet Cleaner . . .. . . . . . . . . . . . . . Wax Stripper (A) .. . . . . . . . .. .. Concentrated Wax Stripper . . . . . . . . . . . . . . . . . . Premium. Paste Nand Cleaner . . . . . . . . . . . . . ... . . Heavy Duty Floor Cleaner . . . . . . . . . Vinyl. Cutting Oil . . . . . . . . . . . . . . . . . d ' l h o n e n e Waterless Hand Cleaner .. . . .. . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . xix 156 157 157 158 158 158 159 159 160 160 160 161 161 161 162 163 163 163 164 164 164 164 165 165 166 167 168 169 170 171 171 172 173 174 174 174 175 175 176 CEELANEQUS . Vinyl.. . . . . . . .. . . . . . . . .. . . . . . . . . . . Terpene Microemulsions . . . . . . . . . . . . . . . . .. . . . .. .. .. . . Luminizing Pet conditioner . Hydrocarbon Solvent Microemulsions Emsol D-110 Formulations . . . . .. .. . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . General Disinfectant Solution . . . . . . . . . . . . . . . . . . . . .. . . . . . . .. . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . and Plastic Cleaner and Restorer . . . . . . . . .. . . . . . . . . . .. . . . . . . . . .. .

. . . . . . . . . . . . . . Car Wash (Calsuds A-Based) . . . .. . . . . . . . . Low Cost Car Wash . . . . . . . . . . . . . . . . . . . . . . . . . . . Paste Car Wash . . . . . Liquid Spray Cleaner for Aluminum Trucks . . Auto Wipe & Shine Polish . . . . . . . . . .. . . . . . . . . . . . . . . . . . . .. CAR AND TRUCK WASH COMPOUN S . . . . . . . . . . . . . . . . . . . . . .. . . . . . . Rinse-off Agent (Water-Repellent) Without Hydrocarbons . . . . . . . . . . . . . . Mild Abrasive Automobile Polish . . . . . Insect Remover . . . . . . . . . . . . . . . General Purpose Car Wash . . . . . . . . . . . . Windshield-Cleaner (Summer) . . . Car Wash (Calsoft LAS-99-Based) . Car and Truck Wash Formula . . .. . .. . . . . . . . . . . Car Wash w/Amphoteric . . . . . . . . . . . .. . . . . . . . . . . . Windshield Washer Concentrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Wheel Cleaner. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Alkaline . . . . . . . . . . . . Liquid . . . . . . . . . . . . . . . . Chrome Polish . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Concentrated Traffic Film Removers . . . Windshield Washer Formulation . . . . . . . . . . . . Foamy Brush Car Wash. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xx Contents and Subject Index SECTION 11 TRANSPORATION CLEANERSl AND POLISHES 15 AUTO CLEANERS AND POLISHES . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid Car Wash . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. Car Wash Concentrate w/Alcohol Ethoxylate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid Car Polish . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Rinse-off Agent (Water Repellent) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . Car Wax . . . . . . . . . . . . . . . . . . .. . . . . Tar Remover . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . Non-Phosphorous Aluminum Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . ~ 184 185 15 8 185 186 186 187 187 187 133 189 189 189 190 10 9 190 10 9 1B 9 191 191 191 192 192 193 194 194 195 195 . . . . . . . . . . . . Windshield-Cleaner (Winter) . . . . . . . CarWash . . . . . . Car Shampoo Concentrate . . . .. . . . . Car Wash (Calsoft T-60-Based) . . . . . . . . . . . . . . . . . . . . . . . . Car Wash (Calsuds A-Based) . . . . . Car Wash powder) . Automobile Car Wash Concentrate . . . . . . . . . Car Wash and Care Car Shampoo with Water-Repellent Effect . . . . . . . . . . . . . . . . . . . . . . . . . . 1’’ 198 19 7 180 181 181 18 11 182 %83 184 16 . . . . . . . . . . . . . . . Aluminum Cleanermrightener . . . . . . . . . .

. . . . . . . . . . . . . . Car Shampoo . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Boat Polish . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . (Phosphate. . . . . . . . . . . . . . Mitewall Tire Cleaner (Zero Phosphate Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Contents and Subject Index Boat Wash & Car Cleaner . . . . . . . . . . . . . . . . . . . . . . . ConcreteDriveway Cleaners For Other Stains . . . . . . . . . . . . . . Car Wash and Wax Shampoo . . . . . . . . . . . Auto Shampoo Concentrate . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . Economy Tnuck/Bus Wash . Auto Care: Hnterior/Exterior Rubber & Vinyl Protectant . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Car Wash . . . . . . . . . . . . . . . . . . Powder) . . Acid Rust Remover . . . Vehicle Wash Detergent (Low pH) (Zero Phosphate. . phosphate Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . Concrete CIeanerDegreaser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . uy Premium Car Wash Concentrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Liquid) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Heavy D t Truck Wash. . . (Liquid. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xxi 195 196 196 197 197 197 198 198 199 199 199 199 200 200 201 201 202 203 203 203 ITEWALL TIRE CLEANERS . . . . Heavy Duty Concrete Cleaner (Phosphate Free) Formula 1C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . (Liquid) . . . . . . . . . . Vehicle Wash Detergent (Low pH) (Zero Phosphate. . Liquid . . . . . . . . Touchless Vehicle Wash Detergent (Zero Phosphate. . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . n SCEEUNEOUS . . . . Heavy Duty Truck Wash. . . . . . Vehicle Wash Detergent (Phosphate. . . . . . . . ressing (A) . . . . . . . . Aircraft Cleaner (Reduced Phosphate. . . . . . . . . . . . . . . . . . . . . . . . Garage Floor Cleaner . . 204 205 205 206 207 208 208 208 209 209 210 210 . . . . . . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . Powder . . . . . . . . . . . . . . Vinyl Dressing . . . . . . . . . . . . . . . . . . . Liquid) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Powder) . . . . . . . . . . . . . . . . . . . . . . . . . Tmck/Bus Wash . . . . . . . . . . . . . . . . low foam) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Touchless Vehicle Wash Booster/Additive (Zero Phosphate. .

. . . . . . . . . . . a ~ ~ . .. . .xxii Contents and Subject Index SECTION III: TRADEMARKED RAW MATE SECTION IV: SUPPLIERS' ADDRESSES s . . . . . . .. . 229 . . . 2nn .

ection I Household and Industrial Cleaners and Polishes 1 .

Bathroom Cleaner a .1.

00 2. I n a d d i t i o n .000 P r o d u c t pH: 1 . The p r o d u c t w i l l become i n c r e a s i n g l y t h i c k e r w i t h t i m e .00 cps BFGoodrich Dowfax 2A1 i2j Stepan Co. Total Actives: C i t r i c a c i d : 25.00 2.35 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-351 .00 DI Water Carbopol 6 7 4 ( 1 ) C i t r i c A c i d (50%) A l k y l benzene s u l f o n i c a c i d 97%) ( 2 ) Sodi u d o d e c y l d i p h e n y l o x i de d i s u l f o n a t e (45%) ( 3 ) m B r o o k f ie l d v i s c o s i t y ( R V T 20 rpm): 4. 4 . 2 . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e w a t e r / c i t r i c a c i d solu t i o n .0 Product C l a r i t y : C l e a r (1) 50. U s i n g moderate a g i t a t i o n ( 8 0 0 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . M i x t h e D I w a t e r and c i t r i c a c i d s o l u t i o n t o g e t h e r .Bathroom Cleaners 3 A c i d i c Toilet Bowl C l e a n e r Carbopol r e s i n s a r e used t o t h i c k e n t h i s a c i d i c t o i l e t bowl c l e a n e r f o r m u l a t i o n . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 30 m i n u t e s . I n s r e d ie n t : 5 43. Cool t h e p r o d u c t t o room t e m p e r a t u r e .00 A l k y l benzene s u l f o n i c a c i d : 1. t h e use o f t h e r e s i n p r o v i d e s v e r t i c a l c l i n g t o increase t h e contact time o f t h e detergent on t h e s o i l e d s u r f a c e and enhance consumer c o n v e n i e n c e .94 Dodecyl d i p h e n y l o x i d e d i s u l f o n a t e : 1.: Procedure: 1 .: B i o s o f t 5-100 ( 3 ) Dow Chemical Co. Add c o l o r and f r a g r a n c e . as d e s i r e d .h e a t i n g t o 40-50C w i l l h a s t e n t h e p r o c e s s .00 3. Add t h e s u l f o n i c a c i d and t h e d i p h e n y l o x i d e d i s u l f o n a t e surfactant.O-2. 3 .

65 5. Magnesium Aluminum Silicate Rhodopol 23. Xanthan Gum Deionized Water B: Diatomaceous Earth (Super Floss) Tetrasodium EDTA (Hampene 100) Sodium o-Phenylphenate (Dowicide A) Sodi um A1 kyl benzene Sul fonate (Cal soft L .%* 1 . Inc. Do not use on natural marble or polished aluminum. Vanderbilt Co.: Formulation No.00 2. Storage Stability: Formulation is freeze/thaw stable through 3 cycles.I. lbs/gal: 8.0 Mixing Procedure: Add ingredients to water in the order given and mix until homogeneous. Slowly add the Part 8 ingredients in the order shown. * A s received basis SOURCE: R.0 5. Continue mixing for 30 minutes. 363 Heavy Duty Acid Bathroom Cleaner Inqredi ents: Hydroxyacetic acid Sulfamic acid Ammonyx LO Water. SOURCE: Stepan Co.oo 0.0 10.4 Advanced Cleaning Product Formulatioris Bathroom Cleaner with Disinfectant Inqredi ents: A: Veegum T. D. Dry blend the Veegum T and Rhodopol 23 and add them to the water while stirring with an homogenizer at 5000 rpm. as is: 1.oo Procedure: 1 . 0 Density. Wt% 5.75 0. 200 .7 Use Instructions: Use as is o r dilute as needed.0 80.25 3.: Formulation No. %: 1 4 .35 86.00 1 . Formulation is stable for 3 weeks @ 50C.0 Solids. mixing each for 5 minutes.. 2. Properties: Appearance: Clear liquid pH. Use gloves. Do not mix with bleach.4 0 ) Butyl Cellosolve Wt .T.

oo Procedure: 4 . C o n t i n u e u n t i l smooth.00 8 : Sodium H y p o c h l o r i t e . S l o w l y s p r i n k l e t h e Van Gel 0 i n t o w a t e r a t room t e m p e r a t u r e w h i l e m i x i n g w i t h a homogenizer o r d i s p e n s e r o p e r a t i n g a t 5000 rpm. F o r m u l a t i o n No. Slow t h e m i x e r t o 1 0 0 0 rpm o r l e s s . Add P a r t B i n g r e d i e n t s s l o w l y i n t h e o r d e r shown.T. V a n d e r b i l t Co. A v o i d a i r e n t r a p m e n t . S l o w l y add t h e w a t e r w h i l e a g i t a t i n g a t maximum a v a i l a b l e s h e a r . M i x u n t i l uniform.55 0.25 50.45 10. m i x i n g a f t e r each a d d i t i o n u n t i l smooth and u n i f o r m . 5 . Anhydrous Procedure: 1 . 50% S o l u t i o n Sodium H y p o c h l o r i t e . 2 5 % Sodium M e t a s i l i c a t e . D r y b l e n d t h e Veegum T and TSPP. Add sodium h y d r o x i d e and m i x u n t i l u n i f o r m l y d i s s o l v e d .00 0. 458 Bowl /Mi 1dew C 1 e a n e r A: Ingredients: Veegum T . 2 .00 1. Magnesium Aluminum S i l i c a t e T e t r a s o d i u m P y r o p h o s p h a t e (TSPP) Water 5.00 10. Add t h e Vanseal NALS-30. C o n t i n u e m i x i n g f o r 40 m i n u t e s . : Suggested F o r m u l a t i o n s . 10% S o l u t i o n ( H y p u r e N ) Vanseal NALS-30 Wt%* 3. I n c . 424 *As r e c e i v e d b a s i s SOURCE: R. 2 . F o r m u l a t i o n No.75 34.00 85.Bathroom Cleaners 5 M i 1dew Remover Ingredients: Van Gel 0 D e i o n i z e d Water Sodium H y d r o x i d e .. 3 .

P h o s p h o r i c A c i d .4 17.5 Sodi urn H y p o c h l o r i t e ( 5 . D . : Suggested F o r m u l a t i o n s . I .5 P e t r o BAF Powder 2. 86% H y d r o c h l o r i c A c i d .0 P h o s p h o r i c A c i d .0 H y d r o x y a c e t i c A c i d . D .0 10.o between Remoz Ingredients: Water.8% pH: 13.3% pH: 1 . 44. A c i d Ingredients: 75.5 Water. F o r m u l a 529 Tub and T i l e C l e a n e r Ingredient: Water.6 Blending Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t io n . Dye B l e n d i n g Procedure: Add Xanthan Gum s l o w l y t o w a t e r w i t h h i g h speed m i x i n g . 37% R e w o t e r i c AM TEG V a r o n i c T202 SR Blending Procedure: Add in g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y each a d d i t i o n .6 Advanced Cleaning Product Formulations Tile.5 0. 7 F o r m u l a 530 H y p o c h l o r i t e Tub and T i l e C l e a n e r a n d M i l * S t a i n 67. 70% q. 7 % ) 52. Perfume. c p s : 293 S o l i d s : 16. P o r c e l a i n a n d Bathroom C l e a n e r . I f p r o b l e m s d e v e l o p a d d i n g Xanthan Gum t o w a t e r .5 F o r m u l a 531 SOURCE: W i t c o C o r p .6 13. p r e m i x t h e Xanthan Gum i n some i s o p r o p a n o l b e f o r e a d d i n g t o water. Typical Properties: V i s c o s i t y . Add r e m a i n i n g i n g r e d i e n t s i n o r d e r l i s t e d . cps: 4 S o l i d s : 3.9 Sodium H y d r o x i d e (30%) 1. I . A l l o w t o m i x u n t i l m a t e r i a l t h i c k e n s . 75% 12. T y p i c a l P r o p e r t ie s : V i s c o s i t y .5 1.o Varox 365 1. I .s. D . Xanthan Gum 0.

M i x u n t i l homogeneous. 8 4 Available Chlorine: 1. l r P o t a s s i u m s i l i c a t e (39%) ( 2 ) Potassium carbonate Sodium h y p o c h l o r i t e ( 1 2 . Total Actives: S i l i c a t e (as Si02): 1.00 5. 5 0 0 c p s P r o d u c t pH: 12-13 P r o d u c t c l a r i t y : Opaque ( 1 ) BFGoodri c h ( 2 ) PQ C o r p . W i t h c o n s t a n t a g i t a t i o n .32 C a r b o n a t e ( a s Na2C03): 3 .00 5. C o n t i n u e a g i t a t i o n and add t h e p o t a s s i u m c a r b o n a t e f o l l o w e d by t h e b l e a c h .OO Amine O x i d e : 3 . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r . 0 0 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-350 .Bathroom Cleaners 7 T o i l e t Bowl C l e a n e r w i t h B l e a c h Carbopol r e s i n s a r e used t o t h i c k e n t h i s t o i l e t bowl w i t h c h l o r i n e b l e a c h f o r m u l a t i o n .00 Procedure: 1 . 2 . Add t h e amine o x i d e s u r f a c t a n t and m i x u n t i l homogeneous.25 5. U s i n g m o d e r a t e a g i t a t i o n ( 8 0 0 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s .00 8. Add c o l o r a n d f r a g r a n c e . 5 . I n qr e d D I Water Carbopol 676 ( 1 ) P o t a s s i um h y d r o x i d e ( 4 5 % ) 2 . 3 . 5 0 % ) Amine O x i d e (30%) ( 3 ) B r o o k f i e l d v i s c o s i t y (RVT-20rpm) : 2 . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. ( 3 ) Lonza. : B a r l o x 12 i-w Wt% 60. a s d e s i r e d . 4 . I n c . t h e use o f t h e r e s i n provides v e r t i c a l c l i n g t o increase the contact time of the d e t e r g e n t on t h e s o i l e d s u r f a c e and enhance consumer c o n v e n i e n c e . add t h e p o t a s s i u m h y d r o x i d e and t h e p o t a s s i u m s i l i c a t e .00 10. I n a d d i t i o n .75 1.

Food and General Industrial Cleaner 8 . Dairy.2.

59n Aqueous S o l u t i o n P o l y s o r b a t e 40 (Tween 4 0 ) W t . C o n t i n u e m i x i n g f o r 60 m i n u t e s . C o n t i n u e m i x i n g f o r 60 m i n u t e s . 3 . V a n d e r b i l t Co.. 3 . F o r m u l a t i o n N o .00 Procedure: 1 . T .20 3. 466 Rust Removal J e l IY Insredi ents: Water Van Gel B Rhodopol 2 3 P h o s p h o r i c A c i d. D r y b l e n d t h e Van Gel 0 and Rhodopol 2 3 and add them t o he w a t e r w h i l e m i x i n g w i t h a p r o p e l l e r s t i r r e r a t 1800 rpm.00 0.D a i q .%* 53. A f t e r a l l t h e a c i d has been added. : Suggested F o r m u l a t i o n s .00 3. Reduce t h e s t i r r e r speed t o produce a s l i g h t v o r t e x and s l o w l y add t h e o x a l i c a c i d s o l u t i o n . Reduce t h e s t i r r e r speed t o produce a s l i g h t v o r t e x and s l o w l y add t h e P h o s p h o r i c A c i d s o l u t i o n . F o r m u l a t i o n No. 467 *As r e c e i v e d b a s i s SOURCE: R . 12. When a l l t h e a c i d has been added.70 2.80 40 0 0 3 00 50% Aqueous Sol u t ion Procedure: 1 . add t h e O c t o x y n o l . Octoxynol-9 WtD/ou 53.9 and mix u n t i l u n i f o r m . 2 . I n c .50 0. Food and General Industrial Cleaners 9 A c i d I n d u s t r i a l and Household C l e a n e r s O x a l i c A c i d Gel Inqredients: Water Van Gel B Rhodopol 2 3 O x a l i c A c i d D i h y d r a t e .80 40. Dry b l e n d t h e Van Gel €3 and Rhodopol 2 3 and add them t o t h e w a t e r w h i l e m i x i n g w i t h a p r o p e l l e r s t i r r e r a t 1800 rpm. 2 . add t h e P o l y s o r b a t e 40 and mix u n t i l u n i f o r m .

0 Wt% 75.0 3.0 1.5 22.0 3.5 4.5 General Formulations SOURCE: Zschimmer & Schwarz GmbH 8.0 0.0 0. : .0 86.0 20.0 0.0 3.0 0.5 2. 48.0 ether Spray C 1 e a n e r Insredients: Water Cublen D50 T r i e t h a n o l ami ne S u l f e t a l 4105 P r o p e t a l 241 Z u s o l a t l005/85 P h o s f e t a l 201 Butyl glycol C i t r u s terpene I n h i b i t o r 4000 F o r m u l a CT 07-06-01 Ingredients water Sul f e t a l 4105 P r o p e t a l 99 Zusolat 1005/85 Butyl glycol Orange t e r p e n e Formula CT 07-06-03 Q 58.5 10.0 5.0 3.0 24. A c i d I n s ed ien t s : water P h o s p h o r i c a c i d (85Oh) S u l p h u r i c a c i d (98%) P r o p e t a l 241 Dodigen 226 F o r m u l a CT 06-06-01 D i ppi n q C1 e a n e r I r ed i n e-n-t-sL itatger Tetrapotassium pyrophosphate C a u s t i c soda D i p r o p y l e n e g l y c o l monomethyl S u l f e t a l 4069 Zusol a t 1008/85 F o r m u l a CT 07-03-01 wts/.0 6.0 2.0 5.0 5. C o .0 3.5 5.10 Advanced Cleaning Product Formulations Cleaners f o r I n d u s t r i a l A p p l i c a t i o n D e s i n f e c t i n q Cleaner.0 4.

p a i n t . wood. p o l y m e r i c A p p l i c a t i o n Methods-Brush Manufacture-Dry blend/Agglomeration n : Composi t i o *STPP M e t s o Beads 2048 Sodi um S u l f a t e PQ Epsom S a l t **Octylphenoxy Polyethoxyethanol. p o l y m e r i c A p p l i c a t i o n Method-Brush Manufacture-Dry blend/Agglomeration Compos i t to^ *STPP M e t s o Beads 2048 Sodium S u l f a t e PQ Epsom S a l t **Octylphenoxy Polyethoxyethanol.0 2. Monohydrate Use L e v e l : 3-6 oz/gallon 9 .0 * ** FMC Rhone-Poulenc I g e p a l CA-630 D e t e r g e n t F o r m u l a t i o n Guide SOURCE: PQ C o r p .0 8. Sodium P e r b o r a t e .6 3 0 Destai ner (Reduced Phosphate.6 oz/ga * ** FMC Rhone P o u l e n c I g e p a l C A .0 38.0 15.0 25.0 25.0 Use D i l u t i o n : 2 . Powder) S o i l .0 2. mold and g r a s s Surface-Cement. p a i n t . mold and g r a s s Surface-Cement.4 . : . Food and General Industrial Cleaners I1 D e s t a in e r (Phosphate. Powder) S o i l .1 0 Moles EO % & 10.0 2.0 8. wood.O r g a n i c s t a i n s : f o o d . 5 % bw ( 3 . V a l f o r 100 Z e o l i t e A Sodium P e r b o r a t e .Dairy. Monohydrate Wt% 25. 3 .0 9- 0 M o l e s EO ion) 38.0 2.O r g a n i c s t a i n s : f o o d .

0 3..2 oz/gallon) psi) Wt% 30.A 1 umi num and s t e e l A p p l i c a t i o n Method-Irnmersion/brush Manufacture-Dry blend/Agglomeration O ~ ~t 1 o n : S l *Sodium C a r b o n a t e *STPP **Nonylphenoxy P o l y e t h o x y e t h a n o l .powder) S o i 1.0 12..H i g h p r e s s u r e s p r a y (700-1400 Manufacture-Dry blend Composi t i o n : Sodium C a r b o n a t e M e t s o Beads 2048 Sodium S u l f a t e V a l f o r 100 Z e o l i t e A * S o d i urn D i c h l o r o i s o c y a n u r a t e 2H20 * * S o d i um A1 k y l a r y l S u l f o n a t e Powder ( 9 0 % ) Use D i l u t i o n : 0 . 1 . .12 Advanced Cleaning Product Formulations Eaa C l e a n e r L x o phosphatS?.A n i m a l f a t and g r e a s e .n g Pan C l e a n e r (Phosphate. Metso Pentabead 2 0 C 9-10 M o l e s € 0 Wt% 35.Powder) S o i l .0 20.0 5.E g g and egg h a n d l i n g e q u i p m e n t A p p l i c a t i o n M e t h o d .1 . SOURCE: . 5 % bw ( 2 o z / g a l l o n ) I g e p a l CO-630 Detergent F o r m u l a t i o n Guide * ** FMC Rhone-Poulenc PQ C o r p .0 12.0 30. 7 5 .0 ** * O l i n Chemical Witco B g k i .0 3. v e g e t a b l e o i l S u r f a c e . 5 % bw ( 1 .P r o t e i n S u r f a c e .0 Use D i l u t i o n .0 50.

I n g r e d i e n t Water and TKPP when m i x e d a r e c l e a r . Add i n g r e d i e n t s i n o r d e r l i s t e d .00 10. T h i s i s a heavy d u t y c l e a n e r f o r f o o d p r o c e s s i n g p l a n t s . 4. 28% Weight% 89. 2-4 o z p e r g a l l o n .00 3. t h e pH i n c r e a s e s t o 1 2 .00 4. F o r m u l a t i o n HDC-004-01 Hard S u r f a c e Spray Cleaner . 4 .00 2. EDTA can b e s u b s t i t u t e d w i t h Na4EDTA t o make a c l e a r f i n a l solution.oo 3. Food and General Industrial Cleaners 13 Heavv D u t v C l e a n e r s A l l Purpose-Food P r o c e s s P l a n t Ingredients: Water EDTA ( E t h y l e n e d i a m i n e t e t r a c e t i c A c i d ) TKPP ( T e t r a P o t a s s i u m P y r o p h o s p h a t e ) P i l o t SXS-40 KOH. 45% Calamide C Weight% 74. Water and EDTA g i v e a m i l k y w h i t e s o l u t i o n . 3 . W i t h t h e a d d i t i o n o f C a l s u d s 81 t h e s o l u t i o n t u r n s c l e a r and has a pH o f 9. Use l e v e l .00 4. 6 . 3 . F o r m u l a t i o n HDC-002-01 SOURCE: P i 1o t Chemical Co. : Suggested Formul a t i ons .Dairy. 5 . 2 .00 1. When iUH40H i s added.00 5.00 Comments a b o u t t h i s f o r m u l a : 1 .00 Comments a b o u t t h i s f o r m u l a : 1 . Upon a d d i n g t h e o t h e r i n g r e d i e n t s t h e s o l u t i o n i s c l e a r .00 5.qredients: In Water TKPP ( T e t r a P o t a s s i u m P y r o p h o s p h a t e ) E t h y l e n e G l y c o l Monobutyl E t h e r C a l s u d s 81 NH40H. 2 . Hazy s o l u t i o n when E t h y l e n e G l y c o l M o n o b u t y l E t h e r i s added.

F o r m u l a t i o n F-762 proper- WtO/o 65. F o r m u l a t i o n F-769 Steam C1eaner Mona NF-20 c o n t r i b u t e s t h e non-foaming and d e t e r g e n c y t i e s i n t h i s formulation. I t e a s i l y displaces o i l y s o i l s from hard surfaces and keeps them f r o m r e d e p o s i t i n g .14 Advanced Cleaning Product Formulations H i qh Foaming A1 k a l ine C l e a n e r M o n a t e r i c EH c o n t r i b u t e s t o d e t e r g e n c y and e f f e c t i v e l y cont r o l s b o t h t h e k r a f f t and c l o u d p o i n t i n t h i s h i g h foaming formulation. : Suggested F o r m u l a t i o n s .0 Sodi u m H y d r o x i de ( 5 0 % ) Sodium M e t a s i l i c a t e ( P e n t a h y d r a t e ) 3.00 10. I n n r e d ie n t s : Wt9/o Water 76.0 Sodium H y d r o x i d e (50%) 10. Typical Properties: Cloud P o i n t : 75C K r a f f t Point: tOC Recommended Use D i l u t i o n : 4-6 o z .0 20. Package.0 Sodium M e t a s i l i c a t e ( P e n t a h y d r a t e ) 2.00 10.0 Dodecyl benzenesul f o n i c a c i d 2.0 Nonoxynol -1 0 2. Recommended Use D i l u t i o n : 1 : 2 0 w i t h w a t e r . I n a r e d ients: Water Potassi u Hydroxide m Sodium M e t a s i l i c a t e (Anhydrous) T e t r a p o t a s s i u Pyrophosphate m Mona NF-20 Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n .0 M o n a t e r i c EH 8. I n c .0 M o n a t e r i c EH 10. Ingredients: Wt% Water 65.0 Nonoxynol -1 0 2.0 Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n .0 Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n .00 3. Package.00 12.00 SOURCE: Mona I n d u s t r i e s . Recommened Use D i l u t i o n : 1 : 2 0 w i t h w a t e r F o r m u l a t i o n F-768 Heavy D u t y A l k a l i n e Degreaser M o n a t e r i c EH a i d s i n t h e removal o f o i l y s o i l s w i t h o u t emuls i f i c a t i o n . / g a l .

0 2.0 5.eaner.0 0.6 4.0 C1 e a n e r . Food and General Industrial Cleaners 15 I n d u s t r i a l and Hiqh Pressure Cleaners . o 4.0 Wt% 80.o 2.0 2.0 5.0 2.0 5.4 1.0 5. Weak1 y A1 k a l ine ( Phosphate-Free1 Ingredients: Water C u b l e n D 50 T r i s o d i um c i t r a t e S u l f e t a l 4105 Z u s o l a t 1008/85 P h o s f e t a l 201 Butyl glycol T r i e t h a n o l ami n e F o r m u l a CT 06-13-04 Wt% 80.0 3. Weakly A1 k a l ine Ingredients: Water Cublen D 50 Tetrapotassium pyrophosphate T r i e t h a n o l ami ne S u l f e t a l 4105 Z u s o l a t 1008/85 P h o s f e t a l 201 Butyl glycol F o r m u l a CT 0 6 .0 2.0 2.0 2 Cleaner.9 0.6 SOURCE: Zschimmer & Schwarz GmbH & C o .o 4.9 4.5 1.0 2. S t r o n q l y A1 k a l i n e (Phosphate-Free) I n g r e d i e c Water Cublen D50 Sodi um m e t a s i 1 i c a t e C a u s t i c soda S u l f e t a l 4105 Z u s o l a t 1008/85 P h o s f e t a l 201 Butyl glycol F o r m u l a CT 06-13-03 @1 eaner. : General Formulations . Strong1 y A1 Kal i ne C1 Inqredients: Water Cublen D 50 Tetrapotassi um pyrophosphate C a u s t i c soda Sodi u m m e t a s i 1 i c a t e S u l f e t a l 4105 Z u s o l a t 1008/85 P h o s f e t a l 201 Butyl glycol F o r m u l a CT 06-13-01 y% w 76. o 2.6 4.0 2.0 Wt% 80.6 4.1 3 .4 1.0 3.0 2.0 4.Dairy.5 1.

polymeric. mop o r b r u s h Manufacture-Mix t a n k w i t h p r o o e l l e r s t i r r e r Composition: Water TKPP (60%) N C l e a r Sodium S i l i c a t e Sodi um H y d r o x i d e (50%) *Phosphate E s t e r **Ethylene Glycol n-Butyl Ether * * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl3. o i l and p r o t e i n Surface-Metal.P e t r o l e u m and a n i m a l o i l and g r e a s e Surface-Metal: Steel A p p l ic a t i on Method-Immersi on Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Water S t a r Sodi um S i 1 ic a t e Sodium H y d r o x i d e (50%) *Phosphate E s t e r * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-C11.16 Advanced Cleaning Product Formulations Metal Cleaner (m S o i l . U n i o n C a r b i d e Rhone-Poulenc R h o d a s u r f LA-7 Detergent F o r m u l a t i o n Guide SOURCE: PQ C o r p .0 3.0 7.6 15.0 6 .1 6 o z / g a l l o n ) Wt% 74.5 6 Moles EO) ** * Rhone-Poulenc Rhodafac RE-610 Rhone-Poulenc R h o d a s u r f 91-6 Food I n d u s t r y C l e a n e r (W S o i l .0 3.3 5. Use D i l u t i o n : 6-12% bw ( 8 .0 5.0 7. glass A p p l i c a t i o n Method-Wipe.6 6. : .t% 65. Use D i l u t i o n : 2%-5% b v w. 5 Moles € 0 ) * ** *** Rhone-Poulenc Rhodafac RE-600 Dow C h e m i c a l .5 2.H e a v y f o o d g r e a s e .5 5. ceramic.

0 (90%) 2. Use L e v e l : 1 .0 3. 30.0 40.F a t and p r o t e i n Surface-Metal A p p l i c a t i o n Method-Wipe o r b r u s h Manufacture-Dry blend/Agglomeration WX/. Powder) S o l 1 . Powder) Sol 1 . : SOURCE: D e t e r g e n t F o r m u l a t i o n Guide . W i t c o PQ C o r p . 2H20 **Sod1 um A 1 k y l a r y l S u l f o n a t e Powder.2 o z / g a l l o n Wt% 20.0 0.0 * ** O l i n Chemical Stepan. Use D i l u t i o n (90%) 35.0 35. Food and General Industrial Cleaners 17 M i l k Can C l e a n e r (Phosphat_e.0 Compo_sition’ *STPP M e t s o Beads 2048 *Sod1 u m C a r b o n a t e +*Sod1 um D i c h l o r o i s o c y a n u r a t e . 2H20 * * * S o d i u m A1 k y l a r y l S u l f o n a t e Powder.F a t and p r o t e i n S u r f ace-Metal A p p l i c a t i o n Method-Wipe o r b r u s h Manufacture-Dry blend Composi t i on : Val f o r 100 Z e o l i t e A Metso Pentabead 20 Sodium C a r b o n a t e *Sodium D i c h l o r o i s o c y a n u r a t e .0 2.75-1 5% bw (1-2 o z / g a l l o n ) * ** *** FMC O l i n Chemical w1 t c o M i l k Can CLea-ner (Zeco Phosphate.Dairy.0 30.0 3.

0 10.0 35. Alcohol ethoxylates are Add components in the order listed. 49. the presoak temperature should be 130-15OF. Cool before adding the enzyme.0 1. wtD/. Inc. F o r optimum results.18 Advanced Cleaning Product Formulations Powdered Enzyme Presoaks Economy Presoak Component: Soda Ash Sodium Metasilicate Pentahydrate Sodium Dodecylbenzenesulfonate Powder Burcosperse AP Powder Burcotase EP-60 Premi um Presoak Component: Soda Ash STPP Neodol 25.0 5. Blend until uniform between each addition.0 10.o Wt% 80.0 10.0 5.0 1-4 i s preferred. : Suggested Formulations .1 0 . 0 preferred. n 5.0 10.0 3.0 3.0 5 40.0 20. 5 .0 5.0 2.0 2.0 5. SOURCE: Burlington Chemical G o . . Enzyme Prespotter f o r Oilv/Smuttv Soils Component: Water Propyl ene G1 ycol Dodecyl benzenesul foni c Acid TEA-85 Burco TME Nonionic Surfactant* Burcotase LL-100 *An HLB of 9 .7 Sodium Metasi 1 icate Pentahydrate Sodium Dodecylbenzenesulfonate Powder Burcosperse AP Powder Burcotase EP-60 The recommended use concentration o f these products i s g/1 in the presoak bath.

Powder)_ S o i l . M e t s o Pentabead 20 Quaternary Germicide Use D i l u t i o n : 0 . u r i n e . ceramic.2 oz/gallon) Wt% 20.0 10.0 10.2 etc.0 30. um A1 k y l a r y l S u l f o n a t e Powder (99%) Use D i l u t i o n : 0 .0 25. e t c . 7 5 .H o s p i t a l s o i l : sebum.0 35.H o s p i t a l s o i l : sebum. polymeric A p p l i c a t i o n Method-Wipe. 5 % bw ( 1 . 5 % bw ( 1 .0 30. Wt% 12 M o l e s EO) 30.0 5. b r u s h Manufacture-Dry blend/Agglomeration Composi t i on : *STPP *Sodi um C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl6. Surface-Metal. b l o o d . Powder) S o i l . 7 5 . 2H20 ***Sod. Surface-Metal.1 . : .1 . b l o o d .0 5.Dairy. polymeric A p p l i c a t i o n Method-Wipe o r b r u s h Manufacture-Dry Blend Composi t 1 1 0 ~ Metso Beads 2048 *Sodium C a r b o n a t e *STPP **Sodi urn D i c h l o r o i s o c y a n u r a t e . u r i n e .Food and General Industrial Cleaners 19 S a n i t i z i n s Cleaner (Phosphate. ceramic.0 * ** *** FMC 01 i n Chemical witco Sani t i z i na A a e n t (Phosphate.0 oz/gallon) * ** FMC Rhone-Poulenc R h o d a s u r f LA-12 Detergent F o r m u l a r y Guide SOURCE: PQ C o r p .

20 .3 Degreaser .

F o r m u l a t i o n DEG-006-01 SOURCE: P i l o t Chemical C o .Degreasers 21 Aqueous D e s r e a s e r Ingredients: Water NaOH.L i monene M i c r o e m u l s i o n Ingredients: d .20 Ether Comments a b o u t t h i s f o r m u l a : 1 .70 4.80 2. 2 . Add t h e w a t e r s l o w l y .00 7.70 6.90 9.50 2. 50% Cal s o f t LAS-99 P i l o t SXS-40 C a l o x y l a t e N-9 TKPP ( T e t r a P o t a s s i u m P y r o p h o s p h a t e ) Sodium M e t a s i 1 i c a t e E t h y l e n e G l y c o l Monobutyl Ether Comments a b o u t t h i s f o r m u l a : D i s s o l v e t h e s a l t s i n t h e water f i r s t .00 Wei q h t % 60. 50% Cal s o f t LAS-99 P i lot SXS-40 Na4EDTA C a l o x y l a t e N-9 E t h y l e n e G l y c o l Monobutyl Ether Sodi urn M e t a s i 1 ic a t e Weight% 68. : Suggested F o r m u l a t i o n s .60 4.80 2.00 3.00 7. 5 % sodium t r i p h o s p h a t e i s s u b s t i t u t e d f o r t h e sodium m e t a s i l i c a t e and Na4EDTA. Use w a t e r t o b a l a n c e i n g r e d i e n t s .00 9. 2 .40 8.93 73.00 5.44 4.00 Comments a b o u t t h i s f o r m u l a : 1 . F o r m u l a t i o n DEG-001-01 Aqueous D e q r e a s e r d .00 5.60 3. F o r m u l a t i o n DEG-002-01 Water Based D e a r e a s e r Ingredients: Water NaOH. T h e r e i s a p h o s p h a t e v e r s i o n where 3 .L i monene C a l s u d s CD-6 C a l imu1 se PRS Diethylene Glycol n-Butyl Water Weight% 9.50 2. A d d i t i o n a l C a l s u d s CD-6 may b e needed t o c l a r i f y t h e sample.

polymeric.C l l .C l l . * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-C11 Use D i l u t i o n : 2%-4% b v W B 6 M o l e s EO) 2 .0 7.0 5. e t c . 5 Moles EO) Use D i l u t i o n : Normal Duty-1.0 3.0 16. 5 M o l e s EO) 42. c o p p e r .6 1 0 R h o d a s u r f 91-6 R h o d a s u r f A-24 Metal De-Oiling L i q u i d Concentrate ( L i quid ) Soi 1 . o i l Surface-Pai n t .0 12. 2 .22 Advanced Cleaning Product Formulatiorrs m r e a s e r Concentrate ( L i q u i d) Soil-Grease.3 . 6 M o l e s EO) * * * * L i q u i d N o n i o n i c S u r f a c t a n t ( C 9 .0 20. : D e t e r g e n t F o r m u l a t on G u i d e . aluminum.0 5. Appl i c a t i o n Method-Spray a n d / o r immersi on Manufacture: Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Water S t a r s o Sodi urn S i 1 i c a t e EDTA.0 * ** Rhone-Poulenc R h o d a s u r f 91-6 Rhone-Poulenc R h o d a s u r f A-24 SOURCE: PQ Corp.0 5.0 10. metal A p p l i c a t i o n Method-Spray o r w i p e Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Water M e t s o Beads 2048 *Sodi urn P o l y a c r y l a t e (40%) **Phosphate E s t e r * * * L i q u i d N o n i o n i c S u r f a c t a n t ( C 9 . T e t r a s o d i u m (37%) Sodium X y l e n e S u l f o n a t e (40%) * L i q u i d N o n i o n i c S u r f a c t a n t (C9-C11.5% bw ( 2 o z / g a l l o n ) Heavy D u t y .0 * ** *** **** Rhone-Poulenc Rhone-Poulenc Rhone-Poulenc Rhone-Poulenc C o l l o i d 226/35 P o l y a c r y l a t e (40%) Rhodafac R E .b a s e d o i 1 S u r f a c e .P e t r o l e u m .0 8. 0 % bw ( 4 o z / g a l l o n ) w"o t/ 67.M e t a l : S t e e l .

U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s .00 2. I n c . 2 .50 0.5 Procedure: 1 . s u l f o n i c a c i d .00 2. 6 . Add t h e sodium h y d r o x i d e u n t i l t h e t a r g e t pH r a n g e i s reached. 5 .2 1.00 1. 4 . 5 moles EO ( 5 ) Isopropanol Sodium h y d r o x i d e (50%) B r o o k f ie l d v i s c o s i t y (RVT-20 P r o d u c t pH: 9 .1 0 P r o d u c t C1 a r i t y : Opaque (1) 9 81.0 2. Add t h e d-limonene w i t h good a g i t a t i o n and mix u n t i l homogeneous.5 2.5 DET-330 . I n q r e d ient : D I Water Carbopol ETD 2623 ( 1 ) d-Limonene ( 2 ) Propylene g l y c o l methyl e t h e r ( 3 ) Alkylbenzene s u l f o n i c a c i d ( 4 ) C12-13 l i n e a r a l c o h o l . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. 5 moles EO: SOURCE: BFGoodrich S p e c i a l t y Chemicals: 10. 3 .18 0. and alcohol ethoxyl ate. Reduce a g i t a t i o n and add t h e g l y c o l e t h e r . : B i o s o f t S-100 S h e l l Chemical: Neodol 23-6. T o t a l Actives: d-limonene: Propylene g l y c o l methyl e t h e r : Sodium a1 k y l b e n z e n e s u l f o n a t e : Psopropanol : C12-13 l i n e a r a l c o h o l .32 10. d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r .aegreasers 23 S o l v e n t Denreaser Carbopol r e s i n s a r e used t o e m u l s i f y and s t a b i l i z e t h i s d-limonene o i l based e m u l s i o n .50 2. 6 . t h e use o f t h e r e s i n provides v e r t i c a l c l i n g t o increase the contact time o f t h e d e t e r g e n t on t h e s o i l e d s u r f a c e and enhance consumer convenience. : H-7892 d-limonene Dow Chemical : Dowanol PM Stepan C o . I n a d d i t i o n . Add c o l o r . 6 . as d e s i r e d . Add t h e i s o p r o p a n o l 5 . .50 rpm) : 750 cps (2) (3) (4) (5) BFGoodrich A r y l e s s e n c e .0 2.

2 .24 0. 2 . F o r m u l a t i o n DEG-003-01 E n q i n e C l e a n e r and Deqreaser Ingredients: Water M I PA C a l imu1s e PRS Dowanol DPM Na4EDTA Comments a b o u t t h i s f o r m u l a : Clear. Kerosene can be s u b s t i t u t e d w i t h A r o m a t i c Naphtha.33 5. p a l e y e l l o w product F o r m u l a t i o n DEG-005-01 SOURCE: P i 1o t Chemi c a l Co.06 3.85 3.02 1. : Suggested Formul a t ions Weight% 58.99 86. Add i n g r e d i e n t s i n t h e o r d e r i n d i c a t e d .24 Advanced Cleaning Product Formulations S o l v e n t Based Deqreaser Insredients: Kerosene Aristonate M Pine O i l T a l l O i l F a t t y Acid C a l o x y l a t e N-9 Hexyl ene G1 y c o l Comments a b o u t t h i s f o r m u l a : 1 . A r i s t o n a t e L can be s u b s t i t u t e d f o r A r i s t o n a t e M~ F o r m u l a t i o n DEG-004-01 S o l v e n t Based Degreaser Ingredients: Aristonate M T r i t o n X-45 T r i t o n N-101 Kerosene Comments a b o u t t h i s f o r m u l a : 1 .08 45.94 20. 3.93 Wei ghP% 72.00 10.06 .00 2.41 W ig h t % e 5.00 10. A r i s t o n a t e M can be s u b s t i t u t e d w i t h A r i s t o n a t e L . Use a l o w o d o r g r a d e o f t a l l o i l f a t t y a c i d .10 5.

lshwashing Detergents 25 .

g l a s s . O r u s e a c o m b i n a t i o n o f A c u s o l 445ND and A c u s o l 479ND ( 2 w t . Powder1 S o i l . o i 1 and p r o t e i n S u r f a c e . p l a s t i c and c e r a m i c A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manufacture-Dry Blend/Agglomeration Composi t i on : Sodi urn C i t r a t e D i h y d r a t e * B r i t e s i l H20 Hydrous P o l y s i l i c a t e Sodi urn C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t ( 3 moles EO) * * * A c u s o l 445ND S o d i um P o l y a c r y l a t e ( 9 2 % sol id s ) ****Sodium P e r b o r a t e Monohydrate V a l f o r 100 Z e o l i t e A Sodium S u l f a t e 10.0 10.0 4. Balance w i t h s u l f a t e . Detergent F o r m u l a t i o n Guide SOURCE: PO C o r p . % each) O r use Sodium D i c h l o r o i s o c y a n u r a t e b l e a c h ( c o n t a i n s c h l o r i n e ) a t 2 w t % .M e t a l .0 15.0 * ** *** **** 2 .0 23.26 Advanced Cleaning Product Formulations A u t o m a t i c Dishwash Deteraent-Consumer ( Z e r o Phosohate.0 20. C h l o r i n e F r e e .0 23. Powder) S o i 1-Food g r e a s e .0 3.0 * ** *** **** FMC Rhone-Poulenc A n t a r o x BL-330 Rohm & Haas.0 15. C h l o r i n e F r e e . : .0 15. 0 w e i g h t r a t i o powder w i t h 1 7 . g l a s s .0 3. 5 % w a t e r Rhone-Poulenc A n t a r o x BL-330 Rohm & Haas.0 10.M e t a l . B a l a n c e w i t h s u l f a t e .0 30. % each) O r u s e Sodi u m D i c h l o r o i s o c y a n u r a t e b l e a c h ( c o n t a i n s c h l o r i n e ) a t 2 w t %.F o o d g r e a s e . o r use a c o m b i n a t i o n o f A c u s o l 445ND and A c u s o l 479ND ( 2 w t . A u t o m a t i c Dishwash Detersent-Consumer (Phosphate. o i l and p r o t e i n S u r f a c e .0 4. p l a s t i c and c e r a m i c A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manufacture-Dry blend/Agglomeration Composi t i on : RU L i q u i d Sodium S i l i c a t e *Sodium C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t ( 3 moles EO) * * * A c u s o l 445ND Sodi um P o l y a c r y l a t e (92% s o l id s ) ****Sodium P e r b o r a t e M o n o h y d r a t e *STPP Sodi um S u l f a t e 15.

0 13. 3 0 % bw ( 0 .Dishwashing Detergents 27 A u t o m a t i c Dishwash D e t e r c i e n t .0 1.0 35. p l a s t i c and c e r a m i c A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manufacture-Solid block Composi t i on : M e t s o Beads 2048 NaOH (50% S o l u t i o n ) *STPP *Sodi um C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t (7-9 Wt% 25.0 12. o i l and p r o t e i n S u r f a c e .0 * ** FMC Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 A u t o m a t i c D i shwashi n g D e t e r g e n t .0 . 2 .I n d u s t r i a l & I n s t i t u t i o n a l (Phosphate.0 25. o i l and p r o t e i n S u r f a c e . C12-15) 3.0 M o l e s EO. c e r a m i c and g l a s s A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition : Water * A c r y s o l ASE 108 ( A c r y l i c P o l y m e r ) * * T r i t o n DF-16 ( N o n i o n i c S u r f a c t a n t ) P o t a s s i um H y d r o x i d e (45%) TKPP (60%) N C l e a r Sodium S i l i c a t e Wt% 50.2 25.9 6. 4 * ** Rohm & Haas.F o o d g r e a s e .I n d u s t r i a1 & I n s t i t u t i o n a l (L iquid) S o i l .9 3. : . S o l i d B l o c k ) S o i l .0 . g l a s s .0 oz/gallon) Use D i l u t i o n : 0 . o r Rhone-Poulenc C o l l o i d 226/35 P o l y a c r y l a t e ( 4 0 % ) o r Rhone-Poulenc A n t a r o x EL-330 Detergent F o r m u l a t i o n Guide SOURCE: PQ C o r p .M e t a l .F o o d g r e a s e . 1 5 . Rohm & Haas.M e t a l .

p l a s t i c and c e r a m i c A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manuf a c t u r e .d .0 10.M e t a l . ! t i g n ~ j (Zero-Phosphate. a t i c P ~ h w a ~ h _ D e t e ~ e _ n ~ .M e t a l . g l a s s . : .0 25.0 26.0 3.9 M o l e s EO. C h l o r i n e F r e e .D r y B1 e n d / A g g l o m e r a t i on Composi t io n : M e t s o P e n t a b e a d 20 Sod1 um C a r b o n a t e * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 .9 M o l e s € 0 . oil and p r o t e i n S u r f a c e . o i l and p r o t e i n S u r f a c e .I n s t i ~ ! .28 Advarrced Clearring Product Formulatiorls A u t o m a t i c D i s h w a s h D e t e r g e n t T I n d u s t r i a l .0 * ** *** **** FMC Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l C h e m i c a l Neodol 2 5 . ~ I ~. O r u s e a c o m b i n a t i o n o f A c u s o l 445ND and A c u s o l 479ND ( 2 w t % e a c h ) . p l a s t i c and c e r a m i c A p p l i c a t i o n Method-Dishwasher ( s p r a y ) Manufacture-Dry Blend/Agglomeration Composition: G t s o P e n t a b e a d 20 *STPP * S o d i um C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . Powde_rj S o i l .F o o d g r e a s e . C12-15) * * * A c u s o l 445ND S o d i um P o l y a c r y l a t e ( 9 2 % sol i d s ) ****Sodium P e r b o r a t e Monohydrate B l e a c h Wt% 30. g l a s s . C h l _ o r i n e _Free. O r use sodium d i c h l o r o i s o c y a n u r a t e b l e a c h ( c o n t a i n s c h l o r i n e ) a t 2 w t % .0 3.0 4. C12-15) * * A c u s o l 445ND Sodium P o l y a c r y l a t e ( 9 2 % s o l i d s ) ***Sodium P e r b o r a t e M o n o h y d r a t e B l e a c h Val f o r 100 Z e o l i t e A Sodium S u l f a t e Wt% 30.0 4.u Stri-a 1 _&-Ins t_ii-tluti_ o?e_a_8 LP h o s p h a t e _ . A u t o m . Balance w i t h s u l f a t e . O r u s e a c o m b i n a t i o n o f A c u s o l 445ND and A c u s o l 479ND ( 2 w t % e a c h ) O r use sodium d i c h l o r o i s o c y a n u r a t e b l e a c h ( c o n t a i n s c h l o r i n e ) a t 2 w t % . Detergent F o r m u l a t i o n Guide SOURCE: PP C o r p .&.0 12.F o o d g r e a s e .Pow_s1ec) S o i l .7 Rohm & Haas.0 10.0 15. Balance w i t h s u l f a t e .0 28.0 * ** *** Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l C h e m i c a l Neodol 25-7 Rohm & Haas.

Screen t h e Carbopol r e s i n i n t . ( 5 ) O o w C h e m i c a l : Dowfax 382 Procedure: 1 .00 15.8 1..000 cps Wt% 44. rpm): 15. A l l o w t o m i x u n t i l homogeneous and f r e e o f p o l y m e r l u m p s .d e c y l d i p h e n y l o x i d e d i s u l f o n a t e ( 4 5 % ) ( 5 ) B r o o k f i e l d v i s c o s i t y (RVT-20 P r o d u c t p H : 12-13 P r o d u c t c l a r i t y : Opaque (1 BFGoodri c h ( 2 The P C o r p . l r p o t a s s i u m s i l i c a t e (39%) ( 2 ) P o t a s s i urn c a r b o n a t e ( 3 ) Sodium t r i p o l y p h o s p h a t e ( 4 ) S o d i um h y p o c h l o r i t e ( 1 2 .25 5. Add c o l o r and f r a g r a n c e . e . A d j u s t t h e pH t o 12-13 u s i n g KOH. 00 n o t u s e a c i d t o r e d u c e t h e pH. Inqredient: 01 w a t e r C a r b o p o l 672 ( 1 ) P o t a s s i um h y d r o x i d e ( 4 5 % ) 2 . O ( 3 Armand (4 FMC C o r p .00 1.Dishwashing Detergents 29 A u t o m a t i c D i s h w a s h i ng Gel w i tJ1_. Add i n t h e p o t a s s i u m h y d r o x i d e a n d p o t a s s i u m s i l i c a t e . 2 .Chlori n e B1 e a c h Carbopol r e s i n s a r e used t o t h i c k e n t h e p r o d u c t t o reduce s p l a s h i n g .00 20. 3 . 0 t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r ( 8 0 0 r p m ) .75 1.00 8. M i x u n t i l t h e r e a r e no more p h o s p h a t e p a r t i c l e s .00 5. Cool t h e p r o d u c t t o b e l o w 30C t o a v o i d e x c e s s i v e b l e a c h d e c o m p o s i t i o n . H e a t i n g t o 50-60C w i l l speed t h i s p r o c e s s . Add t h e b l e a c h and t h e n t h e s u r f a c t a n t . phosphate b u i l d e r s ) i n t h i s AOL f o r m u l a t i o n c o n t a i n i n g c h l o r i n e b l e a c h . The p r o d u c t w i l l become v e r y t h i c k a t t h i s poi n-t. 5 . and c r e a t e a s t a b l e suspension o f i n s o l u b l e s ( i . e s p e c i a l l y a f t e r t h e a d d i t i o n o f t h e b l e a c h . M i x u n t i l homogeneous.9 3.oo Total Actives: Phosphorous c o n t e n t : S i l i c a t e (as Si02): C a r b o n a t e ( a s Na2CO3): Ava i 1a b 1e c ti 1o r ine : SOURCE: 5. M i x u n t i l homogeneous. Add t h e p o t a s s i u m c a r b o n a t e and p h o s p h a t e . Use a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l 1e r s u i t a b 1 e f o r g e n e r a l m i x i ng and b l e n d i n g o p e r a t i o n s .o BFGoodrich S p e c i a l t y C h e m i c a l s : DET-100 .0 3. p r o v i d e c u p r e t e n t i o n i n t h e d i s h w a s h e r . 5 C 0 h ) Sodium n . a s d e s i r e d . 4 .

