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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04051-0R

May 6, 2013

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY


OAK RIDGE, TN

TABLE OF CONTENTS

SECTION

DESCRIPTION

PAGE

Chain of Custody & pH Check Sheet

II

Sample Acknowledgement

III

Case Narrative

0012

IV

Analytical Results Summary

0015

Analytical Standards

0019

VI

Quality Control Sample Results Summary

0025

VII

Laboratory Technician's Notes

0049

VIII

Analytical Data (Isotopic Uranium)

0088

IX

Analytical Data (Isotopic Thorium)

0202

Analytical Data (Radium-226)

0318

XI

Analytical Data (Radium-228)

0428

XII

Barium-133 Analytical Tracer Data

0447

Last Page Number

0523

0004
00

STANDARD OPERATING PROCEDURE

MP-001, Rev. 12
Effective. 10131112
Page 14 of 14

Sample Receiving

Eberline Services -Oak Ridge Laboratory


LABORATORY DATA SUPPORT CHECKLIST

MP-001-3

1_3_-_0_4_0_5_1_____

Eberline Services Work Order #_ _ _

The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial

Initials

Date

Initials

Checklist Items

Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
Sampl~lyzed

Yes? LX:

QNQc.{R~view
I

within Holding Time

J No?

Client in Possession of Data


.... ,
or Hard Coov
Invoiced by Laboratory

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Date/Initials

,......

\_
Date package approved by:

~~
Laboratory Manager

CJ
Copy No. _ _ __

~~lt'?
Date

Radiochemistry Services

-5&63

SECTION I
CHAIN OF CUSTODY
&

pH CHECK SHEET

13-04051

Chain of Custody Record


Project Name:

~LA

Send ReportTo:?I\J

Project Number:
Sampler (Print Name): ~~N

D ~M)

Airbill Number:

j,

--

Laboratory Receiving:

LR-tco

Sample
Date

If

(3(;./

fPLs-~PGw55

~by: (Signature)

\"tV'

lf

-Aelinquished by: (Signature)

\!)

t5d0

~~~

~:;c:;;~r~~
~~ r,.J.t\t.

: Relinquished by: (Signature)

Received by: (Signature)

;:j1~ ~ ~

~~ments, Special

Lab Sample ID

structions, etc.

(to be completed by lab)

\::) (i)
fi'.

\{~ C\J 1-\

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1:.;if

Purcha:,e
Order

C'(

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Number of
Containers f c::_P.

V_~

<)-2;
D-13

)-

Sample
Matrix

I!3Zf0
149.4

l~-r5

LJ<~to'S
P2-- ltn~
~-Cd.

Time

L;/i/13 !1'-15

[)-~1

152 Cf;:J~At5

S~mple

~/ ~~~Jij;

Fax:

p6 ~3o:;t- A-J:

(865) 481-0683 Phone. (885) 483-4621 Fax

:~
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Shipment Method: Gw-t~s-

Field Sample 10

OakRidge,TN37830

clJ :S r!JOo

Sampler (Print Name):

Phone:

Eberllne Services

601 Scarboro Road

1604

00-l

\<_~'S::,.O

Address:

N~

v
I
Date:

'1/l/13
Date:

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Time:

0~

Time:

(()

Sample Custodian Remarks (Completed By Laboratory):


OAJOC Level

Sample Receipt

Turnaround

Total # Containers Received?

T1me:

~h(r; roD
Date:

Level

Routine

Level

II

24 Hour 0

COC Seals Intact?

Level Ill
Other

1 Week o
Other _ _

Received Containers Intact?

Temperature?

COC Seals Present?


!

13-04051
Chain of Custody Record
Project Name: ~LA
Send Report To:~J

k. ov-1

N~

1604

Sampler (Print Name): -::)~

D ~,1\\J

I.~'

AirbiH Number:

/::5

.f~

Laboratory Receiving:

Phone:

.::)

Fax:
S!imple
OQie

Sample
Time

'1/'(8

i5J,~_,

Aeld Sample 10

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Q~~~;&
Heceived by:

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&a-... (',,..\) Ak

I
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f..

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Lab_~~ID

~;neniS,_~aJ
structlons, etc.

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'lil!

Number of
Containers

fi/~B (J/:5)

s-~1

~~

Matrix

[),}JrZi}-

- /Jtu-/03
\

~"P:J-1(Y>J

\1,,
l~,

Lf<:.-iY-/
[),JW I

~pie

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Q:"~

Shipment Method: G..urc:>

Paged-~
C{-Rr~ ~ . ~

iJDaf'6
"'
rl ((!

Sampler (Print Name):

Address:

(865)481.()683 Phone (865) 483-4821 Fax

~/ aot~~

Project Number:

\<_~o

~
~EBERIF!tNE
.. ___

l!bertlne Servlcn
601 Sc:aJbon:l Road
Oak Ridge, TN 37830

