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CHE 411 Separation Processes II

2nd Semester 1427/1428 H

14281 18

Tutorial # 1

Q.1 Gas from a petroleum distillation column has its concentration of H 2S reduced from

0.03 moles H 2S / mole of inert hydrocarbon gas to 1/10 th of this value, by scrubbing

with a triethanolamine-water solvent in a countercurrent plate column operating at

atmospheric pressure.

H 2S is soluble in such a solution and the equilibrium relation maybe taken as conforming to

with a solution containing c grams of H 2S in 1000 grams of solvent , and H = 0.00143 .

The solvent enters the column free of H 2S and leaves containing 0.013 moles of H 2S per

mole of solvent. The mean molecular weight of the solvent is 25 .

If the flow of inert hydrocarbon gas is 100 lbmole / hr calculate:

a. The number of theoretical stages required for this duty.

b. The necessary solvent rate.

Q.2

through a bubble cap tower fed with muriatic acid containing 37% HCl by weight. The

equilibrium data X ,Y for solutions of HCl in water is as follows:

0.35

0.40

0.45

0.50

0.525

0.55

0.575

0.600

X

0.003 0.012 0.027

0.065

0.105

0.165

0.243

0.375

Y

Y lb HCl / lb air

Where : X lb HCl / lb water ,

a. What would be the minimum permissible exit concentration of acid in %HCl by

weight?

b. Find the number of theoretical bubble cap plates required if the exit acid must be

32% HCl by weight.

Q.3 An air/ammonia mixture of y NH 3 = 0.009 enters a packed bed countercurrent scrubber

at a rate of 450 ft 3 / min . The tower is operating at 68o F and 1 atm . The packed bed has a

diameter of 0.5 ft . Pure water enters the top of the column at a rate of 29 lbm / min . The

3

overall gas phase mass transfer capacity coefficient is K y a = 4.5 lb.mol / min . ft .

relationship for the NH 3 / H 2O system is of the form y = 1.25 x (x, y mole fractions). Find

the tower packed height.

Q.4 A packed column is used to scrub a soluble impurity from 100 kgmoles h 1m 2 of

gas by countercurrent absorption in a liquid at atmospheric pressure. The inlet and outlet

concentrations of the solute in the gas are to be 1% and 0.01% by volume respectively. If

1.5 times the minimum liquid flow rate is to be used, calculate the number of transfer units

N OG required.

King Saud University

Chemical Engineering Department

CHE 411

Separation Processes 2

Contents:

1. Topics covered (syllabus)

2. Textbook and reference books

3. Final examination paper + samples of students answers

4. Second mid-term exam (T#2) + samples of students answers

5. First mid-term exam (T#1) + samples of students answers

6. Tutorials and Homework

7. Samples from students answers of Tutorials and Homework

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