0 11 . Insredients: Water.0 30. Formula 1 2 9 W B 16.0 SOURCE: W i t c o C o r p .2 5. W i t c o l a t e ES-3 R e w o t e r i c AM 8-14 Ethanol Sodium C h l o r i d e C o l o r l e s s Manual . S i l i c a t e DeSoni c LFD-97 Sodium Carbonate (Soda Ash) Sodium T r i p o l y p h o s p h a t e Code 185 B l e n d i n g Procedure: B l e n d i n g r e d i e n t s i n t h e o r d e r l i s t e d .0 29. R. I . Anhydrous C a u s t i c Soda Beads 61 e n d i ng P r o c e d u r e : Blend i n g r e d i e n t s i n t h e o r d e r l i s t e d Use D i 1u t u i on : 1 o z / g a l Formula 1 2 7 Low A1 k a l ine Warewashi nq Block I n q r e d ie n t s : Water. o 2. : Suggested F o r m u l a t i o n s .U.0 3. D .3 B l e n d i n g Procedure: Blend i n g r e d i e n t s i n t h e o r d e r l i s t e d .D i s h Wash Wt% 57. When s l u r r y i s produced. D .0 2.30 Advanced Cleaning Product Formulations Clear.0 23.0 Wt% 67. Powder S t a i n l e s s S i l v e r w a r e Pre-Soak I n q r e d ie n t s : Sodium Carbonate (Soda Ash) P e t r o BAF Powder DeSonic 1 1 N T r i sodi u m Phosphate. D i s s o l v e c o m p l e t e l y between each a d d i t i o n . p o u r i n t o molds and a l l o w t o harden.0 5.0 3. I.0 25.5 34. Comment: R e w o t e r i c AM 8-14: Formula 1 3 2 Grease c u t t e r and foam b o o s t e r .

20 1 .30 17. 25% W A S alkanesulphonate:ethersulphate=4:l Ingredi e m A : H o s t a p u r SAS 6 0 Genapol Z R O l i q u i d B: Water Preservative DY e Perfume Tests: v i s c o s i t y (rnPas) : 75 C l o u d p o i n t : <-5C Wto/.50 0. 0.20 4.Dishwashing Detergents 31 Dish Washi nq Agents clear.oo 100 33.90 48.90 44.90 47.30 17.20 Inqredients: A : H o s t a p u r SAS 60 Genapol ZRO l i q u i d B: Water P r e s e r v a t iv e DYe Perfume Genagen LAB Tests: V i s c o s i t y (mPas): Cloud p o i n t : <-5C Inqredients: A : H o s t a p u r SAS 60 Genapol ZRO l i q u i d B: Water Preservative DY e Perfume Genagen LAB 33.30 17. liquid. 0. 33.s.s.10 q. SOURCE: t h e components o f B a r e added t o A Suggested F o r m u l a t i o n s Hoechst A k t i e n g e s e l l s c h a f t : .50 0.10 9. 0.10 q.00 Tests: V i s c o s i t y (mPas): 2 3 0 C l o u d p o i n t : <-5c Manufacturing: One a f t e r a n o t h e r .50 0.s.

00 21.20 1 . 0./.10 q. 4 0 37. Suggested F o r m u l a t i o n s SOURCE: Hoechst A k t i e n g e s e l l s c h a f t : . 40.00 21 .40 0 : Water Preservative DY e Perfume Hoe S 3924 Tests: V i s c o s i t y (mPas) : 420 C l o u d p o i n t : <-5C Ingredients: A : H o s t a p u r SAS 60 Genapol Z R O l i q u i d El: 37.s.10 q. 30% WAS a1 k a n e s u l p h o n a t e : e t h e r s u l p h a t e = 4 : 1 Insredients: A : H o s t a p u r SAS 60 Genapol Z R O l i q u i d €3: W B 40.30 0. t h e components o f 8 a r e added t o A .s. 0.00 Water P r e s e r v a t iv e DY e Perfume Hoe S 3924 Tests: V i s c o s i t y (mPas) : 61 0 C l o u d p o i n t : <-5C Manufacturing: One a f t e r a n o t h e r .oo wt.oo Water Preservative DY e Perfume Genagen LAB Tests: V i s c o s i t y (mPas) : 380 C l o u d p o i n t : <-5C Inqredients: A : H o s t a p u r SAS 60 Genapol Z R O l i q u i d wtsl.10 q.30 0.40 34.00 21.s.30 0.20 4. 0.32 Advanced Cleaning Product Formulations D i s h Washi nq A g e n t s C l e a r . 40. liquid.20 1.

Typical Properties: V i s c o s i t y . cps: 4 S o l i d s : 10.8% pH: 9 .Dishwashing Detergents 33 D i s h Wash w/Am&e lngredients: Water. I . Add e t h a n o l as needed t o l o w e r v i s c o s i t y .1% pH: 6 .0 26. W i t c o n a t e 1240 Varox 1770 W i t c o l a t e SE-5 Oxide/LABS/SLES Wtl 66. F o r m u l a 106 K % 60. Typical Properties: V i s c o s i t y .0 m i x i n g w e l l between SOURCE: Witco Corp.3 10.1 81 e n d i ng P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n . 6 8 F o r m u l a 118 __ Hand Di shwashi ng L i sui d Ingredients: Water W i t c o n a t e AOS W i t c a m i de 128T W i t c o l a t e LES-6OC Blendjng Instructions: Add a l l i n g r e d i e n t s i n t h e o r d e r l i s t e d .2 5. a d d i t i ons . D .8 3.0 13.0 10.0 B1 end? ng P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n .: Suggested F o r m u l a t i o n s .1 8.5. W i t c o n a t e 1240 Varox 1770 W i t c o l a t e LES-6OA Ethanol 70.3 5.0 4. c p s : 620 S o l i d s : 16. 1 2 F o r m u l a 117 D i s h Wash w / A m i n e Oxi de/LABS/ALES I n g r e d i e n t s1 Water.3 18. D . I . A c i d i f y w i t h C i t r i c A c i d t o pH=6.

34

Advanced Cleaning Product Formulations

Foam B o o s t e r :

Ez-4-5

in Hand D i shwashi na L i q u i d s

L i q u i d d i s h f o r m u l a t o r s a r e challenged t o produce low c o s t q u a l i t y p r o d u c t s . Hand d i s h d e t e r g e n t s a r e e x p e c t e d t o foam i n t h e p r e s e n c e o f f o o d s o i l s , c u t g r e a s e and c l e a n . I n a d d i t i o n , a e s t h e t i c s , s k i n m i l d n e s s , and e n v i r o n m e n t a l i m p a c t a r e a l s o m a j o r p r o d u c t c o n s i d e r a t i o n s . The f o l l o w i n g d a t a i l l u s t r a t e d how E-14-5 can b e used t o f o r m u l a t e c o s t e f f e c t i v e p r o d u c t s s u i t a b l e f o r t h e v a r i o u s l i q u i d d i s h soap m a r k e t segments. O p t i m i z e d l i q u i d d i s h d e t e r g e n t s c o n t a i n i n g E-14-5 p r o v i d e t h e optimum i n c o s t p e r f o r m a n c e when compared t o a l l o t h e r t y p e s o f foam b o o s t e r s . A l t h o u g h i t p e r f o r m s w e l l a l o n e , E-14-5 s y n e r g i s t i c a l l y enhances t h e p e r f o r m a n c e o f most t r a d i t i o n a l foam b o o s t e r s a s i l l u s t r a t e d b e l o w w i t h Coco d i e t h a n o l a m i d e . Economy Eormul a t i on
I gredi ent s : n Deionized water Dodecylbenzene s u l f o n a t e , sodium s a l t , (60% s o l i d s ) L a u r y l a l c o h o l e t h e r s u l f a t e - 4 EO, (60% s o l i d s ) Ethyl alcohol Tomah E-14-5 Coco d i e t h a n o l ami de

W. t%
59.7 2 5 . 9 ( 15) 8.4(5)
0

3 3

Standard Formulation

I gredi e n m Deionized water Dodecylbenzene s u l f o n a t e , sodium s a l t , ( 6 0 % s o l i d s ) L a u r y l a l c o h o l e t h e r s u l f a t e - 4 E 0 , (60% s o l i d s ) Ethyl alcohol Tomah E-14-5 Coco d i e t h a n o l ami de
90% Premi u m Formul a t ion Inqredi ents: Deionized water Dodecylbenzene s u l f o n a t e , sodium s a l t , (60% s o l i d s ) L a u r y i a l c o h o e t h e r s u l f a t e - 4 EO, (60% s o l i d s ) Ethyl alcohol Tomah E-14-5 Coco d i e t h a n o ami de

wt>
52.9 31 . 0 ( 1 8 ) 10. l ( 6 ) 1.5 3 3

Wt.%
38.6 38.8(22.5) 12.6(7.5) 4

3

_ Premi urn _ o r _ u l a t i o n _ F m ~ -

~

I n q r e d i en& Deionized water Dodecyl benzene s u l f o n a t e , s o d i um s a l t , (60% s o l i d s ) L a u r y l a l c o h o l e t h e r s u l f a t e - 4 E 0 , (6O0h s o l i d s ) Ethyl alcohol Tomah E-14-5 Coco d i e t h a n o l ami de SOURCE: Tomah P r o d u c t s , I n c . : Suggested F o r m u l a t i o n s

Wt.%
28.3 46.6( 27) 15.1 (9) 4 3 3

Dishwashing Detergents

35

Hand D i s h D e t e r a e n t F o r m u l a t i o n s C l e a r D i shwash

IngredienPs 1

\N t %
12.30 8.00 52.50 18.20 6.00

Water SXS (4O%j C12 A i f a O i e f in s u i f o n a t e ( 2 8 . 7 5 % s o i i d s j Lauryl e t h e r s u l f a t e - 3E0 (27.5% s o l i d s ) Tomah AO-728 S p e c i a l NaCl*

3.00

M i x i ng I n s t r u c t i o n s : Add t h e i n g r e d i e n t s i n t h i s o r d e r . M i x u n t i l homogeneous a f t e r each a d d i t i o n
SpG 2 0 / 2 0 C : 1 . 0 5 pH: 6 V i s c o s i t y : 505 c p s ( B r o o k f i e i d LVT 3 0 rpm s p i n d l e number 2)
NOTES:

*Add more N a c l t o i n c r e a s e v i s c o s i t y .

__ P e a r i e s c e n t U i shwash
ingredients: Water Dodecyibenzene s u i f o n a t e ( 6 0 % s o l i d s ) C a u r y i e t h e r s u l f a t e - 4 E 0 (60% s o i i d s j O p a c i f i e r L a t e x (4OWja P e a r l i z i n g Agent ( 4 7 % j * * Tomah A0-728 S p e c i a i Tomah A m p h o t e r i c L Mixing Instructions: Add t h e i n g r e d i e n t s i n t h i s o r d e r . M i x u n t i i homogeneous a f t e r each a d d i t i o n . SpG 2 0 / 2 0 C : 1 . 0 3 6.5 V i s c o s i t y : 1363 c p s ( B r o o k f i e l d LVT,
PH:
WLL7O

54.40 25.00 8 . 30 0.04 2.30 4.00 6.00

12 rpm,

s p i n d l e number

NOTES:

* **

L y t r o n 295 Mortor! i n t e r n a t i o n a l E u p e r i a n PK-771, Henkei Suggested F o r m u l a t i o n s

SOURCE: Tomah P r o d u c t s , f n c . :

36

Advanced Cleaning Product Formulations

Hand D i s h w a s h i n g L i q u i d C a r b o p o l r e s i n s c a n be used t o b u i l d r h e o l o g y i n p l a c e o f u s i n g h i g h e r s u r f a c t a n t l e v e l s . T h i s w i l l improve t h e s k i n f e e l and m i l d n e s s . A d d i t i o n a l l y , because o f t h e i r h i g h y i e l d v a l u e , t h e use o f Carbopol r e s i n s w i l l i n c r e a s e foam s t a b i l i t y . Inqredient: D I Water Carbopol ETD 2623 ( 1 ) 5 8 0 0 MW p o l y a c r y l i c a c i d ( 2 ) A l p h a s u l f o m e t h y l e s t e r (37%) ( 3 ) TEA (99%) Sodium l a u r y l e t h e r s u l f a t e (28%) ( 4 ) Coconut d i e t h a n o l ami de ( 5 ) B r o o k f i e l d v i s c o s i t y (RVT-20 P r o d u c t pH: 6 . 0 - 7 . 0 Product c l a r i t y : Clear rpm): 400-600 cps Q 38.11 0.70 4.00 27.03 5.50 17.86 2.00

( 1 ) BFGoodrich ( 2 ) BFGoodrich: Good-Rite K-7058 ( 3 ) Stepan Co.: A l p h a s t e p ML-40 ( 4 ) Henkel C o r p . : S t a n d a p o l ES-3 ( 5 ) Stepan C o . : N i n o l 11-CM Procedure: 1 . Use a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s P r e h e a t t h e w a t e r t o 40-5OC. Screen t h e Carbopol r e s i n i n t o t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r (800 r p m ) . A l l o w t o m i x f o r a t l e a s t 15 m i n u t e s o r u n t i l homogeneous and f r e e o f p o l y m e r lumps. 2 . Add i n t h e l o w m o l e c u l a r w e i g h t p o l y a c r y l a t e w i t h c o n s t a n t mixing. 3 . Add i n t h e ASME s u r f a c t a n t w i t h a l o w l e v e l o f a g i t a t i o n t o a v o i d e x c e s s i v e foam g e n e r a t i o n . 4 . Add i n t h e TEA, l a u r y l e t h e r s u l f a t e , and c o c o n u t DEA. 5 . A d j u s t t h e pH u s i n g TEA t o r e a c h t h e t a r g e t r a n g e . Add c o l o r and p e r f u m e , a s d e s i r e d . Cool b a t c h t o room t e m p e r a t u r e . Total Actives: Alpha s u l f o methyl e s t e r : Sodium l a u r y l e t h e r s u l f a t e : Coconut d i e t h a n o l a m i d e : 5 8 0 0 MW p o l y a c r y l i c a c i d : 10.00 5.00 2.00 2.00

SOURCE:

BFGoodrich S p e c i a l t y C h e m i c a l s :

DET-I10

Dishwashing Detergents

37

Hand Dishwashina P a s t e Carbopol r e s i n s a r e used t o t h i c k e n and suspend i n s o l u b l e s i n t h i s hand d i s h w a s h i n g p a s t e . A d d i t i o n a l l y , because o f t h e i r h i g h y i e l d v a l u e , t h e use o f Carbopol r e s i n s w i l l i n c r e a s e t h e foam s t a b i 1it y . I n a r e d ient :
D I water

Wt%
41.50 1 .oo 17.00 5.00 7.50 15.00 5.00 8.00

Carbopol 672 ( 1 ) A l k y l b e n z e n e s u l f o n i c a c i d (9796) ( 2 ) Sodi u h y d r o x i d e (50%) m 2 . 4 r sodium s i l i c a t e (52%) ( 3 ) Sodium t r i p o l y p h o s p h a t e ( 4 ) Sodium c a r b o n a t e Sodium o l e f i n s u l f o n a t e (40%) (5) B r o o k f i e l d v i s c o s i t y (RVT-20 rpm) : 75,000 cps P r o d u c t pH: 10-11 P r o d u c t c l a r i t y : Opaque
( 1) (2) (3) (4)

BFGoodri ch Stepan Co.: B i o s o f t S-100 The PO Corp. F C Corp. M ( 5 ) Stepan Go.: E i o t e r g e AS-40

Procedure: 1 . Use a L i g h t n i n ’ M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t o n s . Screen t h e Carbopol r e s i n i n t o t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r (800 r p m ) . A l l o w t o m i x u n t i l homogeneou and f r e e o f polymer lumps. 2 . Add t h e s u l f o n i c a c i d w i t h c o n t i n u o u s a a i t a t i o n . 3 . Add t h e sodium h y d r o x i d e and sodium s i l i c a t e w i t h c o n t i n u o u s a g i t a t i on. M i x u n t i1 homogeneous. 4 . S l o w l y , add t h e phosphate. M i x u n t i l homogeneous and f r e e o f phosphate p a r t i c l e s . H e a t i n g t h e p r o d u c t t o 50-60C w i l l speed up t h i s p r o c e s s . 5 . Add t h e sodium c a r b o n a t e and o l e f i n s u l f o n a t e . M i x u n t i l homogeneous. 6 . A d d c o l o r and f r a g r a n c e , as d e s i r e d .

T o t a l A c t ives : Phosphorous c o n t e n t : S i l i c a t e (as Si02): Carbonate ( a s Na2C03): Sodium o l e f i n s u l f o n a t e : Sodium a l k y l b e n z e n e s u l f o n a t e :
SOURCE:

3.7 2.7 5.0 3.2 17.6

BFGoodrich S p e c i a l t y Chemicals:

DET-111

1

38

Advanced Cleaning Product Formulations

L i g h t Duty Liquid, Ingredients: Water, D . I . W i t c o l a t e SE-5 W i t c o n a t e 1260 S l u r r y W i t c a m i de 128T P e t r o LBA L i q u i d Sodium S u l f a t e Ethanol Formal i n P e r f u m e , Dye

Premium Hand D i s h w a s h

Wt%
30.2 21.7 36.7 5.0 1.9 2.6 1.8 0.1 9,s.

81 e n d i n g P r o c e d u r e : B l e n d i n g r e d i e n t s i n t h e o r d e r l i s t e d . A d j u s t pH t o 6 . 5 - 7 . 0 using C i t r i c Acid. Typical Properties: V i s c o s i t y , c p s : 230 A p p e a r a n c e : C1 e a r L i q u i d F o r m u l a 113

L i g h t D u t y L i q u i d Low C o s t Hand D i s h w a s h Ingredients:. W a t e r , D . I. W i t c o l a t e SE-5 W i t c o n a t e 1260 S l u r r y W i t c a m i d e 128T P e t r o LBA L i q u i d Sodium C h l o r i d e Formal i n Perfume, Dye

81 . 5

5.5
9.2 1.2 0.5 2.0 0.1 q.s.

Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d . A d j u s t pH=6.5-7.0 using C i t r i c Acid. Typical Properties: V i s c o s i t y , c p s : 170 Appearance: C l e a r L i q u i d Formula 116

SOURCE:

Witco Corp.:

Suggested F o r m u l a t i o n s

00 53. H y d r a t e t h e Van Gel ES s l o w l y b y a d d i n g i t t o t h e a v a i l a b l e w a t e r u s i n g a h i g h speed d i s p e r s e r .00 10. Add B t o A s l o w l y w i t h m i x i n g .75 C: Sodium M e t a a s i l i c a t e . Suggested P a c k a g i n g : Squeeze b o t t l e o r pump. Sodium m e t a s i l i c a t e a d j u s t s t h e f o r m u l a p H . mixing u n t i l dissolved.25 0. Anhydrous Sodium H y p o c h l o r i t e . V i s c o s i t y 1300-1800 c p s .00 20.Dishwashing Detergents 39 Liquid Automatic Dishwasher Deterqent T h i s f o r m u l a t i o n f e a t u r e s Van Gel ES.T. Preblend B i n g r e d i e n t s .00 2.: F o r m u l a t i o n No. 1 2 . C o n s i s t e n c y and pH: Pumpable l i q u i d .00 2. t e c h n i c a l powder Wt% 4.. as a s u s p e n d i n g a g e n t and r h e o l o g y m o d i f i e r . M i x u n t i l u n i f o r m . S p i n d l e 4 a t 60 rpm measured a t room t e m p e r a t u r e a f t e r 3 0 days a g i n g .00 8. magnesium aluminum s i l i c a t e . combine D i n g r e d i e n t s and add w h i l e m i x i n g s l o w l y u n t i l smooth and u n i f o r m ( a v o i d i n c o r p o r a t i o n of air). B r o o k f i e l d Model LVT. t e c h n i c a l powder Sodi um T r i p o l y p h o s p h a t e . Continue mixing w h i l e c o o l i n g r a p i d l y t o 25C. Add C i n g r e d i e n t s i n t h e o r d e r l i s t e d . Inc. c l e a n i n g a g e n t and b l e a c h . 438 . Inqredi ents: A : Van Gel ES D e i o n i z e d Water B : T e t r a p o t a s s i u m P y r o p h o s p h a t e . F i n a l l y . The p h o s p h a t e b l e n d p r o v i d e s d e t e r g e n c y and t h e s u r f a c t a n t s contribute excellent r i n s a b i l i t y . SOURCE: R. V a n d e r b i l t Co. pH a p p r o x i m a t e l y 1 2 . 5 . 5 % s o l n . Sodium X y l e n e s u l f o n a t e Deceth-4-Phosphate D: Procedure: P r e h e a t t h e w a t e r t o 5 5 t o 60C. The sodium h y p o c h l o r i t e f u n c t i o n s as a d i s i n f e c t a n t .

7 .00 0. 2 .00 Procedure: 1 .t h i c k e n e d systems *easy-to-use.40 Advanced Cleaning Product Formulations Manual D i shwashi n q G e l F u n c t i o n s & B e n e f i t s : C a r b o p o l EX-473: * v i s c o s i t y m o d i f i e r f o r h i g h s u r f a c t a n t systems. 3 . 4. l i q u i d form i n i r e d l ent : Wt% DI w a t e r C a r b o p o l EX-473 ( 3 0 % ) * Sodium c i t r a t e Sodium h y d r o x i d e ( 1 8 % ) Ammonium l a u r y l s u l f a t e (30%)** Sodium l a u r y l e t h e r s u l f a t e (30%)*** * V i s c o s i t y modi f i e r : B F G o o d r i c h * * A n i o n i c s u r f a c t a n t : Standapol A : Stepan Chemical * * * A n i o n i c s u r f a c t a n t : S t a n d a p o l ES-3: S t e p a n C h e m i c a l P h y s i c a l P r o p e r t i es : B r o o k f i e l d RVT v i s c o s i t y .00 25. A d j u s t t h e pH w i t h sodium h y d r o x i d e t o d e s i r e d pH. r e a d j u s t w i t h a d d i t i o n a l s o d i u m h y d r o x i d e i f necessary. Add t h e sodium c i t r a t e .50 10.t h i c k e n t r a d i t i o n a l s a l t . M i x u n t i l t h e sodium c i t r a t e i s completely dissolved. Add f r a g r a n c e and c o l o r . a s d e s i r e d . U s i n g s l o w a g i t a t i o n ( 2 0 0 rpm) p r o v i d e d b y a L i g h . independent o f surfactant type *provides high c l a r i t y across s u r f a c t a n t l e v e l * i m p a r t s y i e l d v a l u e f o r s u s p e n s i o n o f .50 2. 5 . f o r i n s t a n c e . 6 . add t h e C a r b o p o l EX-473 r e s i n i n t o t h e D I w a t e r . 0 0 0 C P P r o d u c t pH: 6 . encapsulated actives * a b i l i t y t o p o s t . Add t h e l a u r y l s u l f a t e and l a u r y l e t h e r s u l f a t e s u r f a c t a n t s w i t h s l o w m i x i n g t o a v o i d e x c e s s i v e foam g e n e r a t i o n . 0 Product c l a r i t y : c l e a r 37. M i x u n t i l u n i f o r m a n d homogeneous. 5 . Check pH.00 25.t n i n ' m i x e r o r s i m i l a r v a r i a b l e speed u n . SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-130 .2 0 rpm: 8 .i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i ng o p e r a t i o n s . odorless.

t h i c k e n t r a d i t i o n a l s a l t .t h i c k e n e d systems *easy-to-use. 3 .0 Product c l a r i t y : Clear yt% 43. M i x u n t i l u n i f o r m and homogeneous.00 5. i n d e p e n d e n t o f surfactant type *provides h i g h c l a r i t y across s u r f a c t a n t l e v e l * i m p a r t s y i e l d v a l u e f o r s u s p e n s i o n o f . 2 . 4 . add t h e C a r b o p o l E X .50 I .4 7 3 r e s i n i n t o t h e D I w a t e r .a t e i s completely dissolved. 5 .5-7. DI w a t e r Carbopol EX-473 ( 3 0 % ) Ammonium l a u r y l s u l f a t e (30%)* Sodium l a u r y l e t h e r s u l f a t e ( 3 0 % ) * + Sodium c i t r a t e Sodium h y d r o x i d e (18%) * A n i o n i c s u r f a c t a n t : S t a r i d a p o l A : Stepari Chemical * * A n i o n i c s u r f a c t a n t : S t a n d a p o l ES-3: Stepan Chemical Physical Properties: B r o o k f i e l d R V T v i s c o s i t y . Using slow a g i t a t i o n (200 r p m ) provided by a L i g h t n i n ' Mixer o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . Add f r a g r a n c e and c o l o r .00 25.oo Procedure: 1 . f o r i n s t a n c e . SOURCE: BFGoodrich S p e c i a l t y C h e m i c a l s : DET-120 .00 0.Dishwashing Detergents 41 _ _ D i shwashi nq L i q u i d Manual F u n c t i o n s B B e n e f i t s : Carbopol EX-473: * v i s c o s i t y m o d i f i e r f o r h i g h s u r f a c t a n t systems. l i q u i d form I n g r e d i en t . Add t h e sodium c i t r a t e . M i x u n t i l t h e sodium c i t i . A d j u s t t h e p H w i t h sodium h y d r o x i d e .50 25. Add t h e l a u r y l s u l f a t e and l a u r y l e t h e r s u l f a t e s u r f a c t a n t s w i t h s l o w m i x i n g t o a v o i d e x c e s s i v e foam g e n e r a t i o n . encapsulated actives * a b i l i t y t o p o s t . a s d e s i r e d . odorless.2 0 rpm: 5 0 0 CP Product pH: 6.

I .0 Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d . Powder Sodi um G1 u c o n a t e Sodium M e t a s i l i c a t e .0 10.0 10.5 2.C h l o r i n a t e d M a c h i n e D i s h w a s h i n q Compound.0 1. w i t h each a d d i t i o n . L i g h t D e n s i t y DeSoni c LFD-97 Sodium M e t a s i l i c a t e . F o r m u l a 111 N o n . Ingredients: Sodi um C a r b o n a t e (Soda A s h ) .o 7. Anhydrous C a u s t i c Soda Beads CDB C l e a r o n Powder 30.42 Advanced Cleaning Product Formulations N o n . Inqredi ents: Sodi um C a r b o n a t e (Soda A s h ) .C h l o r i n a t e d M a c h i n e D i shwashi n g Compound.0 30. P e n t a h y d r a t e C a u s t i c Soda 50% P e t r o ULF L i q u i d 81 e n d i ng P r o c e d u r e : Add a l l components i n t h e o r d e r shown.0 1 . m i x i n g w e l l between C h l o r i n a t e d M a c h i n e D i shwashi n q Compound. L i g h t D e n s i t y Sodi um T r i p o l y p h o s p h a t e (STPP) . L i g h t D e n s i t y Sodium T r i p o l y p h o s p h a t e (STPP).o . I n Q r e d ie n t s : Water.0 1.o 8. Sodi um T r i p o l y p h o s p h a t e Versene 2 2 0 . Anhydrous C a u s t i c Soda Beads Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d . D . L i g h t D e n s i t y DeSoni c LFD-97 Sodium M e t a s i l i c a t e . F o r m u l a 112 Powder Wt% 33.0 2.0 25. o 30.0 4. : Suggested F o r m u l a t i o n s .5 1 . mixing thoroughly w i t h each a d d i t i o n .0 25.0 mixing thoroughly SOURCE: W i t c o C o r p . a d d i t i ons F o r m u l a 109 Liquid \Mt% 79.

o approx.9 56. F: >200 Wt% 6. D .0 12. . deg.S t e p MC-48 S t e o l CS-330 N i n o l 30-LL o r N i n o l 40-CO Sodium C h l o r i d e P r o p e r t i es : Appearance: C l e a r y e l l o w l i q u i d pH. 173 D i s h Washina A q e n t s f o r Manual Use Inqredi ents: Water Lumorol 4154 Z e t e s o l NL Z u s o l a t 1008/85 Sodium c h l o r i d e F o r m u l a t i o n CT 02-01-04 m e d ien t s : Water Z e t e s o l 2056 Amphotensid B 4 Z u s o l a t 1008/85 P u r t o n CFD F o r m u l a t i o n CT-02-01-05 79.5 Suggested F o r m u l a t i o n s SOURCE: Zschimmer & Schwarz GmbH & C o . l b s / g a l : 8 . 0 Wt% 76.5 20. : F o r m u l a t i o n No. Comment : The s u r f a c t a n t s used i n t h i s f o r m u l a t i o n a r e d e r i v e d f r o m o l e o c h e m i c a l r e s o u r c e s and a r e b i o d e g r a d a b l e .6 1. 3 c y c l e s : Pass C o l d s t o r a g e @ 4 deg. c p s : 220 S o l i d s .0 6.Dishwashing Detergents 43 P r e m i um Hand D i shwashi ng D e t e r q e n t Inqredients: Water. C . Add 30-LL o r 40-CO and m i x u n t i l homogeneous.o 0.5 Pass M i x i n g Procedure: CHarge w a t e r . % : 39-40 Density. SOURCE: Stepan C o .0 2.0 1. Add MC-48 and CS-330 and m i x . : . 2 weeks: F l a s h p o i n t . A d j u s t p H w i t h s u l f u r i c a c i d o r sodium h y d r o x i d e as n e c e s s a r y . 8 Freeze/thaw. 2 . C .0 1. I . as i s : 6 .7 . 5 V i s c o s i t y @ 25 deg. S l o w l y add sodium c h l o r i d e t o t h i c k e n . A1 p h a . 5 . M i x u n t i l c l e a r .0 5.0 30.

5 General Purpose . 44 .

M i x u n t i l homogeneous. M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous Add t h e low m o l e c u l a r w e i g h t p o l y a c r y l a t e p o l y m e r f o l l o w e d by t h e sodium h y d r o x i d e and sodium s i l i c a t e . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r . U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . (The p r o d u c t w i l l d r o p i n v i s c o s i t y a t t h i s p o i n t . as d e s i r e d . FGoedrich S p e c i a l t y Chemicals: 2.14 30.50 7.80 2. 4. ) Add t h e c a l c i u m c a r b o n a t e and f i n a l l y t h e s u r f a c t a n t w i t h c o n s t a n t a g i t a t i o n .00 1 . Reduce a g i t a t i o n speed and add t h e sodium h y p o c h l o r i t e b l e a c h .960 c p ~ d ~ r ~ 1 .80 2. DET-343 .General Purpose Cleaners 45 Abrasive Cleaner w i t h Bleach Carbopol r e s i n s a r e used t o a c h i e v e a s t a b l e s u s p e n s i o n o f t h e c a l c i u m carbonate a b r a s i v e o a r t i c l e s i n t h e presence o f c h l o r i n e bleach lnqredient : DI[ Water Carbopol 674 o r 691* Good-Rite K-7058 (50%)** Sodi u h y d r o x i d e (50%) m 2 .00 2. 5. 3. Add f r a g r a n c e .76 0.d e c y l d i p h e n y l o x i d e d i s u l f o n a t e (45% *Suspension a i d : BFGoodrich * * A n t i . M i x u n t i l homogeneous.oo **** Physi ea9 P r o p e r t i e s : B r o o k f i e l d RVT v i s c o s i t y Product pH: 12-13 P r o d u c t c l a r i t y : Opaque ~ ~ ~ ~ - 20 rpm: 3. 4 ~ sodium s i l i c a t e (52%) Sodium h y p o c h l o r i t e (14%) C a l c i urn c a r b o n a t e * * * Sodium n .r e d e p o s i t i o n : BFGoodrich + * + A b r a s i v e : W h i t e #8 ( G e o r g i a M a r b l e ) * * * * A n i o n i c s u r f a c t a n t : Dowfax 382 (Dow Chemi Wt% 53.

46 Advanced Cleaning Product Formulations A b r a s i v e Cleaner W i t h o u t B1 each Carbopol r e s i n s a r e used i n t h i s f o r m u l a t i o n t o a c h i e v e a s t a b l e suspension o f t h e h i g h l o a d i n g o f c a l c i u m carbonate abrasives . Insredient: D I Water Ethanol Carbopol 674 ( 1 ) Sodium h y d r o x i d e (50%) Sodium b i c a r b o n a t e Calcium carbonate ( 2 ) C12-15 1in e a r a1 coho1 . 3 moles EO ( 3 ) Coconut d i e t h a n o l ami de ( 4 ) B r o o k f ie l d v i s c o s i t y (RVT-20 P r o d u c t pH: 8-10 P r o d u c t c l a r i t y : Opaque ( 1 ) BFGoodr ich Wt% 62. Add t h e c a l c i u m c a r b o n a t e . Coconut DEA: 30.20 30.500 ( 2 ) G e o r g i a M a r b l e Co.50 0.: G e o r g i a M a r b l e W h i t e # 8 ( 3 ) S h e l l Chemical: Neodol 25-3 ( 4 ) Stepan Co. 3 . Add f r a g r a n c e . Add t h i s t o t h e m i x t u r e formed above and m i x u n t i l homogeneous.: N i n o l 11-CM Procedure: 1 .00 1.5 0. Total Actives: C a l c i u carbonate: m C12-15 l i n e a r a l c o h o l .10 2. 5 .00 0. Add t h e e t h a n o l t o t h e w a t e r .60 1 . U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d by a L i g h t n i n ’ M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . 4 . M i x t h e s l u r r y for a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous.00 2.h o l d i n g back 10 p a r t s o f w a t e r f o r s t e p #3.6 3 moles EO: SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-340 . a l c o h o l e t h o x y l a t e and coconut QEA. as d e s i r e d . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r / e t h a n o l m i x t u r e .60 cps rpm) : 4. P r e p a r e a n e u t r a l i z i n g s o l u t i o n o f t h e 10 p a r t s o f w a t e r w i t h t h e sodium h y d r o x i d e and sodium b i c a r b o n a t e . M i x u n t i l homogeneous. 2 .0 2.

Perfume Dowanol DPnB C a l s o f t L-40 Wei q h t % 4.00 2.00 88.00 15.00 4.00 Ingredients: Na4EDTA Water.00 2.00 8. M i x u n t i l homogeneous.oo 5.00 84. F o r m u l a t i o n APC-002-01 A l l Purpose C l e a n e r Inqredi ent s : d . 3 .General Purpose Cleaners 47 A l l Purpose C l e a n e r Ingredients: Urea Na4EOTA Water 2990 Ammonia C a l s o f t L-40 C a l o x y l a t e N-9 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d . F o r m u l a t i o n APC-001-01 A l l Purpose C l e a n e r Wei q h t % 2.00 42. : Suggested F o r m u l a t i o n s Wei q h t % 40. a t r a d e m a r k o f P r o c t o r & Gamble.00 Weight% 85.00 10. C l e a n .00 1 .00 4. 2 .L i monene Calamide C Calamide C T W Cal imu1 se PRS Water Comments a b o u t t h i s f o r m u l a : 1 . Add w a t e r s l o w l y . F o r m u l a t i o n APC-005-01 A l l Purpose C l e a n e r Inqredi ents: Water Calamide C T W Comments a b o u t t h i s f o r m u l a : Formula t h i c k e n s e f f e c t i v e l y .00 Comments a b o u t t h i s f o r m u l a : Compare t o M r . F o r m u l a t i on APC-003-01 SOURCE: P i l o t Chemical C o .00 4.00 . Add i n g r e d i e n t s f i r s t and m i x .

50 2.50 2. F o r m u l a t i o n APC-008-01 SOURCE: P i l o t Chemical Co.00 5.00 .48 Advanced Cleaning Product Formulations A l l Purpose C l e a n e r Inqredients: Na4EDTA Water Calamide C Calamide C T W P i l o t SXS-40 Laurami ne O x i d e Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d . F o r m u l a t i o n APC-006-01 Wei q h t % 5.00 A l l Purpose C l e a n e r Inqredients: Na4EDTA Water 50% NaOH Cal s o f t LAS-99 P i l o t SXS-40 Calamide C Calamide C T W Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d . F o r m u l a t i o n APC-007-01 Wei q h t % 5. t h e n w i p e w i t h a p a p e r t o w e l .80 2.30 5.00 3.50 2.00 77.00 2.: Suggested F o r m u l a t i o n s Weight% 89.00 3.50 10.00 A l l Purpose C l e a n e r .No R i n s e Inqredients: Water C a l f a x 1OL-45 Na4 EDTA E t h y l e n e G l y c o l Monobutyl E t h e r Calamide C T W Comments a b o u t t h i s f o r m u l a : Spray a s i s .00 76.00 3.10 0.80 5.

7 0.5 3.P u r p o s e C 1 e a n e r Composi t ion : K e l z a n x a n t h a n gum A1 ip a l CD-128 G a f a m i d e CDD 518 B u t y l C e l l o s o l ve S o d i urn M e t a s i 1 ic a t e T r i s o d i urn P h o s p h a t e Water. Perfume 0. SOURCE: M o n s a n t o P e r f o r m a n c e M a t e r i a l s : K e l z a n S u g g e s t e d Formulations A l l Purpose C l e a n e r l n q r e d i en& R h o d a t e r g e SMC STPP Water Wt% 10 2 88 Surfactants & Specialties: Suggested SOURCE: Rhone-Poulenc Formulations .0 1.o 91.7 1.3 Procedure: P r e p a r e w a t e r s o l u t i o n o f K e l z a n x a n t h a n gum b y a d d i n g t h e powder s l o w l y t o t h e s i d e o f t h e v o r t e x w i t h c o n s t a n t a g i t a t i o n .o 82. F o r a e r o s o l u s e .5 Procedure: P r e p a r e w a t e r s o l u t i o n o f K e l z a n x a n t h a n gum b y a d d i n g t h e powder s l o w l y t o t h e s i d e o f t h e v o r t e x w i t h c o n s t a n t a g i t a t i o n .5 1. -ll-Purpose A D i s i n f e c t a n t Cleaner Composi ti= K e l z a n x a n t h a n gum Makon 1 0 Sodium T r i p o l y p h o s p h a t e V e r s e n e 100 Hyarnine 1 O X Water Q 0. Add o t h e r i n g r e d i e n t s as i n d i c a t e d . F o r a e r o s o l u s e . Add o t h e r i n g r e d i e n t s a s i n d i c a t e d .0 3. c h a r g e w i t h a p p r o x i m a t e l y 85 p e r c e n t c o n c e n t r a t i o n and 15 p e r c e n t G e n e t r o n 12.0 3. c h a r g e w i t h a p p r o x i m a t e l y 85 p e r c e n t c o n c e n t r a t i o n a n d 15 p e r c e n t G e n e t r o n 12.3 1.5 10.General Purpose Cleaners 49 A 1 1.

0% pH. 0 2 0 6 Wt.0 2.0 81 e n d i ng P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n .5 W S 90.5 5.I.0 5. 1 2 V i s c o s i t y . 56. c p s : 670 Sol i d s : 33. 50% W i t c o 12988 W i t c a m i de 6 4 4 5 Perfume.50 Advanced Cleaning Product Formulations A l l Purpose C l e a n e r w/Amide/Phosphate Innredi ents: W a t e r .5 2.0 10. l b s . as i s : 9 .0% pH: 8 .0 0. as i s : 9 . : 8 . T y p i c a l P r o p e r t ie s : Speci f ic G r a v i t y : 1 ./Gal. 8 Formula 514 A l l Purpose C l e a n e r Ingredients: Water W i t c o n a t e 1 2 6 0 S1 u r r y Witcamide 6445 Blending Procedure: B1 end i n g r e d i e n t s i n t h e o r d e r 1 is t e d . 5 pH. / G a l . Typical Properties: V i s c o s i t y . .s. Tetrapotassium Pyrophosphate Varami de A-1 0 Emphos 5AP Ester Wt% 83. Dye Blending Procedure: Blend i n g r e d i e n t s i n order l i s t e d . c p s : 145 S o l i d s : 17. : Suggested F o r m u l a t i o n s wto/. c p s : 107 Color: Beige Use D i l u t i o n : 1 .0 2.0 q. Formula 535 SOURCE: W i t c o C o r p . 2 Formula 520 A1 1 Purpose C l e a n e r Ingredients: Water Sodi um T r i p o l y p h o s p h a t e C a u s t i c Soda. Typical Properties: V i s c o s i t y . D.0 5.2 o z .0 38.

5 M o l e s EO) * * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl5. 3 M o l e s EO) Use D i 1u t i o n : 1 .00 2.1 .a s s u p p l i e d Wt% 78.G r e a s e and o i 1 Surface-Paint.3 . 6 .25 5. 5 % b w ( 3 . 40% *Ethylene Glycol n-Butyl Ether Pine O i l * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl3.4 3. : D e t e r g e n t F o r m u l a t i o n Guide . U n i o n C a r b i d e Rhone-Poul enc R h o d a s u r f LA-7 Rhone-Poulenc R h o d a s u r f A-24 SOURCE: PQ C o r p .0 3.General Purpose Cleaners 51 A l l Purpose C l e a n e r C o n c e n t r e (Phosphate. Liquid1 S o i 1 .50 6. polymeric.2 . 3 o z / g a l 1on) Tough D u t y .75 1 . 9-10 M o l e s E O ****Octylphenoxy P o l y e t h o x y e t h a n o l . . metal A p p l i c a t i o n Method-Wipe o r b r u s h Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Water M e t s o Beads 2048 TKPP Sodium X y l e n e S u l f o n a t e .G r e a s e and o i 1 Surface-Paint.0 2.0 6.5 * **( *** **** Rhone-Poulenc R h o d a f a c RE-610 Dow. 78.oo 3. Foam) S o i 1 .00 0.4 o z / g a l l o n ) wto/.L i q u i d . 0 % bw ( 2 . polymeric.0 5. metal A p p l i c a t i o n Method-Spray Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i n o : Water M e t s o Beads 2048 TKPP ( 6 0 % ) *Phosphate E s t e r * * D i p r o p y l e n e G l y c o l Monomethyl E t h e r * * * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l . 5 .00 3.1 2. A r c 0 C h e m i c a l Rhone-Poulenc I g e p a l CA-630 Rhone-Poulenc I g e p a l CA-520 A l l Purpose C o n c e n t r a t e (Phosphate. 5 M o l e s EO Use D i l u t i o n : Normal D u t y . 5 % bw ( 2 o z / g a l l o n ) Heavy D u t y .50 * *l *S* Dow C h e m i c a l .

d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r . The p r o d u c t w i l l become v e r y t h i c k a t t h i s p o i n t .: Neodol 25-3 ( 3 ) Stepan Co. M i x u n t i l homogeneous. 4 . Add t h e sodium h y d r o x i d e t o r e a c h t a r g e t pli.500 c p Raw M a t e r i a l S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) S h e l l Chemical Co. : Georgia Marble White #8 Procedure: 1 . Add t h e c a l c i u m c a r b o n a t e . 3 moles EO ( 2 ) Sodium a l k y l benzene s u l f o n a t e ( 3 ) Calcium carbonate ( 4 ) P h y s i c a l P r o p e r t ies : B r o o k f i e l d V i s c o s i t y (RVT-20 P r o d u c t pH: 8-10 P r o d u c t C l a r i t y : Opaque rpm): 62. 3 moles EO: 1. U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i ng and b l endi ng o p e r a t i o n s . I n q r e d ie n t : D I Water Carbopol ETD 2623 ( 1 ) Sodium h y d r o x i d e (50%) C12-I5 l i n e a r a l c o h o l . Add t h e a l c o h o l e t h o x y l a t e and a l k y l b e n z e n e s u l f o n a t e s u r f a c t a n t s .25 0. : Nacconol SQG ( 4 ) Georgia Marble C o . Add f r a g r a n c e .00 C12-15 l i n e a r a l c o h o l .20 1. M i x u n t i l homogeneous. 2.52 Advanced Cleaning Product Formulations Calcium Carbonate A b r a s i v e Cleaner W i t h o u t Bleach Carbopol r e s i n s a r e used i n t h i s f o r m u l a t i o n t o a c h i e v e a s t a b l e suspension o f t h e h i g h l o a d i n g o f c a l c i u m c a r b o n a t e abrasives .50 0.50 30.00 7. 3 .50 Sodium a1 k y l b e n z e n e s u l f o n a t e : 0. Total Actives: Calcium carbonate: 30. M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s or u n t i l t h e s l u r r y i s homogeneous. as d e s i r e d .50 SOURCE: BFGoodrich S p e c i a l t y Chemicals: BET-341 .10 0. 5.

2 0 rpm: Initial: Age-Up V i s c o s i t y : Week 2 : Week 4 : Week 6: P r o d u c t pH: 1 . a s d e s i r e d . S ~ O W add t h e C i t r i c A c i d w i t h s l o w m i x i n g (200 r p m ) .10 5.00 2. 3 moles EO** C12-13 l i n e a r a l c o h o l . S O U R C E : B F G o o d r i c k S p e c i a l t y ChemicaJs: DET-352 .t o .00 12. Add t h e B i o s o f t S-100 w i t h moderate (300 rpm) m i x i n g and a l l o w t o m i x u n t i l u n i f o r m and smooth. 5oc 50cP 400cP 600cP 400cP 50cP 170cP 250cP 350cP Procedurw: 4. 5 ( o r warm s l i g h t l y i f needed) t o e n s u r e homogeneity. A d d w i t h moderate m i x i n g (300 r p m ) . s p r i n k l e t h e Carbopol ETD 2623 r e s i n i n t o t h e v o r t e x .50 2.6 . 4 Product c l a r i t y : T r a n s l u c e n t S t o r a g e Temperature 25C . 4. 5. Add f r a g r a n c e and c o l o r .d i s p e r s e r e s i n f o r improved and e a s i e r f u l l . M i x ~ Y u n t i l smooth and u n i f o r m . 2. A l l o w t o h y d r a t e f o r 15-20 m i n u t e s o r u n t i l no lumps a r e p r e s e n t . U s i n g J m a r i n e b l a d e p r o p e l l e r and r a p i d a g i t a t i o n (800 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t . M i x t h e Neodol 25-3 and Neodol 2 3 .s c a l e processing Inqiredi e n t : Wt% 78.5: * * r * A n i o n i c s u r f a c t a n t : B i o s o f t 5-100: Stepan P h y s i c a l P r o p e r t iee: B r o o k f i e l d RVT v i s c o s i t y . A l l o w t o mix u n t i l u n i f o r m and smooth. 5 moles EO*** Alkylbenzene s u l f o n i c acid**** C i t r i c A c i d (50%) *V iscos ity modi f ie r : BFGoodr ic h s W o n i o n i c s u r f a c t a n t : Neodol 25-3: She1 1 Chemical S h e l l Chemical >N**Nonionic s u r f a c t a n t : Neodol 23-6.40 0.General Purpose Cleaners 53 C i t r i c A c i d Cleaner F u n c t i a n e 8 B e n e f i t s : Carbopol ETD 2623: * P r o v i d e s l o w p H t h i c k e n i n g v i a hydrogen b o n d i n g w i t h s u r f actant * I m p a r t s y i e l d v a l u e f o r suspension o f a b r a s i v e p a r t i c l e s *Provides v e r t i c a l c l i n g f o r increased s u r f a c e c o n t a c t t i m e *Shear t h i n n i n g r h e o l o g y f o r easy d i s p e n s i n g t h r o u g h t r i g g e r sprayer o r nozzle * E a s y . 6 . 3. Warming t h e d e i o n i z e d w a t e r t o 30C w i l l decrease t h e h y d r a t i o n t i m e and i m p r o v e t h e d i s p e r s i b i l i t y o f t h e Carbopol powder.00 DI Water Carbopo? ETD 2623 R e s i n * C12-15 l i n e a r a l c o h o l .

: D e t e r g e n t F o r m u l a t i o n Guide . Non-Phasphate Powder) S o i l . . c l a y and p a r t i c u l a t e s o i l Surface-Hard surface.54 Advanced Cleaning Product Formulations G e n e r a l P u r p o s e C1 e a n e r (Consumer Low Alkaline. metal. concrete. 9 M o l e s EO) V a l f o r 100 Z e o l i t e A * * * A c u s o l 445ND Sodium P o l y a c r y l a t e (92% S o l i d s ) Sodi um S u l f a t e Use L e v e l : 1-4 o z / g a l l o n 82. p e t r o l e u m o i l and g r e a s e .0 0.5 14. e .C l 5 .0 30.0 15.5 30. Non-Phosphated Powder1 S o i -Food ( f a t and p r o t e i n ) .5% s o l i d s Wt% 30.5 ** * *** 2 .0 0. i . Rhone-Poulenc R h o d a s u r f LA-9 Rohm & Haas G e n e r a l Purpose C l e a n e r (Consumer H i g h A 1 k a l ine.0 15. c e r a m i c . p l a s t i c . 9 M o l e s EO) V a l f o r 100 Z e o l i t e A M e t s o Beads 2048 * * A c u s o l 445ND Sodium P o l y a c r y l a t e (92% S o l i d s ) Use L e v e l : 1-4 o z / g a l l o n R h o d a s u r f LA-9 14. c l a y and p a r t i c u l a t e s o i l Sur ace-Hard s u r f a c e .F o o d ( f a t and p r o t e i n ) . and a s p h a l t A p p l i c a t i on Method-Wi p e o r B r u s h Manufacture-Dry blend/Agglomeration Composi t i o n : Sodi um C a r b o n a t e ( 1 i g h t d e n s i t y ) * B r i t e s i 1 C20 Hydrous P o l y s i 1 i c a t e * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl5.5 Wt% ** * Rhone-Poulenc Rohm & Haas SOURCE: PQ Corp. . ceramic.0 10. p l a s t i c . p e t r o l e u m o i l and g r e a s e . c o n c r e t e . i . 0 w e i g h t r a t i o s i l i c a t e powder. m e t a l . and a s p h a l t App i c a t i o n Method-Wipe o r b r u s h Manufacture-Dry blend/Agglomeration Composi t i o n 1 Sodium S u l f a t e Sodi um C a r b o n a t e ( 1 ig h t d e n s i t y ) * L i q u i d N o n i o n i c S u r f a c t a n t ( C 1 2 .0 10.0 30. e .

a n h y d r o u s P r o p y l ene g l y c o l m e t h y l e t h e r ( 2 ) C12-15 l i n e a r a l c o h o l . Add c o l o r and f r a g r a n c e . 2 .70 0. 4 . a s d e s i r e d . Under s l i g h t a g i t a t i o n . 7 m o l e s EO: wto/. T h i s "no-drip" action w i l l increase the contact time o f t h e detergent on t h e s o i l e d s u r f a c e a s w e l l a s enhance consumer c o n v e n i e n c e . 7 m o l e s EO ( 3 ) B r o o k f i e l d v i s c o s i t y (RVT-20 rpm) : 120 c p s P r o d u c t p H : 12-13 P r o d u c t C l a r i t y : C l e a r t o hazy ( 1 ) BFGoodri c h ( 2 ) Dow C h e m i c a l : Dowanol DPM ( 3 ) S h e l l C h e m i c a l : Neodol 25-7 Procedure: 1 .50 3. 90.General Purpose Cleaners 55 G e n e r a l P u r p o s e S p r a y & Wipe C l e a n e r Carbopol r e s i n s a r e used t o i n c r e a s e t h e y i e l d v a l u e r e s u l t i n g i n v e r t i c a l c l i n g when s p r a y e d on a v e r t i c a l s u r f a c e .5 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-310 . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s or u n t i l t h e s l u r r y i s homogeneous. add t h e EDTA and M e t a s i l i c a t e .20 2.00 2.0 1. 3 . Ingredient: D I Water C a r b o p o l ETD 2 6 9 1 ( 1 ) EDTA ( t e t r a s o d i u m s a l t ) Sodium m e t a s i l i c a t e .30 3. U s i n g m o d e r a t e a g i t a t i o n ( 8 0 0 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . d i s p e r s e o r screen t h e Carbopol r e s i n i n t o t h e D I w a t e r . C o n t i n u e a g i t a t i o n and add t h e g l y c o l e t h e r and a l c o h o l e t h o x y 1a t e .00 1. T o t a l Actives: Propylene g l y c o l methyl e t h e r : C 1 2 .I 5 l i n e a r a l c o h o l .

0 7. 4 V i s c o s i t y I 2 5 deg. C : V e r y t h i n 3 S o l i d s . 575 Ingredients: Water Z e t e s o l 2056 Z u s o l a t 1008/85 82. %: 1 0 . 1 d a y : p a s s F r e e z e / t h a w .: Suggested F o r m u l a t i o n A1 1 -Purpose C1 e a n e r No. l b s / g a l : 8. : . as i s : 9 . Add sodium c i t r a t e and m i x u n t i 1 homogeneous.82%' s o i l removed f r o m t i l e s Above f o r m u l a t i o n p e r f o r m s b e t t e r t h a n c o m m e r c i a l product. 0 Density.66% s o i l removed f r o m t i l e s Above f o r m u l a t i o n . D.0 4.0 2. SOURCE: Stepan Co.0 F o r m u l a t i o n CT 02-04-02 SOURCE: Zschimmer & Schwarz GmbH & C o .0 M i x i n g Procedure: Charge w a t e r and s u r f a c t a n t s and m i x .S t e p MC-48 S t e p a n o l WA-Extra N i n o l 11-CM Wt% 79. Use I n s t r u c t i o n s : Use as i s Comment : The s u r f a c t a n t s used i n t h i s f o r m u l a t i o n a r e d e r i v e d f r o m o l e o c h e m i c a l r e s o u r c e s and a r e b i o d e g r a d a b l e .0 14.I. C.0 2. T y p i c a l P r o p e r t i es : Appearance: C l e a r c o l o r l e s s l i q u i d pH.54 C o l d s t o r a g e @ 4 d e g .0 10. 3 c y c l e s : pass Performance: Gardner S t r a i g h t L i n e W a s h a b i l i t y T e s t : Commercial P r o d u c t . Sodi um C i t r a t e A1 p h a .56 Advanced Cleaning Product Formulations G e n e r a l P u r p o s e Spray & Wipe Ingredients: Water.