~~~
Date:

~~~~~
Date:

1J XJ XJ

X 1J 'A fi
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XX

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'8"0\)

Level Ill

0
0
0

Other

Level II

0
24Hour 0
1 Week 0
Other _ _
Routine

'

Sample Receipt

Turnaround

Total # Containers Received?


Level I

-c1)

Sample Custodian Remms (Completed By laboraiOry):

llme:

llme:

COC Seals Present?

COC Seals Intact?


Received Containers Intact?
Temperature?

EBERLINE
SERViCES

Oak Ridge Laboratory

Internal

Work Order#

13-04051

Chain of

Lab Deadline

4/30/2013

Custody

UUISO - Level 4

Analysis

Water

Sample Matrix

Sample
Fraction

Comments

HP 210/270
Detector Activity

Storage
Location

Initials

Date

Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED

Location (circle one}

Received by

Rough Prep

Prep

Separations

\l~
l \ t./ .,!,1Jl6:t'lrl' ~

Count Room

~~---~-~~-------~~--(9----~-

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

9s

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

~rati~ns)

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Relinquished by

Sample Storage

Rough Prep

Prep

Separatio~unt Roo~

safe~

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Sample Storage

Rough Prep

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Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

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Sample Storage

Rough Prep

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Relinquished by

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Prep

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I~ 4/r~ w~ /b~
~
l
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( ,r;, 'r:+'-to

..

----

......

Printed: 4/9/2013 2:05 PM

Internal
EEIERLINE::

Chain of
Custod

SERVICES

Oak Ridge Laboratory

Work Order#
Lab Deadline

ThiSO- Level4

Sample
Fraction

Comments

HP 210 I 270
Detector Activity

Storage
Location

Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED

Location
Received by

Rough Prep

Separations

Count Room

Separations

Count Room

Sample Storage

Rough Prep

Sample Storage

Rough Prep

Sample Storage

Rough Prep

Prep

Sample Storage

Rough Prep

Prep

Rough Prep

Prep

Separations

Count Room

Count Room

(frS__~

WI?~-I

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Sample Storage

Rough Prep

Prep

Separations

Count Room

Sample Storage

Rough Prep

Prep

Separations

Count Room

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

~~ffl~

'".,.lAo,_.,.

Printed: 4/9/2013 2:05 PM

tlH~tJO

EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-04051

Chain of
Custody

Lab Deadline

4/30/2013
Ra226 - Level 4

Analysis

Water

Sample Matrix

HP 210 I 270
Detector Activity

Sample
Fraction

Comments

Storage
Location

Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED

Initials

Location (circle one)


Received by

Sample Storage

Rough Prep

Prep

Separations

bo ~
ic'\:) j

Count Room

Relinquished by

Sample Storage

RoughPrep~

Separations

Count Room

Received by

Sample Storage

Rough Prep(

Prep

~ar~

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

~~

Count Room

I~

Received by

Sample Storage

Rough Prep

Prep

Separations

::k'

eunfR~

Sample Storage

Rough Prep

Prep

Separations

Received by

~mple Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

.J./h ~~ /')1~)

411 ~',9/~

~ 4-k~ VG~-~-Lf!~

..../

~t~~-

Relinquished by

Date

Mille Vf~

f5oo

~---~--ill~ t~ I(SO~

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tvob

1--

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Printed: 4/9/2013 2:05 PM

Internal
EBERLINE

Work Order#
Lab Deadline

Chain of
Custod

SERVICES

Oak Ridge Laboratory

Ra228 - Level 4

Comments

....

Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL

Sample
Fraction

HP 210/270
Detector Activity

04

46

05

46

06
07

42
... ...........

08

Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED

09
10

....... ....................
.........

45

,.............................. 45

................... !

48
-~~---

48
43

13

43

14

42

15

42

19

.........

--

42

12

18

...............................

11

16
17

Storage
Location

.......................

..............

..............................

, ....
.........................
....................

48

....

i
........ ................

48

..................

Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O
Ul.O

-~--------

37
37

........

. .......
....
. ...........................

---

....

I Jt:f1!l

J../ I (I
Init als

Location (circle one)


Received by

Qample

Stora~

Prep

Separations

Count Room

Rough Prep

Prep

Separations

Count Room

Rough Prep

Relinquished by

Sample Storage

Rough Prep

Received by

Sample Storage

Rough Prep

Date

Relinquished by

Relinquished by

.
Received by

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

iiiiH1
-

Printed: 4/9/2013 2:05PM ~

Page 1 of 1

Printed: 4/9/2013 1:21 PM

Internal Work Order

~ EJ;i E;;_RJ.,.I _.,., E;;

13-04051

Sample Receiving Report

Received By

{Volumes, pH, & CPM)

SERVICES

KCOULSTON
FR
01
02
03

04

ClientiD
LCS
BLANK

DUP
PZ-105-SS TOT /

WA
WA
WA

0
0
0

WA

1
"~'c

OS

PZ-105-SS DIS ""

container Number
1

Containtr Number " "~ ~ PH OiiaF


1

'"

06

S-10 TOT-

1
.

07

S-10 DIS'

WA

,,,,,.

: .. ~

contalnerNumber
1

LR-104 TOT/

10

LR-104 DIS./

,'

11

Container Number
1

.PH Orla

DUP 01 DIS'

"

Container Number
1

:pWOria~

DUP 02 TOT

',,

container Number
1

13

DUP 02 DIS /

...

~
14

FB PZ-110-SS TOT....FB PZ-110-SS DIS'

16
17
18

MW-103 TOT,.

PZ-200-SS DIS

cKruit:exv ~

Ul.O

9.50

''~

'

Ul.O

0.00

43

pH Final

Volume ILl

CPM
43

Ul.O
pHFinal .
7

Ul.O

9.50
~V:olume,fLI

,
9.5000

42
;,'::

~CPM'

42

42

0.00

DH,Final . Vorume:ca.1,., :~::''CPM


42

container Number
1

'pHOria
7

