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GCL

GCL

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Published by Vaibhav Pandere

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Published by: Vaibhav Pandere on Apr 17, 2012
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04/17/2012

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IN-PLANT TRAINING

AT

GHARDA CHEMICAL LTD. LOTE- PARASHURAM

Mr. Vaibhav V. Pandere Roll No. 49

Duration of Training: 6 Weeks [From 16th May. Lote MIDC. Maharashtra. 2011] Plant Explored: Plant-2 Product Studied: Cypermethrin . Dist: Ratnagiri. D-1/2.Training Details Company Name & address: Gharada Chemicals Limited. Lote-Parshuram. Tal: Khed. 2011 to 30th June.

• Awarded the prestigious "Chemexcil Trishul Award" for outstanding exports among large-scale chemical manufacturers for 1995 – 1996 . • Only Indian company to receive U. 8948 million (2009-10) including exports worth Rs. Registration (EPA Approval) for the sale of Chlorpyrifos (Insecticide) and Dicamba (Herbicide) in the U. 4325 million. with world class products and annual sales of Rs.S.A.About Company • Established in 1967 • Among top ranking chemical companies in India.S.

Major Products Insecticides Fiproles Fipronil Neonicotinoid Acetamiprid Organophosphorus Chlorpyrifos Quinalphos Temephos Triazophos Oxadiazine Indoxacarb Synthetic Pyrethroids Alphacypermethrin Cypermethrin Deltamethrin Fenvalerate Permethrin Herbicides Anilofos Clodinafop-propargyl Dicamba Isoproturon Metamitron Napropamide Sulfosulfuron Triclopyr Butoxy Ethyl Ester Fungicides Carbendazim Plant Growth Regulator Mepiquat chloride .

CYPERMETHRIN DELTAMETHRIN ALPHAMETHRIN PLANT 2 PRODUCTS INDOXACARB METAMITRON .

23 g/cc at 20oC Solubility in Water: <9µg/L at 20oC Vapor Pressure: 5.2-dichloroethenyl)-2. It controls a wide range of insect pests on a variety of crops by stomach and contact action.About Cypermethrin Cypermethrin is a highly active synthetic pyrethroid insecticide. • Structure: • Chemical Name : • • • • • cyano(3phenoxyphenyl)methyl 3(2.30 g/mol Density: 1.2dimethylcyclopropanecarboxylate CAS number: 52315-07-8 Molecular Weight: 416.1 x 10-7 Pa @ 70oC .

Chemistry of The Process  Production of cypermethrin PTC CMAC(l) + MPB(l) + NaCN(aq) CMN(l) + NaCl(aq) • Two phase reaction • Reaction conditions.between 9-9.5  Cyanide destruction 2NaCN(aq) + 5NaOCl(aq) + 2NaOH(aq) N2(g) + 5NaCl(aq) +2Na2CO3(aq) + H2O(l)  Reaction in scrubber 2HCN(g) + 5NaOCl(aq) + 4NaOH(aq) N2(g)+ 5NaCl(aq)+2Na2CO3(aq)+3H2O(aq) .680-720 mm of Hg pressure 15-40oC temperature pH.

Steps in Standard Operating Procedure (SOP) • • • • • • • • • • • • • • Preparation of Cyanide Solution in R-2103 MPB Sucking in T-2921 CMAC Sucking in T-2922 Water and Hexane Receiving in R-2921 Cyanide Receiving in R-2921 PTC Sucking in R-2921 NaOH Charging Simultaneous Feeding of CMAC and MPB Maintaining Sampling Phase Separation NaOCl Wash Water Wash Concentration of Cypermethrin .

Block Diagram T-2923 NaOCl T-2909 Water T-2931 NaCN condenser X2921 Scrubber T-2920 NaOH T-2921 MPB T-2922 CMAC Vent T-2924 Hexane R-2921 condenser R-2936 To ETP R-2923 T730 To Plant-3 T2507 .

HEAT EXCHANGERS Sr. 1 2 Ground 1st Floor Shell & Tube 3 1 Graphite Block 0 0 Plate 3 0 3 4 5 6 Total 2nd 3rd 4th Terrace 10 4 1 23 42 5 1 0 2 8 0 0 3 0 6 Total=56 . no.

Floor Vacuum Blowers Reciprocating Centrifugal 1 Ground 1 0 0 49 2 3 4 5 6 Total 1st 2nd 3rd 4th Terrace 0 0 0 1 3 5 0 0 0 0 3 3 0 0 1 6 0 7 8 21 8 6 10 102 Total=117 . no.PUMPS Sr.

Low pressure steam .  Cogen Plant • Used for production of electricity • High pressured steam is sent through the nozzles of the turbine • The steam coming out from the turbine is divided into 3 types with the help of a PRV i.PLANT UTILITY  Boiler House • • • • Consists of 2 boilers with total capacity of 8 tons per hour Coal is used as a fuel Pressure generated is around 9. High pressure steam ii. Medium pressure steam iii.8 Kg/cm2 Temperature is about 180 oC.

STANDARDS AND COMPLIANCES  ISO 9001-2000 (QMS)  ISO 14001-2004 (EMS)  OHSAS 18001-1999 (OHSMS) .

EFFLUENT TREATMENT PLANT Steps In ETP  Oil Separator  Neutralisation Tank  Filter Press  Clariflocculator  Bioreactor  Clarifier Water processed from ETP is sent to • Common ETP • Neighbouring water bodies .

.

TROUBLESHOOTING Some of the problems commonly encountered in Plant 2 during operations include: Vacuum Problem  Flooding  Chocking in line-up.  Reactor leakage  Phase Separation .

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