2 5 % ) Procedure: Add i n g r e d i e n t s w t h a g i t a t i o n .General Purpose Cleaners 57 H y p o c h l o r it e V e r t i c a l S u r f a c e C l e a n e r M o n a t r o p e 1250 i s a h y p o c h l o r i t e s t a b l e s u r f a c t a n t t h a t c o n t r i b u t e s t o w e t t i n g and f o a m i n g c h a r a c t e r i s t i c s .0 15. streak-f ree. Inqredients: Water M o n a t e r g e 779 (DEA-Laureth S u l f a t e ) Propylene Glycol B u t y l Ether Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n .0 5.0 66. In q r e d ie n t s : M o n a t r o p e 1250 Sodium C14-17 A l k y l Sec S u l f o n a t e (60%) Laurami ne O x i d e (30%) P o t a s s i u m H y d r o x i d e (45%) Sodi um T r i p o l y p h o s p h t e Sodium H y p o c h l o r i t e 5 .0 Typical Properties: Appearance: C l e a r y e l l o w l i q u i d p H : 13 Recommended Use D i l u t i o n : Formul a t i on F-783 1:lO w i t h w a t e r Pump S p r a v A l l Purpose C l e a n e r Surfaces w i l l dry A f a s t a c t i o n s p r a y and w i p e f o r m u l a t i o n . Typical Properties: Appearance: C l e a r l i q u i d Recommended Use D i 1 u t i o n : As i s SOURCE: Mona I n d u s t r i e s .0 Package. Wt% 94. : Suggested F o r m u l a t i o n s .0 3.0 3.0 2. Wt% 2.0 10. I n c .

m i x i n g w e l l a f t e r each a d d i t i o n .0.4. SOURCE: Hoechst A k t i e n g e s e l l s c h a f t : Suggested F o r m u l a t i o n . 5 . Ingredients: A : H o s t a p u r SAS 6 0 Genapol ZRO 1 iq u i d Genapol UD-080 B : Water liquid Wt% 10.: F o r m u l a t i o n N o . 29% s o l n . 0 Perfume Preservative Dye Manufacturing: Add one a f t e r a n o t h e r .25 62. 2 5 % s o l n .. Sodium L a u r y l S u l f a t e . Modern s t a n d a r d f o r m u l a t i o n s a r e based on a l k a n s u l p h o n a t e s and noni oni c s E t h e r s u l p h a t e s a r e used i n r a r e cases. Ingredients: A : Van Gel B Water 2. Inc. V a n d e r b i l t Co. Procedure: S l o w l y add Van Gel B t o t h e w a t e r w h i l e a g i t a t i n g a t maximum a v a i l a b l e s h e a r . n e c e s s a r y f o r t h e s t a b i l i t y o f t h e h y p o c h l o r i t e . SOURCE: R .50 20. 0 0.25 '10.58 Advanced Cleaning Product Formulations L i q u i d C 1 eanser w i t R B1 each I n t h i s f o r m u l a Van Gel B i s used t o suspend t h e a b r a s i v e and t o a d j u s t t h e v i s c o s i t y . The sodium c a r b o n a t e b u f f e r h e l p s m a i n t a i n a pH o f a b o u t 1 1 . T h i s l i q u i d c l e a n s e r o f f e r s t h e advantage o f m i l d ness i n u s e and g r e a t e r ease and e f f e c t i v e n e s s on v e r t i c a l s u r f a c e s a s compared t o powders. t h e components o f B t o A . 391 A l l Purpose C l e a n e r Clear.0-15.0 0.00 1 . Phosphates. Add r e m a i n i n g i n g r e d i e n t s i n o r d e r . sodium c a r b o n a t e and ammonia a r e n o t common any 1onger The above g u i d e f o r m u l a t i o n c o v e r s t h e common european p r o d u c t s . . C o n t i n u e m i x i n g u n t i l smooth.1 q.0. T . Consistency: Medium v i s c o s i t y liquid.oo 6 : Diatomaceous E a r t h Sodium c a r b o n a t e Sodium h y p o c h l o r i t e . .2 0.3 .0 1. ad 1 0 0 . Suggested Packaging: P l a s t i c squeeze b o t t l e .s.00 4.

5 M i x i ng Procedure: Combine p i n e o i l . CT 06-09-03 . D .: CT 06-09-02.0 7.General Purpose Cleaners 59 Pine O i l Cleaner Concentrate Ingredients: Pine o i l N i n o l 11-CM Makon 12 Ammonyx LO B i o .0 9. s u r f a c t a n t s and I P A . g 20.0 5.5 7.5 1. 5 % s o i l removed f r o m t i l e s SOURCE: S t e p a n Co. Properties: Appearance: C l e a r y e l l o w l i q u i d Odor: P i n e V i s c o s i t y @ 25C.0 53.5 g 57. c p s : 50 pH ( a s i s ) : 8 . 1 D e n s i t y 1b s / g a l : 8 .5 2.0 5.: F o r m u l a t i o n No.0 Wt% 69. SOURCE: Zschimmer & Schwarz GmbH & Co.0 3.0 3. 208 D i s i n f e c t i n g Cleaner. I . Add water s l o w l y w h i l e under a g i t a t i o n . M i x u n t i l c l e a r .0 10.5 2.0 2. Mix u n t i l c l e a r . 0 6 Freeze/Thaw ( 3 c y c l e s ) : Pass 50 C oven ( 1 week): Pass Use I n s t r u c t i o n s : D i l u t e 1-2 o z s i n t o one g a l l o n Performance: Gardner S t r a i g h t L i n e W a s h a b i l i t y T e s t : Above f o r m u l a t i o n : 73.5 5.0 9.5 25.0 F o r m u l a t i o n s CT 06-09-01.0 0. Ingredients: Water C i t r i c acid Z u s o l a t 1008/85 Lumorol 4192 Trilon A liquid Lonzabac-1230 Ingredients: Water Disodium t e t r a b o r a t e decahydrate Sodi um b i c a r b o n a t e Burdac-114 Z u s o l a t '1008/85 Ingredients: Water Trilon A liquid Citric acid S u l f e t a l 4069 Z u s o l a t 1008/85 Lonrabac-1230 Alkaline Wt% 57.0 20.S o f t S-1 0 0 Isopropanol Water.0 25.0 0.0% s o i l removed f r o m t i l e s Commercial f o r m u l a t i o n : 5 5 .

-g r e d i e n t : In D I Water C a r b o p o l ETD 2691 ( 1 ) A l k y l benzene s u l f o n i c a c i d ( 2 ) C12-13 l i n e a r a l c o h o l . a s d e s i r e d .000 c p Raw M a t e r i a l S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) Stepan Co.25 0. 6 .6 .90 DET-342 . 5 . : Neodol 2 3 . and f r e e o f b i c a r b o n a t e l u m p s .00 Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 rprn): Product pH: 8. Re-check p H and a d j u s t . homogeneous. 5 m o l e s EO: Sodium a1 k y l benzene s u l f o n a t e : SOURCE: B F G o o d r i c h S p e c i a l t y C h e m i c a l s : 50. i f n e c e s s a r y . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 1 5 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. A d j u s t pH t o 8. 6 .50 P r o d u c t C l a r i t y : Opaque 6. 5 m o l e s € 0 ( 3 ) Sodium h y d r o x i d e ( 5 0 % ) Sodium b i c a r b o n a t e ( 4 ) : Grade 1 : Grade 5 : wtsl. 3 . Add c o l o r a n d f r a g r a n c e . 2 . Add t h e s o d i u m h y d r o x i d e . s l o w l y add t h e s o d i u m b i c a r b o n a t e . Add t h e a l k y l b e n z e n e s u l f o n i c a c i d f o l l o w e d b y t h e a l c o h o l e t h o x y l a t e .00 2. 5 ( 4 ) Church & Dwight Procedure: 1 .75 2. W i t h m i n i m a l a g i t a t i o n . M i x u n t i l smooth.60 Advanced Cleaning Product Formulatiorrs Sodi urn B i c a r b o n a t e A b r a s i v e C l e a n e r W i t h o u t B l e a c h Carbopol r e s i n s a r e used i n t h i s f o r m u l a t i o n t o a c h i e v e a s t a b l e s u s p e n s i o n o f t h e h i g h l o a d i n g o r sodium b i c a r b o n a t e abrasives.: B i o s o f t 5-100 ( 3 ) S h e l l C h e m i c a l C o . 44. d i s p e r s e o r screen t h e Carbopol r e s i n i n t o t h e D I w a t e r .50 p r i o r t o t h e next step. M i x u n t i l homogeneous.50 2.50 0. U s i n g moderate a g i t a t i o n ( 8 0 0 r p m ) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s .00 30. M i x u n t i l homogeneous.50 0.00 20. 4 . T o t a l A c t iv e s : S o d i um b i c a r b o n a t e : C12-13 l i n e a r a l c o h o l .

leaners/Polishes 61 .

wipe onto t h e glass.0 9.0 q. ) and Product I n f o r m a t i o n : Product: Benefit : Varox 365 W e t t i n g a g e n t .s. d e g r e a s e r and d e t e r g e n t Adogen 66 A n t i . e t c . F o r m u l a 708 Glass Cleaner.5 0.0 5.1 10.s t a t i c agent Emcol 4500 W e t t i n g a g e n t . c o u p l e r and d e t e r g e n t T h i s f o r m u l a t i o n p r e s e n t s a t h i n b a r r i e r between t h e w a t e r v a p o r ( f o g . D . G e n t l y h e a t i n g can b e used t o f a c i l i t a t e m i x i n g o f t h e Emcol 4500.4 Blending Instructions: Combine i n g r e d i e n t s i n t h e o r d e r shown and m i x t h o r o u g h l y . a d d i t i o n a l I s o p r o p y l Alcohol can be used t o c l a r i f y t h e s o l u t i o n . steam. F o r m u l a 705 SOURCE: W i t c o C o r p . Use I n s t r u c t i o n s : A p p l y f i n i s h e d p r o d u c t t o a t o w e l l e t e (Kimwipe. The a b i l i t y t o l o w e r t h e s u r f a c e t e n s i o n o f t h e w a t e r prevents t h e c l i n g i n g o f i n d i v i d u a l water d r o p l e t s t o the glass. t h e r e f o r e l i g h t i s n o t s c a t t e r e d as much a s i t i s when p a s s i n g through i n d i v i d u a l d r o p l e t s .I 0. ) and t h e g l a s s w h i c h w i l l p r e v e n t f o g g i n g . I . I f p r o d u c t i s hazy. A n t i -Stat ic G l a s s C l eaner I gredients : n Water Isopropyl Alcohol Adogen 66 Varox 365 Emcol 4500 MIBo/o 90. Ingredients: Water. B l e n d i ng P r o c e d u r e : B l e n d i n g r e d i e n t s i n t h e o r d e r 1is t e d . A l l o w t o d r y . : Suggested F o r m u l a t i o n s .0 0. P e t r o BAF L i q u i d Isopropanol E t h y l e n e G l y c o l Monobutyl E t h e r Dye Ready t o Use 84.62 Advanced Cleaning Product Formulations A n t i -Foggi ng . e t c .9 0.

Wt% 77. F o r m u l a 702 Glass Cleaner Concentrate Inqredi ents: Water.0 1. : Suggested F o r m u l a t i o n s .5 82. P e t r o BAF L i q u i d DeSonic 5 N Ammonia.s. I.0 2. D . T h i s p r o d u c t r e q u i r e s a red label.0 3. Wt% 94. D . 29% Dye B l e n d i n g Procedure: Use D i l u t i o n : F o r m u l a 703 Blend i n g r e d i e n t s i n t h e order l i s t e d .5 q.o 2. 1 p a r t c o n c e n t r a t e t o 50 p a r t s w a t e r . 99% P e t r o LBA Powder Monoethanol ami ne Perfume.0 q. K % 7. Dye B l e n d i n g Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d .0 SOURCE: W i t c o C o r p . 26 B e ' B l e n d i n g Procedure: F o r m u l a 704 Blend i n g r e d i e n t s i n t h e order l i s t e d .0 20.o 0. Amrnoniated G l a s s C l e a n e r m r e d ients: Water W i t c o l a t e 231 0 B u t y l C e l l o s o l ve Aqua Ammonia.0 2.0 1. I .Glass CleanerslPolishes 63 G l a s s C l e a n e r C o n c e n t r a t e (Non-Ammoniated) Ingredients: W a t e r . s T h i s c o n c e n t r a t e s h o u l d be m i x e d w i t h n i n e p a r t s o f w a t e r t o one p a r t c l e a n e r t o b e r e a d y t o u s e . I s o p r o p a n o l .

00 Isopropanol: 5. Inaredient: D I Water Carbopol ETD 2623 Isopropanol Ammonium h y d r o x i d e A l k y l b e n z e n e s u l f o n i c a c i d (97%) ( 2 ) Propylene g l y c o l methyl e t h e r (3) Physical Properties: B r o o k f ie l d V i s c o s i t y (RVT-20 rpm) : 200 c p P r o d u c t pH: 9 . 3 . 3 0 Propylene g l y c o l methyl e t h e r : 2. U s i n g moderate a g i t a t i o n ( 8 0 0 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . T h j s "no-drip" a c t i o n w i l l increase the contact time o f t h e detergent on t h e s o i l e d s u r f a c e as w e l l as enhance consumer c o n v e n i e n c e . as d e s i r e d . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r . M i x u n t i l homogeneous. t o r e a c h the t a r g e t pH r a n g e .25 2. i f necessary. Add t h e ammonium h y d r o x i d e . Add t h e s u l f o n i c a c i d and g l y c o l e t h e r w i t h m i n i m a l a g i t a t i o n t o a v o i d e x c e s s i v e foaming.20 0.00 0. 0 Product C l a r i t y : Clear Raw M a t e r i a1 Suppl ie r s : ( 1 ) BFGoodrich ( 2 ) Stepan Chemical: B i o s o f t 5-100 ( 3 ) Dow Chemical: Dowanol PM Procedure: 1 .00 .10 5. Add a d d i t i o n a l ammonium h y d r o x i d e . Add t h e i s o p r o p a n o l .00 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-300 wel 92 * 45 (4.1 0 . 5 . 6 . 5 . Add c o l o r and f r a g r a n c e . 2 . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. Total Actives: Ammonium a l k y l b e n z e n e s u l f o n a t e : 0 .64 Advanced Cleaning Product Formulations G l a s s and Window C l e a n e r Carbopol r e s i n s a r e used t o i n c r e a s e t h e y i e l d v a l u e r e s u l t i n g i n v e r t i c a l c l i n g when s p r a y e d on a v e r t i c a l s u r f a c e . 4 .

F o r m u l a 709 SQURCE: W i t c o G o r p .85 81 endi ng P r o c e d u r e : B l e n d i n g r e d i e n t s i n t h e o r d e r shown. ween each a d d i t i o n . cps: 4 S o l i d s : 0. cps: 4 S o l i d s : 0.0 4. 6. Isopropanol Varox 1770 Methylene Blue Q 89. s 81 e n d i ng P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n . Isopropanol Dowanol EB R e w o t e r i c AM V Wt% q.23% pH: 6 .Glass CleanerslPolishes 65 H o u s e h o l d Window C l e a n e r Inqredients: Water.0 0. T y p i c a l P r o p e r t ies: V i s c o s i t y .3 10. 2 F o r m u l a 707 GI ass @1e a n e r Ingredients: Water.0 0.s. Typical Properties : V i s c o s i t y . D . I . D . D . Isopropanol Varox 365 Methylene Blue Wt% 89.4 10.s.0 0. 4 F o r m u l a 706 Bremi u m Household W i ndow C1 e a n e r Ingredi ents: Water.2% pH: 7 .7 q.6 q. : mixing thoroughly bet- Suggested F o r m u l a t i o n s . Blending Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n . I . I .

o f t h e c o n c e n t r a t e p e r g a l l o n .34 53.66 47. e 62.30 2.80 4.20 33.66 Advanced Cleaning Product Formulations W i n d o w s / G l ass Gl-ass Cl g a n g r C C o n c e n t r a t e ) Ingredients: Water Ethylene G l y c o l Monobutyl Ether Isopropyl Alcohol Ammonia.02 .10 W i ndshjeld-pWashec C o n c e n t y a t e (Low VOC) I r e d i-en t s : ng Water P r o p y l ene G1 y c o l Calsuds 81 Comments a b o u t t h i s f o r m u l a Use l e v e l : 2-4 o z p e r g a l l o n . : Suggested F o r m u l a t i o n s W i gh ts/. F o r m u l a t i o n WIN-003-01 SOURCE: P i l o t C h e m i c a l C o .04 21. F o r m u l a t i o n WIN-002-01 Weigh_% 47.00 W i n-dzhield Washer C c n c e n t r a t e Ingredients: Water Isopropyl Alcohol C a l s u d s 81 Comments a b o u t t h i s f o r m u l a : Use 4 0 2 . 4 % C a l foam SLS-30 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d F o r m u l a t i o n WIN-001-01 We i s h t YO 10.35 5. 2 9 .30 5.

ard Surface Cleaners 67 .

Typical Properties: V i s c o s i t y . l b s : 9. addition.0 8. a s i s : 7 .o 4.085 Wt.0 40. : Suggested F o r m u l a t i o n s . / g a l .8% Appearance: C 1 e a r L i q u i d Use D i l u t i o n : 1-3 o z .04 pH.0 3. c p s : 205 S o l ids : 3 4 . 4 % pH: 1 2 . T e t r a s p o t a s s i u m P y r o p h o s p h a t e . 5 F o r m u l a 516 Hard Surface CleaEer Concentrate ( A l l Ingredients: Water. I . Anhydrous W i t c a m i de 1 PET Emphos 5AP W i t c o 1298S A Blending Procedure: Blend i n g r e d i e n t s i n order l i s t e d ./Gal. I . F o r m u l a 540 P u r p o s e Type) \Ne% 82.0 12.68 Advanced Cleaning Product Formulations A l k a l i n e Hard Surface Cleaner I gredient s : n Water.0 81 e n d i n g P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t io n . D . D .0 m i x i n g w e l l a f t e r each SOURCE: W i t c o C o r p .0 10.0 8.0 1. Sodi um M e t a s i 1 ic a t e Varami de A-83 W i t c o n a t e 30DS W i t c o n a t e SXS L i q u i d 34. 5 7 V i s c o s i t y . Typical Properties: S p e c i f i c G r a v i t y : 1. c p s : 94 3 Freeze/Thaw c y c l e s : Passed 1 Week @ 52C: Passed 4 Weeks Room Temp: Passed S o l i d s : 17.

29% 3.00 C a l s u d s 81 5.00 10.30 9. F o r m u l a t i o n HSC-008-01 Wei q h t % 25. It becomes c l e a r w i t h t h e a d d i t i o n o f C a l s u d s 8 1 .50 Na4EDTA Ethylene G l y c o l Monobutyl E t h e r 5.00 Ingredients: Pine O i l C a l s u d s CD-6 C a l o x y l a t e N-9 IPA Water Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 8.50 Ammonia.00 10. F o r m u l a t i o n HSC-004-01 -i n e P Weight% 20.00 41 .00 9.00 Comments a b o u t t h i s f o r m u l a : 1 .00 5.00 0. A f t e r a d d i t i o n o f E t h y l e n e G l y c o l Monobutyl E t h e r . Use 1-2 o z p e r g a l l o n . F o r m u l a t i o n HSC-009-01 Hard Surface Cleaner-Spray Inqredi ents: Wei q h t % Water 86.30 0.40 P i n e Cleaner Inqredi ents : Pine O i l I PA Calamide C T W Cal o x y l a t e N-9 C a l s o f t LAS-99 Water Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d . 2 . Use a t 1-2 o z p e r g a l l o n . t h e mixture i s cloudy.00 9.Hand Surface Cleaners 69 Concentrated Hard Surface Cleaner Ingredients: D e o d o r i z e d Kerosene Calamide C T W C a l o x y l a t e N-9 E t h y l e n e G l y c o l Monobutyl E t h e r Water N a4 E DTA Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 16. : Suggested F o r m u l a t i o n s .00 10.00 Cleaner Weight% 15.00 54.00 2. F o r m u l a t i o n HSC-007-01 ~~~~~~~ P i l o t Chemical Co.00 57.

79.00 3.00 2. Use 2-4 o z p e r g a l l o n .4 o z p e r g a l l o n .50 0.DO .30 5.00 1O.00 7.00 6.00 3.50 15.50 5.00 2.00 5.00 5.20 2.25 Ingredi ents : Water Sodi um M e t a s i 1 i c a t e Na4EDTA P i l o t SXS-40 Cal imu1 se PRS Dowanol PnB Cal o x y l a t e N-9 Comments s b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .50 2.50 Ingredisnts : Water Sodi um M e t a s i 1 i c a t e Na4EDTA P i l o t SXS-40 Calamide C T W Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .50 8. : Suggested F o r m u l a t i o n s W i_ph % e t 58.00 9.00 5. F o r m u l a t i o n HSC-005-01 Weisht_"L. Use 1 . F o r m u l a t i o n HSC-002-01 H a r d S u r f a c e Cle&ne_r Wi q h t 9 6 74. F o r m u l a t i o n HSC-006-01 SOURCE: P i l o t Chemical C o . 29% P i l o t SXS-40 Calamide CWT Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 8.!-33Cs~_ec1 eaner Irns r e d i en t-s 1 Water Sodi um C i t r a t e Soda Ash Ammonia.25 2.00 6.00 Hardsu.70 Advanced Cleatiing Product Formulations H a r d S u r f a c e Cleanerc Ingredients: Water Sodi um M e t a s i 1 i c a t e Na4EDTA Dowanol PnB P i l o t SXS-40 C a l o x y l a t e N-9 P i n e 01 1 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d F o r m u l a t i o n HSC-001-01 Hard-Surface-C1 @anex weight% 75.

P o t a s s i u m H y d r o x i d e (87%) 10.0 Combine Phase B1 e n d i ng P r o c e d u r e : Combine Phase Phase 11.0 12.8 F o r m u l a 507 H a r d S u r f a c e C l e a n e r C o n c e n t r a t e w/d'Limonene Ingredients: Phase I: Isopropanol Oleic A c i d . cps: 75 S o l i d s : 13.0 8. T y p i c a l P r o p e r t i es : V i s c o s i t y . add Phase I t o SOURCE: W i t c o C o r p .Hand Sqface Cleaners 71 Hard Surface Cleaner w/Amphoteric Inqredi ents: Water.0 2. D . I .2 2.Varoni c K205 d ' L i monene Phase 11: Water.0 4. T y p i c a l P r o p e r t i es : V i s c o s i t y .0 10. cps: 4 S o l i d s : 10. D .0 4. Sodi um C a r b o n a t e R e w o t e r i c AM KSF-40 Dowanol DPM Versene 100 W i t c o n a t e SXS (40%) Wt% 75.2% pH: 10. 2 F o r m u l a 508 I i n g r e d i e n t s and m i x t h o r o u g h l y . I 1 i n g r e d i e n t s and m i x t h o r o u g h l y .0 Blending Procedure: Add i n g r e d i e n t s in o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n .0 62.0 5.8% pH: 1 0 . : Suggested F o r m u l a t i o n s . W h i l e m i x i n g .8 5. I .

o i l and p r o t e i n . 6 Moles EO) * * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-C11. g l a s s A p p l i c a t i o n Method-Spray and w i p e Manufacture-Mix tank w i t h p r o p e l l e r s t i r r e r Composi t i on : Water TKPP N C l e a r Sodium S i l i c a t e Sodium H y d r o x i d e (50%) * D i p r o p y l ene G1 y c o l Monomethyl E t h e r * * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l .4 1. L i q u i d ) S o i l .6 18.00 2. 6 M o l e s EO) * * * L i q u i d N o n i o n i c S u r f a c t a n t ( C 9 . o i l and p r o t e i n .0 5.12 5.88 0.00 ** * Dow Chemical Rhone-Poulenc SOURCE: PQ C o r p .2 Wt% 65. L i q u i d ) S o i l .C l l . p e t r o l e u m g r e a s e and o i l Surface-Metal.72 Advanced Cleaning Product Formulations Hard Surface Cleaner Concentrate IPhosphate. polymeric.00 1.M i x t a n k w i t h p r o p e l 1e r s t i r r e r ComDosition A: Water TSP S t a r s o Sodium S i l i c a t e Sodium H y d r o x i d e (50%) *Phosphate E s t e r * * L i q u i d N o n i o n i c S u r f a c t a n t ( C 9 .C l l .0 2. 5 Moles EO) Composition B: Water TSP S t a r s o Sodi um S i 1 ic a t e Sodium H y d r o x i d e (50%) *Phosphate E s t e r * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-Cl1. p e t r o l e u m g r e a s e and o i l Surface-Metal.0 6. : . 2 . mop o r s p r a y ( d i l u t e d ) M a n u f a c t u r e . g l a s s A p p l i c a t i o n Method-Wipe.4 1.2 * ** *** Rhone-Poulenc Rhodafac RE-600 Rhone-Poulenc R h o d a s u r f 91-6 Rhone-Poulenc R h o d a s u r f A-24 Hard S u r f a c e Spray Cleaner LPhosphate. 2 .0 5.0 4.8 oz/gallon) 71.00 1 . 12-13 M o l e s Use: As i s . spray I g e p a l CA-720 Detergent F o r m u l a t i o n Guide Wt% ~- EO 90.0 2.6 14. ceramic. 5 Moles EO) Use D i l u t i o n : 3-6% bw ( 4 .F o o d g r e a s e .F o o d g r e a s e . polymeric. ceramic.8 1.8 1 .

1 Formula 509 A 1 k a l ine Hard S u r f a c e C l e a n e r I n q r e d ients: Water. c p s : 32 S o l i d s : 1 1 . Typical Properties: V i s c o s i t y . Potassium H y d r o x i d e (87%) Wt% 10.8 2.0 5.0 6. Sodi u M e t a s i 1i c a t e m Varami de A-83 \Mi t c o n a t e 3 0 D S W i t c o n a t e SXS L i q u i d Wt% 62. add Phase I t o Phase X I ~ Typical Properties: V i s c o s i t y .0 12. Combine Phase I 1 i n g r e d i e n t s and m i x t h o r o u g h l y .O% pH: 12.0 8.Hand Surface Cleaners 73 Hard S u r f a c e C l e a n e r C o n c e n t r a t e w/Dipentene I nnredi e n t s : Phase I : Isopropanol Oleic Acid V a r o n i c K205 D i pentene Phase 11: Water. I .0 62. cps: 50 Solids: 13.8% pH: 10.7 3. I .0 B l e n d i n g Procedure: Combine Phase I i n g r e d i e n t s and m i x t h o r o u g h l y . D . W h i l e m i x i n g . : Suggested F o r m u l a t i o n s .0 Formula 515 SOURCE: W i t c o C o r p .2 2.8 5.5 B l e n d i n g Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n . D .

5 2.69 S t o r a g e a t a m b i e n t temp. f l a k e s A l p h a . Add MC-48 and 11-CM and m i x u n t i l homogeneous.0 2.4 15. 6 rpm. B r o o k f i e l d : 4520 c p s s p i n d l e #3. 100 mesh Sodium t a l l o w soap. : t h i x o t r o p i c s p i n d l e #3. l b s / g a l : 11. t a p C a l c i u m c a r b o n a t e .6 0.0 10.0 60. % : 50 D e n s i t y .5 M i x i ng P r o c e d u r e : Charge warm w a t e r and add c a l c i u m c a r b o n a t e w h i l e m i x i n g . B r o o k f i e l d : 3840 c p s s p i n d l e # 3 . o f f . : F o r m u l a t i o n No. s c u f f marks and l i p s t i c k f r o m v i n y l t i l e s s i m i 1 a r t o commerci a1 p r o d u c t s . 3 1 4 T i l e and Sani t a r v C l e a n e r s Inqredi ents: Z u s o l a t 1008/85 Water Xanthan Gum C i t r i c acid Inqredients: Amphotensid B 4 Water Citric acid Wt% 5.: CT 02-10-03 and CT 02-10-04 . Add soap and m i x u n t i l d i s p e r s e d . a s i s : 9 . P r o p e r t i es : Appearance: Opaque. B r o o k f i e l d : 3060 c p s S o l i d s . Add sodium c h l o r i d e t o t h i c k e n . 3 V i s c o s i t y @ 25 deg C .0 79.5 42.5 2.0 Suggested F o r m u l a t i o n s SOURCE: Zschimmer & Schwarz GmbH & Co.w h i t e creamy l i q u i d pH.S t e p MC-48 N i n o l 11-CM Sodi um C h l o r i d e Wt% 48. 1 week: N o s e p a r a t i o n Use I n s t r u c t i o n s : Use as i s Performance: C l e a n s g r e a s e p e n c i l .0 2.74 Advanced Cleaning Product Formulations L i q u i d A b r a s i v e C 1e a n s e r Inqredients: Water. 12 rpm. 30 rpm.0 Wt% 30. SOURCE: S t e p a n C o .

20 0.oo Procedure: 1 . F r a g r a n c e 9.5) Cocamide DEA ( N i n o l 40-CO) P r e s e r v a t i v e . : Van Gel and Veegum i n H a r d S u r f a c e C l e a n e r s and P o l i s h e s : Suggested F o r m u l a t i o n s .oo 0 : Cocamide DEA (Monamid 150-ADD) A1 k o x y l a t e d F a t t y A l c o h o l (P1 u r a f a c C-17) T e t r a p o t a s s i um P y r o p h o s p h a t e P o t a s s i u m Phosphate T r i b a s i c D e i o n i z e d Water C: Ammonium H y d r o x i d e .00 C12-CI3 L i n e a r P r i m a r y A l c o h o l E t h o x y l a t e (Neodol 23-6.00 0. V a n d e r b i l t Co. AS r e c e i v e d b a s i s SOURCE: R . C o n t i n u e m i x i n g f o r 40 m i n u t e s . 2 . 3 .25 0.00 1 . Xanthan Gum D e i o n i z e d Water Wt%* 4. Move t h e b a t c h t o a p r o p e l l e r m i x e r and a d j u s t t h e speed t o produce a s l i g h t v o r t e x . Add P a r t I3 t o P a r t A.50 0. 3 . Xanthan Gum D e i o n i z e d Water Purpose W t .Hand Sutface Cleaners 75 L i q u i d Hard Surface Cleaner Ingredients: A : Van Gel ES. 4 .50 68. C o n t i n u e m i x i n g f o r 20 m i n u t e s . Magnesium Aluminum S i l i c a t e Rhodopol 23.40 B : Calcium Carbonate C: 40. 2.s.50 1. I n c . Magnesi um A1 umi num S i 1 i c a t e Rhodopol 23.75 21 . Move t h e b a t c h t o a p r o p e l l e r m i x e r and a d j u s t t h e speed t o produce a s l i g h t v o r t e x . T . 303 Hard Surface C l e a n e r . F o r m u l a t i o n f r o m S h e l l Chemical Co. Combine t h e P a r t B i n g r e d i e n t s w i t h s l o w s t i r r i n g . 4 .%* 1.40 48. D r y b l e n d t h e Van Gel ES and Rhodopol 23 and s l o w l y add them t o t h e w a t e r w h i l e s t i r r i n g w i t h an homogenizer a t 5000 r p m .oo q. Procedure: 1 . m i x i n g f o r 5 m i n u t e s a f t e r each a d d i t i o n . D r y b l e n d t h e Veegum and Rhodopol 23 and s l o w l y add t h e b l e n d t o t h e w a t e r w h i l e s t i r r i n g w i t h an homogenizer a t 5000 rpm.50 2. Dye.A l l Ingredients: A : Veegum.. 28% 1 . Add t h e P a r t C i n g r e d i e n t s i n t h e o r d e r shown. F o r m u l a t i o n No. Add P a r t B and m i x f o r 10 m i n u t e s . m i x f o r 5 m i n u t e s and t h e n add P a r t C and m i x f o r 5 m i n u t e s .

50 1 . Add c o l o r and f r a g r a n c e .T e r g e PAS-8S Procedure : 1 .50 5. U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i ng and b l e n d i ng o p e r a t i o n s .00 2. M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. Under moderate a g i t a t i o n .0 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-320 . Add t h e a l k a n e s u l f o n a t e . add t h e sodium h y d r o x i d e and t h e metasilicate. I n p r e d ie n t : D I water Carbopol 672 ( 1 ) Sodium h y d r o x i d e (50%) Sodium m e t a s i l i c a t e . add t h e sodium h y p o c h l o r i t e b l e a c h . : B i o . p e n t a h y d r a t e P r i m a r y a l k a n e s u l f o n a t e (40%) ( 2 ) Sodium h y p o c h l o r i t e (15. 5 .00 ( 1 ) BFGoodrich ( 2 ) Stepan C o . Total Actives: Primary alkane sulfonate: Available chlorine: 2. 3.00 7. 2 . 4 . This the contact time o f the deterenhance consumer c o n v e n i e n c e . Under l o w a g i t a t i o n .76 Advanced Cleaning Product Formulations M o l d and M i l d e w Remover Carbopol r e s i n s a r e used t o v e r t i c a l c l i n g when s p r a y e d on "no-drip" a c t i o n w i l l increase g e n t on t h e s o i l e d s u r f a c e and reduce s p l a s h i n g and t o p r o v i d e a v e r t i c a l surface. d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r .0 1.00%) B r o o k f ie l d v i s c o s i t y (RVT-PO P r o d u c t p H : 12-13 P r o d u c t c l a r i t y : Opaque rpm) : 120 cps \Rlt% 84. as d e s i r e d .00 0.

Laundry Products 77 .

3.O-3.o 1 . T h e r e f o r e DDBS-Na must b e employed i n f o r m o f a s p r a y d r i e d powder.0 3.0 3. Powder Sodi um d i s i 1 ic a t e S o k a l a n CP 5 S o k a l a n HP 22 Aquamoll i n BC Powder Perfume Sodium s u l p h a t e Wt% 3.0 25.0 2.0.0 20.0 1.5 q.0-25. T h e r e f o r e DDBS-Na must b e employed i n f o r m o f a s p r a y d r i e d powder. ad 1 0 0 . Powder Sodi um d i s i 1 i c a t e S o k a l a n CP 5 S o k a l a n HP 22 A q u a m o l l i n BC Powder Perfume Sodi um s u l p h a t e Q 3.0 15. ad 100.0 1 . DDBS-Na p a s t e i s not suitable.0 1 .o 0.5 q.0 1 .3.0. *DDBS=Dodecyl Benzene S u l f o n a t e SOURCE: H o e c h s t A k t i e n g e s e l l s c h a f t : Suggested F o r m u l a t i o n s .s. 0 Manufacturing: To b e p r e p a r e d by s p r a y m i x p r o c e s s .s.0 15.o 0. DDBS-Na p a s t e i s not suitable.0 Manufacturing: To b e p r e p a r e d b y s p r a y m i x p r o c e s s . *DDBS=Dodecyl Benzene S u l p h o n a t e Detergent f o r Fine Fabrics-2 Powder Inqredients: Genapol OA-080 DDBS-Na* Z e o l i t h A (Wessalith T a l l o w soap.78 Advanced Cleaning Product Formulations Detergent f o r Fine Fabrics-1 Powder Inpredi ents: Genapol OA-080 DDBS-Na* Thermphos NW T a l l o w soap.

00 Cal s o f t LAS-99 Cal o x y l a t e N .00 18.50 4. F o r m u l a t i o n HDL-006-01 Heavv D u t y L a u n d r y Wei o h t % 42.01 18.00 SOURCE: P i 1o t Chemical Co.00 15.00 3.50 7.00 P i l o t SXS-40 12.00 10.60 Calamide C 7.00 10. 50% 6.00 7. F o r m u l a t i o n HDL-001-01 Heavy D u t y L a u n d r y Inqredients: Water P i l o t SXS-40 Calamide C T W Sodium S i l i c a t e ( S o l i d ) C a l s o f t L-60 EDTA (Ethylenediaminetetraacetic A c i d ) Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d . : Suggested Formul a t i ons .00 5.00 2.00 Comments a b o u t t h i s f o r m u l a : Add C a l o x y l a t e N .90 Sodi um H y d r o x i d e .00 Wei q h t % 42.Laundry Products 79 Heavy D u t y L a u n d r y Ingredients: Wei q h t % Water 28.50 22. F o r m u l a t i o n HDL-007-01 Heavv D u t y L a u n d r y Inqredients: Water TKPP ( T e t r a P o t a s s i u m P y r o p h o s p h a t e ) Sodium S i l i c a t e ( S o l i d ) C a l s o f t L-60 P i l o t SXS-40 Calamide C T W Comments a b o u t t h i s f o r m u l a : May need t o be h e a t e d t o s o l u b i l i z e t h e s u r f a c t a n t .00 2.9 5. F o r m u l a t i o n HDL-008-01 Weight% 78.50 I n q r e d ie n t s : Water C a l f a x DB-45 C a l o x y l a t e N-9 P r o p y l ene G1 y c o l TKPP ( T e t r a P o t a s s i um Pyrophosphate) Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .9 a f t e r 50% o f LAS-99 has been n e u t r a l i z e d .50 5.50 40.

00 10.: Suggested F o r m u l a t i o n s Powder f o r A u t o m a t i c D i s h w a s h i n n M a c h i n e s Ingredients: A Genapol 2908 B Sodium m e t a s i 1 i c a t e x 5H20 C Sodium c a r b o n a t e Sodi um d i c h l o r o i s o c y a n u r a t e Thermphos N W YO by W e i q h t 1 .oo 52. Heavy s o i l s may r e q u i r e s l i g h t l y higher levels. I 1 One a f t e r a n o t h e r . & 4 and b l e n d . Cool t o 1OOF. SOURCE: B u r l i n g t o n Chemical Co. t h e components o f C a r e added t o 1 A p p l i c a t i o n : 1-29 d e t e r g e n t / L d i s h w a s h i n g l i q u o r SOURCE: Hoechst A k t i e n g e s e l l s c h a f t : Suggested F o r m u l a t i o n . 5 % s o l i d s : 26 Lbs/gal : 8.25 0.00 1.50 B u r c o LAF-6 i s used t o c o n t r o l foam as w e l l a s t o p r o v i d e w e t t i n g and d e t e r g e n c y .00 2. Add r e m a i n i n g w a t e r .66 S u r f a c t a n t R i c h D e t e r g e n t f o r N u r s i n o Homes Ingredients: Water TKPP Sodium M e t a s i l i c a t e P e n t a h y d r a t e B u r c o t e r g e DG-40 B u r c o NPS-876 SXS-40% % bv W e i q h t 30 5 5 40 10 10 6-8 ounces p e r 100 pounds o f l a u n d r y . Add 5 and 6 .00 10. 2 . 1% pH: 9 .25 20. 3 . Procedure: Charge 1 / 2 o f w a t e r I3 120F. Add 1 .00 35.00 Manufacturing: I Spray A on B .80 Advanced Cleaning Product Formulations I Components: Water T r i e t h a n o l ami ne 85% D i e t h y l ene G1 y c o l B u r c o l 117 B u r c o l LAF-6 Burcowi t e BBH-PO B u r c o t a s e SL-160 & I L i q u i d Laundrv Detergent w i t h Enzyme & O p t i c a l % by Weisht 50.00 3. B l e n d u n t i l u n i f o r m .00 10.

Sodi u a1 k y l benzene sul f o n a t e : m C12-15 l i n e a r a l c o h o l . 4.: B i o s o f t D-62 PP.00 Carbopol ETD 2691 ( 1 ) 612-15 l i n e a r a l c o h o l . Use a b i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . 3. Add i n t h e pyrophosphate w i t h minimal a g i t a t i o n t o a v o i d a i r entrapment. add i n t h e a l c o h o l e t h o x y l a t e and a l k y l benzene s u l f o n a t e s u r f a c t a n t s . C o n t i n u e a g i t a t i n g and add t h e p o t a s s i u m h y d r o x i d e and metas i li c a t e .00 20.00 20. Add dyes and f r a g r a n c e . anhydrous T e t r a p o t a s s i u m pyrophosphate P h y s i c a l Pi-opert ie s : B r o o k f i e l d V i s c o s i t y (RVT-20 rpm): 900 P r o d u c t pH: 14 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) S h e l l Chemical C o .50 18. : Neodol 25-7 ( 3 ) Stepan Co. A l l o w t o mix u n t i l homogeneous and f r e e o f polymer lumps.00 5. 5. 7 moles EO: T e t r a p o t a s s i u m pyrophosphate: 2.Laundry Products 81 IndustriaT Heavy Duty Laundry L i q u i d Carbopol ETD 2691 is t o p r o v i d e p r o d u c t phase s t a b i l i z a t i o n i n t h i s high a l k a l i n i t y i n d u s t r i a l strength cleaner. I nsredient : D I water Wt% 49.0cedure: I .00 5. W i t h s l o w m i x i n g . Screen t h e Carbopol r e s i n i n t o t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r (800 rpm).50 2.00 0. Total Wcti ves : 3.30 18.00 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-201 . as d e s i r e d . 7 moles EO ( 2 ) Sodium a l k y l b e n z e n e s u l f o n a t e (60%) ( 3 ) Potassium h y d r o x i d e (45%) Sodium m e t a s i l i c a t e .

0 3. Mixed B u i l d e r F o r m u l a t i o n Components: Water 45% KOH B u r c o s p e r s e LP TKPP Burco NPS-816 S t a r Grade Sodium S i l i c a t e % by Weight 31.0 15. Add TKPP and s t i r u n t i l d i s s o l v e d . Add Burco NPS-816.0 F o r m u l a t i o n CT 07-06-01 SOURCE: Zschimmer & Schwarz GmbH & Co. e t c . I n c . temperature.0 5. : Suggested F o r m u l a t i o n s Washi np P a s t e w i t h 81 e a c h i n g A g e n t Ingredients: Water Sodium t r i p o l y p h o s p h a t e Sodium d i t h i o n i t Xanthan Gum Whi t e .0 12.0 65.0 10. t h e n S t a r Grade Sodium S i l i c a t e and b l e n d u n t i l u n i f o r m .0 30. depending on s o i l SOURCE: B u r l i n g t o n Chemical Co.0 Procedure: D i s s o l v e KOH i n w a t e r .0 2.0 Procedure: B l e n d a l l components e x c e p t 50% NaOH. Use l e v e l s a r e 6-12 ounces p e r 100 pounds.0 5.5 23.0 10.82 Advanced Cleaning Product Formulatioris I n d u s t r i a l Laundry D e t e r a e n t s H i g h C a u s t i c FormulaComponents: Burco NPS-816 Burcosperse LP B u r c o l i t e BSGH-255 Dequest 2000 50% NaOH % bv Weiaht 15.5 10. l o a d i n g . Keep t e m p e r a t u r e below 160F. Keep t e m p e r a t u r e below 1 6 0 F d u r i n g t h e e n t i r e agitation.0 10.s p i r i t Lumorol 4154 Zusol a t 1005/85 % b y Weiaht 39.: . S l o w l y add NaOH w i t h a g i t a t i o n .0 10.0 5. S l o w l y add Burcosperse LP w h i l e a g i t a t i n g ..

6 0. body w a s t e .13. L i q u i d ) S o i l .1 24.2 0.3 ** Rohm & Haas S h e l l Chemical Neodol 23-6.0 2.6 0. 9-10 M o l e s €0 Potassium H y d r o x i d e (45%) ***Sodium C i t r a t e ( a n d / o r C i t r i c A c i d ) K a s i l #6 Potassium S i l i c a t e EDTA food s o i l Wt% 37.9 9.1 0. EO 6 .9 . body w a s t e . f o o d s o i l . e . S u r f a c e .B o d y o i l and p e r s p i r a t i o n .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n Method-Household w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition: Water Fluorescent Brightener C a r b o x y m e t h y l c e l l u l o s e (CMC) * A c r y s o l A S E .0 1. make-up. : Detergent Formulary Guide .0 12. 5 M o l e s ) t: Wt% 52.5 4.5 5.I 08 **Nonylphenoxy P o l y e t h o x y e t h a n o l .5 SOURCE: PQ C o r p .5 6.5 8.C o t t o n and c o t t o n .p o l y e s t e r A p p l i c a t i o n Method-Household w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r make-up Composition : Water C a r b o p o l 674 D L i q u i d Sodium S i l i c a t e * A c u s o l 445ND Sodium P o l y a c r y l a t e (92% s o l i d s ) Sodium C a r b o n a t e V a l f o r 100 Z e o l i t e A * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-. 5 . o r Rhone-Poulenc C o l l o i d 225/35 P o l y a c r y l a t e (40%) Rhone-Poul enc I g e p a l CO-630 A d j u s t p H w i t h c i t r i c a c i d t o m a i n t a i n pH f o r e f f e c t i v e enzyme p e r f o r m a n c e ( i . S u r f a c e . 8 .o Enzymes ( P r o t e a s e ) x( ** *** Rohm & Haas. 5 p H ) .Laundry Products 83 L a u n d r y Deteraent-Consumer (Liquid) S o i l .B o d y o i l and p e r s p i r a t i o n .0 10.2 25. Z e r o Phosphate. L a u n d r y Detergent-Consumer I Z e o l i t e B u i l t .

cotton A p p l i c a t i o n Method-Household washing machine Manufacture-Dry blend/agglomeration Composi t i on : B r i t e s i l H20 Hydrous P o l y s i l i c a t e *STPP *Sodium Carbonate Sodi u S u l f a t e m * * L i n e a r A1 k y l benzene Sul f o n a t e (LAS) * * * L i q u i d N o n i o n i c S u r f a c t a n t (7-9 Moles EO.C o t t o n and c o t t o n .0 30.0 2. Neodol 25-7 SOURCE: PQ C o r p .A c i d i c f o o d f a t and p r o t e i n . powder) Rhone-Poulenc Rhodasurf LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 Laundry Detergent-Consumer (Phosphate. Powder) S o i l .0 10.0 0.p o l y e s t e r A p p l i c a t i o n Method-Household Washing Machine Manufacture-Dry Blend/Agglomeration Composition: Sodi u Carbonate m B r i t e s i l H20 Hydrous P o l y s i l i c a t e *Acusol 445ND Sodium P o l y a c r y l a t e (92% s o l i d s ) * * L i n e a r A 1 k y l benzene S u l f o n a t e (LAS) * * * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 .0 30. Perfume Use L e v e l : g r a s s and C12-15) Q 10. O p t i c a l B r i g h t e n e r . Powder) S o i l . C12-15) V a l f o r 100 Z e o l i t e A Sodi u S u l f a t e m O p t i c a l B r i g h t e n e r . dirt Surface-Polyester.84 Advanced Cleaning Product Formulations Laundry Detergent-Consumer ( Z e r o Phosphate. : D e t e r g e n t F o r m u l a t i o n Guide . cotton/polyester.0 30. powder) Rhone-Poulenc Rhodasurf LA-7 o r LA-9 o r S h e l l Chemical Co.5 of 1000 ppm d e t e r g e n t d e l i v e r e d t o wash ( 1 g r a m / l i t e r water) * ** *** FMC Stepan Nacconol 90G (90% a c t i v e .5 1000 ppm d e t e r g e n t d e l i v e r e d t o wash ( 1 gram d e t e r g e n t / l i t e r o f water) * ** *** Rohm & Haas Stepan Nacconol 9OG (90% a c t i v e .9 moles EO. body p e r s p i r a t i o n .A c i d i c f o o d f a t .0 5.0 10. Perfume Use L e v e l : Wt9/o 30. sebum and body waste S u r f a c e . b l o o d .5 0.0 12.0 14.5 10.0 5. o i l grease.

0 10.I n d u s t r i a l (Liquid) & Institutional S o i l . b l o o d .P o l y e s t e r and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .6 10. 25.0 r a t i o Si02/Na20 b w f o r b e s t s t a b i l i t y and i n d u s t r i a l d e t e r g e n c y .P e t r o l e u m o i l and g r e a s e . sebum and body waste S u r f a c e . Laundry B r e a k .Laundry Products 85 Laundry B r e a k .0 30. o i l a n d g r e a s e .50% b y w e i g h t o r 1-2 l b s p e r 100 l b s l a u n d r y N o t e : Use b u i l d e r s o l u t i o n i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) a t 2-4 p a r t s o f b u i l d e r t o 1 p a r t d e t e r g e n t .A c i d i c f o o d f a t .4 18.7-2.I n d u s t r i a l & I n s t i t u t i o n a l ( L i q u i d .I n d u s t r i a l w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition A : Water TKPP P o t a s s i urn H y d r o x i d e (45%) S t a r Sodium S i l i c a t e Sodium H y d r o x i d e (50%) C o m p o s i t i o n B: Water TKPP P o t a s s i u m H y d r o x i d e (45%) S t a r Sodi um S i 1 i c a t e Sodium H y d r o x i d e (50%) Use D i l u t i o n : Light Soil: 34. D o r BJ-120 sodium s i l i c a t e s c a n a l s o b e used as b u i l d e r solutions without blending.C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . : D e t e r g e n t F o r m u l a t i o n G u i d e .25% b y w e i g h t o r 1 l b p e r 100 l b s 1a u n d r y Medium/Heavy S o i l : 0.5 wts/.0 0.1 10.25%-0.50% b y w e i g h t o r 1-2 l b s p e r 100 l b s l a u n d r y Notes: Blend t h i s b u i l d e r s o l u t i o n t o 1.25%-0.25% by w e i g h t o r 1 l b p e r 100 l b s 1a u n d r y Medium t o Heavy S o i l : 0. Use b u i l d e r s o l u t i o n i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) a t 2-4 p a r t s bw o f b u i l d e r t o 1 p a r t d e t e r g e n t .0 7.0 30. SOURCE: PQ C o r p .I n d u s t r i a l w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition: Water N C l e a r Sodium S i l i c a t e Sodium H y d r o x i d e (50%) Use D i l u t i o n : Light Soil: % 0-20 70-90 10-20 0.4 24. Phosphate1 S o i l . g r a p h i t e and c o l o r e d p i g m e n t S u r f a c e .

1 5 ) Use L e v e l : L i g h t S o i l .0 12.9 moles V a l f o r 100 Z e o l i t e A 25.O . * Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 L a u n d r y B r e a k . 5 0 % b y w e i g h t o r 2 l b s p e r 1 0 0 l b s 1a u n d r y Heavy S o i l .0 .O .P o l y e s t e r and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . Powder) S o i l .0 .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . o i l and g r e a s e .0 10. i f l o w e r a l k a l i n i t y i s d e s i r e d and more s u s p e n d i n g / e m u l s i f y i n g power i s needed.I n d u s t r i a l w a s h i n g machine Manufacture-Dry blend/Agglomeration Composi t i on : M e t s o Beads 2048 Sodi um C a r b o n a t e NTA * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . g r a p h i t e and c o l o r e d p i g m e n t S u r f a c e . B r i t e s i l H20 w i l l a l s o i n c r e a s e t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d .I n d u s t r i a l w a s h i n g machine M a n u f a c t u r e . 7 5 % b y w e i g h t o r 3 l b s p e r 1 0 0 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048.0 38. P o w d e d S o i l . sebum and body waste S u r f a c e . p a r t i a l l y or f u l l y . SOURCE: PQ C o r p . 2 5 % by w e i g h t o r 1 l b p e r 1 0 0 l b s 1a u n d r y Medium S o i l . 2 5 % b y w e i g h t o r 1 l b p e r 1 0 0 l b s 1a u n d r y Medium S o i l .I n d u s t r i a l & I n s t i t u t i o n a l (NTA/Zeol it e .0 15.U s e as r e c e i v e d Composi t i on : M e t s o Beads 2048 Use D i l u t i o n : Wt46 100.0 EO.P e t r o l e u m o i l and g r e a s e .O . b l o o d .0 L i g h t S o i l . 5 0 % by w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l .86 Advanced Cleaning Product Formulatiom Laundry D e t e r s e n t . 7 5 % by w e i g h t o r 3 l b s p e r 100 I b s 1a u n d r y at N o t e : Use i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) 2-4 p a r t s b w o f b u i l d e r w i t h 1 p a r t d e t e r g e n t .A c i d i c f o o d f a t .I n d u s t r i a1 & I n s t i t u t i o n a l ( Z e r o Phosphate. C 1 2 .0 . : D e t e r g e n t F o r m u l a t i o n Guide .