WA

Ul.O

0.00

48

Container Number~
1

pHOri!i

. pH Final

VolurniiiLI

CPM
48

Contail)erNurnber

, ::pH Orl!i .
7

WA
'

43
''CPM. ,,,, .
43

I ' :PH Final'' :':Volume 1M::.~


9.5000
7

PHOria

' '~

Received by:

48

WA

19

:"'',: CPM'
48
'CPM,:
48

PHOria
7

contairierNum6er.
1

Date: _t.\...._{

pHOria:

~-_{!"""'-~--

'

48

9.50
Volumeltk,:
9.5000

Container Number.
1

"'

45
CP,..
45

0.00

WA

. '"'"

0.00

.volumefLli

pHOria
7

PZ-200-SS TOT/

Ul.O

45
:CPM ..~
45

PH Final

PHOri!i

container. Num6er
1

MW-103 DIS....-

9.50
''Nolumll..fLt''''
9.5000

WA

.'

cPM
42

Ul.O

PHOria

WA

1
15

42

0.00
votumettl .

WA

.. Container. Num6er'
1

42

, V:ofume lUI' '' I'''" 'CPM:::;


9.5000
42

PH Final
7

Ul.O

WA

Ul.O
... PH

~ '~' pH" Final

WA
... Container"Number

~C

I,,~~

46

9.50
<~

..; : ,,:.GPMi <:"


46

pH Fnat: ' '''Vorumelt.:J.

WA

.. :

~"'
12

PHOria
7

WA

0.00
V:i>fumifiUJ

Ul.O

Container Number:,
1

DUP 01 TOT...-

PHOria'

WA

1
;"

09

Number.
1

46
<CPM,
46

Ul.O

,plfFirial
7

! '

9.50
' Volume ll'~
9.5000

, pHFtilak.

Ul.O

PHOiia
7

WA

1
~Container

08

;pH,FiiUil
7

~PH Orig '""'


7

WA

Rec Vol Ttl CPM Max

Storage
Ul.O
Ul.O
Ul.O
Ul.O

Matrix

Comments

# Btls

Ul.O
::pH Final''''
7

Ul.O
pHFillai'J
7

Ul.O
' ' DHFinal'

9.50

48

votumelt:.l
9.5000

'CPM.~

9.50
Votumefl::.l
9.5000

0.00
'"" Volume'ILI

~:}:,

48

37
'~.

.CPM:
37

37
':, 'CPM;.:.

37

MP-001, Rev 5
Effective: 11/22/02

iii iii i l

SECTION II
SAMPLE ACKNOWLEDGEMENT

Client Name

..

Engineering Management Support, Inc. West Lake


Project Name

~--

ou-11
:

ClientWO

West Lake OU-1


lnternaiiD

Contract/PO

..

Client ID

Project Type

Date Received

Environmental

04/09/2013

28

Sample Disp

Lab Deadline

Internal Deadline

04/30/2013

05/06/2013

West Lake

ou-11

Sample Date

Matrix

Storage

. ...

,.

Required Tur11around Days

13-04051
--.
05/07/2013

IJ

:C
1-

:::l

..

(I)

01

LCS

04/09/13

WA

Ul.O

02

BLANK

04/09/13

WA

Ul.O

03

DUP

04/09/13

WA

Ul.O

04

PZ-105-SS TOT

04/04/13 15:06

WA

Ul.O

OS

PZ-105-SS DIS

04/04/13 15:06

WA

Ul.O

06

S-10 TOT

04/04/13 15:25

WA

Ul.O

07

S-10 DIS

04/04/13 15:25

WA

Ul.O

08

LR-104 TOT

04/04/13 15:52

WA

Ul.O

09

LR-104 DIS

04/04/13 15:52

WA

Ul.O

10

DUP 01 TOT

04/04/13 00:00

WA

Ul.O

11

DUP 01 DIS

04/04/13 00:00

WA

Ul.O

12

DUP 02 TOT

04/04/13 00:00

WA

Ul.O

13

DUP 02 DIS

04/04/13 00:00

WA

Ul.O

14

FB at PZ-110-SS TOT

04/04/13 09:30

WA

Ul.O

15

FB at PZ-110-SS DIS

04/04/13 09:30

WA

Ul.O

16

MW-103 TOT

04/05/13 09:50

WA

Ul.O

17

MW-103 DIS

04/05/13 09:50

WA

Ul.O

18

PZ-200-SS TOT

04/05/13 11:10

WA

Ul.O

19

PZ-200-SS DIS

04/05/13 11:10

WA

Ul.O

Totals Per Analysis (non QA samples)

16

16

Invoice

~
"

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830

EeERLI. NE
SERVICES

Voice

Sample Log In Report

Voice: (865) 481-0683


Fax:
(865) 483-4621
I

16

16

Paul V. Rosasco, P. E.

Report Data

Paul V. Rosasco, P.E.

Engineering Management Support, Inc.

Engineering Management Support, Inc

7220 West Jefferson Avenue, Suite 406

7220 West Jefferson Ave, Suite 406

Lakewood. CO 80235

Lakewood, CO 80235

303-640-3426

Voice

303-940-3426

Fax

Fax

Contact

Lyn Fitzgerald

Voice

303-601-4255

Fax

G',
II-
(.,;~

Printed: 4/9/2013 2:05PM

STANDARD OPERATING PROCEDURE

MP-001, Rev. 12

Effective. 10131112
Page 13 of 14

Sample Receiving

Eberline Services -Oak Ridge Laboratory


SAMPLE RECEIPT CHECKLIST

1 3- 0 4 0 5

1MP-001-2
WORK ORDER# ___________________
SAMPLE MATRIX/MATRICES:

(CIRCLE ONE OR BOTH)


(1\auEOLj!)

NON-AQUEOUS

(CIRCLE EITHER YES, NO, OR N/A)


WERE SAMPLES
Received in good condition?
If aqueous, properly preserved

krJ

N/A

WERE CHAIN OF CUSTODY SEALS


Present on outside of package?
Unbroken on outside of package?
Present on samples?

r0
10

N
N

Unbroken on samples?

Was chain of custody present upon sample receipt?

IM

IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: __________________________________________________________

DATE:

Copy No. _ _ __

'i/q_/IJ

Radiochemistry Services

SECTION III
CASE NARRATIVE

EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD


OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683

FAX (865) 483-4621

EBS-OR-35526
May 7, 2013
Paul V. Rosasco, P.E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 8023 5
CASE NARRATIVE
Work Order# 13-04051-0R
SAMPLE RECEIPT
This work order contains eight water samples received 04/09/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID

LABID

CLIENT ID

LABID

PZ-1 05-SS TOT


PZ-1 05-SS DIS
S-10 TOT
S-10 DIS
LR-104 TOT
LR-104 DIS
DUPOlTOT
DUP 01 DIS

13-04051-04
13-04051-05
13-04051-06
13-04051-07
13-04051-08
13-04051-09
13-04051-10
13-04051-11

DUP02TOT
DUP 02 DIS
FB at PZ-110-SS TOT
FB at PZ-11 0-SS DIS
MW-103 TOT
MW-103 DIS
PZ-200-SS TOT
PZ-200-SS DIS

13-04051-12
13-04051-13
13-04051-14
13-04051-15
13-04051-16
13-04051-17
13-04051-18
13-04051-19

ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using EPA Method 903.0. Radium-228 was analyzed using EPA Method 904.0.
Laboratory qualifiers are as follows:
J-

Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.

U-

Indicates a situation where the result minus the error is less than or equal to zero.

ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.

Page 1 of3

ANALYTICAL RESULTS CONTINUED


ISOTOPIC URANIUM
Samples were filtered to disassociate dissolved and total fractions. Volumetric aliquots from dissolved
fractions were acidified with HN03 All samples were prepared by mixed acid digestions as appropriate.
Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated and
mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical
recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated an
acceptable relative percent difference and normalized difference. Results for the Uranium-234 and