Laundqi Products 87 Laundry D e t e r g e n t . sebum and body waste S u r f a c e .I n d u s t r i a l 8 I n s t i t u t i o n a l (Phosphate.0 10.O . Powder) S o i l . i f l o w e r a l k a l i n i t y i s d e s i r e d and more s u s p e n d i n g / e m u l s i f y i n g power i s needed. i f l o w e r a l k a l i n i t y i s d e s i r e d and more suspendi n g / e m u l s i f y i n g power i s needed. 7 5 % b y w e i g h t o r 3 l b s p e r 100 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048. 5 0 % by w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l .I n d u s t r i a l washing machine Manufacture-Dry blend/Agglomeration Q Composi t i on : Metso Beads 2048 25.0 .A c i d i c f o o d f a t . x< FMC Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 ** Laundry D e t e r g e n t . ' k Rhone-Poulenc Rhodasurf LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 SQURCE: PQ G o r p .I n d u s t r i a l washing machine Manufacture-Dry blend/Agglomeration WtO/o Composition: Metso Beads 2048 25.C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .0 *Sodium C a r b o n a t e *STPP 30. B r i t e s i l H20 w i l l a l s o i n c r e a s e t h e s u r f a c t a n t adosrbency o f d e t e r g e n t b l e n d . C12-15) Use L e v e l : L i g h t Soi 1-0.A c i d i c f o o d f a t .9 moles EO. 7 5 % b y w e i g h t o r 3 l b s p e r 100 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f Metso Beads 2048. o i l and grease.0 Use L e v e l : L i g h t Soi 1-0. o i l and g r e a s e .0 Sodium C a r b o n a t e Sodi um S u l f a t e 10. 5 0 % b y w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l . : D e t e r g e n t F o r m u l a t i o n G u i d e . p a r t i a l l y o r f u l l y .O . b l o o d . sebum and body waste S u r f a c e . Powder) S o i l .25% b y w e i g h t o r 1 l b p e r 100 l b s l a u n d r y Medium S o i l .25% b y w e i g h t o r 1 l b p e r 100 l b s l a u n d r y Medium S o i l .0 35.0 * * L i q u i d N o n i o n i c S u r f a c t a n t (7-9 m o l e s EO. p a r t i a l l y o r f u l l y .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .0 55. b l o o d .0 * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . B r i t e s i l H20 w i l l a l s o i n c r e a s e t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d .I n d u s t r i a l 8 I n s t i t u t i o n a l (Sodium Carbonate. C12-15) 10.O .

0 Carboxymethylcel l u l o s e 2. H i ah A1 k a l in i t v ) S o i l .I n d u s t r i a l washing machine Manufacture-Dry blend/Agglomeration Wt% Composi t i on A : Metso Beads 2048 60.0 .0 Sodium H y d r o x i d e Beads Use D i l u t i o n : L i g h t S o i l . I n s t i t u t i o n a l ( Z e r o Phosphate Powder.0 Metso Beads 2048 Sodium H y d r o x i d e Beads 40. 7 5 % by w e i g h t o r 3 l b s p e r 1 0 0 lbs 1aundry Note: Use t h e s e a l k a l i b u i l d e r s i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) a t 2-4 p a r t s bw o f b u i l d e r w i t h 1 p a r t detergent FMC * Laundrv B r e a k . sebum and body waste S u r f a c e . 5 0 % by w e i g h t o r 2 l b s p e r 1 0 0 I b s 1aundry Heavy S o i l .0 20. b l o o d . o i l and grease.0 . Powder.0 Carboxymethylcellulose 2.0 .0 Sodi u Carbonate m 28.0 Sodium H y d r o x i d e Beads V a l f o r 100 Z e o l i t e A 20.A c i d i c f o o d f a t . b l o o d .4 p a r t s bw o f b u i l d e r w t h 1 p a r t detergent SOURCE: PQ C o r p .0 Sodium H y d r o x i d e Beads 40.C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . H i g h A l k a l i n i t y ) S o i l .I n d u s t r i a l & I n s t i t u t i o n a l (Phosphate. o i l and grease.0 Use L e v e l : L i g h t S o i l . 2 5 % by w e i g h t o r 1 l b p e r 100 l b s 1aundry Medium S o i l . sebum and body waste S u r f a c e . : D e t e r g e n t F o r m u l a t i o n Guide .0 20.0 Composition 8: W S Metso Beads 2048 30.88 Advanced Cleaning Product Formulations Laundry B r e a k . 7 5 % b y w e i g h t o r 3 l b s p e r 0 0 l b s 1aundry N o t e : Use t h e s e a l k a l i b u i l d e r s i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) a t 2 .A c i d i c f o o d f a t .0 *STPP 20.I n d u s t r i a1 8.0 . 2 5 % by w e i g h t o r 1 l b p e r 100 l b s l a u n d r y Medium S o i l . 5 0 % by w e i g h t o r 2 l b s p e r 100 I b s 1aundry Heavy S o i l .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .0 .I n d u s t r i a l washing machine Manufacture-Dry b l end/Agglomeration Wt% Composition A : 60.O .0 *Sodium Carbonate 28.0 Composition 8: Wt% Metso Beads 2048 30.

B r i t e s i 1 H20 w i 11 a1 so i n c r e a s e t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d .A c i d i c f o o d f a t .O .Laundry Products 89 Laundry D e t e r g e n t . C12-15) 10.A c i d i c f o o d f a t .0 * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . sebum and body waste S u r f a c e . 9 6 FMC dc* Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 Laundry D e t e r g e n t .0 10.0 M e t s o Beads 2048 35. : D e t e r g e n t F o r m u l a t i o n G u i d e .0 .0 . sebum and body waste S u r f a c e . C12-15) Use L e v e l : L i g h t S o i l . 5 0 % b y w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l . 7 5 % b y w e i g h t o r 3 l b s p e r 100 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048.0 % * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . 5 0 % b y w e i g h t o r 2 l b s p e r 1 0 0 l b s 1a u n d r y Heavy S o i l .0 *STPP 10.I n d u s t r i a l & I n s t i t u t i o n a l (NTA. B r i t e s i l H20 w i l l also i n crease t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d . b l o o d . o i l and g r e a s e .0 NTA 25.0 .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . 2 5 % b y w e i g h t o r 1 l b p e r 100 l b s l a u n d r y Medium S o i l .9 m o l e s EO. i f l o w e r a l k a l i n i t y i s d e s i r e d and more suspendi n g / e m u l s i f y i ng power i s needed.0 .I n d u s t r i a l w a s h i n g machine Manufacture-Dry blend/Agglomeration Composition: Wt% 25.0 V a l f o r 100 Z e o l i t e A Use L e v e l : L i g h t S o i l . b l o o d .0 *Sodium C a r b o n a t e 20.9 moles EO. o i l and g r e a s e .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . p a r t i a l l y o r f u l l y .0 . Powder) S o i l .I n d u s t r i a1 washi ng machine Manufacture-Dry blend/Agglomeration Composi t i on : Wt% M e t s o Beads 2048 25. p a r t i a l l y o r f u l l y .I n d u s t r i a l 8 I n s t i t u t i o n a l (Reduced Phosphate. 2 5 % by w e i g h t o r 1 l b p e r 1 0 0 l b s l a u n d r y Medium S o i l . Powder) S o i l . *Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 SOURCE: PQ C s r p . 7 5 % b y w e i g h t o r 3 l b s p e r 1 0 0 l b s 1a u n d r y N o t e : U s e B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048. i f l o w e r a l k a l i n i t y i s d e s i r e d and more s u s p e n d i n g / e m u l s i f y i n g power i s needed.0 Sodium C a r b o n a t e 40.

: D e t e r g e n t F o r m u l a t i o n Guide .90 Advanced Cleaning Product Formulations Laundry D e t e r q e n t .0 25.I n d u s t r i a l & I n s t i t u t i o n a l IPhosphate. sebum and body waste S u r f a c e .1 5 ) V a l f o r 100 Z e o l i t e A Use L e v e l : 20. p a r t i a l l y o r f u l l y . S o l i d Block) S o i l . b l o o d .0 35. o i l and grease.0 * ** F C M Rhone-Poulenc Rhodasurf LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 SOURCE: PQ C o r p . sebum and body waste S u r f a c e .25% by w e i g h t o r 1 l b p e r 1 0 0 l b s 1aundry Medium S o i l : 0 . o i l and grease.0 55. B r i t e s i l H20 w i l l a l s o i n c r e a s e t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d .75% b y w e i g h t o r 3 l b s p e r 100 l b s 1 aundry Note: Use B r i t e s i l H20 i n p l a c e o f Metso Beads 2048. * Rhone-Poulenc Rhodasurf LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 Laundry D e t e r g a n t . b l o o d .A c i d i c f o o d f a t . C12-15) 3.I n d u s t r i a l B I n s t i t u t i o n a l (Sodium Carbonate w i t h F l o w A i d . C 1 2 .0 12.C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . 5 0 % b y w e i g h t o r 2 l b s p e r 1 0 0 l b s 1 aundry Heavy S o i l : 0.A c i d i c f o o d f a t .0 5.9 moles EO.0 10.0 Wt% L i g h t S o i l : 0.C o t t o n and c o t t o n / p o l y e s t e r Appl ic a t ion Method-I n d u s t r ia1 wash ing mach i ne Manufacture-Dry blend/agglomeration Composi t ion : Metso Beads 2048 Sodium Carbonate Sodi um S u l f a t e * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 .0 *STPP *Sodium Carbonate * * L i q u i d N o n i o n i c S u r f a c t a n t (7-9 Moles EO. Powder) S o i l .0 10. i f l o w e r a l k a l i n i t y i s d e s i r e d and more susp e n d i n g / e m u l s i f y i n g power i s needed.I n d u s t r i a1 washing machine Manufacture-Sol i d b l o c k Composi t i on : Metso Beads 2048 NaOH ( 5 0 % S o l u t i o n ) Wt% 25.

o i l g r e a s e .9 moles EO. 5 0 % b y w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l . 5 0 % b y w e i g h t o r 2 l b s p e r 100 l b s 1a u n d r y Heavy S o i l . sebum and body w a s t e S u r f a c e . B r i t e s i l H20 w i l l a l s o i n crease t h e s u r f a c t a n t adsorbency o f d e t e r g e n t b l e n d .0 M e t s o Beads 2048 25. C12-15) 18.25% b y w e i g h t o r 1 l b p e r 1 0 0 l b s l a u n d r y Medium S o i l . Powder) S o i l .0 Use L e v e l : L i g h t S o i l .O .D r y B1 end/Aggl o m e r a t i on Composi t ion : Wt% Sodium C a r b o n a t e 44. Powder) S o i l .0 .I n d u s t r i a l w a s h i n g machine Manufacture-Dry Blend/Agglomeration Wt% Composition : Sodi um C a r b o n a t e 35.Laundry Products 91 Laundry D e t e r g e n t . 7 5 % b y w e i g h t o r 3 l b s p e r 1 0 0 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048.P e t r o l e u m o i l and g r e a s e .I n d u s t r i a l and I n s t i t u t i o n a l (Zero Phosphate.A c i d i c f o o d f a t . 2 5 % b y w e i g h t o r 1 l b p e r 100 l b s l a u n d r y Medium S o i l .C o t t o n and c o t t o n p o l y e s t e r A p p l i c a t i o n M e t h o d .P o l y e s t e r and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . i f l o w e r a l k a l i n i t y i s d e s i r e d and more s u s p e n d i n g / e m u l s i f y i n g power i s needed. p a r t i a l l y o r f u l l y . : D e t e r g e n t F o r m u l a t i o n G u i d e .0 15.O .0 30.0 * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 . i f l o w e r a1 k a l in i t y is d e s i r e d and more s u s p e n d i n g / e m u l s i f y i n g powder i s needed. b l o o d . p a r t i a l l y o r f u l l y .0 .0 M e t s o Beads 2048 Use L e v e l : L i g h t S o i 1-0.I n d u s t r i a l and I n s t i t u t i o n a l ( Z e r o Phosphate. 7 5 % b y w e i g h t o r 3 l b s p e r 100 l b s 1a u n d r y N o t e : Use B r i t e s i l H20 i n p l a c e o f M e t s o Beads 2048.I n d u s t r i a l w a s h i n g machine M a n u f a c t u r e .0 . B r i t e s i l H20 w i l l a l s o i n crease t h e s u r f a c t a n t adsorbency o f d e t e r g e n t blend.5 * L i q u i d N o n i o n i c S u r f a c t a n t ( 7 .5 5.0 V a l f o r 100 Z e o l i t e A * * A c u s o l 445ND Sodium P o l y a c r y l a t e (92% s o l i d s ) 2. C12-15) V a l f o r 100 Z e o l i t e A 25. g r a p h i t e and c o l o r e d p i g m e n t S u r f a c e . *Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 L a u n d r y D e t e r g e n t .9 moles € 0 . Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 o r S h e l l Chemical Neodol 25-7 Rohm & Haas ** SOURCE: PQ Corp.

0 .C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .0 (C12-C15.0 4.1 F1 u o r e s c e n t B r i g h t e n e r C a r b o x y m e t h y l c e l l u l o s e (CMC) 0.7 15.50% by w e i g h t or 1-2 l b s p e r 1 0 0 I b s 1a u n d r y Rohm & Haas.0 2.I n d u s t r i a l w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r wts/.I n d u s t r i a l ( L i quid) & Institutional food soi 1 Soi 1-Body o i 1 and p e r s p i r a t i o n .92 Advanced Cleaning Product Formulations Laundry D e t e r q e n t . *PhosphaGe E s t e r **Liquid Nonionic Surfactant food s o i l Wt% 54. S u r f a c e . make-up.25%-0.C o t t o n and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d . L i q u i d ) S o i l .I n d u s t r i a l w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition A: Water TKPP P o t a s s i u m H y d r o x i d e (45%) S t a r s o Sodium S i l i c a t e Sodi um H v d r o x i d e ( 5 0 %. or Rhone-Poulenc C o l l o i d 226/35 P o l y a c r y l a t e (40%) **Rhone-Poulenc I g e p a l CO-630 * SOURCE: PQ C o r p .0 Use D i l u t i o n : 0 .2 P o t a s s i um H y d r o x i d e (45%) TKPP (60%) 40.I n d u s t r i a l & I n s t i t u t i o n a l [ P h o s p h a t e B u i 1t .7 Water 0.5 Use D i l u t i i o n : 0. 7-9 M o l e s € 0 ) C o m p o s i t i o n B: Wt% Water 59.0 **Nonylphenoxy P o l y e t h o x y e t h a n o l . 2 5 % .0 3.1 P o t a s s i u m H y d r o x i d e (45%) 13.7 S t a r s o Sodi um S i 1 i c a t e 15.0 K a s i 1 #6 P o t a s s i um S i 1 i c a t e 12.0 * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-C15.5 * A c r y s o l ASE-108 ( A c r y l i c P o l y m e r ) 6. Composition: 28.2 5. body waste. : Detergent Formulary Guide .B o d y o i l and p e r s p i r a t i o n .0 Sodium H y d r o x i d e ( 5 0 % ) 4.) . 5 0 % b y w e i g h t or 1-2 l b s p e r 1 0 0 l b s 1a u n d r y Rhone-Poulenc Rhodafac RE-610 Rhone-Poulenc R h o d a s u r f LA-7 o r LA-9 * ** Laundry D e t e r g e n t . make-up.5 4. body w a s t e . 9 Moles EO) 3.6 13. S u r f a c e .2 *Phosphate E s t e r 5. 9-1 0 M o l e s EO 10.

I n d u s t r i a l washing Manufacture-Mix t a n k w i t h p r o p e l l e r s t r r e r Composition: Water C a r b o p o l 674 Metso Beads 2048 *Acusol 445N Sodi um P o l y a c r y a t e (45% s o l d s ) Sodium C a r b o n a t e V a l f o r 100 Z e o l i t e A * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-13.0 37.25% by w e i g h t o r 1 l b p e r 100 l b s 1a u n d r y Medium t o Heavy S o i l : 0. b l o o d .50% b y w e i g h t o r 1-2 l b s p e r 100 l b s l a u n d r y N o t e : Use b u i l d e r s o l u t i o n i n c o n j u n c t i o n w i t h l a u n d r y d e t e r g e n t ( u n b u i l t ) a t 2-4 p a r t s bw o f b u i l d e r t o 1 p a r t d e t e r g e n t Laundry D e t e r g e n t .5 2. : D e t e r g e n t F o r m u l a t i o n Guide SOURCE: .5 4.B o d y o i l and p e r s p i r a t i o n . f a t . S u r f a c e . f o o d s o i l . Z e r o Phosphate.25%-0.C o t t o n and.Laundry Products 93 Laundry B u i l d e r .A c i d i c f o o d . 5 PQ C o r p .0 0. o i l and grease.0 52. EO 6 .p o l y e s t e r a c h i ne A p p l i c a t i o n M e t h o d . 5 M o l e s ) 8 make-up WtO/o 57. c o t t o n .0 28.1 24.P o l y e s t e r and c o t t o n / p o l y e s t e r A p p l i c a t i o n M e t h o d .I n d u s t r i a l w a s h i n g machine Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition A : P o t a s s i u m H y d r o x i d e (45%) i C l e a r o r E Sodium S i l i c a t e U C o m p o s i t i o n B: Water Potassium Hydroxide ( S o l i d ) N C l e a r or E Sodium S i l i c a t e Composition C: Water Potassium Hydroxide ( S o l i d ) N C l e a r o r E Sodium S i l i c a t e Sodium H y d r o x i d e ( S o l i d ) Use D i l u t i o n : Light Soil: Wt% 35-45 55-65 Wt% 11.0 52.I n d u s t r i a l (L iquid) & Institutional S o i l .0 Wt% 6. sebum and body waste S u r f a c e . body waste.I n d u s t r i a l & I n s t i t u t i o n a l ( Z e o l i t e B u i l t .0 14.04 9.6 .7 1. L i q u i d ) S o i l .06 0.3 ** Rohm 8: Haas S h e l l Chemical Neodol 2 3 .

55 Procedure: 1 . 2 .20 10.300 cps P r o d u c t pH: 7.0 5. Inaredi ent: D I water Carbopol ETD 2623 ( 1 ) C12-15 l i n e a r a l c o h o l .94 Advanced Cleaning Product Formulations Laundry P r e s o o t t e r S p r a y a b l e Gel Carbopol ETD 2623 i s used i n t h i s f o r m u l a t i o n t o c o s t e f f e c t i v e l y t h i c k e n t h e s u r f a c t a n t system i n t o a g e l f o r m . 4 . Add i n t h e sodium h y d r o x i d e u n t i l t h e pH i s a t t a i n e d . U s i n g moderate a g i t a t i o n ( 8 0 0 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i ng and b l e n d i n g o p e r a t i o n s . 3. Total Actives: C12-15 l i n e a r a l c o h o l .0-8. M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous.0 P r o d u c t c l a r i t y : Opaque ( 1 ) BFGoodrich ( 2 ) S h e l l Chemical Co. 3 moles EO ( 2 ) : C12-13 l i n e a r a l c o h o l . Add c o l o r and f r a g r a n c e . 6 .which can be a p p l i e d t o t h e f a b r i c by b r u s h o r sprayed on due to C a r b o p a l ' s shear t h i n n i n g n a t u r e . 5 males €0 ( 3 ) EDTA ( t e t r a sodium s a l t ) Sodium h y d r o x i d e (18%) B r o o k f i e l d v i s c o s i t y (RVT-20 rpm): 8.: ( 3 ) S h e l l Chemical C o .50 0. 3 moles €0 ( 2 ) C12-13 l i n e a r a l c o h o l . Add i n t h e EDTA.75 0.00 0. as d e s i r e d . M i x u n t i l homogeneous. 5 moles EO ( 3 ) : 10. : Neodol 25-3 Neodol 23-6. 5 .0 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-224 .5 83. 6 . Add i n b o t h o f t h e a l c o h o l e t h o x y l a t e s u r f a c t a n t s . d i s p e r s e o r screen t h e Carbopol r e s i n i n t o t h e D I w a t e r .00 5.

Add i n b o t h o f t h e a l c o h o l e t h o x y l a t e s u r f a c t a n t s . 4 . Total Actives: C12-15 l i n e a r a l c o h o l .: Neodol 2 3 . d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e D I w a t e r . Add i n t h e EDTA.50 0. 5 Procedure: I .Laundry Products 95 Laundry Presootter Sorayable L i q u i d Carbopol ETD 2 6 2 3 i s used i n t h i s f o r m u l a t i o n t o s l i g h t l y t h i c k e n t h e s u r f a c t a n t system and e n a b l e t h e p r o d u c t t o s t a y i n c o n t a c t w i t h t h e s o i l l o n g e r b y r e d u c i n g seepage t h r o u g h t h e fabric. 6 . 0 . Add i n t h e sodium h y d r o x i d e u n t i l t h e pH i s a t t a i n e d . C12-13 l i n e a r a l c o h o l . 3 . as d e s i r e d . Mix u n t i l homogeneous.8 .: Neodol 2 5 . 3 moles €0 ( 2 ) C12-13 l i n e a r a l c o h o l . I n s r e d ie n t : D I water Wt% 84.3 ( 3 ) S h e l l Chemical Co.00 0. 3 moles EO: 6 . 2. 5 .0 5. 5 moles €0 ( 3 ) EOTA ( t e t r a sodium s a l t ) Sodi u h y d r o x i d e (18%) m B r o o k f i e l d v i s c o s i t y (RVT-20 P r o d u c t pH: 7 .00 5.15 Carbopol ETO 2623 ( 1 ) C12-15 l i n e a r a l c o h o l . U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s . Add c o l o r s o l u t i o n and f r a g r a n c e .05 10. M i x t h e s l u r r y f o r a p p r o x i m a t e l y 1 5 m i n u t e s o r u n t i l t h e s l u r r y i s homogen- eous. 5 moles EO: 10. 0 P r o d u c t c l a r i t y : Opaque rpm) : 2 5 0 cps ( 1 ) BFGoodri ch ( 2 ) S h e l l Chemical Co.30 0.6 .0 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-220 .

3 . Add C i t r i c A c i d i f pH i s h i g h o r Sodium C i t r a t e i f pH i s l o w .1 2 .70 22.00 C a l foam ES-303 0. 2 . : Suggested F o r m u l a t i o n s . w i t h h o l d 5% o f t h e w a t e r 2 . pH=7.0-7. F o r m u l a t i o n LDL-004-01 SOURCE: P i l o t Chemical C o .45 Water 7. F o r m u l a t i o n LDL-002-01 for C a l s o f t L-60 w i l l lower L i g h t Duty L i q u i d Detergent Weight% Ingredients: 18.35 0. V i s c o s i t y s h o u l d b e 300 c P s .80 Water 70.4 0 Calamide C C a l f o a m EA-603 C a l s o f t LAS-99 Opaci f i e r Sod1 um C i t r a t e Comments a b o u t t h i s f o r m u l a : 1 . S u b s t i t u t i n g C a l s o f t L-40 p r o d u c t s o l i d s t o 42%.10 C i t r i c Acid 0.60 C a l s o f t LAS-99 0.10 Perfume 0.88 0.30 C a l foam EA-603 0.00 C a l s o f t L-60 5. 3 .31 39.50 P i l o t SXS-40 30. Add t h e o p a c i f i e r t o t h e w a t e r p r i o r t o a d d i n g t o t h e detergent.04 t o a d j u s t pH t o 7.00 Calsuds A 10.00 Calamide C 8.10 K a t h o n CG 1. S o l i d s 45%.oo Opaci f ie r Comments a b o u t t h i s f o r m u l a : 1 .06 7.10 7.56 0.2. I f o p a c i f i e r i s t o be added.96 Advanced Cleaning Product Formulations L i g h t Duty L i q u i d Detergent wej-ghs Ingredients: 48.05 Sodium C i t r a t e Comments a b o u t t h i s f o r m u l a : 1 . Add e i t h e r C i t r i c A c i d o r C a l s o f t LAS-99 Weight% 22. F o r m u l a t i o n LDL-001-01 L i s h t Duty Liquid Detergent Ingredients: Water C a l s o f t L-60 P1 l o t s x s .

29 2. Sodium C i t r a t e / C i t r i c A c i d s h o u l d be added f o r pH a d j u s t m e n t t o 7+. I n g r e d i e n t s s h o u l d be added i n t h e o r d e r l i s t e d t o a i d i n blending.00 Weight% 65.43 19.77 SOURCE: P i l o t C h e m i c a l Co : S u g g e s t e d F o r m u l a t i o n s .52 2. F o r m u l a t i o n LDL-006-01 L i g h t Duty L i q u i d Detergent In g r e d i e n t s : Water P i l o t SXS-40 C a l s o f t T-60 C a l foam ES-303 Calamide C P r e s e r v a t iv e S o d i um C h l o r i d e Comments a b o u t t h i s f o r m u l a : V i s c o s i t y 275 cPs. Sol i d ~ = 3 2 .00 2. 3 .00 40.81 0.20 25.16 6. 2.00 Comments a b o u t t h i s f o r m u l a : 1 .00 6. 5 0 % D i e t h a n o l am1 ne C a l s o f t LAS-99 Comments a b o u t t h i s f o r m u l a : S o l 1 ds=30% Good f o r g r e a s y a p p l i c a t i o n s .00 0.2 F o r m u l a t i o n LOI-007-01 L i g h t Duty L i q u i d Detergent Ingredients: Water P i l o t sxs-40 L i n e a r A1 coho1 E t h o x y l a t e NaOH.3 3 % pH=6. S a l t ( S o d i u m o r Ammonium C h l o r i d e ) w i l l r a i s e t h e v i s c o s i t y .Laundry Products 97 L i g h t -Duty L i q u i d Detergent Ingredi ents : Water C a l s u d s CD-6 P i l o t SXS-40 C a l foam EA-603 Cal s o f t LAS-99 Weight% 50.90 5.00 15.00 6.80 10. F o r m u l a t i o n IDL-006-01 Weight% 36.10 1 .

10 1 .10 15.60 5.00 8.10 .98 Advanced Cleaning Product Formulations L i g h t Duty L i q u i d Detergent I n g r e d i ent-sl Water Ammonium C h l o r i d e P i l o t sxs-40 C a l s o f t L-60 Cal foam ES-303 Calamide C C i t r i c Acid P r e s e r v a t iv e Weight% 13.00 0.0.40 4.00 12.oo 0. F o r m u l a t i o n LDL-011-01 L i g h t D u t y L i q u i d Detergent C a l s o f t LAS-99 Based Ingredients: Water NaOH.20 6.10 0.00 0.D u t y L i q u i d D e t e r q e n t C a l s o f t LAS-99 Based Ingredients: Water NaOH. Add C i t r i c A c i d i n p l a c e o f Sodium C i t r a t e t o l o w e r pH. F o r m u l a t i o n LDL-009-01 Ligh-t. 2 . : Suggested F o r m u l a t i o n s Weight% 52.00 0.oo Weight% 43.70 16.50 2.90 2. 50% Cal s o f t LAS-99 Calamide C P i l o t SXS-40 Cal foam ES-303 C a l o x y l a t e N-9 C i t r i c Acid Opaci f ie r Comments a b o u t t h i s f o r m u l a : Add ingredients i n order l i s t e d .80 21.60 44.40 16.80 4.40 19.30 5.10 Comments a b o u t t h i s f o r m u l a : 1 . “ A s i s ” pH=8. F o r m u l a t i o n LDL-012-01 SOURCE: P i l o t Chemical Co.70 3.10 1. 50% C a l s o f t LAS-99 P i l o t SXS-40 Cal foam ES-303 C a l o x y l a t e N-9 C i t r i c Acid Opaci f ie r Preservative Comments a b o u t t h i s f o r m u l a : A d d in g r e d i e n t s i n o r d e r 1 is t e d .

70 2. 50% Alcohol Ethoxyl a t e Calamide C P i l o t SXS-40 Perfume P r e s e r v a t iv e Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .06 49.05 12.00 2.35 10.oo C i t r i c Acid 0. Formul a t i on LDL-014-01 Dry Cleaner: Weight% 54. 3 . 2 .10 Light DutLLCquid D e t e r E n t Pre-Spot-Water S o l u b l e Ingredients: Weight% Water 75. F o r m u l a t i o n LDY-001-01 Li-ght D u t y Li. 4 .13 L i g h t D u t E L i q u j d Detergent Wool Wash We1 g h t % 50.93 I r e d i g nt s : ng Calsuds A Water Comments a b o u t t h i s f o r m u l a : The room t e m p e r a t u r e v i s c o s i t y i s a b o u t 25 c P s . A c l e a r p r o d u c t i s o b t a i n e d when a l l i n g r e d i e n t s a r e m i x e d together.64 0. V i s c o s i t y i n c r e a s e s as C a l o x y l a t e N-9 i s added.50 0.60 16.48 39. Water C a l s o f t LAS-99 NaOH.qu2d D e t e r g e n t Wool _Wash I c g r e d i ents-: C a l s o f t T-60 C a l ami d e CW-100 C a l f o a m ES-303 C i t r i c Acid Comments a b o u t t h i s f o r m u l a : The room t e m p e r a t u r e v i s c o s i t y i s a b o u t 520 c P s .10 Comments a b o u t t h i s f o r m u l a : 1 . F o r m u l a t i o n LDY-004-01 SOURCE: P i l o t Chemical Co.Laundry Products 99 a h t Duty L i q u i d Detergent __ o f t LAS-99 Based Cals Inaredients. Use l e v e l : d i l u t e 8 : l w i t h w a t e r .00 Calamide C C a l o x y l a t e N-9 11.10 0.30 4. : Stiggested F o r m u l a t i o n s .20 Perfume & C o l o r 0. F o r m u l a t i o n LDY-002-01 -- Wei g h t % 14. Add i n g r e d i e n t s i n o r d e r 1 i s t e d .15 5.00 C a l i mu1 s e PRS 11 . D e t e r g e n t f r a g r a n c e R-1264 can be used i n t h i s f o r m u l a .

Inc. Blend until homogeneous between each addition.5 Procedure: Add components in the order listed.100 Advanced Cleaning Product Formulations Two Part Industria1 Laundry Deteraents Break Formulations Hi q h l v A 1 kal ine Break Components: Water Burcosperse LP Burcolite BSGH-255 Dequest 2000 50% NaOH Mixed Builder Break Components: Water 45% KOH Burcosperse LP TKPP Sodi um Si 1 i cate (Star Grade) % % by Weight 5 10 5 5 75 by Weight 40.: Suggested Formulations .0 10.0 12..85 Procedure: Add components in the order listed.65 5.50 11. Blend until homogeneous between each addition.0 27. Detergent Additive Components: Water Burco NPS-816 Neodol 25-7 Dodecylbenzenesulfonic Acid TEA-85 % by Weight 60.00 12.00 10. Use Level: Break: 4-12 ounces/100 pounds Detergent: 2-4 ounces/100 pounds SOURCE: Burlington Chemical Co. Keep temperature below 160F during bl endi ng.5 10.

3 c y c l e s : pass C o l d s t o r a g e @ 4 deg. 43.8 Q . Ethoxylate. s t o r a g e @ 50 deg.0 5.0 M i x i n g Procedure: Charge w a t e r and MC-48 and m i x . f r a g r a n c e & dye M i x i n g Procedure: Combine A l p h a .S t e p MC-48 46. Add 30-LL and m i x u n t i l homogeneous. Add sodium c h l o r i d e t o t h i c k e n . as i s : 7 . t o 100.0 W a t e r .S t e p MC-48.S t e p MC-48 29. C. A d j u s t p H w i t h c a u s t i c soda o r c i t r i c a c i d i f n e c e s s a r y . F o r m u l a t i o n N o . H e a t t o a p p r o x i m a t e l y 50 deg.4 A l p h a .6 Appearance: C l e a r . F o r m u l a t i o n No. l b s / g a l : 0. a l c o h o l e t h o x y l a t e and w a t e r w h i l e m i x i n g u n t i l s o l u t i o n i s homogeneous. Properties: Appearance: C l e a r y e l l o w l i q u i d pH.0 N i n o l 30-LL 4. D . Comment : The s u r f a c t a n t s used i n t h i s f o r m u l a t i o n a r e d e r i v e d f r o m o l e o c h e m i c a l r e s o u r c e s and a r e b i o d e g r a d a b l e .Laundry Products 101 U l t r a L i q u i d Laundrv Deterqent Ingredients: Wt% A l p h a . 658 F i n e F a b r i c Wash Ingredients: Wt% Water.5 3A A l c o h o l P r o p y l ene G1 y c o l 5. C. 0 F r e e z e / t h a w . %: 2 9 . S . A d j u s t pH w i t h s u l f u r i c a c i d o r sodium h y d r o x i d e as n e c e s s a r y . A l l o w m i x t u r e t o c o o l t o room t e m p e r a t u r e and add t h e r e m a i n i n g i n g r e d i e n t s w i t h m i x i n g . C. I . : Suggested F o r m u l a t i o n s .0 Sodi urn 01e a t e Alcohol. add sodium o l e a t e and m i x u n t i l s o l u t i o n and i s a g a i n homogeneous. 1 week: p a s s Density. c p s : 220 S o l i d s .6 Sodi um c h l o r i d e 6. 1 week: p a s s H i g h temp.3 0. p r o p y l e n e g l y c o l . 358 SOURCE: Stepan C o . 5 V i s c o s i t y @ 25 deg. C.6 Use I n s t r u c t i o n s : Use s m a l l amount f o r hand w a s h i n g o r 1 / 4 cup f o r machine washing.0 Borax 1. l i g h t y e l l o w 1 q u i d Use I n s t r u c t i o n s : Use 1 / 3 c u p p e r n o r m a l s i z e w a s h l o a d Comment: A l p h a .S t e p MC-48 i s an e x c e l l e n t oap s o l u b i l i z e r t h a t c a n make h i g h soap l e v e l s p o s s i b l e i n f i n i s h e d p r o d u c t s .0 PVP K-15 0. 7 19. Typical Formulation Properties: F o r m u l a t i o n D e s c r i p t i o n : SME/Soap Based HDL pfl: 8-10 V i s c o s i t y : 200-350 c p s Density: 8.

9. Metal Cleaners and Polish .

8 15.S. *U.T. m i x i n g w e l l a f t e r each a d d i t i o n u n t i l smooth and un f o r m ( a v o i d i n c o r p o r a t i o n o f a i r ) .0 10. I n c . f r e e f l o w i n g c l e a n e r w i t h good v e r t i c a l s u r f a c e c l i n g . Suggested P a c k a g i n g : P l a s t i c squeeze b o t t l e w i t h p r e c a u t i o n a r y labeling f o r acid.0 A: 6: T e t r a s o d i u m EDTA 1 . Veegum and Rhodopol p r o v i d e s y n e r g i s t i c t h i c k e n i ng w i t h b e t t e r v i s c o s i t y s t a b i l i t y and i n h i b i t i o n o f s y n e r e s i s t h a n i s p o s s i b l e w i t h e i t h e r t h i c k e n e r a l o n e . 392 D i ppi ns C1 e a n e r f o r S i 1v e r Ingredients: Z u s o l a t 1008/85 Thiourea Hydrochloric acid Water 2. : . 4. Diatomaceous E a r t h p r o v i d e s good c l e a n s i n g and p o l i s h i n g ..H y d r o x y e t h y l .8 0.5 F o r m u l a t i o n CT 0 2 .1 0.0 3.253 SOURCE: R.0 86.0 2 SOURCE: Zschimmer & Schwarz GmbH & C o .Metal Cleaners and Polishes 103 Acid Metal Cleaner* The c o m b i n a t i o n o f Veegum and Rhodopol 2 3 suspends t h a a b r a s i v e and p r o v i d e s a s t a b l e . : F o r m u l a t i o n No.1 5 .2 .4 72. pourable l i q u i d . T e t r a s o d i u m EDTA f a c i l i t a t e s t h i s exchange. V a n d e r b i l t Co. P a t e n t No.9 0. Inqredients: Veegum Rhodopol 23 Water y & 0.302. Veegum i s p r o t e c t e d a g a i n s t f l o c c u l a t i o n i n t h i s pH 1 c o m p o s i t i o n t h r o u g h base exchange w i t h t h e i m i d a z o l i n e . Consistency: White. Add B i n g r e d i e n t s i n o r d e r . C o n t i n u e m i x i n g u n t i l smooth.5 8.c a p r y l i m i d a z o l i ine Phosphoric a c i d Diatomaceous E a r t h Procedure: S l o w l y add them t o t h e w a t e r w h i l e B l e n d Veegum and Rhodopol a g i t a t i ng a t maximum a v a i 1ab e s h e a r .

104

Advanced Cleaning Product Formulations

A1 umi num C1 e a n e r / B r i g h t e n e r T r a d i t i o n a l l y , a n i o n i c s u r f a c t a n t s have o f f e r e d b e t t e r d e t ergency t h e n n o n i o n i c s , b u t were n o t c o m p a t i b l e i n a c i d systems. T h i s f o r m u l a t i o n uses Avanel S - 7 0 , an a n i o n i c m o l e c u l e w h i c h p e r f o r m s even a t v e r y low p H ' s and a i d s i n t h e removal o f s u r f a c e o i l s and d e p o s i t s . U n l i k e n o n i o n i c s , Avanel 5-70 w i l l d i s s o l v e r e a d i l y i n t o the formulation without forming gel p a r t i c l e s thus e l i m i n a t i n g t h e need f o r e x c e s s i v e a g i t a t i o n . T h i s f o r m u l a t i o n can be used f o r o v e r - t h e - r o a d aluminum t r a i l e r s , w i r e wheels on a u t o m o b i l e s o r i n t h e p r e p a r a t i o n o f aluminum f o r a n o d i z i n g and c l eani ng. Inqredients: Dei o n i zed Water Phosphoric A c i d ( 8 5 % ) C i t r i c Acid (50%) N i t r i c Acid (70%) Avanel S-70

Wt%
83.0 6.0

8.0

1.o

2.0

Procedure: Charge t h e w a t e r t o a m i x i n g v e s s e l . Under slow a g i t a t i o n and w i t h due c a r e , add t h e a c i d s t o t h e w a t e r . Add t h e Avanel S - 7 0 and m i x 10 m i n u t e s . NOTE: I f a d d i t i o n a l b r i g h t e n i n g i s r e q u i r e d , t h e n i t r i c a c i d c o n c e n t r a t i o n may be i n c r e a s e d t o 1 . 5 % . F o r m u l a t i o n CM-101 Powdered M e t a l C l e a n i n g C o n c e n t r a t e I n a r e d ients: Sodi u H y d r o x i d e m Sodium Carbonate STPP Avanel 5-70 Procedure: Add i n g r e d i e n t s as l i s t e d . A1 u m i num C1 eaner Ingredients: D e i o n i z e d Water Avanel S - 7 0 T e t r a p o t a s s i u m Pyrophosphate Sodium M e t a s i l i c a t e P e n t a h y d r a t e C a r b i t o l Solvent
85.0 6.0

Wt%
58.5

13.5
20.0 8.0

5.0 1.o

3.0

Procedure: Charge v e s s e l w i t h i n g r e d i e n t s i n t h e o r d e r l i s t e d u s i n g mode r a t e a g i t a t i o n . NOTE: Other Avanel p r o d u c t s c o u l d be used i n t h i s f o r m u l a t i o n t o achieve d i f f e r e n t s u r f a c t a n t c h a r a c t e r i s t i c s .

SOURCE:

P G Industries, P

I n c . : Suggested F o r m u l a t i o n s

Metal Cleaners and Polishes

105

A1 umi num C l e a n e r C o n c e n t r a t e F-498

UhWeight
Water Sodium M e t a s i l i c a t e (Anhydrous) T e t r a Potassium Pyrophosphate (Powder) Mona NF-10
75 10 5 10

Procedure: D i s s o l v e sodium m e t a s i l i c a t e and t e t r a p o t a s s i u m p y r o p h o s p h a t e i n w a t e r w i t h m i x i n g , t h e n add Mona N F - 1 0 . Typical Properties: Appearance : C l e a r 1 iq u i d Cloud P o i n t : 8 8 C Recommended Use D i l u t i o n : 1 t o 4 o z / g a l Aluminum Wash F-499
% By Weiaht

Water Sodium M e t a s i l i c a t e (Anhydrous) T e t r a Sodium Pyrophosphate (Powder) B u t y l Carbi t o 1 Mona N F - I 0

88
2

3 2 5

Procedure: D i s s o l v e sodium m e t a s i l i c a t e and t e t r a sodium p y r o p h o s p h a t e i n w a t e r , t h e n add B u t y l C a r b i t o l and Mona NF-10. Typical Properties: Appearance: C l e a r 1 iq u i d pH: 1 2 . 8 Recommended Use D i l u t i o n : 1 : l O w i t h water

SOURCE: Mona I n d u s t r i e s , I n c . :

Suggested F o r m u l a t i o n s

106

Advanced Cleaning Product Formulations

B u f f i nq Compound Remover Component: Water TEA B u r c o t r o p e 1250 B u r c o s p e r s e LP Borax B u r c o TME B u r c o LAF-6 Add components i n o r d e r l i s t e d . each a d d i t i o n .

%
42.5 20.0 12.5 12.5 5.0 5.0 5.0 B l e n d u n t i l homogeneous between

H o t A1 k a l in e P a i n t S t r i p p e r C o n c e n t r a t e

Compo n e n t s : 45% KOH K a s i l #1 B u r c o HCS-50 NF Add components i n t h e o r d e r l i s t e d . between each a d d i t i o n . SOURCE: B u r l i n g t o n Chemical

a
67 32 1

B l e n d u n t i l homogeneous

Co.,

I n c . : Suggested F o r m u l a t i o n s

M e t a l De-Oi 1 in g L i q u i d C o n c e n t r a t e (Liquid) S o i l - Petroleum-based o i l S u r f a c e - M e t a l : S t e e l , c o p p e r , aluminum, e t c . A p p l i c a t i o n Method - Spray a n d / o r i m m e r s i o n Manufacture - Mix tank w i t h p r o p e l l e r s t i r r e r Composi t i on : Water Starso EDTA, T e t r a s o d i u m ( 3 7 % ) Sodi um X y l ene S u l f o n a t e ( 4 0 % ) C9-C11 L i n e a r A l c o h o l , 6 Moles EO C9-C11 L i n e a r A l c o h o l , 2.5 M o l e s EO Use D i l u t i o n : 2%-4% b v SOURCE: The

wtu/,
42.0 12.0 16.0 20.0 3.0

7.0

PQ C o r p . : Suggested F o r m u l a t i o n

Metal Cleaners and Polishes

107

Cutting O i l

Monalube 215 p r o v i d e s e x c e l l e n t l u b r i c i t y , and e x t r e m e p r e s s u r e p r o p e r t i e s . T h i s f o r m u l a t i o n i s used i n machining, stamping and d r a w i n g f e r r o u s and n o n f e r r o u s m e t a l s . Wt% Innredients: 100 P a l e O i l 95.0 Monalube 215 5.0 Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. Typical Properties: Appearance: C1 e a r Amber L i q u i d V i s c o s i ty/4OC: 24 CS Performance Data: Fa1 ex ( D i r e c t S c a l e ) : 2000 Lbs. /56 I n . -Lbs Draw Bead E f f i c i e n c y : 95 Draw Bead E f f i c i e n c y R e f e r e n c e O i l : 115 Formul a t ion F-791

.

Cutting O i 1

Inqredients: 100 P a l e O i l 90.0 Monalube 205 5.0 Monalube 215 5.0 Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. Typical Properties: Appearance: C l e a r Amber L i q u i d V i s c o s i t y ( 4 0 C ) : 25 CS Fa1 e x : 2250 Lbs / 6 0 I n . -Lbs Appl i c a t i ons: F o r machi n i ng s t a m p i n g and d r a w i n g . F o r m u l a t i o n F-792

.

.

Cutting O i l

Wt% Inqredients: 85.0 100 P a l e O i l Monalube 205 5.0 Monalube 215 5.0 5.0 Monalube 225 Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. Typical Properties: Appearance: C1 e a r Amber L i q u i d V i s c o s i t y / 4 0 C : 30 CS Performance Data: F a l e x ( D i r e c t S c a l e ) : 2750 L b s . / 7 0 I n . . - L b s . Draw Bead E f f i c i e n c y : 90 Draw Bead E f f i c i e n c y R e f e r e n c e O i l : 115 Appl i c a t i ons: Heavy d r a w i n g and s t a m p i n g F o r m u l a t i o n F-793 SOURCE: Mona I n d u s t r i e s , I n c . : Suggested F o r m u l a t i o n s

108

Advanced Cleaning Product Formulations

Cutting O i l
Ingredients: 100 P a l e O i l Monalube 215 Monalube 225
% &

90.0 5.0 5.0

Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. T y p i c a l P r o p e r t ie s : Appearance: C l e a r Amber L i q u i d V i s c o s i t y 40C: 27 CS Performance D a t a : F a l e x ( D i r e c t S c a l e ) : 2500 Lbs./6O I n . - L b s . Draw Bead E f f i c i e n c y : 90 Draw Bead E f f i c i e n c y R e f e r e n c e O i l : 115 Formul a t ion F-794 Cuttina O i l Insredients: 100 Pale O i l Monalube 225

WtO/o
95.0 5.0

Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. Typical Properties: Appearance: C1 e a r Amber L i q u i d V i s c o s i t y 40C: 24 C S Performance D a t a : F a l e x ( D i r e c t S c a l e ) : 2750 Lbs./6O I n . - L b s . Draw Bead E f f i c i e n c y : 90 Draw Bead E f f i c i e n c y R e f e r e n c e O i l : 115 Formul a t ion F-795 Cutting Oi1 Inqredients: 100 P a l e O i l Monalube 215 Monalube 325

Wt%
90.0 5.0 5.0

Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C. Typical Properties: Appearance: C l e a r Dark Brown L i q u i d V i s c o s i t y 40C: 22 CS P e r f o r m a n c e Data: F a l e x ( D i r e c t S c a l e ) : 2250 L b s . / 5 5 I n . - L b s . F o r m u l a t i o n F-796 SOURCE: Mona I n d u s t r i e s , Inc.: Suggested F o r m u l a t i o n s

E m u l s i o n .77 2. S o l u b l e O i l .3 TEA.D i l u t e 4 : 7 6 w i t h 160 ppm h a r d w a t e r .60 5.D i l u t e 1 : 3 w i t h 100 SUS n a p h t h e n i c o i l .50 8. Add t h e P r o p y l e n e G l y c o l l a s t .04 61. 3 .10 1. Add t h e w a t e r SLOWLY.D i l u t e 4 : 7 6 w i t h 1 6 0 ppm h a r d w a t e r .98 2.48 Comments a b o u t t h i s f o r m u l a : 1 .60 20. e x c e p t t h e P r o p y l e n e G l y c o l . F o r m u l a t i o n SOL-001-01 Cutting O i 1 C o n c e n t m e I ny.20 0.80 21.Metal Cleaners and Polishes 109 Cutting O i l s Semi-Synthetic-Cutting Ingredients: A r i s t o n a t e M-LF Oleic Acid TEA P r o p y l ene G l y c o l Water Oi1 Wei q h t % 17.50 Comments a b o u t t h i s f o r m u l a : 1 . 2 .. 2 . 45% O l e i c A c i d . Emersol 2 1 3 O l e i c A c i d Diethylene Glycol Water Wei g h t % 60. F o r m u l a t i o n SOF-001-01 C u t t i n g O i 1 Concentrate Ingredi ents: Aristonate M D r e s i n a t e 91 I g e p a l CO-430 KOH. 2 .10 2.25 8. M i x a l l of t h e i n g r e d i e n t s .25 7. : Suggested F o r m u l a t i o n s .60 4. S o l u b l e O i l . 85% Oleic Acid D i e t h y l ene G1 y c o l Water Weight% 51.50 8.75 15.D i l u t e 1 : 3 w i t h 1 0 0 SUS n a p h t h e n i c o i l .00 Comments a b o u t t h i s f o r m u l a : 1 . F o r m u l a t i o n SOL-002-01 SOURCE: P i l o t Chemical Co. E m u l s i o n .edie n t s : Aristonate M Neodol 2 5 .

Typical Properties: Appearance: C l e a r amber l i q u i d S p e c i f i c G r a v i t y : 1 . Typical Properties: Appearance: C1 e a r L i q u i d F o r m u l a t i o n F-784 SOURCE: Mona I n d u s t r i e s . 2 p H o f a 1:10 s o l u t i o n : 9 .I 10 Advanced Cleaning Product Formulations G e n e r a l Purpose Machine C l e a n e r T h i s i s an e x c e l l e n t a l l .00 4.50 M i x we1 1 The f o l l o w i n g f o r m u l a t i o n uses Monamulse 653-838 as an emuls i f i e r i n a m i l i t a r y s p e c i f i c a t i o n (MIL-C-855706) f o r m u l a t i o n .8 Hycar 1422 10.00 I .1 P l u r o n i c F98 1.5 3.7 Water 55.06 pH C o n c e n t r a t e : 1 0 .00 6.6 P a r t B: T r i s o d i u m Phosphate (Dodecahydrate) 2. 8 Recommended Use D i l u t i o n : 1 : 1 0 w i t h w a t e r Cast I r o n B l o c k : Pass Corrosion Test: 1:10 D i l u t i o n F o r m u l a t i o n F-770 A i r c r a f t C l e a n e r Type I V 69.50 6.00 10.00 3. Add P a r t B t o P a r t A .7 7.p u r p o s e c l e a n e r f o r c l e a n i n g a l l t y p e s o f f e r r o u s p a r t s and machine s u r f a c e s .6 Procedure: Add i n g r e d i e n t s o f P a r t A & P a r t 8 s e p a r a t e l y w i t h a g i t a t i o n .5 1.: Suggested F o r m u l a t i o n s . Inaredient: P a r t A: Monamulse 653-0313 Monami ne 1-76 A r o m a t i c 150 Isopar M (Odorless Mineral S p i r i t s ) Diethylene Glycol Butyl Ether Decanol vvts/. Monacor 4000 i s i n c o r p o r a t e d f o r added c o r r o s i o n p r o t e c t i o n . Inc. 7.5 7. I gredients : n Water T r i e t h a n o l a m i ne Monacor 4000 Monami ne CF-1 OOM M o n a t e r i c CyNa-50 T e t r a s o d i u m EDTA (40%) T r i a d i n e 10 ( P r e s e r v a t i v e ) Procedure: Mix t h e i n g r e d i e n t s i n o r d e r a t ambient temperature. A g i t a t e u n t i l u n i f o r m . between each a d d i t i o n a t moderate speed.0 2.

2 . Copper M a c h i n i n a F l u i d Ingredients: Macol 5100 Mazon R I 6 Maphos 8135 Potassi u Hydroxide m B i o c i de Water Procedure: Add i n g r e d i e n t s as l i s t e d .0 6.5 2. 2. Add i n g r e d i e n t s as l i s t e d .0 8. 85% B i o c i de Water Wt96 5.5 Balance Procedure: 4 . : Suggested F o r m u l a t i o n s . 85% 8 i o c i de Water Wt% 38. The c o n c e n t r a t e s h o u l d be f u r t h e r d i l u t e d f r o m 1:lO (heavy d u t y ) t o 1:40 ( l i g h t d u t y ) w i t h water t o form a ready-to-use f l u i d . For i n c r e a s e d l u b r i c i t y i n c r e a s e t h e amount o f l u b r i c a n t o r extreme p r e s s u r e a d d i t i v e . For increased and s t a i n p r o t e c t i o n . Wt% 15.0 12.5 10. T h i s f l u i d i s f o r f e r r o u s m e t a l s . The c o n c e n t r a t e s h o u l d be f u r t h e r d i l u t e d f r o m 1:lO (heavy d u t y ) t o 1:40 ( l i g h t d u t y ) w i t h water t o form a ready-to-use f l u i d .5 Balance SOURCE: PPG I n d u s t r i e s .0 0.0 0. For i n c r e a s e d l u b r i c i t y i n c r e a s e t h e amount o f l u b r i c a n t o r extreme p r e s s u r e a d d i t i v e . For increased r u s t and s t a i n p r o t e c t i o n .0 8. I n c . General Purpose S y n t h e t i c F l u i d (BZ Ingredients: M a s l i p 500 Mazon R I 8 B P r o p y l ene G y c o l 1 T o l y t r i a z o l e (Climax) T r i e t h a n o l a m i ne.0 12.Metal Cleaners and Polishes 111 General Purpose S y n t h e t i c F l u i d ( A ) Ingredients: M a s l i p 501 Bas= Maphos 8135 Mazon R I 4 A T r i e t h a n o l a m i n e . Add i n g r e d i e n t s as l i s t e d . T h i s f l u i d i s f o r f e r r o u s m e t a l s .5 Balance Procedure: 1 .0 0.0 2. i n c r e a s e t h e amount o f Mazon R I 8 B . i n c r e a s e t h e amount o f Mazon R I 4 A .0 7.0 8.

The c o n c e n t r a t e s h o u l d b e f u r t h e r d i l u t e d f r o m 1:lO ( h e a v y d u t y ) t o 1 : 4 0 ( l i g h t d u t y ) w i t h water t o form a ready-to-use f l u i d . i n c r e a s e t h e amount o f Mazon R I 8 A .: Suggested F o r m u l a t i o n s . T h i s f l u i d i s f o r f e r r o u s m e t a l s .0 12.0 0. G e n e r a l Purpose S y n t h e t i c F l u i d ( D ) I n s r e d ients: M a s l i p 501 Base Mazon R I 8 A Maphos 8135 T r i e t h a n o l ami n e . SOURCE: PPG I n d u s t r i e s . F o r i n c r e a s e d l u b r i c i t y i n c r e a s e t h e amount of l u b r i c a n t o r extreme pressure a d d i t i v e .5 5al ance Procedure: 1. T h i s f l u i d i s f o r f e r r o u s m e t a l s . Add i n g r e d i e n t s as l i s t e d . 2 .0 12. B i o c i de Water Mle9/0 30. B i o c i de Water Wt% 12.0 0. i n c r e a s e t h e amount o f Mazon R I 8 8. The c o n c e n t r a t e s h o u l d b e f u r t h e r d i l u t e d f r o m 1 : l O (heavy d u t y ) t o 1 : 4 0 ( l i g h t d u t y ) w i t h water t o form a ready-to-use f l u i d . For increased r u s t and s t a i n p r o t e c t i o n .0 25.5 5 a l ance 85% Procedure: 1 . Add i n g r e d i e n t s as l i s t e d . F o r i n c r e a s e d l u b r i c i t y i n c r e a s e t h e amount o f l u b r i c a n t o r extreme pressure a d d i t i v e .112 Advanced Cleaning Product Formulations G e n e r a l Purpose S y n t h e t i c F l u i d ( C ) Ingredients: M a s l i p 501 A Mazon R I 8 B Maphos 58 T r i e t h a n o l ami ne. Inc.0 6.0 5.0 85% 7. For increased r u s t and s t a i n p r o t e c t i o n . 2 .

0 Use: Heavy d u t y l o w .0 30.0 3.5% bw ( 1 .2 o z / g a l l o n ) ** FMC O l i n P o l y t e r g e n t S-305LF o r Rhone-Poulenc I g e p a l CO-530 A1 umi num C1 e a n e r (Phosphate.Metal Cleaners and Polishes 113 Metal Cleaner (Phosphate.0 * ** *** FMC Rohm 8 Haas A c u s o l 445ND (92% s o l i d s ) .036 bw ( 2 . Use D i l u t i o n : 0.8-1.0 5. : D e t e r g e n t F o r m u l a t i o n Guide SOURCE: .5-3. Powder) Soi 1. Powder) Soi 1 -Drawing l u b r i c a n t .f o a m i n g m e t a l c l e a n e r w h i c h i s good f o r a spray c l e a n i n g process.0 30.0 2.4 o z / g a l ) Wt% 45. Rhone-Poul enc I g e p a l CA-630 PQ C o r p .0 20.0 30.L i g h t d r a w i n g o i 1 Surface-Aluminum A p p l i c a t i o n Method-Spray washer M a n u f a c t u r e .0 25. a n i m a l f a t and g r e a s e Surface-Steel A p p l i c a t i o n Method-Spray M a n u f a c t u r e .D r y b l end/Aggl o m e r a t i on Composi t i on : Metso Beads 2048 *STPP *Sodi um B i c a r b o n a t e **Sodium P o l y a c r y l a t e * * * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l . 9-10 Moles EO Use D i l u t i o n : 1.D r y b l e n d / A g g l o m e r a t on Composi t i on : *STPP *Sodi um C a r b o n a t e **Alkoxylated l i n e a r alcohol nonion c s u r f a c t a n t ( 1ow foam) Metso Beads 2048 Sodi um H y d r o x i d e Beads 10.

0 * ** FMC Rhone-Poulenc I g e p a l CA-630 M e t a l C1 eaner (Phosphate.0 28.0 * Rhone-Poulenc I g e p a l CA-720 SOURCE: P C o r p .0 30.4 . animal f a t and g r e a s e Surface-Steel A p p l i c a t i o n Method-Immersion/electrolytic c l e a n i n g Manufacture-Dry blend/Agglorneration Com o s i t i o n : TSPF TSP Metso Beads 2048 Sodium C a r b o n a t e * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l (12-13 Moles EO) Sodium H y d r o x i d e Beads Use D i l u t i o n : 2 .0 2.0 15. 5 % bw ( 3 .6 o z / g a l l o n ) 20.114 Advanced Cleaning Product Formulations M e t a l C1 e a n e r (Phosphate.0 40.4 . d r a w i n g l u b r i c a n t . Powder) S o i l . 3 .O i l . d r a w i n g l u b r i c a n t .0 2. Powder2 S o i l . : D e t e r g e n t F o r m u l a t i o n Guide O . 5 % bw ( 3 . a n i m a l f a t and g r e a s e Surface-Steel A p p l i c a t i o n Method-Immersion ManufacturekDry blend/Agglomeration Composi t i o m *Sodium C a r b o n a t e *STPP **Octylphenoxy Polyethoxyethanol ( 6 Moles € 0 ) Metso Beads 2048 Sodi um H y d r o x i d e Beads Use D i l u t i o n : 2 .6 o z / g a l ) Wt% 15. 3 .0 5.O i l .0 35.0 8.

0 2.0 38. Metal Cleaner Powder 1 S o i 1 .mposition Co 3 M o l e s EO) 40. f a t . p r o t e i n Surface-Stai nless s t e e l A p p l i c a t i o n Method-Cleaning i n p l a c e Manufacture-Dry blend/Agglomeration Composi t i o n A : *STPP *Sodium C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl3.0 20.0 3.0 2. Powder) S o i 1-Oi 1 . d r a w i n g l u b r i c a n t . 0 % bw ( 2 .0 45. : .0 25.0 12.D r y b l e n d / A g g l o r n e r a t i on n : Composi t i o V a l f o r 100 Z e o l i t e A Sodium C a r b o n a t e * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l (9-10 Moles E O ) Metso Pentabead 20 A c u s o l 445ND Sodi um P o l y a c r y l a t e Use L e v e l : 3-6 o z / g a l l o n g WtO/o 15.0 12.0 i 1.0 43.0 Rhone-Poulenc I g e p a l CA-630 Detergent F o r m u l a t i o n Guide SOURCE: PB C o r p .4 o z / g a l l o n ) * ** FMC Rhone-Poluenc R h o d a s u r f A-24 M e t a l C1 e a n e r ( Z e r o Phosphate. M e t s o Beads 2048 Sodi um H y d r o x i d e Beads .0 0: *STPP *Sodium C a r b o n a t e * * L i q u i d N o n i o n i c S u r f a c t a n t (C12-Cl3.3 . Metso Pentabead 20 Use D i l u t i o n : WtO/o 3 Moles EO) 40. 5 .0 3.Metal Cleaners and Polishes 115 I Phosphate.0 1 . animal f a t and g r e a s e Surface-Steel A p p l i c a t i o n Method-Immersion M a n u f a c t u r e .

w h i t e l i q u i d S p e c i f i c G r a v i t y : 1. and t h e dye added t o t h i s w a t e r w i t d i s s o l v e d dye can t h e n be added t o t h e b a t c h .0 3. Ifdye i s t o be added. w a t e r . c h a r g e t h e r e m a i n i n g i n g r e d i e n t s . b e t t e r c o n t a c t between t h e aluminum s u r f a c e and t h e o r g a n i c a c i d s . F o r m u l a t i o n CM-1034 87. g l u c o n c a c i d and Avanel S . 50% Avanel S-70 D e i o n i z e d Water. NOTE: C e r t a i n dyes may n o t be s t a b l e under t h e s e c o n d i t i o n s .0 1. I n c .o 3.e-l 12. : Suggested F o r m u l a t i o n s . t h i s p r o d u c t may be used i n a D r e s s u r e wash. T h i s f o r m u l a t i o n may b e c u t -!:I w i t h water t o prepare a m i l d hard-surface c l e a n e r .1 2 . c i t r i c a c i d . pump s p r a y o r d i p tank.f r e e aluminum c l e a n e r t h a t p r o v i d e s e x c e l 1e n t c l e a n i ng and b r i g h t e n i ng o f a1 umi num.t h e .7 0 M i x w e l l . windows and door f i x t u r e s . p h o s p h a t e . Depending on t h e a p p l i c a t i o n . 50% G l u c o n i c A c i d . C o n t i n u e m i x i n g f o r a t l e a s t 15 m i n u t e s . Consequently. NOTE: T h i s a l k a l i n e aluminum c l e a n e r has shown e x c e l l e n t c l eani ng p r o p e r t i e s w i t h o u t c h e m i c a l a t t a c k o f t h e m e t a l .7 0 p r o v i d e s f o r removal o f o r g a n i c s u r f a c e d e p o s i t s and. 5 .05 Procedure: Charge t h e w a t e r and d i s s o l v e t h e b u i l d e r s a l t s under a g i t a t i o n . I n a d d i t i o n t o i n d u s t r i a l a p p l i c a t i o n s l i k e c l e a n i n g o v e r . p a r t o f t h e w a t e r s h o u l d be he d good a g i t a t i o n . The Avanel S .0 4. The o u t .0 8.0 SOURCE: PPG I n d u s t r i e s .0 5.116 Advanced Cleaning Product Formulations Non-Phosphorous Aluminum C l e a n e r T h i s i s a t o t a l l y o r g a n i c . Inqredients: C i t r i c A c i d . s h e l f s t a b i l i t y t e s t s s h o u l d be p e r f o r m e d .r o a d aluminum t r a i l e r s and aluminum p r i o r t o a n o d i z i n g . 5 Appearance: C l e a r . by s u r f a c e t e n s i o n r e d u c t i o n .0 Balance Procedure: Charge t h e w a t e r . Dye w. F o r m u l a t i o n CM-102 A 1 k a l ine A1 u m i num C1 eaner I n a r e d ie n t s : Dei o n i zed Water Avanel S .7 0 T e t r a p o t a s s i u m Pyrophosphate Sodium M e t a s i l i c a t e P e n t a h y d r a t e Macol 48 pH ( a s i s ) : 1 1 . t h i s c l e a n e r may also be used i n household a p p l i c a t i o n s such as c l e a n i n g aluminum f l a s h i n g . When d i s s o l v e d .

. Formul a t ion F-800 SOURCE: Mona I n d u s t r i e s . 5% o f c o n c e n t r a t e t o 95% w a t e r f o r m s m i c r o e m u l s i o n . /50 I n . and 6 .0 9.5. and 3 u n t i l c l e a r .L b s .6 Procedure: M i x i t e m s 1. Cast I r o n B l o c k C o r r o s i o n T e s t : Pass Appearance: C l e a r pH: 9 .0 58. 6 F o r m u l a t i o n F-797 Semi S y n t h e t i c InQredients: 100 P a l e O i 1 Monalube 320 Monalube 610 Monalube 220 T r i e t h a n o l a m i n e (99%) Monacor BE Water wt9j0 9./45 I n .6 9.0 13.Metal Cleaners and Polishes 117 Semi S y n t h e t i c T h i s f o r m u l a t i o n i s p a r t i c u l a r l y u s e f u l f o r heavy m a c h i n i n g and l i g h t d r a w i n g f o r f e r r o u s and s t a i n l e s s s t e e l . T y p i ca9 P r o p e r t i es : Appearance : C1 e a r Amber L i q u i d Performance Data ( 5 % i n Water): Appearance: C l e a r L i q u i d pH: 9.: Suggested F o r m u l a t i o n s .8 0.0 wt9j0 9.6 1. . F o r m u l a t i o n c a n be u s e d f o r g r i n d i n g and l i g h t m a c h i n i n g .2 5.5 S u r f a c e T e n s i o n (dynes/cm): 32 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 Lbs. Add i t e m s 4.0 13.8 3.0 58.6 0. Ingredients: 100 P a l e O i l Monalube 320 Monalube 610 Monalube 205 Monalube 215 T r i e t h a n o l ami ne (99%) Monacor BE Water Procedure: Combi ne i n g r e d i e n t s w i t h a g i t a t i o n .2 5.6 3.L b s .2. Inc. Typical Properties: Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Fa1 ex ( D i r e c t S c a l e ) : 2500 L b s .

5 25.6 Procedure: M i x i t e m s 1 .0 58.: Suggested F o r m u l a t i o n s .0 5. / 5 5 I n . -Lbs F o r m a c h i n i n g l i g h t s t a m p i n g and d r a w i n g .0 13.6 1. 5% o f c o n c e n t r a t e added t o w a t e r f o r m s m i c r o e m u l s i o n .6 3. and 3 u n t i l c l e a r . /57 I n .2 5.0 9. -Lbs F o r m u l a t i o n F-801 .5 . SOURCE: Mona I n d u s t r i e s .I18 Advanced Cleaning Product Forniulations Semi S y n t h e t i c Inaredients: 100 P a l e O i l Monalube 225 TEA Monalube 610 Water Typical Properties: Appearance: C 1 e a r Amber L i q u i d Performance Data ( 5 % i n w a t e r ) : Appearance: C1 e a r L i q u i d pH: 9 . F o r m u l a t i o n F-799 Semi S y n t h e t i c Inqredients: 100 P a l e O i l Monalube 320 Monalube 610 Monalube 205 T r i e t h a n o l a m i n e (99%) Monacor BE Water y& 10. 2.0 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1 e x ( D i r e c t S c a l e ) : 2500 L b s . Inc. Wt% 9.0 47. 0 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1 ex ( D i r e c t S c a l e ) : 2750 Lbs.5 Surface Tension: 27. Typical Properties: Appearance: C l e a r Amber L i q u i d Performance Data ( 5 % i n Water): Appearance: C l e a r L i q u i d pH: 9. Add i t e m s 4 and 5 t h e n 6 . S u g g e s t e d f o r g r i n d i n g and m a c h i n i n g f o r b o t h f e r r o u s and n o n f e r r o u s metals.5 7.

50 Product C l a r i t y : P a s t e 1 .48 0. Procedure: 4 .00 1 0 .00 2. t o become permanently suspended The r e s i n a1 so p r e v e n t s "creami ng" o r phase separa t i o n by suspending and s e p a r a t i n g t h e o i l d r o p l e t s . Add t h e ammonium h y d r o x i d e t o r e a c h t h e t a r g e t pH. Mix u s i n g a h i g h shear m i x e r . B r o o k f i e l d V i s c o s i t y (RVT-20 rpm): P r o d u c t pH: 8.00 20.00 14. T o t a l A c t ives : Silicone f l u i d : Stoddard s o l v e n t : Re1ease c o a t i ng : Abras i vet 1 . ( 3 ) Exxon Corp. Inc.oo 20. The polymer w i l l wet o u t i n a few m i n u t e s . such as a b r a s i v e s . D i s p e r s e t h e Carbopol i n t o t h e w a t e r (16. ~ Insredient: SF96 S i l i c o n e F l u i d (350) ( 1 ) Dow C o r n i n p 20 Release C o a t i n g ( 2 ) S t o d d a r d S o l v e n t (3) P r i f a c 2922 L a u r i c A c i d D I Water Morphol ine Carbopol EZ-2 ( 4 ) Ammoni u h y d r o x i d e m b g o p g l i e K a o l i C l a y (5) ysp c a f Proper€+es.48 p a r t s ) and t h e morphol ine. C o n t i n u e t o m i x . 2 . Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s .oo 2.Metal Cleaners and Polishes 119 Silver and M e t a l Polish I n a d d i t i o n t o t h i c k e n i n g . r e l e a s e c o a t i n g .00 FGoodrich S p e c i a l t y Chemicals: DET-563 .86 0.00 2.00 Wt% 43. 5 .35 0. 4 . Add t h e c l a y and mix u n t i l u n i f o r m .31 14. s o l v e n t . and l a u r i c a c i d P o a v e s s e l .00 p a r t s ) by s i m p l y "dumping" i t i n . and add t h e water (43. Add t h e s i l i c o n e f l u i d . 3 . Add t h e d i s p e r s i o n t o t h e above m i x t u r e w i t h good a g i t a t i o n . 0 0 0 cps Raw M a t e r i a l S u p p l i e r s : ( 1 ) General E l e c t r i c ( 2 ) Dow C o r n i n g Corp. ( 4 ) BFGoodrich (5) Kaopolite.

0 Procedure: Combine above i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 5 0 C .0 20. 8 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 1750 L b s .-Lbs. . F o r m u l a t i o n F-803 Soluble O i 1 Ingredients: 100 P a l e O i l Monalube 605 Wt% 85.0 20.0 Procedure: Combine a l l i n g r e d i e n t s w i t h a g i t a t i o n w h i l e warming t o 50C.0 15.120 Advanced Cleaning Product Formulations Soluble O i 1 Ingredients: 100 P a l e O i l Monalube 605 P a r o i l 160 WtO/o 80. : Suggested F o r m u l a t i o n s . Appl i c a t i o n : For g r i n d i n g and v e r y l i g h t m a c h i n i n g . 5 F a l e x ( D i r e c t S c a l e ) : 2750 L b s .L b s . Above f o r m u l a t i o n f o r heavy d u t y m a c h i n i n g and d r a w i n g f o r use on s t a i n l e s s s t e e l and f e r r o u s m e t a l s . Typi c a l P r o p e r t i es : Appearance: C l e a r Dark Brown Performance Data (5% i n w a t e r ) : Appearance: M i 1 ky L i q u i d pH: 8 . / 4 7 I n . Formul a t ion F-804 SOURCE: Mona I n d u s t r i e s . I n c . Typical Properties: Appearance: C l e a r L i g h t Brown L i q u i d Performance Data (5% i n w a t e r ) : Appearance: M i 1 ky Emulsion pH: 8 . / 6 0 In.

0 2. F o r m u l a t i o n F-806 SOURCE: Mona I n d u s t r i e s .0 Procedure: M i x above i n g r e d i e n t s w i t h a g i t a t i o n ./45 . 0 Falex ( D i r e c t S c a l e ) : 1250 Lbs.-Lbs. Typical Properties: Appearance: C l e a r Amber L i q u d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Aooearance: M i 1 k v E m u l s i o n pH: 8 .0 15.. 0 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1 ex ( D i r e c t S c a l e ) : 2500 L b s . Warm t o 12OF. F o r m u l a t i o n F-805 Soluble O i 1 Ingredients: 100 P a l e O i l Monalube 6 0 5 Monalube 215 Wt% 85.0 Procedure: Combine i n g r e d i e n t s w i t h a g i a t i o n w h i l e warming t o 50C.0 5. In. . Typical Properties: Appearance: M i l k y E m u l s i o n P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: M i 1 ky Emu1 s i o n pH: 8 . / 5 5 I n . : Suggested F o r m u l a t i o n s . a d j u s t w i t h t a l l o i l f a t t y a c i d . I f s o l u t i o n i s s l i g h t l y hazy.0 10. The above f o r m u l a t i o n i s s u g g e s t e d f o r g r i n d i n g and l i g h t machining. I n c .0 5.L b s . The above f o r m u l a t i o n i s s u g g e s t e d f o r g r i n d i n g and l i g h t machining.Metal Cleaners and Polishes 121 S o l u b l e Qi 1 Inaredients: 100 P a l e O i l Monalube 6 0 5 Wonalube 2 1 5 T EA Wt% 78.

Ingredients: N a p h t h e n i c O i l (lOOSUS/lOO) Monalube 225 Monalube 605 T r i e t h a n o l a r n i n e (99%) Procedure: Add i n t h e o r d e r l i s t e d w i t h a g i t a t i o n . : Suggested F o r m u l a t i o n s brass.0 5.0 wto/.0 . b r a s s . and EP p r o p e r t i e s i n t h i s m a c h i n i n g f l u i d . b r o n z e . b r o n z e c o p p e r and s t a i n l e s s s t e e l .0 20. T o r q u e 60 i n c h pounds Formul a t i on F-766 SOURCE: Mona I n d u s t r i e s . I n c .0 30. 15.122 Advanced Cleaning Product Formulations Soluble O i l Machining F l u i d Monalube 225 p r o v i d e s l u b r i c i t y . T h i s f o r m u l a t i o n was d e s i g n e d f o r m a c h i n i n g c a r b o n s t e e l .0 55. Ingredients: Monalube 225 T r i e t h a n o l a m i n e (99%) Water Procedure: Add i n t h e o r d e r l i s t e d w i t h a g i t a t i o n . F a l e x EP T e s t : D i r e c t Load S c a l e : 2 7 5 0 l b s Torque: 47 i n c h pounds Use D i l u t i o n s : G r i n d i n g : I-2% i n water L i g h t M a c h i n i n g : 3-5% i n w a t e r M o d e r a t e M a c h i n i n g : 5-7% i n w a t e r Heavy M a c h i n i n g : 8-10% i n w a t e r F o r m u l a F-764 S y n t h e t i c Machininq F l u i d T h i s f o r m u l a t i o n i s i d e a l f o r machining carbon s t e e l . Wt% 72. aluminum and s t a i n l e s s s t e e l . F a l e x EP T e s t P r o c e d u r e : C o n c e n t r a t i o n : 20% Aqueous s o l u t i o n D i r e c t Load S c a l e 3000 l b s . c o p p e r .0 3.

.5 12.0 0. F o r m u l a t i o n i s d e s i g n e d f o r b o t h f e r r o u s and n o n f e r r o u s systems p r i m a r i l y f o r g r i n d i n g . I n c .Metal Cleaners and Polishes 123 Svnthetic Ingredients: Monalube 210 T r i e t h a n o l a m i n e (99%) Water A n t i foam Procedure: Combine in g r e d i e n t s w i t h a g i t a t i o n . Typical Properties: Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 8 . / 5 6 I n .1 K % 12. F o r m u l a t i o n F-820 Wt% 16. / 5 6 I n . Typical Properties: Appearance: C l e a r Amber L i q u i d Performance Data (5% i n Water): Appearance: C l e a r L i q u i d pH: 8 . Formul a t i on F-819 Synthetic Inqredi ents: Monalube 210 Monalube 315 T r i e t h a n o l a m i n e (99%) Water Procedure.5 25.6 33.L b s .L b s . 5 S u r f a c e T e n s i o n : 42 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s . : Suggested F o r m u l a t i o n s .0 SOURCE: Mona I n d u s t r i e s . The f o r m u l a t i o n i s d e s i g n e d f o r f e r r o u s and n o n f e r r o u s m e t a l s primarily f o r grinding.: Combine i n g r e d i e n t s w i t h a g i t a t i o n .3 50. .0 50. 0 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s .

0 20.0 10. Ingredients: Monalube 225 T r i e t h a n o l a m i n e (99%) Monalube 315 Water Procedure: Add i n t h e o r d e r l i s t e d w i t h a g i t a t i o n . Ingredients: Paraffinic O i l Monalube 225 Wt% (300SUS/lOO) 90. T o r q u e 55 i n c h pounds F o r m u l a t i o n F-765 O i 1 Based Drawi ng/Stampi ng F1ui d 15.00 SOURCE: Mona I n d u s t r i e s . making s u r e each ingredient i s dissolved before next addition.00 3.0 Monalube 225 p r o v i d e s l u b r i c i t y .00 2. Inc.00 4.0 35.00 5.: Suggested F o r m u l a t i o n s . F o r m u l a t i o n F-751 75. F a l e x EP T e s t P r o c e d u r e : C o n c e n t r a t i o n : 20% Aqueous s o l u t i o n D i r e c t Load S c a l e 3 0 0 0 l b s .00 11. EP and c o n t r i b u t e s t o t h e c o r r o s i o n p r o t e c t i o n p r o p e r t i e s i n t h i s heavy-duty stamping/ d r a w i n g f 1u i d .124 Advanced Cleaning Product Formulations S y n t h e t i c Drawing/Stampinp F l u i d T h i s f o r m u l a t i o n i s i d e a l f o r stamping hot o r c o l d r o l l e d s t e e l .0 Procedure: B l e n d Monalube 225 i n t o t h e o i l F a l e x EP T e s t : D i r e c t Load S c a l e : 3000 l b s T o r q u e 57 i n c h pounds F o r m u l a t i o n F-763 S p r a y M e t a l C1 e a n i n g C o n c e n t r a t e Ingredients: Water Sodi um M e t a s i 1 i c a t e Sodium C a r b o n a t e Sodi um H y d r o x i d e M o n a t r o p e 1250 Alkyl Polyal kylene Ether Procedure: Add i n o r d e r l i s t e d w i t h a g i t a t i o n .0 30.

/ 4 7 I n .: Suggested F o r m u l a t i o n s . T h i s f o r m u l a t i o n i s d e s i g n e d f o r b o t h f e r r o u s and n o n f e r r o u s systems f o r a r e a s o f m a c h i n i n g and g r i n d i n g a t 10% f o r m i l d s t a m p i ng.Metal Cleaners and Polishes 125 S y n t h e t i c Formula Inqredients: Monalube 205 Monalube 210 T r i e t h a n o l a m i n e (99%) Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n .0 10.L b s . . .0 55. Inc. F o r m u l a t i o n F-813 S y n t h e t i c Formula Inqredients: Monalube 205 Monalube 210 Monalube 315 T r i e t h a n o l ami ne (99%) Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n .0 30. Typical Properties: Appearance: C1 e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: Wyt 5. T h i s f o r m u l a t i o n i s d e s i g n e d f o r b o t h f e r r o u s and n o n f e r r o u s systems f o r a r e a s o f m a c h i n i n g and g r i n d i n g a t 10% f o r m i l d s t a m p i ng.0 30.0 45. / 5 7 I n . F o r m u l a t i o n F-814 wt% 5. Typical Properties: Appearance: C1 e a r Amber L i q u i d Performance Data ( 5 % i n Water): Appearance: C1 e a r L i q u i d pH: 8 .7 S u r f a c e T e n s i o n : 27 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s .0 10.L b s .0 8.0 SOURCE: Mona I n d u s t r i e s .0 10. 0 S u r f a c e T e n s i o n : 32 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2750 L b s .

SOURCE: Mona I n d u s t r i e s . 5 F a l e x ( D i r e c t S c a l e ) : 2 5 0 0 Lbs. 3. 0 Surface Tension: 32 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass Falex ( D i r e c t S c a l e ) : 2500 Lbs. F o r m u l a t i o n F-815 S y n t h e t i c Formula C l e a r product designed f o r f e r r o u s g r i n d i n g . w%% 4.126 Advanced Cleaning Product Formulations S y n t h e t i c Formula Inqredients: Monalube 2 0 5 Monalube 2 2 0 T r i e t h a n o l a m i n e (99%) Monalube 315 Water Procedure: M i x i t e m s 1.0 20.0 45. 2 .0 27. Ingredients: Monalube 210 Mona1ube 1 1 0 Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . I n c .L b s . Typical Properties: Appearance: C l e a r Amber L i q u i d Performance Data (5% i n W a t e r ) : Appearance: T r a n s l u c e n t S o l u t i o n pH: 9 ./47 I n . Add w a t e r and mix u n t i l homogeneous.5 9.0 In.0 39.0 40.-Lbs. Excess DEA i n Monalube 110 n e u t r a l i z e s PE. ./45 N o t e : No TEA needed. F o r m u l a t i o n F-816 15.5 and 4 . Typical Properties: Appearance: C1 e a r Sol u t i on Performance Data (5% i n W a t e r ) : Appearance: C1 e a r L i q u i d pH: 7 . : Suggested F o r m u l a t i o n s .

6 33.0 In. / 4 5 I n . Inc.: Suggested F o r m u l a t i o n s . A l s o some v e r y l i g h t s t a m p i n g .3 0.L b s . Typical Properties: Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 8 . P r o d u c t d e s i g n e d f o r machi n ng f e r r o u s and n o n f e r r o u s m e t a l .0 45. 0 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s . Typical Properties : Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C1 e a r L i q u i d pH: 8 .0 10.1 50. F o r m u l a t i o n F-817 S y n t h e t i c Formula Inaredients: Monalube 215 T r i e t h a n o l ami ne (99%) A n t i foam Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . ./44 F a l e x ( D i r e c t S c a l e ) : 2500 Wt% 15.Metal Cleaners and Polishes 127 S y n t h e t i c Formula P r o d u c t d e s i gned f o r g r i n d i ng and 1 ig h t m a c h i n i n g Ingredients: Monalube 2 1 0 T r i e t h a n o l a m i n e (99%) Monalube 315 Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . F o r m u l a t i o n F-818 SOURCE: Mona I n d u s t r i e s .0 30.-Lbs.0 Wt% 16. 5 S u r f a c e T e n s i o n : 42 bs.

Typical Properties: Appearance: C l e a r Amber L i q u i d Performance Data (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 1 1 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1ex ( D i r e c t Scal e ) : 2250 Lbs. Q 16.128 Advanced Cleaning Product Formulations S y n t h e t i c Formula Ingredients: Monalube 210 Monoethanol ami ne Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . 3 S u r f a c e T e n s i o n (dynes/cm): 24 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1ex ( D i r e c t S c a l e ) : 2500 Lbs / 5 5 In.0 . T h i s i s t h e most u n i v e r s a l f o r m u l a s i n c e i t can be used on all m e t a l l u r g y a t 1% t o 2%.3 50. T y p i c a l P r o p e r t i es : Appearance: C l e a r Amber L i q u i d Performance Data (5% i n W a t e r ) : Appearance: C1 e a r L i q u i d pH: 8 . /58 I n . . F o r m u l a t i o n F-822 SOURCE: Mona I n d u s t r i e s .6 33. I t a l s o can be used f o r g r i n d i n g a t 5% t o 8% f o r m a c h i n i n g and a t 8% t o 15% f o r r e a l heavy m a c h i n i n g .1 50.: Suggested F o r m u l a t i o n s .4 S y n t h e t i c Formula Ingredients: Monalube 205 T r i e t h a n o l a m i n e (99%) A n t i foam Water Procedure: Combi ne in g r e d i e n t s w i t h a g i t a t i o n .L b s .6 33. -Lbs 16. F o r m u l a t i o n F-821 Ferrous metals o n l y .3 0. Inc. . Formulated f o r g r i n d i n g a p p l i c a t i o n s .

-Lbs. F o r m u l a t i o n F-823 *thetic Ingredients: Monalube 2 0 5 Monoethanol ami ne Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n .: Suggested F o r m u l a t i o n s . Typical Properties: Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: Wt% 10.0 10 C a s t I r o n B l o c k : Pass Fa1 ex ( D i r e c t S c a l e ) : 2000 Lbs.L b s .Metal Cleaners and Polishes 129 S v n t h e t i c Formul a Inaredi ents: Monalube 205 Monalube 1 1 0 Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . Inc. .0 Formula 25./5O I n . F o r f e r r o u s systems f o r m a c h i n i n g and g r i n d i n g .0 25. 0 S u r f a c e T e n s i o n : 28 C a s t I r o n B l o c k C o r r o s i o n e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2250 Lbs. F o r use i n m a c h i n i n g and 1 g h t s t a m p i n g f o r f e r r o u s and nonferrous metals.0 60. 10 i s enough t o n e u t r a l i z e t h e NOTE: Excess DEA i n Monalube phosphate e s t e r . Formul a t ion F-824 SOURCE: Mona I n d u s t r i e s .0 50. Typical Properties: Appearance: C l e a r S o l u t i o n P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C1 e a r L i q u i d ptl: 8 .0 30. /50 I n .

T y p i c a l P r o p e r t i es : Appearance: C l e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C1 e a r L i q u i d pH: 8 .0 forming.L b s . T y p i c a l P r o p e r t i es : Appearance: C l e a r C o n c e n t r a t e P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 8 . 6 S u r f a c e T e n s i o n : 41 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2750 Lbs. 5 S u r f a c e T e n s i o n ( d y n e s / c m ) : 42 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s . I n c . t h e n add w a t e r .0 30. -Lbs F o r heavy d u t y s t a m p i n g o f f e r r o u s m e t a l s a t 1 0 t o 20% i n w a t e r .0 Procedure: M i x Monalube 225 w i t h t r i e t h a n o l a m i n e and add Monalube 315.0 25. / 4 6 I n . For machining.0 30. : Suggested F o r m u l a t i o n s ./55 I n . 10.130 Advanced Cleaning Product Formulations Synthetic Formulation Inqredients: Monalube 210 Monalube 225 TEA Water Procedure: Combine i n g r e d i e n t s w i t h a g i t a t i o n . M i x u n t i l c l e a r .0 40 0 ~ 40. F o r m u l a t i o n F-808 SOURCE: Mona I n d u s t r i e s .0 10. Forrnul a t i on F-807 and s t a m p i n g a l l m e t a l s S y n t h e t i c Formulat Inqredients: Monalube 225 Monalube 3 1 0 T r i e t h a n o l ami ne (99%) Water 15.

.0 30. 2. 5. / 5 1 I n . forming. 0 S u r f a c e T e n s i o n : 32 Cast I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2750 L b s .0 25. and 4 . / 5 7 I n .0 55.0 3.0 10. wtsl.L b s . 7 Surface Tension: 35 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2250 L b s . 2.0 3 . Application: F o r f e r r o u s and n o n f e r r o u s systems f o r and s t a m p i n g . and 4 .0 50. . Inc. Typical Properties: Appearance: C1 e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 8 . Formul a t ion F-809 Synthetic Formulation Inqredients: Monalube 205 Monalube 225 T r i e t h a n o l a m i n e (99%) Water Procedure: Mix items 1.: Suggested Formu a t i ons .L b s F o r s t a m p i n g . F o r m u l a t i o n F-810 mach n i ng.Metal Cleaners and Polishes 131 Svnthetic Formulation I n g r e d i en t s : Monalube 2 0 5 Monalube 210 Monalube 220 T r i e t h a n o l a m i n e (99%) Water Procedure: M i x i t e m s 1. SOURCE: Mona I n d u s t r i e s .0 10. d r a w i n g and b r o a c i n g 10 t o 20% i n w a t e r . 5.0 10. Then add w a t e r . t h e n add w a t e r and m i x . Typical Properties: Appearance: C l e a r L i q u i d Performance Data (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 9 .

0 S u r f a c e T e n s i o n : 42 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass Fa1 ex ( D i r e c t S c a l e ) : 2500 Lbs.0 SOURCE: Mona I n d u s t r i e s .L b s . F o r m u l a t i o n F-812 and s t a m p i n g f o r a1 1 m e t a l 1u r g y Inc. T y p i c a l P r o p e r t i es : Appearance: C1 e a r Amber L i q u i d P e r f o r m a n c e D a t a (5% i n W a t e r ) : Appearance: C l e a r L i q u i d pH: 0. .0 10.0 30.: Suggested F o r m u l a t i o n s Wt% 9.132 Advanced Cleaning Product Formulations Synthetic Formulation Inqredients: Monalube 215 Monalube 220 T r i e t h a n o l a m i n e (99%) Water Procedure: Combine in g r e d i e n t s w i t h a g i t a t i o n .0 46.0 9.0 36.7 S u r f a c e T e n s i o n : 35 C a s t I r o n B l o c k C o r r o s i o n T e s t : Pass F a l e x ( D i r e c t S c a l e ) : 2500 L b s . -Lbs Use i n m a c h i n i n g and s t a m p i n g f o r b o t h f e r r o u s and n o n f e r r o u s metallurgy. Typical Properties: Appearance: C l e a r Amber L i q u i d Performance Data (5% i n Water): Appearance: C l e a r L i q u i d pH: 9 . For machining. forming.0 5. / 3 5 I n . / 4 7 I n . F o r m u l a t i o n F-811 Synthetic Formulation Inqredients: Monalube 205 Monalube 220 T r i e t h a n o l a m i n e (99%) Water Procedure: Combine in g r e d i e n t s w i t h a g i t a t i o n .0 55. .

A.70 0.0 Procedure: D i s s o l v e K e l z a n x a n t h a n gum i n w a t e r . u n t i l a homogeneous g e l f r e e o f lumps h a s been o b t a i n e d I I . Tests : V i s c o s i t y ( B r o o k i e l d RVT. 1 1 1 .00 0.s.0 3. 1 0 m i n -1.Metal Cleaners and Polishes 133 U n i v e r s a 1 S c o u r i na P a s t e Inqredients: A : T y l o s e CBR 10000 WtO/o 5. s p r e a d e v e n l y on t h e s u r f a c e t o b e c l e a n e d and a l l o w s u f f i c i e n t t i m e f o r t h e c l e a n i n g a c t i o n t o be accomplished.0 trace 85. 8 0 21. To u s e . w h i c h i s added b y c o n t i n u i n g s t i r r i n g . 6. t h e components o f C t o I . s h o u l d s w e l l . Add one a f t e r a n o t h e r .o 4.80 10.0 3.0 4.00 51 . SOURCE: Monsanto P e r f o r m a n c e M a t e r i a l s : Formulation K e l z a n Suggested .0 3 0 K o m p e r l a n KD NaCl Preservative. Add t h e c i t r i c and p h o s p h o r i c a c i d s f o l l o w e d b y 5 u t y l C e l l o s o l v e a n d T e r g i t o l NP.00 5: Water (50C) C: H o s t a p u r SAS 60 Genapol ZRO 1 iq u i d Genapol U D . 25C): 49b00 mPas SOURCE: Hoeckst A k t e n g e s e l l s c h a f t : Suggested F o r m u l a t i o n A1 u m i n u m C 1 e a n e r Comoosi t i o n : K e l z a n x a n t h a n gum Butyl Cellosolve T e r g i t o l NP Phosphoric A c i d (85%) Citric Acid S o d i um D i c h r o m a t e Water Wt% 1 . F i n a l l y D i s added. M a n u f a c k u r i ng: I.70 2. Perfume 0: q. sp.

o 70.0 5.6 I n d o p o l H-100 Odor1 ess M i n e r a S p i r i t s 11 ance Procedure: Add i n g r e d i e n t s as l i s t e d .2 0.6 Mazon R I 6 7-1 2 M a s i l SF-10 0.5 70.9 Penetrating O i l I n a r e d ie n t s : Wt% S-Maz 80 2.0 1 . WD-40 Type L u b r i c a n t C o n c e n t r a t e I r e d ien t s : nq S-Maz 8 0 Mazawet 7 7 H i t e c E-515 ( E t h y l ) Palmetic Acid S h e l l f l e x 213 S h e l l Sol 135 Procedure: Add i n g r e d i e n t s as l i s t e d . I f more c o r r o s i o n i n h i b i t o r i s r e q u i r e d .1 5%). NOTE: A p o r t i o n o f t h e m i n e r a l s p i r i t s may be d e l e t e d and s u b s t i t u t e d w i t h a n a p h t h e n i c o i l ( 5 .7 1. Wt% 10.8 1. 85% 10. B u r n i s h i n s Compound Ingredients: Mazamide 65 Mafo 1 3 MOD 1 Mazon R I 4 A T r i s o d i u Phosphate m EDTA Water Procedure: Add i n g r e d i e n t s as l i s t e d .0 Water Balance Procedure: Add i n g r e d i e n t s as l i s t e d .0 7.0 Mazon R I 8 B 12.1 0.0 SOURCE: PPG I n d u s t r i e s .0 7.134 Advanced Cleaning Product Formulations Water Sol u b l e Stampi ng F1u i d Ingredients: \nit% M a s l i p 501 Base 30. add more Mazon R I 8 8.7 10.1 Nekal WT-27 Gafac RE-40 0. : Suggested F o r m u l a t i o n s .1 0. I f more l u b r i c i t y i s r e q u i r e d . add Macol 5 1 0 0 . Use 1O:l d i l u t i o n r a t e f o r heavy d u t y a p p l i c a t i o n .0 D i e t h a n o l ami ne 8. I n c .2 P r o p y l ene G1 y c o l T r i e t h a n o l a m i n e .Q 5. W 3.

Grill and Hot Plate Cleaners .10. Oven.

2 .00 5. M i x each f o r 5 m i n u t e s . Make t h e 4. I n c . Package.00 C: Butyl Carbitol Aminomethyl P r o p a n o l (AMP-95) Sodium Cocoamphoacetate ( M o n a t e r i c CM-36s) 50% S o l u t i o n '10. 2 . 4 . S l o w l y add P a r t D and m i x u n t i l u n i f o r m .136 Advanced Cleaning Product Formulations C a u s t i c Oven C l e a n e r Inaredients: A : Van Gel C..00 1. Sodium H y d r o x i d e .oo Procedure: 1 . S l o w l y add t h e r e m a i n i n g i n g r e d i e n t s i n t h e o r d e r shown. 50% S o l u t i o n Wt%* 62. 468 *As r e c e i v e d b a s i s SOURCE: R.00 D . C o n t i n u e m i x i n g f o r 30 m i n u t e s . Add t h e P a r t C i n g r e d i e n t s i n t h e o r d e r l i s t e d . 4. C o n t i n u e m i x i n g f o r 60 m i n u t e s .C a u s t i c Oven C l e a n e r Inqredi ents: A : Water Van Gel C. m i x i n g each u n t i l u n i f o r m . Add t h e r e m a i n i n g P a r t A w a t e r t o t h e i n d i c a t e d amount o f d i s p e r s i o n and m i x u n t i l uniform.T. D r y b l e n d t h e Van Gel C and Rhodopol 50MD and add t h e m i x t u r e t o t h e w a t e r w h i l e s t i r r i n g w i t h a homogenizer o p e r a t i n g a t 5000 r p m . V a n d e r b i l t Co.00 5.25 5. 25% Aqueous S o l u t i o n Vanseal NACS-30. Procedure: 1 .50 0. 8 p a r t s b y w e i g h t o f Van Gel C i n t o 9 5 . S l o w l y add P a r t B and a d j u s t homogenizer speed as r e q u i r e d t o a c h i e v e good m i x i n g o f e n t i r e b a t c h . 3 . : Suggested F o r m u l a t i o n s .50 45. 461 N o n .75 5. A v o i d e n t r a p m e n t o f a i r and g e n e r a t i o n o f foam.8% Van Gel C d i s p e r s i o n b y s l o w l y a d d i n g 4 .00 28. Xanthan Gum 6 : D i e t h a n o l ami n e Triethanolamine T r i p r o p y l e n e g l y c o l M e t h y l E t h e r (Dowanol TPM) P o t a s s i u m C a r b o n a t e .00 1. F o r m u l a t i o n No. w h i l e m i x i n g w i t h a homogenizer a t 5000 rpm.25 5. Sodium L a u r o y l S a r c o s i n a t e Wt%* 55. 2 p a r t s b y w e i g h t o f w a t e r o f a t room t e m p e r a t u r e .75 0. Magnesium Aluminum S i l i c a t e Rhodopol 50MD. 8 % Aqueous D i s p e r s i o n Dei o n i zed Water B: Sodium H y d r o x i d e .00 0. F o r m u l a t i o n N o .

00 C8-16 a l k y l p o l y g l y c o s i d e : 1.00 P r o p y l e n e g l y c o l m e t h y l e t h e r : 3. : Glucopon 425CS (1) Wei Qht P e r c e n t 71.00 3. d i s p e r s e o r s c r e e n t h e Carbopol r e s i n i n t o t h e DI w a t e r . M i x t h e s l u r r y f o r a p p r o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. 3 . Grill and Hot Plate Cleaners 137 H i g h C a u s t i c Oven C l e a n e r Carbopol r e s i n s a r e used t o t h i c k e n t h i s h i g h c a u s t i c f o r m u l a t i o n . Add t h e APG s u r f a c t a n t . 5. U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d b y a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s .78 2.03 69.50 FGoodrich S p e c i a l t y Chemicals: OET-360 . Inaredient: D I Water Carbopol 674 ( 1 ) Potassium h y d r o x i d e (45%) Propylene g l y c o l methyl e t h e r ( 2 ) C8-16 a l k y l p o l y g l y c o s i d e (50%) ( 3 ) B r o o k f i e l d v i s c o s i t y (RVT-20 Product pH: Product c l a r i t y : 8FGoodrich ( 2 ) Dow Chemical : Dowanol PM ( 3 ) Henkel C o r p .00 0.Oven. I n a d d i t i o n .22 22. M i x u n t i l homogeneous.00 3. Add t h e g l y c o l e t h e r . as d e s i r e d .75 22. Total Actives: Potassium h y d r o x i d e : 10. Add f r a g r a n c e . Add t h e p o t a s s i u m h y d r o x i d e w i t h c o n t i n u o u s m i x i n g .22 3.00 rpm) : 250 CPS 13-14 Clear 5. 2 .000 CPS 13-14 Clear Procedure: 1 . t h e use o f t h e r e s i n p r o v i d e s v e r t i c a l c l i n g t o i n c r e a s e t h e c o n t a c t t i m e o f t h e d e t e r g e n t on t h e s o i l e d s u r f a c e and enhance consumer c o n v e n i e n c e . 4 .00 3.

40 1. Formulation from I n t e r n a t i o n a l S p e c i a l t y Products. P y r r o l i d o n e (M-Pyrol) 20. Magnesium Aluminum S i l i c a t e Dei o n i zed Water 8 : n-Methyl W t %* 1 . Xanthan Gum D e i o n i z e d Water B: VVt%* 0. 3 .00 10. D i s p e r s e t h e Veegum T i n t h e w a t e r u s i n g a homogenizer a t 5000 r p m . 3 .40 Sodium H y d r o x i d e .00 Procedure: 1 . h e a t t o 70C. Move t h e b a t c h t o a p r o p e l l e r m i x e r and a d j u s t t h e speed t o p r o d u c e a s m a l l v o r t e x . 6 . 4 .20 80. w h i l e h e a t i n g t o 70C. Add t h e P a r t B i n g r e d i e n t s i n t h e o r d e r shown. C o n t i n u e m i x i n g for 20 m i n u t e s . Magnesium Aluminum S i l i c a t e Rhodopol 23. 50% Deceth-4 Phosphate (Rhodafac RA-600) 8. *As r e c e i v e d b a s i s SOURCE: R. 2 . 2 .25 Nonoxynol ( I g e p a l CO-630) 1 .00 D i s o d i u m C o c o a m p h o d i p r o p i o n a t e ( M i r a n o l C2M-SF C o n c . Inc. C o n t i n u e m i x i n g f o r 20 m i n u t e s . V a n d e r b i l t Co.138 Advanced Cleaning Product Formulations Oven C l e a n e r Ingredients: A : Veegum T. 5 . 4 . D r y b l e n d t h e Veegum T and Rhodopol 23 and s l o w l y add them t o t h e w a t e r . m i x i n g f o r 5 m i n u t e s a f t e r each a d d i t i o n . F o r m u l a t i o n f r o m Rhone-Poulenc S u r f a c t a n t s & S p e c i a l t i e s A e r o s o l Oven C1 e a n e r Ingredients: A : Veegum T. NOTE: I t i s p a r t i c u l a r l y i m p o r t a n t t h a t t h e Sodium H y d r o x i d e s o l u t i o n be added v e r y s l o w l y w i t h good m i x i n g o f t h e e n t i r e batch.. h e a t i t t o 85-9OC and m i x w i t h an homogenizer a t 5000 rpm. Add P a r t B t o P a r t A and c o o l w h i l e m i x i n g t o 30C.: Suggested F o r m u l a t i o n s . Package i n a e r o s o l can u s i n g Propane/Butane p r o p e l l a n t . Cool t o 55C. Combine t h e i n g r e d i e n t s o f P a r t 8 .50 74.25 .oo Procedure: 1 .T. Move t h e b a t c h t o a p r o p e l l e r m i x e r and a d j u s t t h e speed t o provide a s l i g h t vortex. Weigh w a t e r and p l a c e on h o m o g e n i z e r . Weigh t h e w a t e r . ) 3.

Oven.2 4.3 2.2 0 : K e l zan Formul a t i ons .0 Procedure: P r e p a r e w a t e r s o l u t i o n o f K e l z a n x a n t h a n gum t h e n add A n t a r o n . S e p a r a t e l y . S i l i c o n e and hexane s e p a r a t e l y . M i x t h e B r i j 96.2 82. Grill and Hot Plate Cleaners 139 Oven C l e a n e r Composition: K e l z a n x a n t h a n gum T r i s o d i um Phosphate Sodi urn m e t a s i 1 ic a t e S u l f o n a t e OA5 B r i j 96 S i 1 icone 2 0 0 F l u i d 3 5 0 c s Hexane Water 0.1 3.0 10.0 87. SOURCE: Monsanto P e r f o r m a n c e M a t e r i a l s : T e c h n i c a l B u l l e t i n 1 .l 2. Then add w a t e r s o l u t i o n t o t h e s i l i c o n e / h e x a n e m i x w i t h c o n s t a n t a g i t a t i o n . Heavy D u t y Oven C l e a n e r Compos i t i on : Kelzan xanthan gum A n t a r o n FC-34 Sodi um h y d r o x i d e Water Wt% 0.2 1. p r e p a r e t h e 40% sodium h y d o x i d e s o l u t i o n and s l o w l y add t o m i x . F o r a e r o s o l use c h a r g e w i t h 80% m i x t u r e and 20% o f 1 : l m i x o f G e n e t r o n 1 2 and 1 1 4 .0 4. F o r a e r o s o l u s e c h a r g e w i t h 90% conce n t r a t e and 10% G e n e t r o n 1 2 .1 Procedure: P r e p a r e w a t e r s o l u t i o n o f K e l z a n x a n t h a n gum as b e f o r e and add n e x t t h r e e i n g r e d i e n t s .1 3.

p o u r Phase I1 i n t o Phase I . M i x t h o r o u g h l y t h e n add Phase 1 1 .6 5. c p s : 96 pH: 1 3 . D .1 3. 9 F o r m u l a 1114 Oven C l e a n e r w/Phosphate Ingredient s : Phase I : Water.4 2. 4 1. : Suggested F o r m u l a t i o n s . Sodi urn C i t r a t e Sodi um M e t a s i 1 ic a t e Sodium H y d r o x i d e .2 3.1 Blending Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i on. I . W h i l e m i x i n g .3 15.1 4. Formula 1115 SOURCE: W i t c o C o r p .4 3.1 3. D .9 Blending Procedure: Combine Phase I i n g r e d i e n t s and m i x u n t i l homogeneous. 6 2. 40% Monoethanol ami ne Dowanol PM R e w o t e r i c AM HC W i t c o 1298SA DeSonic 9 N \Mt96 71 . I . I . Typical Properties: V i s c o s i t y .1 2. P o t a s s i u m H y d r o x i d e . D .2 6.140 Advanced Cleaning Product Formulatioris Oven C 1 e a n e r w / A m p h o t e r i c Ingredients: Water.5 4. Combine Phase I1 i n g r e d i e n t s i n s e p a r a t e v e s s e l and m i x t h o r o u g h l y . C a r b o p o l 940 Phase 11: Water. 87% Tetrapotassium Pyrophosphate Phase 111: R e w o t e r i c AM HC 71 .

Coatings and Finishes 141 .dishes.

C o n t i n u e s t i r r i n g u n t i l t h e t e m p e r a t u r e reaches 45C. Total Actives: 0. Hoechst Wax S. add t h e m o r p h o l i n e u n t i l t h e m i x t u r e i s homogeneous. 2. 3. Add t h e C a r d i s Wax.00 Product C l a r i t y : P o l i s h Raw M a t e r i a l S u p p l i e r s : ( 1 ) BF G o o d r i c h ( 2 ) P e t r o l i t e S p e c i a l t y Polymers ( 3 ) Hoechst Celanese ( 4 ) General E l e c t r i c 2.25 0. 5.10 0.20 0.142 Advanced Cleaning Product Formulations F u r n i t u r e P o l i sh I n a d d i t i o n t o t h i c k e n i n g .00 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-530 . Add t h e TEA. 4.08 0. and o l e i c a c i d t o a vessel.00 P a r t B: C a r d i s 36 Wax ( 2 ) Hoechst Wax S ( 3 ) Oleic Acid Morphol i ne D I Water Part C: SM2133 S i l i c o n e Emulsion ( 4 ) SM2135 S i l i c o n e Emulsion ( 4 ) Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 rpm): Product pH: 7.500 cps Procedure: 1 . D i s p e r s e t h e Carbopol i n t o t h e w a t e r b y s i m p l y "dumping" i t i n . Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s . Add i n t h e s i l i c o n e e m u l s i o n s w i t h m i l d m i x i n g .50 T o t a l Wax : T o t a l S i l i c o n e : 6. t o become p e r m a n e n t l y suspended.00 9. b r i n g t h e temperature up t o 96-IOOC. Add t h e w a t e r a t 95C.25 0. The p o l y m e r w i l l wet o u t i n a few m i n u t e s . M i x u n t i l homogeneous. such as a b r a s i v e s .20 0. With m i l d s t i r r i n g . When m e l t e d . Add P a r t B. Cool t o room temperature.10 1.82 4. P r e p a r e P a r t B. Inqredient: P a r t A: D I Water Carbopol EZ-2 TEA wp9b (1) 91. The r e s i n a1 so p r e v e n t s "creaming" o r phase separa t i o n b y suspending and s e p a r a t i n g t h e o i l d r o p l e t s .

Total A c t i wes: Silicone Fluid: Mineral S p i r i t s : 5.00 20. I n j u s t a few m i n u t e s .00 19. 4 . 3 . t o become p e r m a n e n t l y suspended. 4 0 p a r t s o f Carbopol i n t o 49. The r e s i n a1 so p r e v e n t s "creami ng" o r phase s e p a r a t i o n b y suspending and s e p a r a t i n g t h e o i l d r o p l e t s .00 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-540 . Add t o t h e above m i x t u r e w i t h good a g i t a t i o n .40 Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 rpm): P r o d u c t pH: 8 .00 20. 5 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : (1) I C I Surfactants ( 2 ) General E l e c t r i c ( 3 ) BFGoodrich 3. t h e polymer w i l l c o m p l e t e l y wet o u t .oo DI Water Renex 20 ( 1 ) Morphol ine SF96 S i l i c o n e F l u i d ( 3 5 0 ) Oleic Acid Mineral S p i r i t s 01 Water Carbopol EZ-2 ( 3 ) 5.Polishes.60 p a r t s o f w a t e r b y s i m p l y "dumping" t h e p o l y m e r i n t o t h e w a t e r .200 c p s Procedure: 1 . D i s s o l v e t h e Renex 2 0 and m o r p h o l i n e i n t h e w a t e r w i t h m i l d agitation. Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s . 2 . D i s s o l v e t h e s i l i c o n e f l u i d and t h e o l e i c a c i d i n t h e m i n e r a l s p i r i t s .00 2.60 0. such as a b r a s i v e s . M i x u n t i l homogeneous. d i s p e r s e 0 . I n q r e d ie n t : Wt% 50. I n a s e p a r a t e v e s s e l . Add t h i s d i s p e r s i o n t o t h e above m i x t u r e .00 2. Coatings and Finishes 143 Leather/Plastic Polish I n a d d i t i o n t o t h i c k e n i n g .00 (2) 1.