Uranium-238 laboratory control sample demonstrated an acceptable percent recovery.
ISOTOPIC THORIUM
Samples were filtered to disassociate dissolved and total fractions. Volumetric aliquots from dissolved
fractions were acidified with HN03 . All samples were prepared by mixed acid digestions as appropriate.
Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated and
mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232. Chemical
recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228, Thorium-230 and Thorium-232 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
RADIUM-226
Samples were filtered to disassociate dissolved and total fractions. Volumetric aliquots from dissolved
fractions were acidified with HN03 . All samples were prepared by mixed acid digestions as appropriate.
This was followed by selective sulfate precipitations of the Radium. Samples were then mounted by
semi-micro-precipitations onto micro-porous filters. Samples were counted by alpha spectroscopy using
an energy specific region of interest for Radium-226. Chemical recovery was calculated by the use of a
Barium-133 tracer, which was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium226 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-226 laboratory control sample
demonstrated an acceptable percent recovery.

Page 2 of3

ANALYTICAL RESULTS CONTINUED


RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium228 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-228 laboratory control sample
demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.

M.R. McDougall
Laboratory Manag
Date: 5/7/2013
Ebcrlinc Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.cbcrlincscrviccs.com/clicnt.htm to provide us with feedback on our services.

Page 3 of3

5Hi18

SECTION IV
ANALYTICAL RESULTS SUMMARY

Client Sample ID

c;,
Q)

ft.ll
Q~

Lab Sample ID

Final Report of Analysis


Date: 5/7/2013
Page 1 of 5

Project: West Lake OU-1


SDG: 1304051
Received: 04/09/2013
Matrix: Water

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Analysis Date/Time

Analvte

LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01

13-04051-01
13-04051-01
13-04051-01
13-04051-0 1
13-04051-01
13-04051-01
13-04051-01
13-04051-01

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

14:39:26
08:17:44
13:48:50
13:48:50
13:48:50
11:36:31
11:36:31
11 :36:31

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02
8 LANK 13-04051-02
BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02

13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02

04/19/2013 14:39:27
04/29(2013 08:17:45
04/20/2013 13:48:51
04/20/2013 13:48:51
04/20/2013 13:48:51
04/19/201311:36:32
04/19/201311:36:32
04/19/2013 11:36:32

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

FB at PZ-110-SS TOT DUP


FB at PZ-11 0-SS TOT DUP
PZ-105-SS TOT DUP
PZ-105-SS TOT DUP
PZ-105-SS TOT DUP
PZ-105-SS TOT DUP
PZ-105-SS TOT DUP
PZ-105-SS TOT DUP

13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03

04/19/2013 14:39:28
04/29/2013 08:17:45
04/20/2013 13:48:52
04/20/2013 13:48:52
04/20/2013 13:48:52
04/19/201311:36:33
04/19/2013 11:36:33
04/19/2013 11 :36:33

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-1 05-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT

13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04

04/19/2013 14:39:28
04/29/2013 08:17:45
04/20/2013 13:48:53
04/20/2013 13:48:53
04/20/2013 13:48:53
04/19/201311:36:34
04/19/2013 11:36:34
04/19/2013 11 :36:34

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

2J
~EBER~I ..... E

Result

Error

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

10.63
9.72
5.19
5.36
5.22
7.85
0.43
8.02

1.15
0.89
0.81
0.83
0.81
1.07
0.17
1.09

0.17
1.04
0.14
0.08
0.08
0.09
0.08
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.12
0.59
0.00
0.10
0.00
0.05
0.04
0.02

0.12
0.39
0.03
0.07
0.02
0.05
0.06
0.05

0.17
0.76
0.09
0.05
0.05
0.07
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

-0.03
0.13
-0.02
0.13
0.01
2.60
0.11
1.82

0.04
0.43
0.06
0.09
0.04
0.46
0.09
0.36

0.15
0.91
0.15
0.08
0.09
0.09
0.07
0.06

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

1.79
0.87
0.04
0.08
0.01
2.62
0.11
1.64

0.40
0.46
0.06
0.07
0.02
0.45
0.09
0.33

0.14
0.88
0.10
0.08
0.06
0.08
0.09
0.06

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

FAX

0.09

865/483-4621

Qualifier

Units
pC~

~~
pC~
pC~

~~
pC~
pC~
pC~

~~

pC~

pC~

pC~

u
u
u
u

~~

~~

pC~
pC~
pC~

pC~

~~

pC~

~~
~~

pC~

~~
~~

pC~

pC~

~~
~~

pC~

pC~

~~

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample 10
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS

~lt
I'\)
~~-

Lab Sample 10 Analysis Date/Time

Analvte

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

14:39:29
09:09:03
13:50:08
13:50:08
13:50:08
11 :36:35
11 :36:35
11 :36:35

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

S-10 TOT
S-10TOT
S-10 TOT
S-10 TOT
S-10 TOT
S-10TOT
S-10 TOT
S-10 TOT

13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

14:39:30
09:09:03
13:50:09
13:50:09
13:50:09
11 :36:36
11 :36:36
11 :36:36

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

S-10
S-10
S-10
S-10
S-10
S-10
S-10
S-10

13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

15:00:27
09:09:03
13:50:10
13:50:10
13:50:10
11 :57:43
11 :57:43
11 :57:43

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08

04/19/2013 15:00:29
04/29/2013 09:09:03
04/20/2013 13:50:11
04/20/201313:50:11
04/20/2013 13:50:11
04/19/2013 11 :57:45
04/19/2013 11 :57:45
04/19/2013 11 :57:45

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT

EBERLINE'
SERVICES

Result

Error

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

1.22
1.03
0.01
0.24
0.03
2.58
0.08
1.42

0.33
0.42
0.05
0.12
0.05
0.44
0.07
0.30

0.17
0.77
0.12
0.08
0.08
0.07
0.09
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.03
0.06
0.03