M i x u n t i l homogeneous. The polymer w i l l wet o u t i n a few m i n u t e s . D i s p e r s e t h e Carbopol i n t h e w a t e r b y s i m p l y "dumping" i t i n . 4 . D i s p e r s e t h e Carbopol i n t o t h e w a t e r . 5 0 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) Rhone-Poul enc (3) Kaopolite Procedure: 1 .00 I g e p a l 630 ( 2 ) 3. DET-552 Rust Removing P o l i s h Carbopol r e s i n s a r e used i n t h i s f o r m u l a t o t h i c k e n t h e g l u c o n i c a c i d t o e n a b l e improved a p p l i c a t i o n e f f i c a c y . M i x u n t i l smooth. DET-560 . Mix u n t i l homogeneous. SOURCE: BFGoodrich S p e c i a l t y Chemicals: Suggested Formulations . The r e s i n a1 so p r e v e n t s "creami ng" o r phase s e p a r a t i o n by suspending and s e p a r a t i n g t h e o i l d r o p l e t s . A d d t h e sodium h y d r o x i d e w i t h a g i t a t i o n . 700 cp P r o d u c t pH: 7 . 2 . Add t h e s u r f a c t a n t w h i l e m i x i n g under moderate a g i t a t i o n . T h i c k e n i n g will o c c u r immedi a t e l y 3 .20 Carbopol EZ-2 ( 1 ) Mineral S p i r i t s 15.30 Physical Properties: B r o o k f ie l d V i s c o s i t y (RVT-20 rpm) : 1 I . Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s . M i x u n t i l t h e e m u l s i o n becomes homogeneous.000 c p P r o d u c t p H : 13. Add t h e diatomaceous e a r t h . Add t h e g l u c o n i c a c i d s o l u t i o n . I n q r e d ie n t : Wt% D I Water 44.86 Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 r p m ) : 3.00 T r i e t h a n o l ami ne 0. 3 . The p o l y m e r w i l l a l s o i m p a r t v e r t i c a l c l i n g t o e n a b l e a p p l i c a t i o n s on v e r t i c a l o r angled surfaces. such as a b r a s i v e s .71 G l u c o n i c a c i d s o l u t i o n (50%) ( 2 ) 17. Add t h e m i n e r a l s p i r i t s .70 Diatomaceous e a r t h ( 3 ) 8. Add t h e TEA.90 Product C l a r i t y : T r a n s l u c e n t Procedure: 1 . t o become p e r m a n e n t l y suspended.144 Advanced Cleaning Product Formulations M a r b l e P o l ish I n a d d i t i o n t o t h i c k e n i n g .64 1-79 Carbopol €2-2 ( 1 ) Sodium h y d r o x i d e (50%) 35. 2. Ingredient: we% D I Water 74.80 0.

2 . S i m p l e a p p l i c a t i o n . Coatings and Finishes 145 S c r a t c h e d Wood P o l i s h Ingredients: Veegum T. detergent r e s i s t a n t f i n i s h on non-porous s u b s t r a t e s . Add t h e P a r t C i n g r e d i e n t s t o t h e P a r t B m i x t u r e i n t h e o r d e r shown.s D: P r e s e r v a t i v e . Formulation Properties: C o n t a i n s no wax High g l o s s Detergent r e s i s t a n t E a s i 1 y a p p l ied SQURCE: Genesee P o l y m e r s C o r p .50 16. Fragrance Procedure: 1 . D e t e r q e n t R e s i s t a n t P o l ish A wax-free p o l i s h . m i x i n g each f o r 10 m i n u t e s . 6 . M i x u n t i l homogeneous and package. Add P a r t B+C t o P a r t A and m i x f o r 10 m i n u t e s .4 70. *As r e c e i v e d b a s i s SOURCE: R. M i n e r a l Spi r it s 99% 2.50 16.: F o r m u l a t i o n No. Ingredients: ( 1 ) GP-121 S i l i c o n e P o l i s h A d d i t i v e ( 2 ) GP-RA-159 S i l i c o n e P o l i s h A d d i t i v e ( 3 ) Stoddard Solvent ( 4 ) Mineral S p i r i t s (Odorless) ( 5 ) GP-227 S i l i c o n e S u r f a c t a n t S o l u t i o n ( 6 ) K a o p o l i t e SF ( 7 ) S o f t Water ( 8 ) Bactericide Wt% 9. add P a r t D. and m i x u n t i l u n i f o r m .25 4. r e s u l t s i n b o t h d e p t h o f g l o s s and d e t e r g e n t r e s i s t a n c e f o r e x t e n d e d p r o t e c t i o n ..50 31.50 A: B: S t e a r i c A c i d Carnauba Wax Beeswax. Dye.00 q. 2 1 0 Gloss. Weigh t h e w a t e r and m i x w i t h a p r o p e l l e r m i x e r a t 1800 rpm.0 0. 3 . 5 .5 9.5 3. : Non-smeari ng Cost e f f i c i e n t Cold b l e n d (Only m i x i n g r e q u i r e d ) Resistant t o wash-off Formula 20-12 .75 27. Combine t h e P a r t B i n g r e d i e n t s and h e a t t o 9OC. w i t h o u t hard r u b b i n g o r b u f f i n g . Ye1 1ow C: T r i e t h a n o l ami ne.Polishes. V a n d e r b i l t Co. 4 . which provides a high-gloss. Magnesium Aluminum S i l i c a t e Dei o n i zed Water Wt% 1. Cool t h e b a t c h t o 35C.5 3. H i qh Inc.0 1. S l o w l y add t h e Veegum T and m i x f o r 20 m i n u t e s w h i l e h e a t i n g t o 9OC.1 Combine i n o r d e r shown w i t h h i g h s h e a r m i x i n g u n t i l t h i c k e n i n g o c c u r s .T.0 3.

12. Rinse Aids 146 .

%: 4 0 Formula 131 R i nse A i d Ingredients: Water.0 Blending Procedure: 51 end i n g r e d i e n t s in t h e o r d e r 1 is t e d . P e t r o 22 Powder DeSoni c LFD-97 Hydroxyacetic Acid.0 5.0 . c p s : 80 C l o u d P o i n t . Typical Properties: S p e c i f i c G r a v i t y : 1.0 35. 5 8 pH. 4 V i s c o s i t y . C : 68 S o l i d s : 40% Formula 130 SOURCE. c p s : 85 C l o u d P o i n t . as i s : 6 .Rinse Aids 147 R i nse A i d .0 35. l b s : 8 .105 Wt/Gal. C : 59 S o l i d s . 2 1 V i s c o s i t y . : Suggested Formul a t ions Wt% 60. l b s : 9 . P e t r o 22 Powder DeSoni c LFD-97 Typical Properties: S p e c i f i c G r a v i t y : 1.0 10.0 70% 5. I . D . Acid Inqredients: Water. I . D .029 Wt/Gal. W i t c o C o r p . Wt9/o 50.

Carpet. Floor. Upholstery Shampoos an 148 . Rug.13.

I n c .o 0. S t e a m Rug C l e a n e r .0 15.0 7.Rug.25 0. 5 w a 5.0 84.0 10.0 1.0 80.0 10.0 1.0 5.8 Wt% 6.0 10.25 wt% Low Foam C a r p e t Shampoo Ingredients: Macol 2LF Ethylene Glycol Methyl Ether Sodi urn T r i p o l y p h o s p h a t e Sodi urn X y l ene S u l f o n a t e Mazu DF 210 SX Water ( s o f t ) Procedure: Add i n g r e d i e n t s as l i s t e d .5 0. Upholstery Shampoos and Cleaners 149 C a r p e t C1 e a n e r I n qr e d i e n t s : Water T r i s o d i urn Phosphate Tetrapotassium Pyrophosphate P l u r a f a c D-25 A1 ip a l CO-436 Mazawet 7 7 EDTA ( T e t r a s o d i u m S a l t ) M Tinopal 5 B Procedure: Add i n g r e d i e n t s as l i s t e d . 56. : Suggested F o r m u l a t i o n s Wt% 3. Carpet.A Ingredients: Macol OP 1 0 SP Sodium S i l i c a t e Sodi urn X y l ene S u l f o n a t e Water Procedure: Add i n g r e d i e n t s as l i s t e d . Steam Rua C l e a n e r .0 Inqredients: Macol OP 1 0 SP Sodi um S i 1 ic a t e Sodium X y l e n e S u l f o n a t e Water Procedure: Add i n g r e d i e n t s as l i s t e d SOURCE: PPG I n d u s t r i e s .0 10.0 . o 1 .0 10.0 3.5 81 . Floor.

o 5. SOURCE: Hoechst A k t i e n g e s e l l s c h a f t : .0 5.0 2. o Wt% 75. o 3. B: W a t e r . wtu/.0 1 .00 72. : G e n e r a l F o r m u l a t i o n s C a r p e t Shampoo Liquid.0 4.0 3.0 1. transparent Ingredients: A : Hostapur 0s l i q u i d M e d i a l a n KA c o n c .0 10. Suggested F o r m u l a t i o n Preservative Manu f a c t u r i ng : One a f t e r a n o t h e r .o 5.0 4.00 t h e components o f A a r e added t o 8 .150 Advanced Cleaning Product Formulations Carpet Cleaners f o r t h e Spray-Extraction Process Inqredients: C u b l e n 0 50 Tetrapotassium pyrophosphate P r o p e t a l 241 P r o p e t a l 281 S u l f e t a l 4105 Isopropanol Water F o r m u l a CT 02-08-01 Ingredients: Water Soap S u l f e t a l 4105 P r o p e t a l 99 Cont raspum 3 0 0 U b a t o l TR 1138 Isopropanol F o r m u l a C T 02-08-02 W S 1. 25.00 3.0 81 .0 SOURCE: Zschimmer & Schwarz GmbH & C o .

5 4.0 ** *** **** * FMC Rhone-Poulenc Rhodafac RE-610 DeSoto Rhone-Poulenc I g e p a l CA-620 RUQ Steam C l e a n e r S o i 1 -Food ( f a t and p r o t e i n ) . Upholstery Shampoos and Cleaners 151 I Phosphate. and p a r t i c u l a t e S u r f a c e . 4 % b w ( 6 . : .2 o z / g a l l o n ) Wt% 62. Floor.5 2.0 3.P o l y e s t e r and n y l o n A p p l i c a t i o n Method-Rug s c r u b b e r Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Water *TSP *STPP K a s i 1 # 6 P o t a s s i um S i 1 ic a t e **Phosphate E s t e r ***Sodi um A1 k y l naphtha1 ene S u l f o n a t e ****Octylphenoxy P o l y e t h o x y e t h a n o l . Carpet.F o o d ( f a t and p r o t e i n ) . 7 .Rug.8 M o l e s EO Use D i l u t i o n : 0 . and p a r t i c u l a t e S u r f a c e . p e t r o l e u m o i l and g r e a s e .1 .0 3.0 6. o r She1 1 Chemical Neodol 25-1 2 Detergent F o r m u l a t i o n Guide clay 84.0 5. 5 % bw ( 1 .0 20. 7 .P o l y e s t e r and n y l o n A p p l i c a t i o n Method-Rug s c r u b b e r Manufacture-Mix t a n k w i t h p r o p e l l e r s t r r e r Composi t i on : Water Wetso Beads 2048 Sodi um X y l ene S u l f o n a t e .0 SOURCE: PQ C o r p . 40% * M i r a n o l JEM C o n c e n t r a t e (34%) Use D i l u t i o n : 4 .1 2 o z / g a l l o n ) *Rhone-Poul enc.9 .0 5. C a r p e t Shampoo L i quid) clay S o i l .0 5. p e t r o l e u m o i l and g r e a s e . 8 .

152

Advanced Cleaning Product Formulations

C a r p e t Shampoo,
I Q r e d ie n t s : n Water P e t r o BAF L i q u i d W i t c o l a t e WAC-LA

H i s h Foam

WtS/o
78.3 5.0 16.7

B1 e n d i n g P r o c e d u r e : B1 end in g r e d i e n t s i n t h e o r d e r 1 is t e d . P e t r o BAF, i n c o m b i n a t i o n w i t h sodium l a u r y l s u l f a t e , r e d u c e s t h e low temperature cloud p o i n t , g i v i n g e x c e l l e n t freeze/thaw p r o p e r t i e s . The P e t r o BAF c o m b i n a t i o n d r i e s l e s s t a c k y t h a n sodium l a u r y l s u l f a t e a l o n e . F o r m u l a 908 C a r p e t Shampoo, H i g h Foam Inqredients: Water P e t r o BAF L i q u i d W i t c o l a t e WAC-LA B l e n d i n g P r o c e d u r e : B 2nd i n g r e d i e n t s i n t h e o r d e r Use L e v e l :
1 t o 2 ounces p e r g a l l o n . is
I

Wt%
71.1 6.7
22.2

Comments : P e t r o BAF, i n c o m b i n a t i o n w i t h sodium l a u r y l s u l f a t e , r e d u c e s t h e low t e m p e r a t u r e c l o u d p o i n t , g i v i n g e x c e l l e n t f r e e z e / t h a w p r o p e r t i e s . The P e t r o BAF c o m b i n a t i o n d r i e s l e s s t a c k y t h a n sodium l a u r y l s u l f a t e a l o n e . F o r m u l a 910 C a r p e t S p o t Remover Inqredients: Water, 13.1. W i t c o l a t e WAC-LA P e t r o BA L i q u i d G l y c o l E t h e r DPM Glycol Ether P M FC-129 ( 1 % S o l i d s ) Blending Procedure: Blend ingredients i n t h e order l i s t e d .

Wt%
90.3 3.3 0.5 3.5 2.3 0.1

Typical Properties: S p e c i f i c G r a v i t y : 0.999 Wt./Gal. l b s . : 8.33 pH: 1 0 . 3 5 Use D i l u t i o n : Use as i s F o r m u l a 945 SOURCE: W i t c o C o r p . : S u g g e s t e d F o r m u l a t i o n s

Rug, Floor, Carpet, Upholstery Shampoos and Cleaners

153

Carpet 8 U p h o l s t e r y Cleaner T h i s o e n e r a l Duroose s t a i n remover f o r m u l a t i o n is o a r t i c u l a r l v e f f e c t i v e i n removing o i l s t a i n s . Ingredient : Wt% D e i o n i z e d Water ( h o t ) 37.0 SMA-2625 R e s i n 2.4 Aqua Ammonia 0.7 W i t c o l a t e WACLA 18.0 W i t c o n a t e 60T L i q u i d 4.0 Avanel 5-70 4.0 Dei o n i zed Water 34.0 Dye, Fragrance, e t c . (2.5. pH ( a s i s ) : 8.0-9.0 Appearance: C l e a r l i q u i d S p e c i f i c G r a v i t y : 1.016 Procedure: 1 . Charge t h e h o t w a t e r t o a m i x i n g v e s s e l and s t a r t a g i t a t i o n . S l o w l y s i f t i n t h e SMA-2625 R e s i n t o a v o i d c l u m p i n g . Add t h e Aqua Ammonia, a p p l y c o o l i n g , and mix w e l l u n t i l t h e r e s i n i s dissolved. 2 . Reduce a g i t a t i o n and add t h e r e m a i n i n g i n g r e d i e n t s . S t o p a g i t a t i o n t o permit deaeration o f t h e product p r i o r t o filling off. 3 . I f t h i s p r o d u c t i s t o be c o l o r e d , a p o r t i o n o f t h e f i n a l w a t e r s h o u l d be r e s e r v e d f o r d i s s o l v i n g t h e dye. A f t e r t h e dye is t h o r o u g h l y mixed, t h e dye s o l u t i o n may be added NOTE: Use " a s i s " on c a r p e t i n g . D i l u t e 1 O : l and 5 : l w i t h water f o r u pholstery.
V i n y l Dressing ( 8 ) Ingredient: Wt% Part A: M a s i l EM 250 C 18.0 M a s i l EM 10,000 C 10.0 Dei o n i zed Water 30.0 P a r t B: Macol OP-10 SP 2.0 G1 y c e r i ne 1.o D e i o n i r e d Water 38.0 Sodium Benzoate 1.o Procedure: 1 . To a m i x i n g v e s s e l , c h a r g e t h e M a s i l EM 250 C and M a s i l EM 10,000 C . S t a r t g e n t l e a g i t a t i o n . S l o w l y add t h e w a t e r so as n o t t o b r e a k t h e e m u l s i o n . 2. I n a s e p a r a t e m i x i n g v e s s e l , c h a r g e t h e Macol OP-10 SP and g l y c e r i n e t o t h e water. Mix w i t h g e n t l e a g i t a t i o n u n t i l a l l components a r e d i s s o l v e d , and t h e s o l u t i o n i s f r e e o f " f i s h e y e s " . Charge t h e sodium b e n z o a t e and m i x u n t i l d i s s o l v e d . 3 . Under g e n t l e a g i t a t i o n , add P a r t 0 t o P a r t A. C o n t i n u e m i x i n g g e n t l y t o a v o i d a i r e n t r a p m e n t . NOTE: T h i s f o r m u l a i s d e s i g n e d to b e used "as i s " . I f d e s i r e d , UV a b s o r b e r s and o t h e r compone n t s may be added t o t h e f o r m u l a t i o n . SOURCE: PPG I n d u s t r i e s , I n c . : Suggested F o r m u l a t i o n s

154

Advanced Cleaning Product Formulations

Carpet & Upholstery Cleaner Ingredients: Dei o n i zed Water ( H o t ) SMA-2625 R e s i n Aqua Ammonia Sodi u m L a u r y l S u l f a t e R i chami de 5725 Avanel 5-70 Dei o n i zed Water Dye, F r a g r a n c e , E t c .
pH (as i s ) : 8.0-9.0 Appearance: C l e a r l i q u i d S p e c i f i c G r a v i t y : 1 .016

Wt%
37.0 2.37 0.67 18.0 4.0 4.0 33.96 As d e s i r e d

Procedure: Charge t h e h o t w a t e r t o t h e m i x i n g v e s s e l and s t a r t a g i t a t i o n . S l o w l y s i f t i n t h e SMA-2625 r e s i n t o a v o i d c l u m p i n g . Add t h e Aqua Ammonia, a p p l y c o o l i n g and m i x w e l l u n t i l t h e r e s i n i s d i s s o l v e d . Reduce a g i t a t i o n and add t h e r e m a i n i n g i n g r e d i e n t s . I f t h e p r o d u c t i s t o be c o l o r e d , a p o r t i o n o f t h e f i n a l water s h o u l d b e r e s e r v e d f o r d i s s o l v i n g t h e d y e . A f t e r t h e dye i s t h o r o u g h l y m i x e d , t h e d y e s o l u t i o n may b e added t o t h e p r o d u c t . Stop a g i t a t i o n t o p e r m i t deaeration o f t h e product p r i o r t o filling off. Notes : T h i s i s a g e n e r a l p u r p o s e o i l y s t a i n remover. T h i s f o r m u l a t i o n i s p a r t i c u l a r l y e f f e c t i v e a t r e m o v i n g o i l s t a i n s . Use a s - i s on c a r p e t i n g . D i l u t e 1 O : l and 5 : l w i t h w a t e r f o r u p h o l s t e r y . N o t e : The dye s h o u l d b e t h o r o u g l y s c r e e n e d t o a v o i d f a b r i c staining. F o r m u l a t i o n CP-101 L i q u i d Steam C a r p e t C 1 e a n e r F o r H a r d Water Systems Ingredients: Sodium M e t a s i 1 i c a t e A Tetrapotassium Pyrophosphate Emphos PS-331 Macol NP 11 D e i o n i z e d Water Procedure: Add i n g r e d i e n t s as l i s t e d .

Wt%
7.5 12.5 4.0 1.o 76.0

SOURCE: PPG I n d u s t r i e s , I n c . : Suggested F o r m u l a t i o n s

Rug, Floor, Carpet, Upholstery Shampoos and Cleaners

155

F1oor C l e a n e r Ingredients:
M a z a m i de 1281

wtsl, 8.0
2.0 2.0 88.0

Sodi urn T r i p o l y p h o s p h a t e T e t r a p o t a s s i u m Pyrophosphate Water Procedure: Add i n g r e d i e n t s as l i s t e d . L i q u i d F l o o r Cleaner Ingredients: Macol NP 9 . 5 Sodi urn T r i p o l yphosphate T r i s o d i urn Phosphate Sodi urn M e t a s i 1i c a t e P e n t a h y d r a t e Maphos 60A Water Procedure: A d d i n g r e d i e n t s as l i s t e d . NOTE: T h i s f o r m u l a t i o n i s s t a b l e t o 120F. F l o o r Scrubber Ingredients: Sodi urn M e t a s i 1 ic a t e Tetrasodium Pyrophosphate Emphos PS-331 D e i o n i z e d Water Mazami de 1281 Sodium H y d r o x i d e , 50% Procedure : Add i n g r e d i e n t s as l i s t e d .

Q 7.0 8.0 2.0 2.0 3.0 78.0

2.0 18.0 15.0 53.95 6.0 5.05

SOURCE:

PPG I n d u s t r i e s ,

Inc.:

Suggested F o r m u l a t i o n s

156

Advanced Cleaning Product Formulations

Household Carpet F r e s h e n e r / A n t i s t a t InQredients: P a r t A: P u f f e d Borax ( 1 0 l b s / c u f t ) Fragrance Sodi um B i c a r b o n a t e L a r o s t a t 519 P a r t 6: Sodi um B i c a r b o n a t e

Wt%
1.8 0.2 15.0 3.0 80.0

Procedure: I n a r i b b o n m i x e r o r V - b l e n d e r , c h a r g e t h e p u f f e d b o r a x and f i r s t p o r t i o n o f sodium b i c a r b o n a t e . S t a r t m i x i n g and s l o w l y add t h e f r a g r a n c e . A f t e r a l l o f t h e f r a g r a n c e has been added, c o n t i n u e m i x i n g f o r 5 m i n u t e s t o c o m p l e t e a b s o r p t i o n . Add t h e L a r o s t a t 519 and t h e r e m a i n i n g sodium b i c a r b o n a t e . M i x f o r 15 m i n u t e s more. Notes : T h i s i s a powdered c o m b i n a t i o n consumer f r e s h e n e r / a n t i s t a t . The p r o d u c t i s d e s i g n e d t o b e shaken o n t o t h e c a r p e t , l i g h t l y r u b b e d i n t o t h e c a r p e t and t h e n t h e e x c e s s removed b y vacuuming. F o r m u l a t i o n SP-I01 Pump S p r a y C a r p e t A n t i s t a t Ingredients: P a r t A: Water Isopropyl Alcohol L a r o s t a t 264 A Appearance: C l e a r , w a t e r - w h i t e S p e c i f i c G r a v i t y : 0.98 t o pale-yellow l i q u i d

94.3 5.0 0.7

Procedure: To a m i x i n g vessel, charge t h e water, f o l l o w e d by t h e i s o p r o p y l a l c o h o l and L a r o s t a t 88. M i x u n t i l c l e a r . Notes : T h i s i s a n o n - a e r o s o l , pump s p r a y c a r p e t a n t i s t a t f o r t h e removal o f n u i s a n c e s t a t i c . T o remove s t a t i c f r o m c a r p e t i n g and other surfaces, spray l i g h t l y w i t h t h i s formulation. It i s not necessary t o s a t u r a t e t h e surface. I f a d d i t i o n a l p r o t e c t i o n i s needed, i t i s p r e f e r a b l e t o have r e p e a t a p p l i c a t i o n s r a t h e r t h a n one, t o i n s u r e even t r e a t m e n t . F o r m u l a t i o n SP-102

SOURCE: PPG I n d u s t r i e s ,

Inc.:

Suggested F o r m u l a t i o n s

e t c .0 5. A l t e r n a t i v e l y . InQredients: W i t c o n o l NP-100 Dowanol PM G l y c o l E t h e r Isopropyl Alcohol Amy1 A c e t a t e Water Benefit : Detergent and degreaser S o l v e n t and c o u p l i n g a g e n t Solvent Sol vent Vinyl. A l t e r n a t i v e l y .5 1.0 5. ) and w i p e o n t o t h e s u r f a c e t o b e c l e a n e d . V i n v l . ) and w i p e o n t o t h e s u r f a c e t o b e c l e a n e d . t h e n r i n s e . a l l o w t o s e t a few m i n u t e s . Product I n f o r m a t i o n : W i t c o n o l NP-100 Dowanol PM G l y c o l E t h e r Amyl A c e t a t e I s o p r o p y l A1 coho1 Formula 1001 Benefit : D e t e r g e n t and d e g r e a s e r S o l v e n t and c o u p l i n g a g e n t Sol vent Sol vent SOURCE: W i t c o C o r p .0 2. t h e n r i n s e o r hose o f f . s p r a y o n t o t h e s u r f a c e t o b e c l e a n e d . Use I n s t r u c t i o n s : A p p l y f i n i s h e d p r o d u c t t o a t o w e l o r t o w e l l e t e (Kimwipe. Floor. and P l a s t i c C l e a n e r Wt% 10. t h e n r i n s e . Upholstery Shampoos and Cleaners 157 h i qlai d L e a t h e r .Rug. Use I n s t r u c t i o n s : A p p l y f i n i s h e d p r o d u c t t o a t o w e l o r t o w e l l e t e (Kimwipe. Carpet.5 1 .5 Blending Instructions: Combine i n g r e d i e n t s i n t h e o r d e r shown and m i x t h o r o u g h l y .0 2. s p r a y o n t o t h e s u r f a c e t o b e c l e a n e d . 5 Blending Instructions: Combine i n g r e d i e n t s i n t h e o r d e r shown and m i x t h o r o u g h l y . e t c . Product I n f o r m a t i o n : Product: DeSonic 9N Dowanol PM G l y c o l E t h e r Amyl A c e t a t e Isopropyl Alcohol Formula 1000 L i q u i d Leather. a l l o w t o s e t a few m i n u t e s . : Suggested F o r m u l a t i o n s .o 81. a n d P l a s t i c C l e a n e r and R e s t o r e r Inqredients: DeSonic 9N Dowanol PM G l y c o l E t h e r Isopropyl Alcohol Amy1 A c e t a t e Water Wt% 10. t h e n r i n s e o r hose o f f .o 81 .

0 56.0 4. Use D i l u t i o n : 1-2 o z / g a l Formula 904 Heavy D u t y Steam E x t r a c t i o n C a r p e t C l e a n e r Inqredi ents: Sodium C a r b o n a t e (Soda Ash) T r i s o d i u m Phosphate.: Suggested F o r m u l a t i o n s .0 65. o 5.0 29. Medium D u t y Steam E x t r a c t i o n C a r p e t C l e a n e r Inqredients: Sodi um T r i p o l y p h o s p h a t e . P e n t a h y d r a t e P e t r o 2 2 Powder Optical Brightener Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d .0 0. P e t r o 22 Powder EDTA Powder Perfume 81 e n d i n g P r o c e d u r e : B1 end i n g r e d i e n t s in t h e o r d e r 1 isteci. C r y s t a l Sodium M e t a s i l i c a t e .158 Advanced Cleaning Product Formulations Low Cost E x t r a c t i o n C a r p e t C l e a n e r Ingredients: Water.0 4. I . D . Use D i l u t i o n : 1-2 o z / g a l F o r m u l a 901 91 . P e n t a h y d r a t e Sodium S u l f a t e ( S a l t Cake) P e t r o 2 2 Powder B l e n d i n g Procedure: F o r m u l a 905 Blend i n g r e d i e n t s i n t h e order l i s t e d Wt% 10.0 q.0 10. L i g h t D e n s i t y Sodi urn M e t a s i 1 i c a t e . of w a t e r Premium.0 20.5 Use D i l u t i o n : 1-2 o z / g a l SOURCE: Witco Corp. s .5 5.

25 2.0 6.7 3.: Suggested F o r m u l a t i o n s RUQ Steam C l e a n e r (Liquid) S o i l . Use C o n c e n t r a t i o n : 2-3 ounces p e r g a l l o n i n e x t r a c t o r . 4 % bw ( 6 . 12 M o l e s EO Use D i 1u t i on : 4 . Add B u r c o s p e r s e A P Powder ( a n d i f d e s i r e d ) B u r c o t a s e SP-60.Rug s c r u b b e r Manufacture .0 2. p e t r o l e u m o i l and g r e a s e . t h e n Sodium B i c a r b o n a t e and b l e n d u n t i l u n i f o r m . B l e n d u n t i 1 u n i f o r m .P o l y e s t e r and n y l o n A p p l i c a t i o n Method .5 1.Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition: Water M e t s o Beads 2048 Sodium X y l e n e S u l f o n a t e .Rug. .o as d e s i r e d Procedure: S p r a y LAF-6 ( a n d i f d e s i r e d ) f r a g r a n c e o n t o STPP and b l e n d u n t i l a b s o r b e d . Add B u r c o S Z S . and p a r t i c u l a t e S u r f a c e .9 . : Suggested F o r m u l a t i o n clay Wt% 79.5 0.Food ( f a t and p r o t e i n ) .9 . Carpet.6 7. 40% C12-Cl5 L i n e a r A l c o h o l . SOURCE: B u r l i n g t o n Chemical C o . Inc. Upholstery Shampoos and Cleaners 159 Low Foaming C a r p e t E x t r a c t o r D e t e r g e n t Component: Sodi um B i c a r b o n a t e STPP B u r c o LAF-6 Burco SZS B u r c o s p e r s e AP Powder B u r c o t a s e SP-60 ( i f d e s i r e d ) Fragrance Wt% t o 100% t o t a l 47. Floor. 7 .1 2 o z / g a l 1o n ) SOURCE: The PQ C o r p .

Typical Properties: S o l i d s : 8.0 2. Formula 932 Heavy D u t y F l o o r Cleaner Ingredients: Water. T y p i c a l Propert ies : S o l i d s : 22.0 5.0 4. Sodi u Carbonate m Rewoteric AM 8-14 Versene 100 Butyl Cellosolve \Mt% 79.160 Advanced Cleaning Product Formulations No Rinse F l o o r Cleaner I npredie n t s : Water.0 2.0 Blending Procedure: Add i n g r e d i e n t s i n order shown and d i s s o l v e completely between each a d d i t i o n .0 5.0% Formula 933 No-Rinse F l o o r Cleaner Deareaser Ingredients: Deionized water Sodium carbonate Rewoteric AM V Versene 100 Butyl Cellosolve WtO/o 79. : Suggested Formulations .9 V i s c o s i t y : 4 cps Formula 951 SOURCE: Witco Corp.0 Blending Procedure: Add i n g r e d i e n t s i n order shown and d i s s o l v e completely between each addi t ion.0 81 end$ng Procedure: Add i n g r e d i e n t s i n order shown and d i s s o l v e completely between each a d d i t i o n .0 10.I.0 10.I.0 4. D.0 5. Varami de A-1 2 T r i sodi u Phosphate m Sodium Tripolyphosphate Wt% 78.1% pH: 10.0 7.0 10. D.

Upholstery Shampoos and Cleaners 161 Wax S t r i p p e r ( A ) Inqredients: Oleic Acid Monoethanol ami ne Avanel S .0 2.5 Procedure: Add i n g r e d i e n t s as l i s t e d .o 1 . Wax S t r i p p e r ( B ) Inaredients: Oleic Acid Monoethanolamine Avanel S .5 1 .0 2. 50% m Versene 100 Dowanol TBA Water Procedure: Add i n g r e d i e n t s as l i s t e d .Rug. : Suggested F o r m u l a t i o n s .o 1 . 5 . P Mac01 NP 1 0 . Mafo CB-40 can be s u b s t i t u t e d f o r t h e Mazox LDA. 5 EDTA. d i l u t e 1 : l O t o 1:30.o 1 .o 8 .0 2.o 0.0 81 . Floor. 45% Sodi u H y d r o x i d e . Carpet.0 7. I n c . 45% Sodi u H y d r o x i d e . C o n c e n t r a t e d Wax S t r i p p e r Inaredients: Sodium H y d r o x i d e . o 5.7 4 Potassium H y d r o x i d e . To use. Macol NP 9 .o 8.7 4 Potassium H y d r o x i d e .o WtO/o 50% 1 .0 1 . SOURCE: PPG I n d u s t r i e s .o 1 . 5 can be s u b s t i t u t e d f o r t h e Macol N 9 .0 2.5 8 .o 1 .o 1 5.5 1 6. 40% Mazox LDA B a r q u a t MB-50 Monoethanolami ne Water Wt% 7. 50% m Versene 1 0 0 E t h y l e n e G1 y c o l Monobutyl E t h e r Water Procedure: Add i n g r e d i e n t s as l i s t e d .0 1 .

14. Miscellaneous 1 fi7 .

7 Blending Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n . 84. I .Miscellaneous 163 B a c t e r i o s t a t i c C o n c e n t r a t e w/Pine 021 I n q r e d ie n t s : Wt% Phase I : Isopropanol 10. D .0 5.0 Oleic Acid 8. V a r q u a t 5 0 MC G1 y o x a l ( 4 0 % ) R e w o t e r i c AM DML-35 Blending Procedure: Add i n g r e d i e n t s 1 n o r d e r shown and d i s s o l v e c o m p l e t e l y each add1 t ion. 68.2 P o t a s s i um H y d r o x i d e (87%) 2. cps: 5 S o l i d s : 10. cps: 4 Sol 1 d s : 1 3 .6 V a r i q u a t 50 MC Varox 365 4. Typical Properties: Viscosity. D . 2 Formula 304 SOURCE: Witco Corp.0 10.0 Phase 11: Water.7% pH: 1 2 . 1 Formula 3 0 3 -~r e d i Ing Hospital D is infectant ents: Wt% Water. Combine Phase I T i n g r e d i e n t s and m i x t h o r o u g h l y .8 5.: Suggestecl F o r m u l a t i o n s .0 between Ingredi e n t s : Water. W h i l e m i x i n g . cps: 4 S o l i d s : 6.0 17.6% pH: 9 . 0 % pH: 7 . add Phase I t o Phase 1 1 . I .0 Varox 1 7 7 0 Pine O i 1 12.0 81 e n d i ng P r o c e d u r e : Combine Phase I i n g r e d i e n t s and m i x t h o r o u g h l y .2 9. 62.5 Sod1 urn H y d r o x i d e ( 3 0 % ) 0. D . T y p i c a l P r o p e r t i es : V i s c o s i t y . Typical Properties: V l s c o s l t y . I . 3 Formula 302 _ e n e r a l D i s_n f _ c t_ n _ S_ l u t i o n ~ G ~ ~ _ i e a t o _ _ ~ wtsl.0 Versene 100 1.

30 P i l o t SXS-40 2.30 C a l o x y l a t e N-9 7.00 I g e p a l CO-430 20.00 100 SUS N a p h t h e n i c O i l 28.50 0.00 0.20 Na4 EDTA 1.00 C a l s o f t F-90 Sodi um S i 1 ic a t e 30.00 30.20 1.00 Sodium C a r b o n a t e Sodi um H y d r o x i d e 25.D i l u t e 1 : 3 w i t h 100 SUS n a p h t h e n i c o i l .I64 Advanced Cleaning Product Formulations C u t t i n g O i l Concentrate Ingredients: Wei s h t % Aristonate M 36.90 1.D i l u t e 4 : 7 6 w i t h 160 ppm h a r d w a t e r .D i l u t e 4 : 7 6 w i t h 160 ppm h a r d w a t e r .00 TEA. : Suggested F o r m u l a t i o n s . S o l u b l e O i l .00 8. F o r m u l a t i o n CON-001-01 White Wall Cleaner Wei s h t % Insredients : Water 60.00 Comments a b o u t t h i s f o r m u l a : V i s c o s i t y o f t h e p r o d u c t i s a b o u t 160 cPs a t room t e m p e r a t u r e . A c t i n o l FA-1 C a l a m i d e SM 100 SUS N a p h t h e n i c O i l Water Comments a b o u t t h i s f o r m u l a : E m u l s i o n .75 C o n c r e t e C 1e a n e r Ingredients: Weight% 5.00 Sodi um T r i p h o s p h a t e 10.65 85.20 C a l s o f t L-40 29.00 Comments a b o u t t h i s f o r m u l a : 1 . 85% T a l l O i l A c i d . 85% Oleic A c i d 8. F o r m u l a t i o n SOL-003-01 Cutting Oi 1 Ingredients: Aristonate M TEA. E m u l s i o n . F o r m u l a t i o n SOL-004-01 Wei q h t % 10. F o r m u l a t i o n TIR-001-01 SOURCE: P i l o t Chemical Co. 2 .00 Comments a b o u t t h i s f o r m u l a : G r i n d m i x t u r e t o g e t h e r t o y i e l d a s l i g h t l y t a c k y w h i t e powder.

0 2. I .0 7. Typical Properties : Appearance. D . I .0 10. H e a t t o 140F. 4 Formula 1120 Heavy Cream P a s t e Hand C l e a n e r Ingredients: Water. c p s : 6360 S o l i d s : 19. T r i s o d i u m Phosphate Sodium C i t r a t e Glycerin Phase 11: d . Room Temp. Typical Properties: V i s c o s i t y . 7 Formula 1121 SOURCE: W i t c o C o r p . Combine Phase I1 i n g r e d i e n t s i n s e p a r a t e v e s s e l and m i x t h o r o u g h l y .: S o l i d s : 12.Miscellaneous 165 d L i monene Water1 e s s Hand C1 e a n e r Ingredients: Phase I : Water.0 10.o 2.0 2. : Suggested F o r m u l a t i o n s . O 1 .L i monene DeSonic 9N V a r o n i c T202 Wt% 81 .0 5.0% pH: 1 0 . add Phase 11 Po Phase I.0 10. Heat t o 140F.5% pH: 8 . Varami de MA-1 R e w o t e r i c AM 8-15 W i t c o l a t e SE-5 WtS/o 70. W h i l e m i x i n g r a p i d l y .0 81 e n d i n g P r o c e d u r e : Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i on.Cool q u i c k l y t o s t a b i l i z e e m u l s i o n .0 B l e n d i n g Procedure: I n v e s s e l fit1 combine Phase I i n g r e d i e n t s and m i x t h o r o u g h l y . D .

c : 19 CPH. Inc. d i p e n t e n e i s t h e same as l i m onene.80 0. D i s s o l v e t h e sodium m e t a s i l i c a t e ( i f used) i n t h e w a t e r and add i t t o t h e e m u l s i f i e r s and d i p e n t e n e w i t h m i x i n g . c : 11 CPH.: B u l l e t i n : Terpene M i c r o e m u l s i o n s . ) O t h e r components o f commercial d i p e n t e n e i n c l u d e c a r e n e and a l p h a .and b e t a .10 79.90 Add and m i x t h e f i r s t f o u r i n g r e d i e n t s ( d i p e n t e n e and emulsi f i e r s ) . D-limonene i s one o f t h e 2 o p t i c a l i s o m e r s o f d i p e n t e n e .00 0.80 1 . ( S t r u c t u r a l l y .40 1.00 8. SOURCE: Tomah P r o d u c t s . c : 1 1 CPH.80 87 00 ~ 1.80 1.00 14.166 Advanced Cleaning Product Formulations Dipentene Microemulsion Formulations D i p e n t e n e i s d e s c r i b e d as a p r o d u c t o f f r a c t i o n a t i o n o f p i n e o i l s c o n t a i n i n g r e l a t e d monocyclic t e r p e n e hydrocarbons.60 Ingredients: D i p e n t e n e 122 Tomah E-14-5 Tomah E-14-2 Tomah A l k a i S u r f a c t a n t Water C P L . C : 50 Emu1 s i f e r / D i p e n t e n e R a t i o : VVt.00 6.00 1.% 10.p i n e n e . Non-alkaline Formulations Ingredients: D i p e n t e n e 122 Tomah E-14-5 Tomah E-14-2 Tomah A l k a l i S u r f a c t a n t Water CPL. C : 41 Emulsifier/Dipentene Ratio: Wt.% 20.10 1. predomin a n t l y d i p e n t e n e . C P L i s " l o w t e m p e r a t u r e c l o u d p o i n t " w h i l e CPH i s " h i g h temperature cloud p o i n t " .40 0.10 Inaredients: D i p e n t e n e 122 Tomah E-14-5 Tomah E-14-2 Tomah A l k a l i S u r f a c t a n t Water CPL.80 62. C : 30 Emulsifier/Dipentene Ratio: & % 5.

00 0.60 1.00 8.50 1 . ( S t r u c t u r a l l y . c : 20 CPH.00 Ingredients: D i p e n t e n e 122 E-14-5 E-14-2 A1 k a l i S u r f a c t a n t Water Sodium M e t a s i l i c a t e P e n t a h y d r a t e CPL.50 1. D-limonene i s one o f t h e 2 o p t i c a l i s o m e r s o f d i p e n t e n e .00 0.00 17. C : 18 CPH.30 56.5 E-14-2 A1 k a l i S u r f a c t a n t Water Sodium M e t a s i l i c a t e P e n t a h y d r a t e Wt.20 CPL. A l k a l i n e Formulations Ingredients: D i p e n t e n e 122 Wt.25 73.50 1 . d i p e n t e n e i s t h e same a s l i m o n ene.I0 Add and m i x t h e f i r s t f o u r i n g r e d i e n t s ( d i p e n t e n e and e m u l s i f i e r s ) . ) O t h e r components o f commercial d i p e n t e n e i n c l u d e c a r e n e and a l p h a . : B u l l e t i n : Terpene M i c r o e m u l s i o n s . I n c . C : 43 E m u l s i f i e r / D i p e n t e n e R a t i o : 1 . C : 4 4 Emulsifier/Dipentene Ratio: 2.% 10. C : 46 Emulsifier/Dipentene Ratio: Wt.50 Ingredients: D i p e n t e n e 122 E.70 E-14-5 E-14-2 A1 k a l i S u r f a c t a n t Water Sodium M e t a s i l i c a t e P e n t a h y d r a t e CPL.10 3.00 12.80 1. C : 15 CPH.% 20.75 2.96 5. D i s s o l v e t h e sodium m e t a s i l i c a t e ( i f used) i n t h e w a t e r and add i t t o t h e e m u l s i f i e r s and d i p e n t e n e w i t h m i x i n g .and b e t a .30 1.1 4 .50 83.p i n e n e . CPL i s " l o w t e m p e r a t u r e c l o u d p o i n t " w h i l e CPH i s " h i g h temperature cloud p o i n t " . SOURCE: Tomah P r o d u c t s . predomi n a n t l y d i p e n t e n e .Miscellaneous 167 D i p e n t e n e M i c r o e m u l s i o n Formul a t i o n s ( C o n t i nued) D i p e n t e n e i s d e s c r i b e d as a p r o d u c t o f f r a c t i o n a t i o n o f p i ne o i l s c o n t a i n i n g r e l a t e d m o n o c y c l i c t e r p e n e h y d r o c a r b o n s .

5 Wt.% 30.0 23.1 4 . These m i c r o e m u l s i o n s s h o u l d be c l e a r and s t a b l e i n t h e tempe r a t u r e r a n g e f r o m 20-37C.0 17. O u t s i d e t h a t r a n g e t h e y may c l o u d o r s e p a r a t e .6 Add each component i n t h e o r d e r g i v e n and m i x u n t i l homogeneous b e f o r e a d d i n g t h e n e x t component.1 6. Add t h e w a t e r i n p o r t i o n s with mixing.9 10.168 Advanced Cleaning Product Formulatioris H y d r o c a r b o n S o l v e n t M i c r o e m u l s i ons Developed i n o r d e r t o o f f e r replacements f o r expensive d . b u t w i l l r e g a i n c l a r i t y upon r e t u r n i n g t o room tempe r a t u r e . Exxsol D-I10 Formula A: Ingredients: E x x s o l D-110 Tomah E-14-2 Tomah E-14-5 Tomah A l k a l i S u r f a c t a n t S o f t Water Formula 8 : Inaredients: E x x s o l D-110 Tomah E-14-2 Tomah E .4 4.% 40.5 37. I n c . a s m a l l amount o f a d d i t i o n a l Tomah A l k a l i S u r f a c t a n t s h o u l d b e added.% 20. They a l l have f l a s h p o i n t s above I O O C and l o w VOC c o n t e n t .3 58. SOURCE: Tomah P r o d u c t s . I f i t i s necessary t o r a i s e t h e c l o u d p o i n t temperature.l i m o n e n e and p i n e o i l i n m i c r o e m u l s i o n c l e a n e r s .8 8.9 8.0 11. : Suggested F o r m u l a t i o n s .4 Wt.7 16.9 5.5 Tomah A l k a l i S u r f a c t a n t S o f t Water Formula C : Inqredients: E x x s o l D-110 Tomah E-14-2 Tomah E-14-5 Tomah A l k a l i S u r f a c t a n t S o f t Water Formulations \Nt.

I n c .0 S t a r t b y d i s s o l v i n g t h e sodium m e t a s i l i c a t e ( i f u s e d ) i n t h e w a t e r .6 1. : Suggested F o r m u l a t i o n s .7 4. E-14-5.7 1. Unbui 1 t : Component: S o f t Water Sodium Metas l i c a t e P e n t a h y d r a t e Tomah E-14-2 Tomah E-14-5 Tomah A1 k a l i S u r f a c t a n t I s o p a r Wi Wt.a 7. Isopar M F o r m u l a t i o n s I s o p a r M can b e s u b s t i t u t e d d i r e c t l y f o r t h e E x x s o l D-110 i n t h e above f o r m u l a t i o n s .0 L i g h t l y b u i 1t : Component: S o f t Water Sodium M e t a s i l i c a t e P e n t a h y d r a t e Tomah E-14-2 Tomah E-14-5 Tomah A l k a l i S u r f a c t a n t Isopar M Wt. Then add t h e E-14-2.% 83. The c l o u d p o i n t c a n be r a i s e d f u r t h e r b y a d d i n g a s m a l l amount o f a d d i t i o n a l A l k a l i Surfactant.0 0. t h e n s h o u l d c l e a r a s t h e l a s t o f t h e I s o p a r M i s added. F i n a l l y add t h e I s o p a r M i n p o r t i o n s w i t h m i x i n g .6 6. a n d A l k a l i S u r f a c t a n t . t w o f o r m u l a t i o n s w i t h l o w e r s o l v e n t c o n t e n t have been d e v e l o p e d . M i x u n t i l homogeneous. The m i x t u r e w i l l c l o u d .l i m o n e n e and p i n e o i l i n m i c r o e m u l s i o n c l e a n e r s .% 79. These m i c r o e m u l s i o n s w i l l b e c l e a r and s t a b l e i n t h e t e m p e r a t u r e r a n g e f r o m 20-5OC. SOURCE: Tomah P r o d u c t s .0 4.6 5.Miscellaneous 169 Hydrocarbon S o l v e n t Microemulsions ( C o n t i n u e d l Developed i n o r d e r t o o f f e r r e p l a c e m e n t s f o r e x p e n s i v e d . I n a d d i t i o n .o 5. They a l l have f l a s h p o i n t s above 1OOC and l o w VOC c o n t e n t .0 1.

00% BFGoodrich S p e c i a l t y Chemicals: DET-510 . M i x u n t i l uniform.70 15. o t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r ( 8 0 0 r p m ) . Add t h e Makon 10 and m i x u n t i l homogeneous.I70 Advanced Cleaning Product Formulations .20 0. Add t h e T E A . Use a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s S c r e e n t h e Pemuleri r e s i n i n t .00 0.30 rpm): 1. 83.3 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a1 S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) Stepan C o . 3 . 2 .Emu s resins S i l i c o n e o i l c a n b e e m u l s i f i e d and s t a b i l i z e d v i a t h e u s e o f Pemulen r e s i n s .si-o~n-UsinxPemulen . Add t h e s i l i c o n e o i l w i t h v i g o r o u s a g i t a t i o n . 4 . Inycedi e n t l D I Water Pemulen 1622 ( 1 ) Makon 10 ( 2 ) Dow 200 S i l i c o n e F l u i d ( 3 ) Triethanolamine Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 Product pH: 7. ( 3 ) Dow C o r n i n g Procedure: 1 .80 0..h. V i_s_cosi_tv_s_jlicon 1. Total Actives: Silicone O i l : SOURCE: W t"/. !o L .000 c p 15. A l l o w t o m i x u n t i l homogeneous and f r e e o f p o l y m e r l u m p s . The r e s i n s s t a b i l i z e e m u l s i o n s v i a e l e c t r o s t a t i c s t a b i l i z a t i o n . T h i s r e l i e v e s t h e c o n s t r a i n t o f s e e k i n g an appropr i a t e surfactant emulsifier. M i x u n t i l smoot.

5 . Cool t o 40C.0 25.2 0. Inc. The Monaquat TG p r o v i d e s body b u i l d i n g c o n d i t i o n i n g and d e t a n g l i n g w h i l e l e a v i n g a s o f t smooth f e e l .0 0.L i monene Wt% 70. Monaquat I S I E S i s an e f f e c t i v e l o n g l a s t i n g a n t i s t a t t h a t controls d i r t attraction. s p r i n k l e i n h y d r o x y e t h y l c e l l u l o s e and t u r n h e a t o n . f r a g r a n c e and p r e s e r v a t iv e . m i l d detergent which w i l l leave your p e t Ingredients: Water M o n a t e r g e 779 d . Monaquat I S I E S . Inaredients: Water Hydroxyethyl C e l l u l o s e Stearic acid Stearyl alcohol Monaquat TG Monaquat I S I E S ( I s o s t e a r y l E t h y l m i d o n i u m E t h o s u l f a t e ) P h o s p h o l i p i d EFA ( L i n o l e a m i d o p r o p y l PG-Dimonium C h l o r i d e Phosphate) Sodium C h l o r i d e Wt% 85. A d d c o l o r .0 2. Heat and m i x t o 70-75C ( a smooth c r e m e ) .0 5.0 0. A d j u s t pH t o 7 . P h o s p h o l i p i d EFA.Miscellaneous 171 Lumi n i z i n g P e t C o n d i t i o n e r P h o s p h o l i p i d EFA adds s h i n e and a s i l k y t e x t u r e t o t h e a n i m a l ' s c o a t o r mane. and sodium c h l o r i d e . 0 . Add c o l o r and p r e s e r v a t i v e .: Suggested F o r m u l a t i o n s .0 Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n . s t e a r y l a l c o h o l .5 Procedure: Change w a t e r w i t h a g i t a t i o n . Typical Properties: Appearance: Opaque v i s c o u s l o t i o n Recommended Use D i l u t i o n : As i s F o r m u l a t i o n F-777 P e t Shampoo A h i g h foaming. A d j u s t pH t o 4 . f r e s h and c l e a n . Typical Properties: Appearance: C l e a r y e l l o w l i q u i d Recommended Use D i l u t i o n : F o r m u l a t i o n F-774 1:50 w i t h water SOURCE: Mona I n d u s t r i e s . 0 . Package.5 2. Monaquat TG.8 2. Package.0 7. 5 . A t 50-60C add s t e a r i c a c i d .

L i monene Monamul se dL-1273 Water I Wt% 10.0 18.0 Wt% 65. Formula Inqredients: d . Add water s l o w l y w i t h s t i r r i n g .172 Advanced Cleaning Product Formulations M i cro-Emu1 s i ons with d-Li monene The f o l l o w i n g c o n c e n t r a t e s a r e c l e a r . The f o r m u l a t h e m s e l v e s a r e c l e a r and e x h i b i t a bloom e f f e c t upon d i l u t i o n .L i monene Monamulse dL-1273 Isopropanol Water Formula I11 Ingredients: d . mix s u r f a c t a n t w i t h d-Limonene u n t i l d i s s o l v e d .0 12. Recommended Use D i l u t i o n : 1 : 1 0 w i t h w a t e r SOURCE: Mona I n d u s t r i e s .0 Procedure: I n a l l c a s e s . These f o r m u l a s a r e g e n e r a l l y used b y u t i n g i n w a t e r a r e v e r y e f f e c t i v e f o r r e m o v i n g many o i l y .0 28. I r e s i n o u s s o i l s .0 5. I n c . : F o r m u l a t i o n F-786 .L i monene Monamul s e dL-1273 Water F o r m u l a I1 Inqredients: d .e m u l s i o n s o f imonene and w a t e r .0 Wt% 35. m i c r o .0 62. Add o t h e r i n g r e d i e n t s e x c e p t w a t e r . .0 32. M i x u n t i l homogeneous.0 23.

0 71 .0 55.0 Clear Procedure: B l e n d i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n . The f o r m u l a s t h e m s e l v e s a r e c l e a r and e x h i b i t a bloom e f f e c t upon d i l u t i o n . Inc.0 20.0 45.0 5.0 20.0 5. Formula 1 Inaredients: Pine O i l Monamulse TRP Water Appearance: C l e a r D i l u t i o n (1% i n t a p w a t e r ) : && y 35. They r e p r e s e n t t h e r a n g e o f p i n e o i l and w a t e r concent r a t i o n s commonly used.O Blooms Formula 4 Inqredients: Pine O i l Monamul se TRP Water Appearance: C l e a r D i l u t i o n (1% i n t a p w a t e r ) : WtO/o 2.0 Blooms Formula 3 Ingredients: Pine O i l Monamul se TRP Isopropanol Water Appearance: C1 e a r D i l u t i o n (1% i n t a p w a t e r ) : Wt% 9.: Suggested F o r m u l a t i o n s . Package Recommended Use D i l u t i o n : 1 : l O w i t h w a t e r F o r m u l a F-785 SOURCE: Mona I n d u s t r i e s .Miscellaneous 173 M i cro-Emu1 s i ons w i t h P i ne O i 1 The fol 1owi ng f o r m u l a s a r e c l e a r m i c r o e m u l s i ons o f p i ne o i 1 and w a t e r .0 10.0 93.0 Blooms Formula 2 I ngredients : Pine O i l Monamul s e TRP Isopropanol Water Appearance: C1 e a r D i l u t i o n (1% i n t a p w a t e r ) : WtO/o 20.0 10.