0.26
0.12
0.23
0.03
0.24

0.05
0.51
0.09
0.15
0.10
0.11
0.05
0.12

0.10
1.09
0.18
0.11
0.10
0.08
0.08
0.08

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.01
0.37
0.05
0.10
0.01
0.13
0.02
0.09

0.04
0.36
0.11
0.12
0.05
0.10
0.04
0.09

0.09
0.73
0.21
0.16
0.12
0.11
0.09
0.11

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.63
1.58
0.08
0.16
0.05
2.60
0.16
2.11

0.25
0.46
0.08
0.10
0.06
0.44
0.10
0.38

0.12
0.80
0.09
0.08
0.07
0.05
0.09
0.06

Method

13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05

LR-104
LR-104
LR-104
LR-104
LR-104
LR-104
LR-104
LR-104

G'll

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

Final Report of Analysis


Date: 5/7/2013
Page 2 of 5

Project: West Lake OU-1


SDG: 1304051
Received: 04/09/2013
Matrix: Water

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

865/481-0683

FAX 865/483-4621

Qualifier

u
u
J

u
u
u
J

u
u
J

u
u
u
J

u
u
u
J

u
J

Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------,

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

~,

lil,
W<,)

,.,,,

Lab Sample ID

Final Report of Analysis


Date: 5/7/2013
Page 3 of 5

Project: West Lake OU-1


SDG: 1304051
Received: 04/09/2013
Matrix: Water

Analysis Date/Time

Analyte

LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS

13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

15:00:31
09:09:07
13:50:12
13:50:12
13:50:12
11 :57:40
11 :57:40
11 :57:40

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DUP01TOT
DUP01TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP01 TOT

13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

15:00:32
09:09:07
13:50:13
13:50:13
13:50:13
11 :57:41
11 :57:41
11 :57:41

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP

01
01
01
01
01
01
01
01

13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11

04/19/2013 15:00:35
04/29/2013 09:09:07
04/20/201314:11:33
04/20/201314:11:33
04/20/2013 14:11:33
04/19/2013 11 :57:49
04/19/2013 11 :57:49
04/19/2013 11 :57:49

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP

02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02TOT

13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12

04/19/2013 15:00:37
04/29/2013 09:09:08
04/20/2013 14:11 :34
04/20/201314:11:34
04/20/2013 14:11:34
04/19/2013 11 :57:46
04/19/2013 11 :57:46
04/19/2013 11 :57:46

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

r2J

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

~EBER!,-I ...... E

Result

Error

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.39
1.00
0.03
0.06
-0.01
2.72
0.16
1.94

0.18
0.47
0.07
0.07
0.03
0.45
0.10
0.36

0.10
0.88
0.12
0.10
0.11
0.06
0.09
0.05

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.32
0.89
0.08
0.19
0.05
0.26
0.01
0.12

0.17
0.43
0.09
0.12
0.06
0.11
0.03
0.07

0.12
0.81
0.13
0.10
0.10
0.05
0.06
0.05

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.19
0.65
0.01
0.10
-0.04
0.20
0.03
0.14

0.13
0.45
0.03
0.08
0.03
0.11
0.06
0.09

0.11
0.89
0.07
0.09
0.12
0.07
0.10
0.08

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.45
1.61
0.10
0.17
0.07
0.16
0.01
0.10

0.21
0.48
0.12
0.14
0.09
0.10
0.04
0.09

0.17
0.85
0.16
0.11
0.12
0.08
0.10
0.12

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

FAX

865/483-4621

Qualifier

Units

~~
~~
~~

u
u
u

pC~
pC~

~~

~~
~~
~~
~~

~~
~~

pC~

~~
~~

J
J

~~

pC~

~~
~~

pC~

~~
~~

pC~

pC~

u
u

~~
~~
~~
~~
~~

pC~

~~
~~

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

Lab Sample ID

Analvsis Date/Time

Analvte

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13

04/19/2013 15:00:40
04/29/2013 10:21:09
04/20/2013 14:11 :30
04/20/201314:11:30
04/20/201314:11:30
04/19/2013 11:57:47
04/19/2013 11 :57:4 7
04/19/2013 11:57:47

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-11 0-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT

13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14

04/19/2013 15:00:42
04/29/201310:21:09
04/20/2013 14:11:31
04/20/201314:11:31
04/20/201314:11:31
04/19/2013 14:33:37
04/19/2013 14:33:37
04/19/2013 14:33:37

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

FB
FB
FB
FB
FB
FB
FB
FB

13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15

04/19/2013 15:00:44
04/29/2013 10:21:09
04/20/2013 14:11 :27
04/20/201314:11:27
04/20/2013 14:11:27
04/19/2013 14:33:38
04/19/2013 14:33:38
04/19/2013 14:33:38

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16

04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02

at
at
at
at
at
at
at
at

PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-11 0-SS
PZ-11 0-SS
PZ-110-SS
PZ-110-SS

MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103TOT
MW-103TOT
MW-103 TOT

t:U
Q)
~"\.)
(,.~

Final Report of Analysis


Date: 5/7/2013
Page 4 of 5

Project: West Lake OU-1


SDG: 1304051
Received: 04/09/2013
Matrix: Water

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

EBERLINE
SERVICES

15:00:47
10:21:09
14:11:28
14:11 :28
14:11 :28
14:33:33
14:33:33
14:33:33

Result

Error

MDA

Qualifier

Units

0.11
0.50
0.03
0.10
0.04
0.10
0.09
0.09

0.13
0.97
0.06
0.09
0.09
0.07
0.07
0.07

J
J

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.12
0.85
0.01
0.15
0.00
0.18
0.12
0.13

pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.12
1.16
0.15
0.15
0.04
0.02
0.03
-0.01

0.09
0.57
0.13
0.13
0.07
0.03
0.04
0.02

0.06
1.08
0.11
0.11
0.13
0.06
0.06
0.06

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.03
0.45
0.02
0.25
-0.01
0.04
0.00
-0.01

0.05
0.59
0.04
0.14
0.04
0.07
0.04
0.03

0.07
1.22
0.08
0.09
0.09
0.12
0.12
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.78
0.88
1.38
1.22
1.19
4.07
0.37
3.72

0.25
0.49
0.36
0.32
0.32
0.67
0.17
0.63

0.12
0.96
0.09
0.06
0.06
0.12
0.10
0.09

865/481-0683

FAX 865/483-4621

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

u
J

u
J
J
J
J
J
J

u
u
u
u
u
u
u
u
u
u
u
J

pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