5 39.5-5. keep t h e r a t i o o f t h e components t h e same. A s l i g h t s i l i c a t e p r e c i p i t a t e may o c c u r upon l o n g s t a n d i n g . Inc.5% I t i s recommended t h a t t h e BSGH-270 and NPS-225 b e d i s s o l v e d i n an e q u a l amount o f w a t e r and t h e c a u s t i c added t o t h a t p r e m i x .0% 0.5-5. B o t t l e Wash F o r m u l a t i o n s Low Foam Inqredie n t s : 50% NaOH B u r c o BSGH-270 B u r c o HCS-50NF Add BSGH-270 and HCS-50 NF t o 50% NaOH. End use c o n c e n t r a t i o n s w i l l depend o n d e g r e e o f s o i l t o b e removed.0 Wt% 26.0 Add components i n o r d e r l i s t e d .5 19. T o defoam t h i s f o r m u l a t i o n use a 3/1 r a t i o o f NPS-225/Burco LAF-I 25.0% 0. SOURCE: B u r l i n g t o n Chemical Co..5% W O To 100% T o t a l 2. M o d e r a t e Foam Inqredients: 50% NaOH B u r c o BSGH-270 B u r c o NPS-225 Water y & To 100% T o t a l 2.0 8. a 2% end use c o n c e n t r a t i o n i s s u f f i c i e n t f o r b o t t l e cleaning.5-2.5-2.0 7.174 Advanced Cleaning Product Formulations P l a s t i c B o t t l e Wash Stable i n hard water Inqredients: Water KOH-45% K a s i l #I STPP B u r c o HCS-5ONF % S o l i d s : 31.0-7. so t h a t t h e b a l a n c e o f t h e f o r m u l a t i o n i s n o t d e s t r o y e d . B l e n d between a d d i t i o n s . To f o r m u l a t e a l o w e r a c t i v i t y p r o d u c t .5% 3.: Suggested F o r m u l a t i o n s . N o r m a l l y .

0 Tomah E-14-5 Tomah E-14-2 1. ) .0 Water % t o t a l s u r f a c t a n t : 16. Heavy g r e a s e would r e q u i r e a h i g h e r c o n c e n t r a t i o n o f d-limonene.0 12.0 T a l l O i l Fatty Acid 1.6 64. About 1-2% d .5 Tomah A l k a l i S u r f a c t a n t 1.5 1.% D-Li monene 20.0 Tomah E-14-5 19.6 Monoethanolamine 0.0% Emul s i f i e r / T e r p e n e r a t i 0 : 0 . Formula A: D-Limonene 40.0 12. N o t e t h a t o t h e r p i n e o i l s may n o t work i n t h e s e f o r m u l a t i o n s .0% Emulsifier/Terpene r a t i o : 1.0 % t o t a l s u r f a c t a n t : 15.0 Tomah E-14-5 22. 7 0 0 F o r m u l a 5: Wt.000 Add each component i n t h e o r d e r g i v e n and m i x u n t i l homogeneous b e f o r e a d d i n g t h e n e x t component.4 Tomah E-14-2 2.0 Monamid 7 0 5 4.o/a D-Li monene 15. 8 0 0 Formula C : Wt.4 Tomah A l k a l i S u r f a c t a n t 2.8 Tomah E .0% E m u l s i f i e r / T e r p e n e r a t i o : 0. Concentrated Formula Formula: 70. : B u l l e t i n : T e r p e n e M i c r o e m u l s i o n s .9/o D-Li monene 30.0 % t o t a l s u r f a c t a n t : 24.0 D-Limonene Tomah E-14-5 14.4 Water 10.0 % t o t a l s u r f a c t a n t : 28.0 SOURCE: Tomah P r o d u c t s . Add t h e w a t e r i n p o r t i o n s w i t h mixing.Miscellaneous 175 Teroene M icroemul s i ons The f o r m u l a t i o n s g i v e n h e r e w i l l p r o d u c e c l e a r s t a b l e m i c r o e m u l s i o n s c o n t a i n i n g f r o m 15% t o 40% d .l i m o n e n e i n t h e f o r m u l a t i o n s t o g i v e a f l a s h p o i n t above 1 4 0 F .8 Tomah A l k a l i S u r f a c t a n t 2. A t y p i c a l use l e v e l w o u l d b e a t 1 0 / 1 t o 4 0 / 1 w i t h w a t e r .6 Tomah E-14-2 Tomah A l k a l i S u r f a c t a n t 1.1 4 . a p i n e o i l d e r i v a t i v e can b e s u b s t i t u t e d f o r d .800 Formula D: Wt. I n c .0% Emul s i f ie r / T e r p e n e r a t i 0 : 0 .8 Water 32. G l i d s o l 180 ( f r o m SCM G l i d c o O r g a n i c s C o r p .l i m o n e n e a t use l e v e l i s u s u a l l y s u f f i c i e n t .2 Tomah E-14-2 2.l i m o n e n e .4 Water 46.5 Water 70.

T h i s r e l i e v e s t h e c o n s t r a i n t o f s e l e c t i n g an appropriate surfactant emulsifier. The r e s i n s s t a b i i z e e m u l s i o n s v i a e l e c t r o s t a t i c s t a b i l i z a t i o n . 4 . Use a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s Screen t h e Pemulen r e s i n i n t o t h e v o r t e x o f t h e r a p i d l y a g i t a t i n g w a t e r (800 rpm). Heat t h e Pemulen d i s p e r s i o n t o 9OC. 2 . ( 2 ) American Hoechst Corp.00% SOURCE: BFGoodrich S p e c i a l t y Chemicals: vytsb 12. 3 . ( 3 ) BFGoodrich Procedure: 1. M e l t t h e waxes t o g e t h e r i n a v e s s e l .00 0. a p p r o x i m a t e l y a t 9 0 C . Total Actives: T o t a l Wax: 20. A l l o w t o mix u n t i l homogeneous and f r e e o f p o l y m e r lumps.20 ~ DET-501 . Ingredient: Bareco C-36 Wax ( 1 ) Hoechst Wax E ( 2 ) Pemulen 1622 ( 3 ) 01 Water Morphol ine Physical Properties : P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) P e t r o l i t e Corp.176 Advanced Cleaning Product Formulatioris Wax Emulsion U s i n g Pemulen R e s i n s T h i s wax e m u l s i o n can be c r e a t e d and s t a b i l i z e d v i a t h e use o f Pemulen r e s i n s . Add t h e Pemulen d i s p e r s i o n t o t h e m e l t e d wax w i t h v i g o r o u s a g i t a t i o n .00 8. Add t h e m o r p h o l i n e and cool q u i c k l y .30 79 5 0 0.

Section II sportation Cleaners and Polishes 177 .

Auto Cleaners and Polis 178 .15.

Auto Cleaners and Polishes 179 Chrome P o l i s h I n a d d i t i o n t o t h i c k e n i n g . D i s s o l v e t h e s i l i c o n e o i l . d i s p e r s e 0 . 4 .85 24.48 p a r t s o f w a t e r by s i m p l y "dumping" t h e polymer i n t o t h e w a t e r .50 2. I n j u s t a few m i n u t e s .00 9.25 1.19 PO Procedure: 1 .65 24.85 4. 0 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) General E l e c t r i c ( 2 ) Hercules ( 3 ) Rhone-Poul enc ( 4 ) H e n k e l : Standamid ( 5 ) BFGoodri c h r p m ) : 10. add t h e pumice and Snow F l o s s . and o l e i c a c i d i n t h e m i n e r a l s p i r i t s . Add t h i s d i s p e r s i o n t o t h e above m i x t u r e .25 DET-551 FGoodrich S p e c i a l t y Chemicals: . 1 9 p a r t s o f Carbopol i n t o 4.30 0.46 1. B l e n d t h o r oughl y 5. Add i n t h e TEA l a u r y l s u l f a t e and Standamid PD. S l o w l y add i n t o t h e above m i x t u r e w i t h rapid agitation. t h e polymer w i l l c o m p l e t e l y wet o u t . such as a b r a s i v e s .800 c p 39.25 1. Ingredient: D I Water Morphol ine Pumice Snow F l o s s SFSB S i l i c o n e F l u i d ( 3 5 0 ) ( 1 ) Yarmor 302 P i n e O i l ( 2 ) Oleic Acid Mineral S p i r i t s TEA l a u r y l s u l f a t e ( 3 ) Cocamide DEA ( 4 ) D I Water Carbopol EZ-2 ( 5 ) Physical Properties: B r o o k f i e l d V i s c o s i t y (RVT-20 P r o d u c t pH: 9 .85 0.46 0. B l e n d thorough1y . 3 . The r e s i n a l s o p r e v e n t s "creaming" o r phase s e p a r a t i o n by suspending and s e p a r a t i n g t h e o i l d r o p l e t s . t o become p e r m a n e n t l y suspended. 2 . T o t a l Asti ves : Silicone Fluid: Total Surfactant: Mineral S p i r i t s : T o t a l Abrasives: 1. .39 14. D i s s o l v e t h e morpholine i n t h e water. p i n e o i l . Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s .50 4. I n a s e p a r a t e v e s s e l . W i t h r a p i d a g i t a t i o n .50 23.

50 2. I n a s e p a r a t e v e s s e l . such as a b r a s i v e s .50 Mineral S p i r i t s : 11 .50 2. t o become p e r m a n e n t l y suspended. M i x u n t i l homogeneous. The r e s i n a l s o p r e v e n t s "creaming" o r phase s e p a r a t i o n by suspending and s e p a r a t i n g t h e o i l d r o p l e t s .30 p a r t s o f Carbopol i n t o 19.40 5. Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s . 3.20 2. m i n e r a l s p i r i t s .00 8.50 Silicone Fluid: 1.I80 Advanced Cleaning Product Formulations L i q u i d Car Polish I n a d d i t i o n t o t h i c k e n i n g .00 1. I n c . TEA. M i x u n t i l homogeneous. and t h e t w o r e a c t i v e amine polymers t o g e t h e r .00 49. o l e i c a c i d . The polymer w i l l wet o u t i n a few minutes. and t h e m o r p h o l i n e 2 . I n a s e p a r a t e v e s s e l . 5 .200 cps P r o d u c t pH: 8-9 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) see EiFGoodrich L i t e r a t u r e DET-501 ( 2 ) General E l e c t r i c ( 3 ) BFGoodrich ( 4 ) General E l e c t r i c (5) Kaopolite. I n a s e p a r a t e v e s s e l .30 0. Insredient: D I Water T r i e t h a n o l ami ne Wax Emulsion ( 1 ) Morphol ine SF90 S i l i c o n e F l u i d (350) ( 2 ) Oleic Acid Kerosene Mineral S p i r i t s D I Water Carbopol EZ-2 ( 3 ) Isopropanol Mineral S p i r i t s SF1706 R e a c t i v e Amine Polymer ( 4 ) SF1705 R e a c t i v e Amine Polymer ( 4 ) Kaopolite kaolin clay (5) Wt96 37.50 10.80 8. M i x u n t i l homogeneous. M i x t o g e t h e r t h e w a t e r . Procedure: 1 .10 8. Add t o t h e above m i x t u r e . S l o w l y add i n t h e c l a y . d i s p e r s e 0. Add t h i s d i s p e r s i o n t o t h e above m i x t u r e .70 p a r t s o f water by s i m p l y "dumping" i t i n . Add t h i s t o t h e above m i x t u r e w i t h v i g o r o u s a g i t a t i o n . mix t h e s i l i c o n e f l u i d .50 SOURCE: BFGoodrich S p e c i a l t y Chemicals: DET-BOO . 4 .00 1 * 50 2.50 Physical P r o p erties: B r o o k f i e l d V i s c o s i t y (RVT-20 rpm): 3. mix t h e i s o p r o p a n o l .oo 3. Total Actives: T o t a l Wax : 0.70 0. kerosene and t h e m i n e r a l s p i r i t s t o g e t h e r .60 React ive A m i ne Polymer : Abrasive: 8. wax emulsion.

o 2. 50% Avanel 5-70 Water. Dye Wt% 12. 50% G l u c o n i c A c i d . 70% Avanel S-70 Water Wt% 6.0 3. D i l u t e one p a r t c l e a n e r w i t h f i v e p a r t s w a t e r t o use. Add t h e dye t o t h e w a t e r w i t h good a g i t a t i o n and t h e n add t h e w a t e r t o t h e b a t c h . g l u c o n i c a c i d and Avanel S-70 t o t h e G i x i n g v e s s e i .0 77.5%.Auto Cleaners and Polishes 181 L i q u i d Spray C l e a n e r f o r A l u m i n u m T r u c k s Bngredi e n t s : Water Phosphoric A c i d . F o r m u l a t i o n CM-101 Non-Phosphorous A l u m i n u m C l e a n e r Inaredi ent : C i t r i c A c i d . add t h e a c i d s t o t h e w a t e r . M i x w e l l .0 1.0 Procedure: Charge t h e w a t e r t o t h e m i x i n g v e s s e l . A 1 umi n u m C l e a n e r / B r i n h t e n e r Pnaredi e n t : Phosphoric A c i d . 50% N i t r i c A c i d . Add t h e Avanel S .0 3. c i t r i c a c i d .d y e i s t o be added. Formu 1a t ion CM. Note: I f a d d i t i o n a l b r i g h t e n i n g i s r e q u i r e d .0 3. 85% C i t r i c A c i d .0 4.0 ~ r ~ c ~ d U r ~ ~ Add i n g r e d i e n t s i n o r d e r as l i s t e d .0 8.0 8.0 83. I f . Under s l o w a g i t a t i o n and w i t h due c a r e .0 20. 75% C i t r i c Acid Macol 48 Ammoni u B i f 1u o r i de m Avanel S-30 Wt% 50.7 0 and mix f o r 10 m i n u t e s . p a r t of t h e water s h o u l d be h e l d o u t . : Suggested F o r m u l a t i o n s . I n c .0 PPOC@dUr&?: Charae t h e w a t e r .0 10.102 UWCE: PPG I n d u s t r i e s . t h e n i t r i c a c i d may be i n c r e a s e d t o 1.

I n a s e p a r a t e v e s s e l . Apply c o o l i n g . I n c .15 10. SOURCE: PPG I n d u s t r i e s . A s t i f f e r p a s t e can be p r e p a r e d by i n c r e a s i n g t h e o l e i c a c i d charge. p r e p a r e P a r t D by a d d i n g t h e K a o p o l d t e SF t o t h e w a t e r under a g i t a t i o n . I n s e p a r a t e v e s s e l s .8 .0 2.5 0.75 12. 5 Appearance: Cream-Colored Paste Procedure: 1 . 2. 5 .1 45.0 14.0 6.1 0 1 . add P a r t B t o t h e v e s s e l f o l l o w e d by P a r t C . NOTE: The f i n i s h e d p r o d u c t i s a p a s t e . charge P a r t B and P a r t C components. 3 .0 2.0 9QC. When P a r t A reaches 9OC and a l l t h e wax has m e l t e d . Charge t h e components i n P a r t A t o a steam-heated m i x i n g v e s s e l equipped w i t h a g i t a t i o n .182 Advanced Cleaning Product Formulations M i l d A b r a s i v e A u t o m o b i l e Polish I n q r e d ie n t : Part A: Masi 1 SF 1 . S t a r t a g i t a t i o n and h e a t t o Wt% 4.5 1. : F o r m u l a t i o n S A .0 2. 0 0 0 Oleic Acid Carnauba Wax #1 Y e l l o w Isopar M Mazami de SS-1 0 P a r t B: Isopar M M a s i l 123 Part C : I sopar M Morphol ine P a r t D: Water K a o p o l i t e SF pH ( a s i s ) : 7 . Add P a r t D t o P a r t A and c o n t i n u e c o o l i n g .

0 r and Truck Wash Compounds 183 .

0 7.5 Appearance: C l e a r .0 Sodium M e t a s i l i c a t e .06 Procedure: Charge t h e f i r s t p o r t i o n o f w a t e r t o t h e m i x i n g v e s s e l and s t a r t a g i t a t i o n . NOTE: T h i s i s a h i g h l y a l k a l i n e c l e a n e r d e s i g n e d t o be used i n commercial a u t o m a t i c c a r washes a t a d i l u t i o n r a t e o f 1-2 ounces p e r g a l l o n .o D e i o n i z e d Water 52.184 Advanced Cleaning Product Formulations Car Shampoo C o n c e n t r a t e T h i s f o r m u l a t i o n produces c o p i o u s amounts o f foam w h i l e c l e a n i n g a u t o m o t i v e f i n i s h e s .5-13.0 Macol LF 120 Mazamide 00 2. 40% 3.0 pH ( a s i s ) : 8 . A u t o m a t i c Car Wash C o n c e n t r a t e w. S t o p a g i t a t i o n and p e r m i t t h e p r o d u c t t o d e a e r a t e p r i o r t o f i l l i n g o f f . 2 . l i g h t .0 T e t r a p o t a s s i u m Pyrophosphate 2. Add t h e i n g r e d i e n t s i n t h e o r d e r l i s t e d and mix u n t i l c l e a r .5 W i t c o n a t e 60 T L i q u i d Macol TD-12 4.y e l l o w l i q u i d S p e c i f i c G r a v i t y : 1.0 Potassi u Hydroxide m 2.0 Dei o n i zed Water 6. 0 Appearance: C l e a r .0 Maphos 60-A 3. Anhydrous 2.5 P a r t 8: Mafo CSB-50 5. 85% 1.0 0.00 Procedure: 1 .0 T r i e t h a n o l ami ne.9 .0 pH ( a s i s ) : 12.0 Macol 48 3. Inc. I t i s m i l d t o b o t h t h e u s e r and t h e automotive f i n i s h . Do n o t use d i r e c t l y on a u t o m o t i v e f i n i s h e s F o r m u l a t i o n CA-102 SOURCE: PPG I n d u s t r i e s . Add t h e r e m a i n i n g i n g r e d i e n t s i n t h e o r d e r l i s t e d .t% I n a r e d ie n t s : 50.: Suggested F o r m u l a t i o n s 1 .0 D e i o n i z e d Water 27. 0 . l i g h t .y e l l o w l i q u i d S p e c i f i c Gravity: 1 .0 Sodium X y l e n e S u l f o n a t e . Charge t h e f i r s t p o r t i o n o f w a t e r t o a m i x i n g v e s s e l and d i s s o l v e t h e sodium c i t r a t e i n i t . NOTE: Use c o n c e n t r a t i o n i s 1-2 ounces p e r g a l l o n o f warm w a t e r . Ingredient: Part A: Dei o n i zed Water Sodi u C i t r a t e m Wt% 30.

80 4.00 1 .80 1.00 Wei a h t % 64.00 5.70 7.30 2. F o r m u l a t i o n CWC-005-01 SOURCE: P i l o t Chemical C o . 50% D i e t h a n o l ami ne C a l s o f t LAS-99 Calamide C P i l o t SXS-40 Cal foam EA-603 Ammonium C h l o r i d e Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .oo Weight% 70.50 10. 50% Cal s o f t LAS-99 Calamide C P i l o t SXS-40 C a l foam EA-603 C a l o x y l a t e N-9 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s in o r d e r 1 is t e d F o r m u l a t i o n CWC-007-01 Car Wash ( C a l s u d s A-Based) Ingredients: Water Calsuds A C a l foam EA-603 C a l s u d s CD-6 Ammonium C h l o r i d e Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 2.oo Wei q h t % 59.35 16.10 3. : Suggested F o r m u l a t i o n s Weight% 72. F o r m u l a t i o n CWC-008-01 Car Wash ( C a l s o f t LAS-99-Based) Ingredients: Water NaOH.00 .50 2.40 0.05 12.Car and Truck Wash Compounds 185 Car Wash ( C a l s o f t LAS-gg-Basedl Ingredients: Water NaOH.00 5.50 3.00 2. F o r m u l a t i o n CWC-006-01 Car Wash ( C a l s o f t T-60-Based) Ingredients : Water C a l s o f t T-60 Pi l o t sxs-40 C a l o x y l a t e N-9 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 20.80 4.20 28.00 2.

0 .0 30. Add c o l o r . h e a t t o 70C.0 0.0 50.0 Procedure: Add i n g r e d i e n t s i n t h e o r d e r l i s t e d w i t h a g i t a t i o n .5 2.0 6.0 24.186 Advanced Cleaning Product Formulatioris Car Wash Readi l y removes a w i d e v a r i e t y o f r o a d s o i 1 s . d e p t h o f g l o s s . Ingredients: Water Monaterge ALX-100s (Cocamide DEA ( a n d ) DEA D o d e c y l benzenesulfonate (and) Diethanolamine) 70. Add P a r t I I s l o w l y t o P a r t I w i t h good a g i t a t i o n .: Suggested Formu a t i o n s .0 10. f r a g r a n c e and p r e s e r v a t i v e .5 Procedure: P r e p a r e each phase s e p a r a t e l y . Ingredients: P a r t I: M o n a s i l PCA Dimethicone (12. Inc. Typi c a l P r o p e r t i e s : Appearance: C l e a r y e l l o w l i q u i d Recommnded Use D i l u t i o n : 1 : 2 0 w i t h w a t e r F o r m u l a t i o n F-772 P a s t e Car Wax T h i s e a s i l y a p p l i e d a u t o m o b i l e p a s t e wax f o r m u l a w i l l p r o v i d e i m p r o v e d c l e a n i n g . S t i r coo t o 40-50C and package. Package. l a s t i n g b e a u t y and s h i n e t o new and o l d e r a u t o m o b i l e f i n i s h e s .0 3. F o r m u l a t i o n F-826 SOURCE: Mona I n d u s t r i e s . A d j u s t pH t o 7 . M o n a s i l PCA w i l l p r o v i d e s h i n e and d e t e r g e n t r e s i s t a n c e t o any p a s t e wax f o r m u l a .500 c s t ) Carnauba Wax #1 Y e l l o w T a l l O i l Fatty Acid Isopar K Kaopol it e 11 5 2 P a r t 11: Water TEA (99%) We96 4.

c p s : 290 S o l i d s : 29.0 60. d i l u t e up t o 2 9 : l f o r summer u s e .5 2. 30% W i t c o 1298SA wt% 55. F o r m u l a 666 W i n d s h i e l d Washer F o r m u l a t i o n Inqredi ents: W i t c o n a t e 1240 Isopropanol Water 1.5 Use " a s i s " i n w i n t e r .5% pH: 8 .0 20.0 1. D .0 10.0 30.o 39. I . 38% B l e n d i n g Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d . Sodi um T r i p o l y p h o s p h a t e R e w o t e r i c AM 8-14 V a r o n i c DM-55 Sodi um H y d r o x i d e . F o r m u l a 867 SOURCE: W i t c o C o r p . : Suggested F o r m u l a t i o n s .0 9. B1 e n d i ng Wt% 56. 9 F o r m u l a 630 W i n d s h i e l d Washer C o n c e n t r a t e Ingredients: Water. Typical Properties: V i s c o s i t y . D .0 Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e compl e t e l y between each a d d i t i o n .Car and Truck Wash Compounds 187 Car Wash w / A m p h o t e r i c Ingredients: Water.o 0.0 t h e n add i s o p r o p a n o l Wt% 51 e n d i ng P r o c e d u r e : D i s s o l v e W i t c o n a t e 1240 in w a t e r .0 4. I .0 2. Isopropanol P e t r o BAF Powder DeSophos 5AP EDTA.

0 8. 7 F o r m u l a 61 1 Car Wash C o n c e n t r a t e w / A l c o h o l Ingredients: Water.0 . W i t c o l a t e SE-5 W i t c o n a t e 1260 S l u r r y P e t r o LBA L i q u i d DeSonic 81-6 W i t c a m i d e 128T B l e n d i n g P r o c e d u r e : B1 end i n g r e d i e n t s i n t h e o r d e r 1 is t e d .188 Advanced Cleaning Product Formulations Car Wash C o n c e n t r a t e w / A l c o h o l I n q r e d ie n t s : Water.3 13.0 7. %: 37.8 5. I . c p s : 335 A c t i v e s .0 Ethoxylate W S 43. T y p i c a l P r o p e r t ie s : V i s c o s i t y . W i t c o l a t e SE-5 W i t c o n a t e 1260 S l u r r y P e t r o LBA L i q u i d DeSonic 81-6 W i t c a m i d e 128T Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d .0 3.8 Blend ingredients i n t h e order l i s t e d Typical Properties: V i s c o s i t y . : Suggested F o r m u l a t i o n s Ethoxylate 36. I . I .0 15. 0 F o r m u l a 611 SOURCE: W i t c o C o r p .9 27. D . D .0 6. c p s : 315 A c t i v e s .7 1. %: 4 3 . c p s : 210 A c t i v e s . %: 2 3 .5 F o r m u l a 611 Car Wash C o n c e n t r a t e w / A l c o h o l I n a r e d ie n t s : Water.9 8.0 30.0 3.0 5.3 5. W i t c o l a t e SE-5 W i t c o n a t e 1260 S l u r r y P e t r o LBA L i q u i d DeSonic 81-6 W i t c a m i d e 128T B l e n d i n g Procedure: Ethoxylate 64.3 16. Typical Properties: V i s c o s i t y . D .

: Suggested F o r m u l a t i o n s Wei g h t % 50.18 C a r Wash ( C a l s u d s A-Based) Inqredients: Calsuds A C a l foam EA-603 C a l o x y l a t e N-9 Water Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .00 10.00 25.17 10.04 44. T h i s i s l o w e r p H f o r m u l a t h e n CWC-001-01. F o r m u l a t i o n CWC-002-01 Car Wash [Powder) Ingredients: Sodi um T r i p o l y p h o s p h a t e C a l s o f t F-90 Cal o x y l a t e N-9 Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .76 Wei q h t % 19.00 2. F o r m u l a t i o n CWC-001-01 Car a n d T r u c k Wash F o r m u l a Ingredients: C a l f a x DB-45 C a l s o f t L-40 D i s o d i um Phosphate Water Comments a b o u t t h i s f o r m u l a : 1 .83 24.00 .00 5. H e a t i n g i s n e c e s s a r y t o homogenize. F o r m u l a t i o n CWC-003-01 Wei q h t % 85. F o r m u l a t i o n CWC-004-01 SOURCE: B1 io t Chemi c a l Co.02 45.Car and Truck Wash Compounds 189 C a r and T r u c k Wash F o r m u l a Ingredients: C a l f a x DB-45 C a l s o f t L-40 T r i s o d i um Phosphate Water Comments a b o u t t h i s f o r m u l a : Add i n g r e d i e n t s i n o r d e r l i s t e d .95 10. 2 .00 Wei q h t % 20.00 45.00 3.

0 Wt% 45.0 6 .7 64.0 8.0 1.: Suggested Formulations .3 11 . 17.0 8.190 Advanced Cleaning Product Formulations Car Wash and Care Car Shampoo with Water-Repellent Effect Ingredients: Autopur WK 4332 Amphotensid 0 4 Water Formula CT 0 4 . o Co.0 63.0 6 .0 6.0 6.0 7 wtu/.0 1 Innredi ents: Water Zetesol NL Zusol at 1 0 0 8 / 8 5 Isopropanol Formula CT 0 4 .0 50.9 20.2 6.0 3 .0 Rinse-off Aqent (Water-Repellent) Without Hydrocarbons Ingredients: Autopoon GK 4008 Mulsifan RT 1 Produkt 2058 Butyl di glycol Water Formula CT 04-05-03 Windshield-Cleaner (Summer) Inqredi ents: Water Ethanol Zusol at 1 0 0 5 / 8 5 Zusolat 1 0 0 8 / 8 5 Formula CT 0 4 .0 4 SOURCE: Zschimmer & Schwarz GmbH & Wt% 17.0 3.0 60.0 Wt% 67.0 2 Rinse-off ARent (Water-Repellent) Ingredients: Autopoon GK 4004 Mulsifan RT 1 Produkt 2058 Pine oil Butyl di glycol Water Formula CT 0 4 .0 5.0 5.0 6.0 5 .0 6.9 Wt% 23.

0 0.0 4.5 70.0 4.1 1 . : General Formulations .0 4.0 2.0 10.0 .0 0.0 15.5 Wt% 15.0 5.0 5. A 1 k a l in e Wt% 77.5 3.0 4 T a r Remover Inqredients: M u l s i f a n K 326 S p e z i a l Whi t e .0 SOURCE: Zschimmer & Schwarz GmbH & C o .0 60.0 79.0 2.s p i r i t n-butanol Oleic acid Water F o r m u l a CT 04-13-02 (Winter) Wtl 29.0 3.5 Wt% 4.0 7.Car and Truck Wash Compounds 191 Car Wash and C a r e Windshield-Cleaner Ingredients: Water Isopropanol Z e t e s o l 2056 F o r m u l a CT 04-06-07 I n s e c t Remover Inqredi ents: S u l f e t a l 4105 Z u s o l a t 1008/85 P h o s f e t a l 201 Trilon A liquid Monoethanol ami ne Butyl d i g l ycol Water F o r m u l a CT 04-07-01 Wheel C 1 e a n e r Ingredients: Water Tetrapotassium pyrophosphate Lumorol 4192 Z u s o l a t 1005/85 Butyl diglycol Orange t e r p e n e F o r m u l a CT 0 4 .

0 3. add t h e m o r p h o l i n e .0 8. 70 SUS Part 0 : Morphol ine Carbopol 934 Triethanolamine Water 3.0 3. add t h e o l e i c a c i d .6 1. Add P a r t A t o P a r t 0 and b l e n d .0 3. and Wax S w i t h h i g h speed m i x i n g . I n c . 2 .000 C f r o m P a r t C t o t h e c o n c e n t r a t e w i t h s l o w m i x i n g . D i s p e r s e t h e Carbopol 934 i n t h e w a t e r . h e a t t h e w a t e r t o 85C. 3 . A u t o Wipe B S h i n e P o l i s h Ingredient.2 1. add t h e t r i e t h a n o l amine. When c o m p l e t e l y d i s s o l v e d .5 5. Part A: M a s i l SF 100 A-C 617A Oleic Acid M i n e r a l O i 1 . Add P a r t B t o P a r t A w i t h h i g h shear m i x i n g . Add t h e M a s i l EM 250 C and M a s i l EM 10.0 1.192 Advanced Cleaning Product Formulations Car Wax Ingredient: Part A: Morphol ine Water P a r t B: Wax S Oleic Acid M i n e r a l Spi r i t s Kerosene Part C: M a s i l EM 250 C M a s i l EM 1 0 .2 0.0 9.6 Procedure: 1 . I n P a r t B .5 2. F o r P a r t B.0 10. T h i c k e n w i t h t h e Carbopol 941 s o l u t i o n . kerosene.o 18.2 85.4 0. 0 0 0 C Snow F l o s s Kaopol it e SF Carbopol 941 ( 1 % i n w a t e r ) Wt% 0. : Suggested F o r m u l a t i o n s . 3. Then.0 As needed Procedure: 1 .8 44. m i n e r a l s p i r i t s . Add t h e i n g r e d i e n t s i n P a r t A as l i s t e d and h e a t t o 9OC. SOURCE: PPG I n d u s t r i e s . Add t h e m o r p h o l i n e t o t h e w a t e r w i t h h i g h speed m i x i n g . 2 . Add t h e Snow F l o s s and K a o p o l i t e S F .

5% a c t i v e s . I n c .00 8.00 10. These f o r m u l a t i o n s were made up and f o u n d t o b e f r e e z e .00 16. a n h y d r o u s a m p h o t e r i c s and amine o x i d e s are not.5% a c t i v e s .00 S u r f a c t a n t / b u i l d e r r a t i o : 1. t h e c o m b i n a t i o n o f w h i c h s h o u l d do as w e l l as t h e n o n i o n i c f o r h a r d s u r f a c e c l e a n i n g .10 10. and n o t c o r r e c t e d f o r t h e w a t e r c o n t e n t .Car and Truck Wash Compounds 193 Concentrated T r a f f i c F i l m Removers Two f o r m u l a t i o n s were d e v e l o p e d w h i c h c o n t a i n 50% t o t a l w a t e r .5 % anhydrous b u i l d e r : 9. F o r m u l a 1 was d i l u t e d 1/20 w i t h w a t e r t o 2.00 10. so t h e absence o f n o n i o n i c d i d n o t adversely a f f e c t t h e performance o f t h e concentrated f o r m u l a t i on.00 N o t e t h a t sodium m e t a s i l i c a t e p e n t a h y d r a t e i s a c t u a l l y a b o u t 57% sodium m e t a s i l i c a t e on an anhydrous b a s i s . and t e s t e d b y s p r a y i n g on a d i r t y c a r . Mix i n t h e order given: Formula 1: Component: Water Versene 1 0 0 Sodium M e t a s i l i c a t e P e n t a h y d r a t e Tomah A l k a l i S u r f a c t a n t Tomah AO-14-2 Tomah Q-17-2 % anhydrous b u i l d e r : Wt% 22. No s i g n i f i c a n t d i f f e r e n c e s were seen.00 8. Versene 100 i s a b o u t 38% t e t r a s o d i u m EDTA on an a n h y d r o u s b a s i s .i s b a s i s . Thus t h e s e f o r m u l a t i o n s a r e a b o u t 50% t o t a l w a t e r when c a l c u l a t e d on an a n h y d r o u s b u i l d e r b a s i s .70 4. One c o n t a i n s n o n i o n i c .00 38. t h e o t h e r h a s no n o n i o n i c b u t has more AO-14-2 and A l k a l i S u r f a c t a n t .68 Mix i n t h e order given: Formula 2 : Component: Water Versene 100 Sodium M e t a s i l i c a t e P e n t a h y d r a t e Tomah A l k a l i S u r f a c t a n t Tomah AO-14-2 Tomah Q-17-5 Noni o n i c NP-9.00 10.82% S u r f a c t a n t / b u i l d e r r a t i o : 4.00 19.t h a w s t a b 1 e. The s u r f a c t a n t s were c o n s i d e r e d on an a s . i n c l u d i n g t h e w a t e r i n t h e sodium m e t a s i l i c a t e p e n t a h y d r a t e .20 19. It was compared w i t h F o r m u l a t i o n T-107 T r a f f i c F i l m Remover a l s o a t 2.% 36.07 Wt.00 8. SOURCE: Tomah P r o d u c t s . Anhydrous sodium m e t a s i l i c a t e and a n h y d r o u s t e t r a s o d i u m EDTA a r e r e a d i l y a v a i l a b l e . : Suggested F o r m u l a t i o n s .

T y p i c a l P r o p e r t i es : S p e c i f i c G r a v i t y : 1. 50% W i t c o 1298SA W i t c o l a t e SE-5 P e t r o BAF L i q u i d W i t c a m i d e 128T Formal i n Sodi um C h l o r i d e Blending Procedure: Blend i n g r e d i e n t s i n t h e order l i s t e d . Dye Wt% 89. F o r m u l a 609 SOURCE: W i t c o C o r p .s. Inqredients: Water.0 0.1 4.75 Sodium C h l o r i d e i s add 0 .9 1 . F o r m u l a 621 Liquid Wtg 79.8 .00 3. D .o 6. cps: 410 D i l u t i o n R a t i o a t Wand=l : 4 0 * I f u n s o f t e n e d t a p w a t e r i s used.75 1. t o counteract hardness. Blending Procedure: Blend t h e i n g r e d i e n t s i n t h e order l i s t e d . l b s .46 pH. used t o a d j u s t v i s c o s i t y o f t h e p r o d u c t . 2 5 % l i q u i d EDTA. 0 . The Sodium C h l o r i d e i s used t o a d j u s t t h e v i s c o s i t y o f the f i n a l product.00 0.194 Advanced Cleaning Product Formulatioris Foamy B r u s h Car Wash./Gal.0 3.10 0.00 3. 40% Low C o s t Car= Ingredients: Water. : Suggested F o r m u l a t i o n s . 5 . I . : 8. I . A d j u s t t h e p H = 7 .s.015 Wt. D .00 7. 4. a s i s : 9 . 8 V i s c o s i t y . * C a u s t i c Soda.40 5. P e t r o LBA Powder W i t c o l a t e SE-5 W i t c a m i d e 128T Formal in Sodi um C h l o r i d e Perfume.

O liquid 85% pH ( a s i s ) : 8 . : Suggested F o r m u l a t i o n s 39. F o r m u l a t i o n CA-103 L i q u i d Car Wash Ingredient: Water W i t c o n a t e 60 T L i q u i d Macol OP-10 SP Mazamide 80 Hexyl Carbi t o 1 Methanol Procedure: Add i n g r e d i e n t s i n o r d e r a s l i s t e d . 5 W i t c o n a t e 60 T L i q u i d Procedure: Add i n g r e d i e n t s i n o r d e r as l i s t e d .0 10.0 vvt% . o 5.0 10.Car and Truck Wash Compounds 195 G e n e r a l Purpose C a r Wash T h i s i s a c o p i o u s .0 9.o 1.5 3.0 45.0 10. B o a t Wash & CarPCleaner ~~ ~~~~ 34. 5 . a l l .02 Procedure: Charge t h e f i r s t p o r t i o n o f w a t e r t o a m i x i n g v e s s e l and s t a r t slow a g i t a t i o n (excessive a g i t a t i o n w i l l produce a f o a m i n g p r o b l e m ) .9 . 5 Appearance: C l e a r .y e l l o w S p e c i f i c G r a v i t y : 1.5 1.0 6. Add t h e r e m a i n i n g i n g r e d i e n t s i n t h e o r d e r l i s t e d and m i x u n t i l c l e a r . NOTE: Use c o n c e n t r a t i o n i s 1-2 ounces p e r g a l l o n o f warm w a t e r . l i g h t . I n c . y e t e f f e c t i v e i n t h e removal o f r o a d g r i m e and o t h e r s o i l s . Insredient : D e i o n i z e d Water Mazon 98 Macol TD-3 W i t c o l a t e WACLA Mazamide 80 Macol 48 Triethanolamine.p u r p o s e c a r wash f o r m u l a t e d t o b e s a f e on c a r f i n i s h e s .0 NtS ~ Ingredient: Water Mazamide 80 Macol NP 9 . SOURCE: PPG I n d u s t r i e s . D e i o n i z e d Water w b 50.0 30.0 1.f o a m i n g .5 31 .5 2.0 11 .

00 2. 47.25 55.50 5. Add M e t a s i l i c a t e . * I f d y e i s used. L i g h t D e n s i t y DeSophos 5AP DeSonic 9N Sodium M e t a s i l i c a t e ./Gal.0 2.042 Wt.0 4. M i x u n t i l p r o d u c t i s u n i f o r m i n a p p e a r a n c e . L i g h t D e n s i t y Sodium T r i p o l y p h o s p h a t e . Anhydrous Sodium S u l f a t e ( S a l t Cake) C a u s t i c Soda Beads Dye* wtd/.0 3.0 3. : 8. Typical Properties: S p e c i f i c G r a v i t y : 1.196 Advanced Cleaning Product Formulatiom Heavy D u t y T r u c k Wash. m i x w i t h t h e DeSonic 9N. L i q u i d Inqredients: Water. Add DeSonic 9 N w h i l e m i x i n g .5 m i n u t e s ) . T r i s o d i um Phosphate.69 pH. : Suggested F o r m u l a t i o n s .0 3. a s i s : 1 2 . Powder Inqredients: Sodi um C a r b o n a t e (Soda A s h ) .0 2.0 Heavy D u t y T r u c k Wash.05 B1 e n d i ng P r o c e d u r e : P r e m i x Soda Ash and T r i p o l y t o g e t h e r and s l o w l y add DeSophos 5AP w h i l e m i x i n g .90 7. 7 D i l u t i o n R a t e : D i l u t e 1 : 4 0 a t Wand F o r m u l a 603 70. D .00 2.00 10. C r y s t a l C a u s t i c Soda Beads W i t c o 1298 S o f t A c i d P e t r o BAF L i q u i d Sodium S i l i c a t e 40 Be' ( S t a r ) W i t c o l a t e SE-5 E t h y l e n e G l y c o l M o n o b u t y l E t h e r (EB) Emcol 6744 Blending Procedure: B l e n d i n g r e d i e n t s in o r d e r 1 i s t e d .0 3. l b s .0 10.30 0. I . F o r m u l a 604 SOURCE: W i t c o C o r p . M i x u n t i l t h e p r o d u c t l o o k s d r y ( 4 . S a l t Cake and t h e n C a u s t i c Soda beads.

0 S o l i d s : 9. c p s : 160 S o l i d s : 35. cps: 2100 S o l i d s : 6.4% pH: 8.9 17. T y p i c a l P r o p e r t i es : V i s c o s i t y .8 17. as i s : 9 . 3 Formula 615 A u t o Shampoo C o n c e n t r a t e P n g r e d ie n t s : Water.00 51ending Procedure: Blend i n g r e d i e n t s i n o r d e r l i s t e d . : Suggested F o r m u l a t i o n s . R e w o t e r i c A KSF-40 M W i t c o l a t e SE-5 Wt% 80.4 Formula 629 Car Wash Ingredients: Water T e t r a p o t a s s i um Pyrophosphate. T y p i c a l P r o p e r t i es : V i s c o s i t y .Car and Truck Wash Compounds 197 Premium Car Wash C o n c e n t r a t e Ingredients: Water.7 5. I .6 46. I . 5 Formula 628 SOURCE: W i t c o C o r p .8% pH. Typical Properties: V i s c o s i t y . Ethanol Varox 1 7 7 0 W i t c o n a t e AOS L i q u i d W i t c o l a t e SE-5 Wt% 11. Add W i t c o l a t e SE-5 l a s t i n s m a l l a l i q u o t s a l l o w i n g c o m p l e t e d i s s o l u t i o n between additions. i n o r d e r shown and d i s s o l v e completel’y between each a d d i t i o n .0 15.33 5. cps: 4. D .0 5. D . W i t c a m i de 6445 Wt% 60% 91.0% ptl: 9 .6 B l e n d i ng P r o c e d u r e : Add a l l i n g r e d i e n t s e x c e p t W i t c o l a t e SE-5.0 Blending Procedure: Add in g r e d i e n t s in o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n .67 3.

2 pounds o f d e t e r g e n t p e r g a l l o n o f w a t e r o u t p u t t o t h e s p r a y n o z z l e .D r y B1 end/Aggl o m e r a t i on Composition: \nrt36 Sodium C a r b o n a t e 25-30 M e t s o Beads 2048 20-25 *Sodium P o l y a c r y l a t e (92% s o l i d s ) 1. 1 . M i x powder d e t e r g e n t i n t a n k and m e t e r i n t o c a r wash s y s t e m .3. M i l d a b r a s i v e c l e a n i n g and p o l i s h i n g e f f e c t o f T u r b o b r i t e i s e x t r e m e l y e f f e c t i v e i n h i g h p r e s s u r e s p r a y wash systems f o r r e m o v i n g o i l and w a t e r d e p o s i t s . 1 2 5 pounds o f d e t e r g e n t p e r g a l l o n o f w a t e r o u t p u t t o t h e s p r a y n o z z l e .9 B r i t e s i 1 H20 Hydrous Sodi um P o l y s i 1 i c a t e 21 .0 . C o n s t a n t a g i t a t i o n i n t a n k i s n e c e s s a r y t o keep V a l f o r 100 suspended i n s o l u t i o n . p a r t i c u l a t e s o i l s . : Detergent F o r m u l a t i o n Guide . water d e p o s i t s .0-2. Surface-Painted metal surface.0 5-1 0 Surfactant T u r b o b r i t e A1 umi n o s i 1 ic a t e 25-35 F i 1l e r s Balance D i l u t i o n : 1. road f i l m . Polymeric A p p l i c a t i o n Method-High p r e s s u r e s p r a y (700-1400 p s i ) M a n u f a c t u r e . Rohm & Haas Low Foam: Rhone-Poulenc A n t a r o x BL-330 ( 3 moles E O ) H i g h Foam: S h e l l Chemical Neodol 23-6. Polymeric A p p l i c a t i o n Method-High p r e s s u r e s p r a y (700-1400 p s i ) Manufacture-Dry blend/Agglomeration Composi t i on : Wt% Sodium C a r b o n a t e 27. 1 2 5 p o u n d s / g a l l o n ) Add 0 . o * A c u s o l 445ND Sodi um Pol y a c r y l a t e (92% s o l id s ) 3.0 .0. p a r t i c u l a t e s . c l a y . p a r t i c u l a t e s o i l s . and haze f r o m body p a r t s and w i n d s h i e l d s . p a r t i c u l a t e s . o i l . 2 pounds/gallon) Add 0 . Powder) Soil-Grease.1 V a l f o r 100 Z e o l i t e A * D i l u t i o n : 1 . V e h i c l e Wash D e t e r g e n t (Low pH) ( Z e r o Phosphate. 5 % by w e i g h t ( 0 . s a l t .198 Advanced Cleaning Product Formulations T o u c h l e s s V e h i c l e Wash D e t e r a e n t l Z e r o Phosphate. s a l t .0 36.5 o r Neodol 25-7 * ** SOURCE: PQ C o r p .0% by weight ( 0 . water deposits. 1 . D i s s o l v e powder d e t e r g e n t i n t a n k and m e t e r i n t o c a r wash s y s t e m . o i l . C o n s t a n t a g i t a t i o n i n t a n k i s n e c e s s a r y t o keep T u r b o b r i t e suspended. Powder) Soil-Grease. M i l d a b r a s i v e c l e a n i n g and p o l i s h i n g e f f e c t o f V a l f o r 100 i s e x t r e m e l y e f f e c t i v e i n h i g h p r e s s u r e s p r a y wash s y s t e m s f o r r e m o v i n g o i l and w a t e r d e p o s i t s . and haze f r o m body p a r t s and w i n d s h i e l d s .0 **Liquid Nonionic Surfactant 12. c l a y . road f i l m Surface-Painted metal surface.

0 2. p r e s e r v a t i v e Formula D 12/2 % by Weiqht 10.0 3.0 Car Wash and Wax Shampoo Ingredients: Zusol a t 1008/85 Wachsemul s i on 1864 Isopropanol Water. : Suggested F o r m u l a t i o n s Car Shampoo I g r e d ien t s : n Z e t e s o l 2056 Lumo WW 75 Z u s o l a t 1008/85 P u r t o n CFD Water Formula D 1 1 / 1 0 % by Wei a h t 15.0 10..Car and Truck Wash Compounds 199 Truck/Bus Wash Components: Burco TME B u r c o s o l v TM Neodol 91-6 TEA 85% % by Weight 7 Burcene 1 0 0 Water 5 20 5 2 8 a l ance D i l u t e 50:l t o 1OO:l depending on degree o f s o i l t o be removed Economy Truck/Bus Wash Components: Water Burco TME Meodol 1. 0 SOURCE: Zschimmer & Schwarz GmbH & Co.0 10. SOURCE: B u r l i n g t o n Chemical Co. I n c .0 q .: Suggested F o r m u l a t i o n s .0 1. t o make 1 0 0 .5 C i t r i c A c i d L i q u i d 50% KOH. o 75. 45% Ammonyx LO TEA 85% % by Weight 76 D i l u t e 20:l t o 50:l depending on degree o f s o i l t o be removed. s .

1 2 5 p o u n d s / g a l l o n ) D i s s o l v e i n s t o c k t a n k and meter i n t o wash system.0 *STPP 40.0 **Sodium X y l e n e S u l f o n a t e (40%) 8. s a l t .0 Composition 8: Wt% Metso Pentabead 20 30. : D e t e r g e n t F o r m u l a t i o n Guide * ** *** **** . FMC Witco Rhone-Poulenc Rhodasurf 91-6 Rhone-Poulenc I g e p a l CA-620 Rhone-Poulenc I g e p a l CA-520 * ** *** **** ***** V e h i c l e Wash D e t e r g e n t ( L i q u i d . road f i l m Surface-Painted metal surface.200 Advanced Cleaniris Product Formulations V e h i c l e Wash D e t e r g e n t e h o s p h a t e . Compos P i on 6 can be u t i l i z e d i n h i g h p r e s s u r e s p r a y carwash systems and s u p p l i e s adequate s o i l r e m o v a l . Polymeric A p p l i c a t i o n Method-High p r e s s u r e s p r a y Manufacture-Dry blend/Agglomeration Composition A : We9/0 Metso Beads 2048 20. low foam) Soil-Grease.0 *Sodi um C a r b o n a t e 20. c l a y . water deposits.0 **Sodium A 1 k y l a r y l Sul f o n a t e Powder (90%) 5. p a r t i c u l a t e s . water deposits.C l l . o i l . p a r t i c u l a t e s . s a l t . 0 CMC 1 0 **Sodium A l k y l a r y l S u l f o n a t e Powder (90%) 5 0 5 0 * * * * O c t y l p h e n o x y P o l y e t h o x y e t h a n o l . Polymeric A p p l i c a t i o n Method: H i g h p r e s s u r e s p r a y (700-1400 p s i ) Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composi t i on : Wt% Water 79.0 Metso Beads 2048 *Sodium P o l y a c r y l a t e (40%) 5.0 * * * * L i q u i d N o n i o n i c S u r f a c t a n t ( C 9 . 5 % b y w e i g h t ( 0 . 6 Moles EO) 10.0 2.0 *STPP 44. 2 . 0 *Sodi um C a r b o n a t e 10.0 * * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-C11. 5 Moles € 0 ) Use D i l u t i o n : 10% bw ( 1 3 o z / g a l l o n ) Rhone-Poulenc C o l l o i d 226/35 (40%) Stepan.0 3. 5 Moles EO 5 0 Use D i l u t i o n : 1 . o i l . 7-8 Moles EO *****Octylphenoxy P o l y e t h o x y e t h a n o l . 6 Moles EO) 3. Powder1 Soil-Grease.0 *TSP 5. c l a y .0 * * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-10. road f i l m Surface-Painted metal surface. W i t c o Rhone-Poulenc R h o d a s u r f 91-6 Rhone-Poulenc Rhodasurf A-24 SOURCE: PQ C o r p .

M i l d a b r a s i v e c l e a n i n g and p o l i s h i n g e f f e c t o f T u r b o b r i t e i s e x t r e m e l y e f f e c t i v e i n removing o i l . o i l . p a r t i c u l a t e s o i l s . Rohm & Haas Low Foam: Rhone-Poulenc A n t a r o x BL-240 H i g h Foam: S h e l l Chemical Neodol 23-6.66 Carbopol 674 0. and haze f r o m body p a r t s and w i n d s h i e l d . D i l u t e T u r b o b r i t e L / s u r f a c t a n t b l e n d a t h i g h p r e s s u r e pump w i t h w a t e r (128: 1 ) .1 *Acusol 445N Sodi u P o l y a c r y l a t e (45% s o l i d s ) m 1. M i l d a b r a s i v e c l e a n i n g and p o l i s h i n g e f f e c t o f T u r b o b r i t e i s e x t r e m e l y e f f e c t i v e i n removing o i l . s a l t . T u r b o b r i t e L can be used as an a d d i t i v e o r b o o s t e r f o r conv e n t i o n a l t o u c h l e s s .3 D i l u t e l i q u i d d e t e r g e n t w i t h w a t e r ( 1 g a l l o n d e t e r g e n t : 64 g a l l o n s w a t e r ) and d e l i v e r t o h i g h p r e s s u r e s p r a y wash system. : D e t e r g e n t F o r m u l a t i o n G u i d e . w a t e r d e p o s i t s .5 o r Neodol 25-7 * ** T o u c h l e s s V e h i c l e Wash B o o s t e r / A d d i t i v e L Z e r o Phosphate. and haze f r o m body p a r t s and w i n d s h i e l d . c a r b o n b l a c k . p a r t i c u l a t e s o i l s ( c l a y s . water d e p o s i t s . % a c t i v e T u r b o b r i t e A l u m i n o s i l i c a t e S1u r r y ) 100.5 * * L i q u i d Nonionic Surfactant 4. and o t h e r d e t a i l ing p r o d u c t s . h i g h p r e s s u r e carwash o r f l e e t w a s h d e t e r gents. road f i l m Surface-Painted metal s u r f a c e . road f i l m Surface-Painted metal s u r f a c e .0 D i l u t e l i q u i d T u r b o b r i t e L a t h i g h p r e s s u r e pump w i t h w a t e r ( 1 g a l l o n d e t e r g e n t : 128 g a l l o n s w a t e r ) and d e l i v e r t o h i g h p r e s s u r e s p r a y wash system. p a r t i c u l a t e s . p a r t i c u l a t e s . T u r b o b r i t e L a l s o works i n waxes. c l a y . L i q u i d ) Soil-Grease.1 Sodium Carbonate T u r b o b r i t e A 1 umi n o s i 1 ic a t e 24. Polymeric Appl ic a t i on Method-Hi gh p r e s s u r e s p r a y (700-1400 p s i ) Manufacture-Mix t a n k w i t h p r o p e l l e r spray Composi t i on : Wt% Water 51. Polymeric A p p l i c a t i o n Method-High p r e s s u r e s p r a y (700-1400 p s i ) Manufacture-Mix t a n k w i t h p r o p e l l e r s t i r r e r Composition: Wt% T u r b o b r i t e L (25 w t .Car and Truck Wash Compounds 201 V e h i c l e Wash D e t e r g e n t (Low PH) ( Z e r o Phosphate. b r a k e d u s t ) .84 9. SOURCE: PQ C o r p . c l a y .5 D L i q u i d Sodium S i l i c a t e 8. o i l . water d e p o s i t s . O r make a d e t e r g e n t by b l e n d i n g T u r b o b r i t e L w i t h 1-2% lowfoaming n o n i o n i c s u r f a c t a n t t o make f o r b e s t c l e a n i n g r e s u l t s . s a l t . L i q u i d ) Soil-Grease. w a t e r d e p o s i t s . p o l i s h e s .