tn

ili'J!)
W\)
.11:::::

Final Report of Analysis


Date: 5/7/2013
Page 5 of 5

Project: West Lake OU-1


SDG: 1304051
Received: 04/09/2013
Matrix: Water

Lab Sample ID

Analvsis Date/Time

Analvte

MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS

13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17

04/19/2013 15:00:50
04/29/2013 13:17:02
04/21/201314:27:41
04/21/201314:27:41
04/21/2013 14:27:41
04/19/2013 14:33:34
04/19/2013 14:33:34
04/19/2013 14:33:34

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT

13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18

04/20/2013
04/29/2013
04/21/2013
04/21/2013
04/21/2013
04/19/2013
04/19/2013
04/19/2013

13:48:54
13:17:02
14:27:42
14:27:42
14:27:42
14:33:35
14:33:35
14:33:35

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS

13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19

04/20/2013 13:48:55
04/29/201313:17:02
04/21/2013 14:27:40
04/21/2013 14:27:40
04/21/2013 14:27:40
04/19/2013 14:33:36
04/19/2013 14:33:36
04/19/2013 14:33:36

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS

EBERLINE
SERVICES

Result

Error

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.24
1.08
-0.02
0.12
0.07
3.17
0.27
3.00

0.15
0.57
0.06
0.10
0.08
0.55
0.14
0.53

0.09
1.09
0.18
0.12
0.09
0.06
0.11
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

2.44
1.38
0.00
0.14
0.01
0.54
0.06
0.52

0.58
0.88
0.06
0.10
0.04
0.18
0.07
0.17

0.25
1.73
0.15
0.11
0.10
0.08
0.07
0.06

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

1.84
1.37
0.03
0.10
-0.01
0.53
0.04
0.58

0.45
0.60
0.07
0.08
0.03
0.18
0.06
0.18

0.22
1.12
0.13
0.07
0.08
0.09
0.09
0.06

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

fAX

865/483-4621

Qualifier

u
J

u
J

u
u
J

u
J

u
u

Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

SECTIONV
ANALYTICAL STANDARDS

LL-8

QA/OG REVIEWED CERTIFICATE OF CALffiRATION


t,q(lnitialsA ALPHA STANDARD SOLUTION
Date
Radionuclide:
(4.468
Half Life:
Catalog No.:
Source No.:

7338
479-50

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:

TMAEBERLINE
Customer:
OR2778
P.O.No.:
12:00 PST.
Reference Date:
January 11995
Contained Radioactivity: (Total U) 8.016 p,Ci
Contained Radioactivity: (Total U) 297 k:Bq

U-238NAT
0.005) x IOA9 years

..

,.

:~:

65.2896 g in a SO ml flame sealed ampoule

'

Uranyl Nitrate in H20


None
Approximately 1.3202

d. Density:

,....~. .

Refer to attached technical data sheet

Radioimpurities
Radioactive Daughters

Refer to attached technical data sheet


~

..

Radionuclide Concentration

':

(fotal U) 0.1228

pCi/g.

Method of Calibration

.........

.'-;

.:,

..... -

-Activity calculations are based upon known specific activity and mass .

..... .,
.:

.,.

.-.:;

-:

::>:. .... ;

:-.!
. .. . ' .

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibrntion:
b. Random uncertainty in assay:

3.0%
0.0%
2.0%
3.6%

c. Random uncertainty in weighing(s):


d. Total uncertainty at the 99% confidence level:

.: ...

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.

Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
\~

. .

. :.;.::.

1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986 .
2. IPL participates in an NIST measurement assurance program to et.tablish and maintain implicit traceability for a number of nuclides,
based on the blind aSBlly (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

EEftlvAuA7
YCONTROL
-p;/

...,,_.
,:'

7eter.1h:% t??'fDate Signed


:;

ISOTOPE PRODUCTS LABORATORIES

<

3017 N. SAN FERNANDO BLVD.


BURBANK, CALIFORNIA

91504

8188437000

8188436168

FAX

,.. . '

:-!

........

, .. ..
.:.:

,,

. .

;: .. i
-~

... -

<:.;

..

:"'!.

;;.'

._.:<::""::::-;'!"

. '""

.'

~.

-v

..

QUALITY CONTROL PROGRAM


MP-009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES- OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION


MP009

Half Life, Years

I~

\ :4.466e.+osl

Ampoule /Solution Gross


97.6400 Weight, Grams
Empty Ampoule <'32:5020 Weight, Grams
Solution Net
65.1380 Weight, Grams
Total Activity in Ampoule
8.0160 JA.CI
Chemical Com osition of Standard Solution

. . , .....

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofl . .. 1000:00.

Certified Total Activity ofl

j1MHNO
. ....... 3 ...:

. ..

...........

Imilliliters

Which Eauals

1.780E+07ldpm at the date listed above


This activity concentration is based on the original

And after dilution the activity of this solution is 1.77955E+04ldpm/ml-eterence date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date: September 6, 2913

o:....o....o

Date: _ _9.;;.;./2;;.;6:.;.;/2;;;;.;0;..;.1-..2....

Date:

--'~/.;;;..u.~/-t~--

~EBEF;L~~~fi I QUALITY CONTROL PROGRAM


MP.009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solution$ & Records

EBERLINE SERVICES- OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference # IPL479-;50 .
Principal Radionuclide
Half Llfe1 Years
:.

:~;2~.2381J

9/6/2012 0:001
Date I
u~aa
1
Solution#!
Half Life1 Dals
. .. 1.632E+12I
0

. .

,..... . I

I< '4;4sae+osl

Radionuclide of Interest:~~ za&~2iJ :1


Parent Solution Cone. .1 >TZ96E+04 dpm/ml

Reference Date

Chemical Compasition of Standard Solution


1Uranty.Nitratelr1~

HN03

. . ...

I'

..., ...

'-11111995 o:oo I

. I

<\

Dilution Instructions:

.. ..

j1MHNOd

Dilution Solvent Used

0
0

'

>I

> ..

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: 21,tOOOO ml
Total Activity: 7.1182E+04 dpm
Final Volume:
1000.00 ml

Final Activity Concentration:!

7.1182E+01Jdpmlml

This activity concentration is based on the original


referem:e date listed above. All activities are
corrected to the date and time of analysis by the
Jabon tory data processing software.

NOTES:
Isotopic Distribution as:
U-238 Atom % 48.239
U-235 Atom % "' 2.25
U-234 Atom o/o = 49.501
All values +/- 3.6%

U-238 = 71.182 dpmlml X 0.48249 34.345 dpmlml