17. Whitewall Tire Cleaners 202 .

0 Valfor 100 Zeolite A * A c u s o l 4 4 5 N D Sodium P o l y a c r y l a t e ( 9 2 % Solids) * * L i q u i d N o n i o n i c S u r f a c t a n t (C9-Cll.P.f. Soil-Clay.M i x t a n k w i t h propeller s t i r r e r C o m q . 6 m o l e s E O ) * R h o n e .0 FMC WRitewal.D r y b 1 end/Agg 1 o m e r a t i On c_q.1z e ro Whi tena 1 1 Ti. 6 nroles € 0 ) 45.0 16.P o u l e n c Rhodasurf 91 -6 * 30.0 12. o i l .. 6 M o l e s E D ) Sodium A l k y l a r y l S u l f o n a t e M e t s o Beads 2 0 4 8 Sodium Carbonate Rohm & Haas Rhone-Pou 1 e n c R h o d a s u r f 91 .r&C!ean.w&cl Soil-Clay.0 *STPP GTSP **tiquid Noninnic Surfactant Sodium A l k y l a r y l Sulfonate Met50 B e a d s 2 0 4 8 * a R h o n e . p a r t i c u l a t e . p a r t i c u l a t e . o i l . g r e a s e Surface-Whi tewal1 t i r e s Application M e t h o d s .0 2.0 10.t.% t (C9-Cll.bn: S flL?b 70.V :. p a r t i c u l a t e .6 S O U R C E : FQ Corp.H i g h Manufacture-Dry blend pressure spray/brush/wipe Cs-mmeo s.&!ea_n_er (.. p r e a s e Surface-Whi tewall tires A p p l i c a t i o n Method-High p r e s s u r ’ e s p r a y / b r u s h / w i p e M a n u f a c t u r e .0 10.0 5.0 2. o n l Nt% 35.P o u l e m R h o d a s u r f 91 .e w n 1Pbes?batePowde. grease Surface-Whitewal 1 t i r e s Application Method-High pressure s p r a y / b r u s h / w i p e M a n u f a c t tire .Ti re. o i l .Lictuj.e a -T i.1.!’l C L Y C ~e 1: Soil-Clay.0 10.0 wi j.b-s phate -?. ~!.0 10. : D e t e r g e n t F o r m u l a t i o n G u i d e .0 * ** 35.0 Water Potassium H y d r o x i d e 145%) N C l e a r o r S t a r Sodium Silicate S o d i uni A 1 k y l a r y l Sulfonate ( 6 0 % ) * L i q u i d N o n i o n i c S u r f a c t a n t (CS-Cll.m3osi t i .r. .it j P.d).6 8. Y!.ey .0 2.

Miscellaneous 204 .18.

0 8.0 8.6 .0 * ** *%Xc F C M DeSoto.0 30.0 20.D r y b l end/Aggl o m e r a t i on Composi t i on : Metso Pentabead 20 *STPP Ammonium B i f l u o r i d e *TSPP **Sodium A1 k y l n a p h t h a l e n e S u l f o n a t e ***Sodi u A1 k y l a r y l Sul f o n a t e Powder (90%) m Use D i l u t i o n : 1 .0 8. c a r b o n b l a c k . Witco Inc. m e t a l A p p l i c a t i o n Method-High p r e s s u r e s p r a y (700-1400 p s i ) Manufacture-Dry b l e n d / A g g l o m e r a t i on Composi t i on : Metso Pentabead 20 V a l f o r 100 Z e o l i t e A Ammoni u m B i f 1u o r ide TSPP *Sodi um A1 k y l naphtha1 ene Sul f o n a t e **Sodium A l k y l a r y l S u l f o n a t e Powder (90%) Use D i l u t i o n : Wt% 30. May use 0.0 20. A i r c r a f t 61 eaner (Phosphate.096 bw (2-8 oz/gallon) ** * Rhone-Poulenc S u p r a g i l N K Witco N o t e : C o n s t a n t a g i t a t i o n i s r e q u i r e d i n s t o c k t a n k t o keep V a l f o r 100 suspended i n s o l u t i o n . Powder) Soi 1 .25% w t Carbopol 647 (BFGoodrich) as a suspending a g e n t .Miscellaneous 205 A i r c r a f t Cleaner (Reduced Phosphate. c a r b o n b l a c k . 5 .8 o z / g a l l o n ) Wt% 30.5-6.0 1. Powder) S o i l . p e t r o l e u m o i 1 and grease Surface-Aluminum. 0 % bw ( 2 .0 4. p e t r o l e u m o i l and grease Surface-Metal A p p l i c a t i o n Method-High p r e s s u r e s p r a y (700-1400 p s i ) M a n u f a c t u r e .0 30.P a r t i c u l a t e s .0 8.P a r t i c u l a t e s . OURCE: PQ C o r p .0 4. : D e t e r g e n t F o r m u l a t i o n Guide .

206

Advanced Cleaning Product Formulations

A u t o Care:

I n t e r i o r / E x t e r i o r Rubber B V i n y l P r o t e c t a n t

F u n c t i ons 8 Benef it s : Pemul an 1622 : *Primary e m u l s i f i e r f o r s i l i c o n e o i l *NO s u r f a c t a n t s and no s o l v e n t s r e q u i r e d e q u a l s z e r o VOC *Imparts y i e l d value f o r v e r t i c a l c l i n g * E x c e l l e n t w e t t i n g f o r " s p r a y and no-wipe" a p p l i c a t i o n s *Improved d u r a b i l i t y and w a t e r - r e s s t a n c e Good-Rite K-752: * R e d u c t i o n i n emu1s i on v i s c o s i t y w t h o u t l o s s i n s t a b i l i t y I n q r e d ient : D I water Pemulen 1622* 1000 c S t s i l i c o n e o i l * * DC Q2-5211*** T r i e t h a n o l a m i n e (99%) Good-Rite K-752 (63%)**** * E m u l s i f i e r : BFGoodrich * * P r o t e c t a n t : DC 200 F l u i d : Dow C o r n i n g * * * S u p e r - w e t t i n g a g e n t : DC (12-5211: Dow C o r n i n g * * * * V i s c o s i t y r e d u c t i o n : BFGoodrich Physical Properties: B r o o k f i e l d RVT v i s c o s i t y - 2 0 rpm: 150 CP P r o d u c t pH: 5.5-6.0 P r o d u c t C l a r i t y : Opaque Procedure: 1 . U s i n g moderate a g i t a t i o n (800 rpm) p r o v i d e d by a L i g h t n i n ' M i x e r o r s i m i l a r v a r i a b l e speed u n i t and an i m p e l l e r s u i t a b l e f o r g e n e r a l m i x i n g and b l e n d i n g o p e r a t i o n s , d i s p e r s e o r s c r e e n t h e Pemulen r e s i n i n t o t h e D I w a t e r . Mix t h e s l u r r y f o r appr o x i m a t e l y 15 m i n u t e s o r u n t i l t h e s l u r r y i s homogeneous. 2. Add t h e s i l i c o n e f l u i d w i t h good a g i t a t i o n . 3. Add t h e DC Q2-5211 s u p e r - w e t t i n g a g e n t w i t h moderate a g i t a t i o n 4 . Add t h e t r i e t h a n o l a m i n e w i t h moderate a g i t a t i o n . 5 . Reduce a g i t a t i o n and add t h e Good-Rite K-752 p o l y m e r . The v i s c o s i t y w i l l d r o p f r o m a b o u t 3,000 CP t o <200 CP w i t h t h i s addition. 6. A d j u s t t h e pH w i t h a d d i t i o n a l t r i e t h a n o l a m i n e , i f n e c e s s a r y . 7 . Add f r a g r a n c e and c o l o r , as d e s i r e d .

Wtl
78.55 0.20 20.00 0.50 0.25 0.50

SOURCE: BFGoodrich S p e c i a l t y Chemicals:

DET-512

Miscellaneous

207

Boat Polish I n a d d i t i o n t o t h i c k e n i n g , Carbopol r e s i n s i m p a r t y i e l d v a l u e a l l o w i n g p a r t i c l e s , such as a b r a s i v e s , t o become p e r m a n e n t l y suspended. The r e s i n a l s o p r e v e n t s "creaming" o r phase separa t i o n by suspending and s e p a r a t i n g t h e o i l d r o p l e t s . Inqredi ent :

Wt%
37.80 0.20 2.50 2.00 1.50 2.50 10.00 6.00 5.00 1.50 8.50

#I Water
Carbopol EZ-2 ( 1 ) Morphol ine SF96 S i l i c o n e F l u i d (350) ( 2 ) V i s c a s i l F l u i d (10,000) ( 2 ) Oleic Acid Mineral S p i r i t s Hoechst Wax E (3) M i n e r a l Spi r i t s SF1 706 React ive A m i ne Polymer Kaopolite kaolin clay (4) Physical P r o p erties: B r o o k f ie l d V i s c o s i t y (RVT-20 rpm) : 7,200 cps P r o d u c t pH: 9.00 P r o d u c t C l a r i t y : Opaque Raw M a t e r i a l S u p p l i e r s : ( 1 ) BFGoodrich ( 2 ) General E l e c t r i c ( 3 ) Hoechst Celanese (4) Kaopolite, Inc.

Procedure: 4 . D i s p e r s e t h e Carbopol i n t o t h e w a t e r by s i m p l y "dumping" i t i n . The polymer w i l l wet o u t i n a few m i n u t e s . 2 . Add t h e m o r p h o l i n e , m i x w i t h good a g i t a t i o n . Heat t o 60-65C. 3 . I n a s e p a r a t e v e s s e l , combine t h e s i l i c o n e f l u i d , V i s c a s i l , o l e i c a c i d , and t h e wax i n t h e m i n e r a l s p i r i t s . Heat t o 90-95C u n t i l t h e wax m e l t s and t h e m i x t u r e appears homogeneous. Add to t h e above m i x t u r e w i t h good m i x i n g . 4 . When homogeneous, c o o l t o 60-65C. 5. I n a s e p a r a t e v e s s e l , combine t h e m i n e r a l s p i t i t s and t h e r e a c t i v e amine p o l y m e r . Add t o t h e above m i x t u r e w i t h h i g h shear m i x i n g . 6. S l o w l y add i n t h e c l a y . M i x u n t i l homogeneous. Total Actives: 1.50 T o t a l Wax : Total Silicone Fluid: 4.50 R e a c t i v e A m i ne Polymer : 2.00 Mineral S p i r i t s : 13.00 Abrasive: 12.00
$ ~ BFGoodrich ~ p e c i a l t y Chemicals: ~ S ~ ~ :

DET-520

208

Advanced Cleaning Product Formulations

C o n c r e t e Cleaner/Deqreaser I n g r e d ie n t s : Water, D . I . Sodium T r i p o l y p h o s p h a t e T r i s o d i u Phosphate m Varami de A-83 V a r o n i c DM55

WtB
81 . O 2.0
1.o

6.0 10.0

B l e n d i n g Procedure: Add i n g r e d i e n t s in o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t ion. T y p i c a l P r o p e r t i es : V i s c o s i t y , cps: 0 S o l i d s : 19.0% Formula 937 Garage F l o o r C1eaner I n s r e d ie n t s : Water T r i s o d i u Phosphate m Emphos PS-236 W i t c o n a t e 45 L i q u i d

Wt%
82.0 8.0 4.0 6.0

B l e n d i n g Procedure: Blend i n g r e d i e n t s i n t h e o r d e r l i s t e d . A l l o w f o r complete b l e n d i n g between a d d i t i o n s . Formula 941 A c i d Rust Remover I n q r e d ients: Water, D . I . Phosphoric A c i d , C i t r i c Acid Varox 365

\Me%
86%
81 . O 15.0 3.0 1.o

B l e n d i n g Procedure: Add i n g r e d i e n t s i n o r d e r shown and d i s s o l v e c o m p l e t e l y between each a d d i t i o n .

T y p i c a l P r o p e r t ies : V i s c o s i t y , cps: 4 S o l i d s : 16.2% pH: 1.3 Formula 1116

SOURCE: W i t c o C o r p . : Suggested F o r m u l a t i o n s

Miscellaneous

209

Concrete/Driveway

Cleaners

F o r l e a f and o t h e r t a n n i n s t a i n s - u s e as i s . Wet s p o t . S p r i n k l e FB Sodium P e r c a r b o n a t e o n t o s p o t . S c r u b i n and r i n s e w i t h hose when s p o t i s removed.

For O t h e r S t a i n s
Component: Soda Ash (Dense) B r i t e s i 1 H-24 TSP Anhydrous B u r c o s p e r s e AP Powder Dry S u r f a c t a n t * FB-Sodi um P e r c a r b o n a t e

Wt%
25 15 20 5 5 30

Wet s p o t . S p r i n k l e c l e a n e r o n t o a r e a . S c r u b i n and a l l o w t o s t a n d . R i n s e w i t h hose. *Sodium L a u r y l S u l f a t e , Sodium Dodecylbenzene S u l f o n a t e o r Sodium Cocoyl T a u r a t e s can b e used.

SOURCE:

B u r l i n g t o n Chemical C o . :

Suggested F o r m u l a t i o n

Neavv D u t y C o n c r e t e C l e a n e r ( P h o s p h a t e F r e e ) F o r m u l a 1C

Wt%
Water, D . I . EDTA, 38% Sodium M e t a s i l i c a t e , P e n t a h y d r a t e Sodium C a r b o n a t e (Soda Ash) W i t c a m i d e S-780 W i t c o n o l NP-120 B u t y l Cel l o s o l v e Mineral S p i r i t s KOH, 45% W i t c o n a t e SXS L i q u i d Pine O i l Blending Procedure: Blend i n g r e d i e n t s i n order l i s t e d , addition. Typical Properties: S p e c i f i c G r a v i t y : 1 .022 Wt./Gal. I b s . : 8.52 pH, as i s : 1 3 . 1 8 3 Freeze/Thaw C y c l e s : Passed 1 Week @ 52C: Passed 4 Weeks Room Temp: Passed S o l i d s : 13.5% Use D i l u t i o n : As s t r o n g as needed,
SOURCE:

75.0 0.5 2.0 1.5 6.5 1.5 3.0 4.0 2.5 1.5 2.0

m i x i n g w e l l a f t e r each

d e p e n d i n g on t y p e o f s o i l .

Witco Corp.:

F o r m u l a 949

210

Advanced Cleaning Product Formulations

__ n y l Dressing Vi
I g r e d i& n Part A: M a s i l EM 250 C Dei o n i zed Water

~Wt%
30.0 30.0

P a r t 8: M a c o l NP 9 . 5 G1 y c e r i n e D e i o n i z e d Water Sodium B e n z o a t e

1.5 1.5 36.9 0.1

Procedure: 1 . To a m i x i n g v e s s e l , c h a r g e t h e M a s i l E 250 C and s t a r t M g e n t l e a g i t a t i o n . S l o w l y add t h e w a t e r s o a s n o t t o b r e a k t h e emu1 s i o n . 2 . I n a s e p a r a t e m i x i n g v e s s e l , c h a r g e t h e Macol NP 9 . 5 a n d g l y c e r i n e t o t h e water. Mix w i t h g e n t l e a g i t a t i o n u n t i l a l l components a r e d i s s o l v e d , and t h e s o l u t i o n i s f r e e o f " f i s h e y e s " . Charge t h e sodium b e n z o a t e a n d m i x u n t i l d i s s o l v e d . 3 . Under g e n t l e a g i t a t i o n , c h a r g e P a r t B t o P a r t A . C o n t i n u e m i x i n g g e n t l y t o a v o i d a i r e n t r a p m e n t . NOTE: T h i s f o r m u l a i s d e s i g n e d t o be u s e d " a s i s " as a d r e s s i n g f o r r u b b e r and v i n y l p r o d u c t s . I f d e s i r e d , UV a b s o r b e r s a n d o t h e r components may be added t o t h e f o r m u l a t i o n . F o r m u l a t i o n SV-101

Inqredient: M a s i l EM 1 0 , 0 0 0 M a s i l EM 2 5 0 C Macol NP 9 . 5 Glycerine B a r q u a t MB-50 Water

C

& % 10.0 18.0

2.0
1.5 0.1 68.4

Procedure: Add t h e s i l i c o n e e m u l s i o n t o a b l e n d e r . S l o w l y a d d a p o r t i o n o f t h e w a t e r and a g i t a t e . Add t h e M a c o l NP 9 . 5 and g l y c e r i n e . M i x f o r 10 m i n u t e s . Add t h e b a l a n c e o f t h e w a t e r a n d m i x f o r 15 minutes.

SOURCE:

PPG I n d u s t r i e s ,

Inc.:

Suggested F o r m u l a t i o n s

Section Ill demarked Raw Materials 211 .

212 Advanced Cleaning Product Formulations RAW MATERIAL A-C 617A CHEMICAL DESCRIPTION Polyethylene Cationi c surfactant P o l y a c r y l a t e (40%) Tall o i l f a t t y acid Sodium p o l y a c r y l a t e (92% s o l i d s ) Sodium p o l y a c r y l a t e Anti-static agent SOURCE Allied Tomah Acid Thickener A c r y s o l AS€-108 Actinol FA-I Rohm& A r i zon A c u s o l 445ND Acusol 479ND Rohm& RohmB Witco Adogen 66 A 1 ip a l CO-128 A1 ip a l CO-436 Alkylaryl Alpha-Step Anionic surfactant Anionic surfactant Rho ne RhoneWitco S u l f o n i c A c i d (98%) MC-48 Alpha s u l f o methyl e s t e r Alpha s u l f o methyl e s t e r Amine o x i d e A m i nomethyl p r o p a n o l Amphoteric s u r f a c t a n t A m p h o t e r i c (35% a c t i v e ) Hydrotrope Amphoteric s u r f a c t a n t L i q u i d nonion c s u r f a c t a n t L i q u i d nonion c s u r f a c t a n t Surfactant (37%) Stepan Stepan Stepan Angus Zschim A 1 p h a .S t e p ML-40 Ammonyx LO AMP-95 A m p h o t e n s i d 84 A m p h o t e r i c SC A m p h o t e r i c TC A n t a r o n FC-34 A n t a r o x BL-240 A n t a r o x BL-330 A n t a r o x LF-330 Aquamoll i n BC Powder Aristonate M A r i s t o n a t e M-LF A r o m a t i c 150 Tomah Tomah RhoneRhoneRhoneRhone- P e t r o l e u m s u l f o n a t e (61%) Petroleum s u l fonate Pi l o t Pilot Sol v e n t Exxon .

mrlOX 12 Amine o x i d e (30%) Q u a t e r n a r y ammonium compound Lonza Lonza B a r q u a t NIB-50 BiQSOft D-62 B i o s o f t s-100 Sodium a l k y l benzene s u l f o n a t e ( 6 0 % ) Stepan Alkylbenzene s u l f o n i c a c i d . linear Stepan Stepan Stepan PO B i o t e r g e AS-40 B i o t e r g e PAS-8S 83-120 Sodium o l e f i n s u l f o n a t e (40%) P r i m a r y a l k a n e s u l f o n a t e (40%) b q u i d Sodi um S i 1 ic a t e Surfactant Hydrous sodium p o l y s 1 i c a t e Hydrous sodium p o l y s 1 ic a t e Hydrous sodium p o l y s 1 i c a t e B r i j 96 B r i t e s i 1 c20 B r i t e s i I H20 B r i t e s i 1 H24 ICI PQ PQ PQ Burcene I00 Burco BSGH-270 Burco WCS-SONF NPS-225 NPS-816 Burl i n Proprietary t e x t i l e auxiliary Proprietary t e x t i l e auxiliary Proprietary t e x t i l e auxiliary Proprietary t e x t i l e auxiliary Proprietary t e x t i l e auxiliary Proprietary t e x t i l e auxiliary Burl i n Burl i n Burl i n Burl i n Burl i n Burl i n SZS LAF-6 .Trademarked Raw Materials 213 RAW MATERIAL Autopoon GK4004 Autopoon GK4008 A u t o p u r WK4332 Avanel S-30 Avanel S-70 Avanel S-74 CHEMICAL DESCRIPTION Blend o f s u r f a c t a n t s Blend o f s u r f a c t a n t s Blend o f s u r f a c t a n t s Anionic surfactant Sodium l i n e a r a l k y l p o l y e t h e r Anionic surfactant SOURCE Zschim Zschim Zschim PPGMaz PPGMaz PPGMaz 5.

21 4 Advanced Cleaning Product Formulations RAW M A T E R I A L B u r c o l 117 B u r c o l i t e BSGH-255 B u r c o s o l v TM B u r c o s p e r s e AP Powder B u r c o s p e r s e LP B u r c o s p e r s e SP-60 B u r c o t a s e LL-100 B u r c o t a s e EP-60 B u r c o t a s e SL-160 B u r c o t e r g e DG-40 B u r c o TME B u r c o t r o p e 1250 B u r c o w h i t e BBH-20 Burdac-114 Butyl Carbi t o 1 Butyl Cellosolve CHEMICAL D E S C R I P T I O N Proprietary t e x t i l e auxiliary SOURCE Burli n Burlin Water s o l u b l e s o l v e n t m i x t u r e S o d i um p o l y a c r y l a t e Sodium p o l y a c r y l a t e s o l u t i o n Sodium p o l y a c r y l a t e P r o p r i e t a r y d e t e r g e n t enzyme P r o p r i e t a r y d e t e r g e n t enzyme P r o p r i e t a r y d e t e r g e n t enzyme Detergent concentrate Proprietary t e x t i l e a u x i l i a r y Burli n B u r l in Burli n B u r l in Burl i n B u r l in Burli n Burlin Burl i n Burlin B u r l in I n d u s t r i a1 s o l v e n t Ethylene g l y c o l monobutyl e t h e r UnCarb UnCarb Calamide C C a l a m i d e CW-100 Calamide C T W C a l a m i d e SM C a l f a x DB-45 C o c o n u t d e r i v e d ami de Coconut d i e t h a n o l a m i d e 100% Super ami de Non-DEA 1 iq u i d ami d e Sodium a l k y l ( b r a n c h e d ) d i p h e n y l o x i d e d i s u l f o n a t e 45% S o d i um a1 k y l ( 1 in e a r ) d i p h e n y l o x i d e d i s u l f o n a t e 45% Liquid detergent Pilot Pilot Pilot Pilot Mona C a l f a x 1OL-45 Mona C a l foam EA-603 Pilot .

b l e n d o f a n i o n i c d e t e r g e n t s and amides M o d i f i e d c o c o n u t diethanolamidelOO% P i l o t Conc. b l e n d o f a n i o n i c d e t e r g e n t s and amides I n d u s t r i a l solvent T h i c k e n i n g agent T h i c k e n i n g agent T h i c k e n i n g agent Suspension a i d Thickening agent Thickening agent T h i c k e n i n g agent Resin v i scosi t y m o d i f i e r Resin v i s c o s i t y m o d i f i e r Pilot UnCarb BFGood BFGood BFGood BFGood BFGood BFGood BFGood BFGood BFGood Calsuds 8 1 Carbi t o 1 Solvent Carbopol 672 Carbopol 674 Carbopo 1 676 Ca r b o p o l 69 1 Ca rbopo 1 934 Carbopol 940 Carbopol 941 Carbopol ETD 2623 Ca rbopol ETD 2691 .Trademarked Raw Materials 215 RAW MATERIAL Cal foam ES-303 Cal foam SLS-30 Gal i mu1 se PRS Caloxylate M-9 C a l s o f t F-90 C a l s o f t L-40 C a l s o f t L-60 Cal s o f t LAS.99 C a l s o f t T-60 Calsuds A Calsuds CD-6 CHEMICAL DESCRIPTION Sodium l a u r y l e t h e r s u l f a t e (30%) Sodium l a u r y l s u l f a t e 30% Emu1s i f ie r SOURCE Pilot Pi l o t Pilot Nonyl p h e n o l e t h o x y l a t e ( 9 M o l e EO) P i l o t L i n e a r a1 k y l a t e s u l f o n a t e Sodi u 1 inear a1 k y l benzene m s u l f o n a t e 1 i q u i d 40% Sodi u 1 inear a1 k y l benzene m s u l f o n a t e p a s t e 60% L i n e a r a1 k y l benzene s u l f o n a c i d 99% C Pilot Pilot Pilot Pi l o t Pilot Pilot TEA l i n e a r a l k y l benzene su f o n a t e 60% Conc.

w e t t i n g agent DowCor Decanol Dequest 2000 DeSonic LFD-97 DeSonic 5N DeSonic 9N DeSonic 11N DeSonic 81-6 DeSophos 5AP Diatomaceous E a r t h Organophosphorous p r o d u c t Nonionic s u r f a c t a n t Nonioni c s u r f a c t a n t Detergent/degreaser Nonionic s u r f a c t a n t Nonionic s u r f a c t a n t Phosphate e s t e r I\iiCN7san DeSoto DeSoto DeSoto DeSoto DeSoto DeSoto Kaopol PQCorp Dow or Arc0 D L i q u i d Sodium S i l i c a t e D i p r o p y l e n e G l y c o l Monoethyl E t h e r S o l v e n t Dodigen 226 Dowanol DPM Dowanol DPnB Glycol ether Glycol ether Dow Bow .216 Advanced Cleaning Product Formulations RAW MATERIALS Carbopol EX-473 Carbopol EZ-2 C a r d i s 36 Wax CDB C l e a r o n CHEMICAL DESCRIPTION (30%) V i s c o s i t y modi f i e r SOURCE: BF600d V i scosi t y modi f ie r BFGood Petrol O x i d i z e d m i c r o c r y s t a l l i n e wax C h l o r i n a t e d is o c y a n u r a t e P o l y a c r y l a t e (40%) P o l y a c r y l a t e (40%) G l y c o l e t h e r defoamer 0 in 1 RAOPa@ C o l l o i d 225/35 Col 1o i d 226/35 Contraspum 300 Cublen D50 Rhone Zschi e DC (22-5211 S u p e r .

P h e n y l p h e n a t e Dowicide A Dow DowCor Dow Dow 200 S i l i c o n e F l u i d ( 1 0 0 0 c S t ) Dowfax 2A1 S o d i um d o d e c y l d i p h e n y l o x i de d i s u l f o n a t e (45%) Anionic surfactant R o s i n soap Dowfax 382 D r e s i n a t e 91 Dow Hercul E L i q u i d Sodium S i l i c a t e Emcol 4500 Emcol 6744 E m e r s o l 213 Emphos PS-236 Emphos PS-331 Emphos 5AP E m u l s i f i e r F o u r HF W e t t i n g agent Surface-active Oleic acid Phosphate e s t e r s u r f a c t a n t Phosphate e s t e r s u r f a c t a n t Phosphate e s t e r s u r f a c t a n t D i a1 k y l q u a t e r n a r y ( 7 5 % a c t i v e ) PQ W itco agent Witco Henkel Witco W itco Witco Tomah Tomah Tomah PQ Emul s i f ie r 827 Emul s i o n C340 Epsom S a l t Mixed d i a l k y l q u a t e r n a r y (75% a c t ) .Trademarked Raw Materials 21 7 RAW MATERIAL Dowanol EB Dowanol P M Dowanol PnB Dowanol TBA Dowanol TPM CHEMICAL DESCRIPTION Ethylene glycol n-butyl ether P r o p y l e n e g l y c o l methy Glycol ether Glycol ether T r i p r o p y l e n e g l y c o l me ether ether SOURCE Dow Dow Dow Dow Dow DowCor Dow Dow C o r n i n g 20 R e l e a s e C o a t i n g Dowfax 382 S o d i um n .d e c y l d i p h e n y l o x d e d i s u l f o n a t e (45%) Sodium o .

218 Advanced Cleaning Product Formulations RAW MATERIAL Ethylene G l y c o l n-Butyl E u p e r l a n PK-771 CHEMICAL DESCRIPTION SOURCE Ether Solvent Dow or Union @ a r b P e a r l iz i ng a g e n t (47%) Henkel Foam B o o s t e r 14 Def oamer Tornah Gafac RE-40 Gafamide CDD 518 Genagen LAB Genapol OA-80 Genapol UD-030 Genapol UD-080 Genapol ZRO l i q u i d Genapol 2908 Anionic surfactant Ethanolamide C12C14 a l k y l d i m e t h y l b e t a i n e Alcohol ethoxylate C11 0x0 e t h o x y a t e ( 3 moles EO) A l c o h o l ethoxy a t e Alkyltriglycol ether sulfate soln Rhone Rhone Hoechs Hoechs H Q ~ C ~ S Hoechs Hoechs Hoechs GaMarb Ashlan Henkel Alcohol ethoxylate G e o r g i a M a r b l e W h i t e #8 c a l c i u m c a r b o n a t e G l u c o n i c A c i d S o l u t i o n (50%) G ucopon 425CS 1 G l y c o l E t h e r DPM Glycol Ether P M Good-Ri t e K-752 Good-Rite K-7058 GP-RA-159 V i s c o s i t y reducer 5800 MW p o l y a c r y l i c a c i d C8-16 a l k y l p o l y g l y c o s i d e (50%) BFGood BFGood Genes Genes Genes S i 1 icone P o l ish A d d i t i v e GP-121 S i l i c o n e P o l i s h A d d i t i v e GP-227 S i l i c o n e S u r f a c t a n t S o l u t i o n .

9-10 moles € 0 Viscous polybutene A1 kanolami ne b o r a t e I s o p a r a f f i n solvent I s o p a r a f f i n solvent RhoneRhoneRhoneRhone- Amoco Zschim Exxon Exxon M .Trademarked Raw Materials 219 RAW MATERIAL H-7892 d-Limonene Hampene 100 Hexyl C a r b i t o 1 H i t e c E-515 Hoe S3924 Hoechst Wax E Hoechst Wax S Hostapur Wax Wax CHEMICAL D E S C R I P T I O N T e t r a s o d i u EDTA m SOURCE A r y l es Grace UnCarb Ethyl Hoechs Hoechs Hoechs Hoechs I n d u s t r ia1 s o l v e n t 0s Liquid Secondary a l k a n e s u l f o n a t e Q u a t e r n a r y ammonium compound Secondary h y p o c h l o r i t e . 12-13 moles EO Nonionic ethoxylat e s u r f a c t a n t A1 k o x y l a t e d 1 in e a r a1 coho1 n o n i o n i c s u r f a c t a n t (low foam) Nonylphenoxy p o l y e t h o x y e t h a n o l . g EO RhoneOctylphenoxy p o l y e t h o x y e t h a n o l . 8 EO RhoneO c t y l p h e n o x y p o l y e t h o x y e t h a n o 1 . 10% s o l n Hostapur SAS6O Hyamine 1 O X Hypure N Hoechs Lonza I g e p a l CA-520 I g e p a l CA-620 Pgepal CA-630 I g e p a l CA-720 I g e p a l CO-430 I g e p a l CO-530 I g e p a l 60-630 Pndopol H-100 I n h i b i t o r 4000 Isopar K Isopar O c t y l p h e n o x y p o l y e t h o x y e t h a n o l . 5 EO RhoneO c t y l p h e n o x y p o l y e t h o x y e t h a n o l .

Polystyrene emulsion Zschirn Zschim Morton Macol NP 9 .220 Advanced Cleaning Product Formulations RAW MATERIAL Kaopol it e K a o p o l i t e SF Kaopol it e 1 152 K a s i l #1 K a s i l #6 K a t h o n CG K e l zan CHEMICAL DESCRIPTION Kaolin clay A n h y d r o u s a l u m i num s i 1 ic a t e A n h y d r o u s a l u m i n u m s i 1i c a t e P o t a s s i um s i 1 i c a t e P o t a s s i um s i 1 ic a t e Fungicide (biocide) Xan h a n gum SOURCE Kaopol Kaopol Kaopol PQ PQ Rohrn& Kel co Kerr- Kerr-McGee M i n e r a l S e a l O i K o m p e r l a n KD L a r o s t a t 88 L a r o s t a t 264A L a r o s t a t 519 L a u n d r y A d d i t i v e LA-5 Lonzabac-1230 Lumo WW 75 Lumorol 4154 L u m o r o l 4192 L y t r o n 295 Ant s t a t Antistat Anti stat PPGMaz PPGMaz PPGMaz Tomah Lonza Zschim Surfactant blend Surfactant blend Opacifier.1 2 & 2LF & 48 & 5100 M a f o CSB M a f o 13 MOD 1 Amphoteric s u r f a c t a n t Amphoteric s u r f a c t a n t PPGMaz PPGMaz PPGMaz . 5 & NP-11 & P o l y o x y e t h y l e n e f a t t y e t h e r OPlOSP & TD-3 & T D .

(34%) Sodium mixed C8-amphocarboxylate Monacor BE Corrosion i n h i b i t o r Corrosion i nhi bi t o r Monacor 4000 Monalube 110 & 205 & Synthetic lubricants 210 & 215 & 220 & 225 & 310 & 315 & 320 & 325 Ik 605 & 610 Monamid 150-ADD Cocamide DEA Mona .000 & 123 M a s l i p 500 & 501A & 501 Base Mazamide SS-10 80 & 1281 Mazawet 77 Mazon R I 4A & R I 6 & RI 8A & R I 88 & 98 Mazox LDA Mazu DF 210 SX Synthetic lubricant additives S p e c i a l t y alkanolamides Surfactant Specialty proprietaries F a t t y amine o x i d e Def oamer PPGMaz PPGMaz PPGMaz & 65 & PPGMaz PPGMaz PPGMaz M e d i a l a n KA Conc. Anhydrous sodium m e t a s i l i c a t e Sodium m e t a s i l i c a t e p e n t a h y d r a t e D i s o d i u cocoamphodi p r o p i o n a t e m PQ PQ RhoneRhoneMona Mona Mona M i r a n o l J E M Conc.OOOC & SF-10 & SF-100 & SF-1. Metso Beads 2048 Metso Pentabead 20 M i r a n o l CPM-SF Conc.Trademarked Raw Materials 221 RAW MATERIAL Makon 10 Makon 12 Maphos 58 Maphos 60A Maphos 8135 CHEMICAL DESCRIPTION A l k y l phenol e t h e r A l k y ? pheno7 e t h e r Phosphate e s t e r Phosphate e s t e r Phosphate e s t e r SOURCE Stepan Stepan PPGMaz PPGMaz PPGMaz PPGMaz M a s i l EM250C & Silicone fluids EM10.

Mona ISP Zschim Zschim Nacconol 9 0 G Linear alkylbenzene sulfonate(LAS) Stepan PQ RhoneShell N C l e a r Sodium S i l i c a t e Sodium m e t a s i l i c a t e N e k a l WT-27 Neodol 1 .c a p r y l im i d a z o l i fie ( 5 0 % a c t iv e ) M i I d amphoteric detergent/emulsifier Mona Monaterge 779 M o n a t e r i c CM-36s M o n a t e r i c CyNa-50 Mona Mona Mona M o n a t e r i c EH Mona Monat r o p e 1 2 5 0 M-Pyrol M u l s i f a n K326 S p e z i a l M u l s i f a n RTI n-Methyl-2-pyrrolidone Emulsifier for solvents Fatty acid ethoxylate.H y d r o x y e t h y l e n e . 5 A n i o n i c w e t t i n g agent Ethoxylate.2 . Emulsifier.2 0 Monamulse TRP & 653-83D Monaquat I S I E S CHEMICAL DESCRIPTION 2 : 1 f a t t y a1 k a n o l a m i d e s SOURCE Mona P r o p r i e t a r y emu1 s i f ie r / s o l u b i 1 iz e r s Mona Surfactants L i q u i d e m u l s i f i e r and s o l u b i l i z e r I s o s t e a r y l e t h y l d i m o n i urn e t h o sulfate Q u a t e r n a r y p h o s p h o l i p i d compound Mona Mona Mona Monayuat TG M o n a s i l PCA M o n a t e r g e ALX-100s Mona Mona Cocami de DEA & DEA-Dodecyl benzenes u l f o n a t e & diethanolamine DEA-Laureth s u l f a t e Sodium c o c o a m p h o a c e t a t e 1 .222 Advanced Cleaning Product Formulations RAW MATERIAL Monamine CF-100M & 1-76 Monamulse dL-1273 Mona NF-10 & N F . Linear primary alcohol .

6 .Trademarked Raw Materials 223 RAW MATERIAL Neodol 23-6. 5 Cf2-15 moles EO SOURCE Shel 1 Shel 1 Shel 1 Shel 1 Shel 1 Stepan Stepan Stepan l i n e a r a l c o h o l . 3 moles EO C12-15 l i n e a r a l c o h o l . Ethoxylate Coconut d i e t h a n o l a m i d e .5 Neodol 25-3 Neodol 25-7 Neodol 25-12 Neodol 91-6 N i n o l 11-CWI N i n o l 30-LL N i n o l 40-CO CHEMICAL DESCRIPTION C12-13 l i n e a r a l c o h o l . A1 k y l o l a m i d e Cocamide DEA modified P a r o i l 160 Pemulen 1622 P e t r o BW L i q u L i q u i d & BAF LBA L i q u i d & ULF L i q u i d & P h o s f e t a l 201 Phosphol ip i d EFA P i l o t SXS-40 P l u r a f a c C-17 P l u r a f a c 0-25 P o l y t e r g e n t S-305LF PQ Epsom S a l t Chlor nated p a r a f f i n Resin d & BAF A n i o n c s u r f a c t a n t / d s p e r s a n t Powder & LBA Powder & 22 Powder Phosphoric a c i d e s t e r L i ndeamidopropyl PE-Dimoni u m c h l o r i d e phosphate Sodi u x y l e n e s u l f o n a t e 40% m A1 k o x y l a t e d f a t t y a1 coho1 Linear alcohol ethoxylate. MW:930 Dover BFGood DeSoto Zschi m Mona Pilot BASF BASF Alkoxylated l i n e a r alcohol nonionic O l i n s u r f a c t a n t ( l o w foam) PQ P r i f a c 2922 P r o d u k t 2058 P r o p e t a l 99 Lauric acid Fatty alcohol f a t t y acid ester A1 k y l p o l y a l k y l e n e g l y c o l e t h e r Uni che Zschi m Zschi m . 7 moles EO Linear primary alcohol Linear primary alcohol.

224 Advanced Cleaning Product Formulations RAW MATERIAL P r o p e t a l 241 P r o p e t a l 281 P u r t o n CFD PVP K-15 CHEMICAL DESCRIPTION A1 k y l p o l y a l k y l e n e g l y c o l e t h e r A1 k y l p o l y a l k y l e n e g l y c o l e t h e r F a t t y a c i d alkanolamide P o l y v i n y l p y r r o l i d o n e polymer SOURCE Zschirn Eschirn Zschi m Rhone- Renex 2 0 R e w o t e r i c AM 8-14 R e w o t e r i c AM B-15 & AM D L 35 & AM HC & M AM KSF 40 & AM TEG & AMV Rhodafac RA-600 Rhodafac RE-600 Rhodafac RE-61 0 Rhodasurf A-24 Rhodasurf LA-7 Rhodasurf LA-9 Rhodasurf LA-12 Rhodasurf 91 -6 Rhodaterge S C M Rhodopol 23 Rhodopol 50MD R i chami de 5725 Surfactant Grease c u t t e r & foam b o o s t e r Surfactants ICI Wi t c o w i eco Linear alcohol ethoxylate Phosphate e s t e r Phosphate e s t e r L i q u i d nonionic surfactant. moles EO L i q u i d nonionic surfactant. moles EO L i q u i d nonionic surfactant. moles EO L i q u i d nonionic surfactant. moles EO Cleaner c o n c e n t r a t e Xanthan gum Xanthan gum 2. moles EO Liquid nonionic surfactant.5 7-9 RhOneRhOn@- RhoneRhoneRhone- 9 12 6 Rhone- Rhone- RhoneRhoneRhoneRichar RU L i q u i d Sodium S i l i c a t e c o r r o s i o n i n h i b i t o r PO .

Sodium l a u r y l e t h e r s u l f a t e (30%) Sodium s i 1 i c a t e 4QBe' L i q u i d sodium s i l i c a t e Alcohol ether s u l f a t e DeSoto Church F C M Olin F C M Stepan.Trademarked Raw Materials 225 RAW M A T E R I A L SF96 S i l i c o n e F l u i d CHEMICAL DESCRIPTION Polydimethyl s i l i c o n e f l u i d SOURCE GE GE S F I 705 R e a c t i ve S i 1 icone Polymer S F I 706 R e a c t i v e S i 1icone Polymer S h e l l f e x 213 S h e l l S o l 135 Rubber p r o c e s s o i l Solvent GE Shel 1 Shel 1 GE GE SM2133 S i 1 icone Emu1s i on SM2135 S i l i c o n e Emulsion SMA-2625 R e s i n S-Mar Cop01ymer r e s i n Sorbitan f a t t y ester M i n e r a l f i 1l e r Arco PPGMaz 80 Snow F l o s s JM W itco Sodium A l k y l a r y l S u l f o n a t e Powder (99%) Sodium A l k y l n a p h t h a l e n e S u l f o n a t e Sodium B i c a r b o n a t e (Grades 1 & 5 ) Sodium Carbonate Sodium D i c h l o r o i s o c y a n u r a t e . 2H20 Sodi u T r ipol yphosphate m Sodium Xylene S u l f o n a t e (40%) Sokalan CP5 B HP22 Standamid PD Standapol A Standapol ES-3 Star Cocamide DEA A n i o n i c s u r f a c t a n t . W i t c o Hen k e l Stepan Stepan PQ Starso PO Stepan Steal CS-330 . Ammonium l a u r y l s u l f a t e (30%) A n i o n i c s u r f a c t a n t .

h i g h foaming (50% a c t 1 Quaternary Quaternary Nonionic surfactants Rohm . Anionic surfactant Fatty alcohol s u l f a t e .226 Advanced Cleaning Product Formulations RAW MATERIAL S t e p a n o l WA-Extra Stoddard S o l v e n t STPP S u l f e t a l 4069 S u l f e t a l 4105 Sul f o n a t e OA5 Super F l o s s S u p r a g i l NK S u r f o n i c N-150 CHEMICAL DESCRIPTION Hydrotrope SOURCE Stepan Exxon FMC Fatty alcohol s u l f a t e . Anionic surfactant W e t t i n g agent Diatomaceous e a r t h Sodium a l k y l n a p h t h a l e n e s u l f o n a t e S u r f a c e a c t i v e agent Zschim Zschim Tennes JM RhoneTexaco TEA L a u r y l S u l f a t e RhoneNonoxynol UnCarb Hoechs Hoechs F l u o r e s c e n t w h i t e n i n g agent C i ba- T e r g i t o l NP Thermphos Thermphos N W T i n o p a l 5BM Tomah A l k a l i S u r f a c t a n t Amphoteric Tomah Amphoteric Tomah AO-14-2 Tomah A0-728 Tomah Q-14-2 Tomah Q-17-2 T r i l o n A Liquid T r i t o n DF-16 & N-101 & x-45 Special L (35% a c t i v e ) Toma h Tomah Tomah Tomah Toma h Tomah Zschim M i I d surfactant E t h e r amine o x i d e (50% a c t i v e Amine o x i d e .

Trademarked Raw Materials 227 R A W MATERIAL Tur b o b r i t e Turbobrite L Tween 40 T y l o s e CBR 10000 U b a t o l TR1138 V a l f o r 100 CHEMICAL DESCRIPTION Aluminosilicate Aluminosilicate slurry P o l y s o r b a t e 40 SOURCE PO PQ ICI Zeolite A builder PQ Van Gel B & C & ES & 0 Magnesium aluminum s i l i c a t e s Vanseal NACS-30 Vanseal NALS-30 Varami de A-1 0 & A . germicide W itco witCO W itco w itco RTVan Dow GE Magnesi um a1 umi num s i 1 ic a t e s C h e l a t i n g agents a F l u i d ( 1 0 .1 2 & A-83 & MA-1 V a r o n i c DM-55 & K205 8 T202 & T202SR Varox 365 8 1770 V a r q u a t 50MC Veegum & Veegum T Versene 100 & 220 V i scasi RTVan RTVan RTVan Sodi u 1a u r o y l s a r c o s i n a t e m D e t e r g e n t a1 kanolami des Nonionic w e t t i n g agents W e t t i n g agents S p e c i a l t y quaternary. O O O ) S i 1 icone Wachsemulsion 1864 Witcamide S-780 & 128T A l k a n o l a m i d e s u r f a c t a n t s & 6445 Zschim W i tco W i t c o 12986 W i t c o 1298SA W i t c o l a t e ES-3 & LES-6OA & LES-6OC & S E .5 & WAC-LA & 2310 W itco Soft acid Sulfated surfactants W i tco witco .

228 Advanced Cleaning Product Formulations RAW MATERIAL W i t c o n a t e AOS & SXS & 30DS & 45 L i q u i d & 60T L i q u i d & 1240 & 1260 S l u r r y W i t c o n o l NP-100 CHEMICAL D E S C R I P T I O N Surfactants SOUWGE \Mi ~ C O Detergents & degreasers Zeolith P Pine o i l Fatty alcohol ether s u l f a t e Fatty alcohol ether s u l f a t e A1 k y l p o l y e t h y l e n e g l y c o l e t h e r Alkyl polyethylene glycol ether w i tco & NP-120 Wessalith P Ya rmor 3 02 Z e t e s o l 2056 Z e t e s o l NL Zusol a t 1005/85 Zusol a t 1008/85 Hercul Zschim Pschi I Zschim Zschi rn PQ 2 . l r Potassium s i l i c a t e (39%) 2 . 4 r Sodium s i l i c a t e (52%) BQ .

Section IV pliers' Addresses .

P r o s p e c t Rd. 100 C h e r r y H i l l Rd. TX 77079 (904)-785-6700/(800)-526-5294 Ash1 and Chemical Co. NY 12188 (201)-316-3000/(800)-526-1072 B u r l i n g t o n Chemical Co. M I 48674 (8 0 0 )-2 5 8 . NC 27215 C i ba-Gei gy Corp. OH 44622 (800)-321 -8805 Dow Chemical USA M i d l a n d . 1001 E . (313)-238-4966 Georgia Marble Co. Des P l a i n e s . N o r t h b r o o k . GA 30144 (919)-584-0111/(800)-672-5888 (404)-421-6500 B. (215)-359-2000 A r izona Chemical Co. O . P . I L 60018 991 1 B r e c k s v i 1 1 e Rd .O. Fenton Rd. Box 0994 M i d l a n d . M I 48686 (312)-856-3200/(800)-621-8888 Angus Chemical Co. G o o d r i c h G o .F. M t . N J 07054 GE S i l i c o n e s 260 Hudson R i v e r Rd. Chicago. P a r s i p p a n y . B r e c k s v i l l e . Philadelphia. P 19103 A (215)-299-6000/(800)-526-3649 (614)-889-3333/(800)-848-7485 BASF Corp. B u r l i n g t o n . Box 2219 Columbus. OH 44141 (216)-447-5000/(800)-331-1~44 (312)-391-9000 . Kennesaw. B u s i n e s s Hwy 98 Panama C i t y . Box 1 1 1 615 Huffman M i l l Rd./P. PA 19073 (517)-496-4000 E t h y l Corp. 1700 S . I n c . 1201 R o b e r t s B l v d . P . Box 2332R M o r r i s t o w n .C H E M Dow C o r n i n g Corp.O. NJ 07962 Dover Chemical Corp W15 & D a v i s (201)-455-2000/(800)-526-0717 Amoco Chemical Co. W a t e r f o r d . (914)-374-4700/(800)-431-1900 DeSoto I n c . M 2000 Market S t . NY 10532 (518)-237-3330/(800)-255-8886 Genesee Polymers Corp. Box 40 Dover. 200 E. Box 7047 F l i n t . 2211 Sanders Rd. P . O . M I 48507 Inc. OH 43216 (713)-870-6000/(800)-231-6f333 F C Corp. 3801 West C h e s t e r P i k e Newtown Square. 451 F l o r i d a Baton Rouge. 7 Skyline Drive Hawthorne. O . Randolph D r . FL 32401 LA 70801 (504)-388-7556/(800)-535-3030 Exxon Chemical Americas 13501 K a t y Frwy Houston. I L 60062 (708)-498-6700/(800)-323-6209 A r c o Chemical Co.230 Advanced Cleaning Product Formulations A1 1 ied-Si g n a l . I L 60601 P.

LaGrange. 5325 S . O . Box 425 P a t e r s o n . I n c . CA 90670 (310)-723-0036 PPG/Mazer One PPG P l a c e P i t t s b u r g h . N3 07544 (201)-345-8220/(800)-553-6662 Monsanto Chemical Co. L i n d b e r g h B l v d . C 06904 T (203)-356-2000/(800)-243-9171 P e t r o l i t e Corp. T u l s a . NJ 07410 (201)-794-2400/(800)-777-1875 . 76 E . CO 80217 Kaopolite. Grace 8 Co. Inc. Kerr-McGee C t r . 11756 Burke S t . P . NJ 07828 (201 )-691-7100 Johns-Manvi 11e Ken C a r y l Ranch Denver. DE 19894 (800)-247-4372 Woechst Celanese Corp. N i n t h Ave. 1 4 S t .. 2444 M o r r i s Ave. MO 63167 (708)-530-7300/(800)-543-7370 blercul es I n c . PA 15272 (412)-434-3131/(800)-243-6774 P Corp. Union. Santa Fe S p r i n g s . R i v e r s i d e P l a z a Chicago. MA 02173 ( 6 1 7 )-861 -6600 Henkel Corp. H e r c u l e s P1aza W i l m i n g t o n . L e x i n g t o n . S t . L o u i s . 1717 R t a 208 F a i r Lawn. O . W J 07083 (9081-789-0609 Kel c o D i v i s i on Merck & Co. P . 801 Water S t . CA 92123 (61 9)-292-4900 Kerr-McGee Chemical Corp. W i 1m i n g t o n . I L 60525 Mona I n d u s t r i e s I n c . P . V A 23704 (804)-393-3100/(800)-368-2822 I C I Specialties Concord P i k e & New Murphy Rd. OK 74112 (918)-836-1601 P i l o t Chemical Co. 8355 Aero D r i v e San Diego. 24 S t . I L 60606 (312)-807-2000/(800)-367-33 O l i n Corp.Suppliers' Addresses 231 W. 55 Hayden Ave. O . 6910 E. PA 19482 (215)-293-7200 Quest I n t e r n a t i o n a l Fragrances 400 I n t e r n a t i o n a l D r i v e Mount O l i v e . DE 19897 (302)-886-3000/(800)-822-8215 (314)-694-1000/(800)-325-43 Morton I n t e r n a t i o n a l 100 N. Box 840 V a l l e y Forge.R. 120 Long Ridge Rd. OK 73125 (405)-270-1313/(800)-654-3911 Lonfa I n c . O . Box 1355 Stamford. Q P . 800 N. Portsmouth. 80x 25861 Oklahoma C i t y .

I L 60093 (708)-446-7500/(800)-745-7837 Tennessee Chemical Co. V a n d e r b i l t Co. I L 60609 (312)-376-9000/(800)-833-2884 Union C a r b i d e Corp. W I 53563 (608)-868-68ll/(800)-441-0708 Uni chema Chemicals I n c . Houston.232 Advanced Cleaning Product Formulatioris Rhone-Poul enc P r o s p e c t P l a i n s Rd. NY 10022 Inc. I L 60018 Rohm & Haas Co. Independence M a l l West P h i l a d e l p h i a . 39 O l d Ridgebury Rd. T . GA 30326 Tomah P r o d u c t s . 2400 East Devon Ave. 520 Madison Ave. Des P l a i n e s . Box 2463 Houston. Cranbury. New York. T X 77056 (713)-961-3711 3 M 3 Center M S t .. 3400 Peachtree Rd NE A t l a n t a . Chicago. O . Norwalk. N o r t h f i e l d . 1012 T e r r a D r i v e M i 1t o n . P a u l . 3040 Post Oak 8 l v d . I n c . (203)-853-1400/(800)-243-6084 (212)-605-3941/(800)-634-4010 Zschimmer & Schwarz Max-Schwarz-Strabe 3-5 D-56112 L a h n s t e i n/RH D 26 21/120 (404)-239-6700/(800)-241-1912 Texaco Chemical Co. Danbury. 4650 S . 22 W . PA 19105 (215)-592-3000 S h e l l Chemical Co. Racine Ave. MN 55144 (612)-733-5454 . TX 77252 (713)-241-6161 Stepan Co. CT 06856 W i t c o Corp. CT 06817 (203)-794-2000 R . F r o n t a g e Rd. Box 5150 30 W i n f i e l d S t . O . P . P . N J 08512 (609)-860-4000/(800)-626-2613 Richardson Co.

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