U-235 = 71.182 dpmlmiX 0.0225"' 1.602 dpmlml
U-238 71.182 dpm/ml X 0.49501 = 35.236 dpm/ml

Expiration Date: September 6, 2013


Isotopic ratios from manufacturer's data sheet

f\.

~~.

Verified & Approved

QCApproval

_::5tlfk.tAl L(~ 1\I

Date:

9/26/2012 0:00

Date:

r4ZbJrz. .

RECORD COPY
Tracer Solution for Environmental Analysis & Disequililirium Studies
Product Description & Measurement Certificate
Description

Principal radionuclide:
Daughter Nuclide:

uranium 232 (U-232)


Th-228

Measurement

Reference date:
Radioactive concentration U-232
which is equivalent to
Volume of solution
Total activity ofU-232
which is equivalent to

Accuracy

Radionuclidic
Purity

Product code: UDPl 0050


Batch Number: 921232/67
01 March 2000
6.739E+03 becquerels per gram of solution
1.821E-Ol nrlcrocwies per gram of solution
! .35" gr--~15
5.035 millilitres
3.61E+04 becquerels
9.76E-Ol microcuries

Method ofmeasurement (see reverse of this certificate)


Random uncertainty is: 0.7%
Systematic uncertainty: 0.5%
Overall uncertainty in the radioactive concentration quoted above: :I: 1.7%
Overall uncertainty is defmed on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
of the activity of the principle radionuclide at the reference date.
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00

Isotopic
Purity

...,....ne isotopic composition, exprP.ssed as atom per cent at the reference date .
!~Ot measured

Chemical
Composition

Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.

Physical
Data

Recommended halflif~;: of uranium 232: 6.980E+Ol ye!U's


Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.00/o
Branching ratio for alpha emission: 100%
Calculated specific activity ofuraniwn 232: 8.167E+05 Bq per microgram U-232.

Remarks

For safety information and notes to ensure correct usage by all persons handling this radioqctive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 9001.

Approved
Signatory

Project Ref. AE231S

Roger Wiltshire
Prepared and characterised in the UK, for world wide distribution by lsotrak, AEA Technology, QSA.

Trkcert.wps 10/03/00

AEA Techn'>logy is the trllding name of AEA Technology !lLc

~623

QUALITY CONTROL PROGRAM


MP.009

Rev.8; 11/01/03
1itle: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION


MP009

Half Life, Years


7.200E+011

Ce~lon,.:::,9.~E~11~CI
Certified Concentration . . . .. . . .. . . JJ.CI per gram

Reference Date! \ ... 3/1/200.0 O:Ool

>

Ampoule /Solution Gross~


:. . . Weight, Grams
Empty Ampoule . ... . ... Weight, Grams
Solution Net . . . .Weight, Grams
Total Activity in Ampoule
0.9760 JJ.CI
Chemical Composition of Standard Solution

Dilution Solvent Used

Dilution Instructions:
Dilute to a volume ofl'

Certified Total Activity of

1000.00

I ... 0.9760IJ1CI

Imilliliters

Which Eauals

I .. 2.167E+06jdpm at the date listed above


This activity concentration is based on the original

And after dilution the activity of this solution Is j 2.167E+03Idpmfml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data

processing software.

Expiration Date: December 7, 2013

Date:
Date:

12113/2012 0:00

1~

~E ...

EF<LINE

--~ ---seftv~

I QUALITY CONTROL PROGRAM


MP-tl09

Rev.6; 11/01103
Title: Radioactive Reference Standanls Solutions & Records

EBERLINE SERVICES- OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP009
Solution Reference # AENAmersham 92/232167
Principal Radionucllde
Half Life, Years
.m.u.. . I
1.. 1.2ooE.+01I

1217/2012 0:001
U~10a
< I
Half Life, Dal!
2.630E+04I

I .. . . .

R~~~nn~c~i:~:~!~n~=1.~~.1=~~~' ldpm/ml

Reference Datel ' ... ... . 3J112ooo

Chemical Com~sitlon of Standard Solution


.. U(N~)6 m 2M HN03 .

lm . .. . . . .

Dilution Instructions:

DateI
Solution #I

:o:oo I

I
I2MHN03

Dilution Solvent Used

:: ... ...

.'.

.. ;._.'

:,

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution:
Total Activity:
Final Volume: I

. 10.0000 ml
2.1670E+04 dpm
. 1000~00 ml

Final Activity Concentration:!

2.1e70E+01Idprnlml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:l December 7. 2013

c~
l\
~~

Verified & Approved By

ac Approval6~a
~

.kJJJ j( ~\

Date:
Date:

12/13/2012 0:00

t~lta:
I

RTIFICATE OF CALffiRATI~t~
q\
PHA STANDARD SOLUTION" oe' ft_~~t\\\\\\
TMA EBmull\t.V.\\\~\\ \.'0
Th-230
Customer:
(7 .54 0.03) x 10"4 years
P.O.No.:
TT4944
\\\\l
Catalog No.:

7230

Reference Date:
November 1 1991
Contained Radioactivity:
1.036

Source No.:
Desaiption of Solution
a.
b.
c.
d.

Mass of solution:
Chemical form:
Carrier content:
Density:

5.0042
Th(N03)4 in O.lN HN03
None added
1.0016

12:00 PST.

grams.

Radioimpurities
See attached technical data sheet

Radioactive Daughters

See attached technical data sheet


Radionuclide Concentration
0.207

I'Cilgnun.

Method of Calibration

Weighed aliquots of the solution were assayed using a liquid scintillation counter.

Uncertainty of Measurement
a. Systematic uncertainty in iustruinent calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:

2.0%
0.5%
0.2%
2.7%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes
1. Nuclear data were taken from Table of Isotopes", Seventh Edition, edited by Vi.Iginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintaiu implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatoty Guide 4.15)

ISOTOPE PRODUCTS LABORATORIES


1800 No. Keystone Street.,
Burbank, California 91504
818 843 - 7000

$&32

~
E EJ E RLI hll;; I QUALITY CONTROL PROGRAM
~
MP-009

SERVICI!$

Rev.8; 11101(03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES -OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION

MP-009
Solution Reference# IPL ~.116 ;: .
Half Life, Years

I 7054oE+b41

Reference DateV

/11/111~1J>:ool

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used


SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: .. );.\10;0000 ml


Total Activity: 2,2999E+04 dpm
Final Volume: :1000'00 ml

Final Activity Concentratlon:l

2.2999E+01Jdpmlml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:

Recertified

Date:

Verified & Approved By

Date:

QCApproval

Date:

March 4, 2014

312112013 0:00

j~l'~
~r~

..\ {"

QUALITY CONTROL PROGRAM


MP-009
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES -OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIF/CA T/ON
MP009
3/4/2013 O:OOI
CURRENT DATEL
SOLUTION REFERENCE #lr:':IP"""t~::3=a'=="'&~l1~.6,_
. ,.,....
.......,..,.,....
.. ,:.,../-.~,....<. . . .,.....:=
SOLUTION #I:. ~/ Jh~1>:_. .1
Principal Radionuclide
2

> ~h

Half Life, Years

Half Life, Days


2.754E+07l

:7:540E~..041

Radionuclide ~;,P:rhe>riurn;
Certified Activity 'J:.036E+()O ~-tCI
Certified Concentration I_ / . > ; :. <: \' ~-tCi per gram

Reference Datel

: ':''11I1/199l:o:bol

<. 9.266.0 Weight, Grams


Ampoule /Solution Gross
Empty Ampoule 1 <: t6218 Weight, Grams
Solution Net . 4:6442 Weight, Grams
Total Activity in Ampoule .. . 1~0360 ~-tCi
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume of

Certified Total Activity ofl

I 10oo;oo:

>1.0360lllCI

>!milliliters

Which Eauals

2~3QOE+06ldpm at the date listed above


This activity concentration Is based on the original

And after dilution the activity of this solution Is I 2.300E+03ldpm/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:

'March 4, 2014 .

3/21/2013 0:00
----'-----

Date: ___.,.,.../:u
.....,..,f.....
r 3...___ _

1h-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Half Life:
Catalog No.:
Source No.:

TMAEBERLINE
Customer:
VH1632
P.O.No.:
Reference Date:
November 11993
12:00 PST.
Contained Radioactivity:
(Th-232) 0.0933
~i.
Contained Radioactivity:
(Th-232) 3.45
kBq.

Th-232
(1.~5 0.006) x 10" 10 years
7232
435-104-2

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:

11.9712 g (in a 10 ml flame sealed ampoule)


Th(N03)4 in water
None added
Approx. 1.21

Radioimpurities

g/ml @ZOc.

None detected (other than daughters).

Radioactive Daughters
.
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Po-212, TI-208
Radionuclide Concentration
(Th-232) 0.00779

p.Ci/g.

Method of Calibration
Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:

3.0%
0.0%
2.0%
3.6%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data '\Yete .lakCn from "'!:able of Radioactive Isotopes", edited by Virginia S. Shirley,.l986.
2. IPL participines ill an NIST mc-ment assurance program 1o establish and maintain implicit traceability for a number of nucJi~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (Aa in NRC Regulatory Guide 4.15).

QUALITY CONI'ROL

Al,zv.

<6' I

I 1 9>

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

fiUi35

~EBERLINE I
~

QUALITY CONTROL PROGRAM


MP~09

SEAVIC:I!:S

Rev.B; 1/10/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES -OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009

Half Life, Years

I'H'/~:tjS4o5gt:1'ol

AmpOule /Solution Gross ;;>'D>\t8ia4t5


Empty Ampoule 2ii~:i~6i;92a6
Solution Net . . 1t9l19
Total Activity in Ampoule <; o.:09$3

Weight, Grams
Weight, Grams
Weight, Grams
J.LCI

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofi\\Y''t()()O;"OO//}lmllllllters

Certified Total Activity

otl .. ._. . <0"0933lJJ.Ci

Which Eauals

1. ' :: :2;071E+o5ldpm at the date listed above

And after dilution the ar;tivity of thi$ $Oiution isi2;071E+02Idpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date :I OCtober 9,:2013

Date: _ _10/9/2012
0:00
.:.:::.:::..=.;::..:.=...::.:.;;..;;..

~EBEBLU>LE I QUALITY CONTROL PROGRAM


MP-009

SttRVICE$

Rev.8; 1/10103
Title: Radioactive Reference Standards Solutions & RecordS

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION

DataL

MP-Q09
Solution Reference #IIPL 435~1 ~2
Principal Radionuclide
Half Llfe1 Years

.228&232Th l

Solution#!

Th;.;sb . I

Half Life1 Dals

I 1.4o5E.1o!

Reference Date j

228 "'~Th
2;07E+02 dpm/ml

Radionucllde of lnteresd
Parent Solution Cone. I

11/9/2012 O:OOj

<

5.132E12I

. 111111ses:o:oo 1

Chemical Come2sltion of Standard Solution

1Th(N03}4 in1%HN03 ...> . . .. . . : . ..

Dilution Instructions:

I
11% NitrieAeid

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: .. . . soo;oooo ml
Total Activity: 1. 0365E.+06 dpm
. 1000.00' ml
Final Volume:

This activity concentration Is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:

Verifted &

1.0366E.+02Idpm/ml

Final Activity Concentration:!

Approved~ ~
QCAppraval

~~AI'v (\\J"ll J t[J"'


-

"9

~v

Date:
Date:

I . October 9, 2013 I

1119/2012 0:00

1\

,..,_I 1'1..
I

f!Hi

1 f Isotope Products

lh-18

24937 Avenue Tibbitts


Valencia, California 91355

Laboratories
An Eckert &Ziegler Company

Tel 6613091010
Fax 6612578303

CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radio nuclide:
Half-life:
Catalog No.:
Source No.:

Th-229
7340 160 years

Customer:
P.O. No.:
Reference Date:
Contained Radioactivity:
(Th-229 only}

7229
867-54

Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. Density:

EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
~-tCi
37.48

kBq

5.0147 g in 5 ml flame-sealed ampoule


Th(N03)4 in 0.1 M HN0 3
10J.Jg Th/mL
1.0016 g/mL@ 20C.

Radioimpurities:
None detected (daughters in equilibrium)

Radionuclide Concentration:

0.2020

lJCi/g,

kBqfg

7.474

Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in !JCifg was determined

using gamma ray spectrometry.


Peak energy used for integration:
193.5 keV
Branching ratio used:
0.0441 gammas per decay

Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type 8 (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence revel:

0.7%
3.0%
0.0%
3.1%

Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.

Quality 'Control

Date Signed

IPL Ref. No.:

867-54

- - - - - - - - - - - - - - - - - - 1509001 CERTIFIED - - - - - - - - - - - - - - - - - -

Medical Imaging Laboratory


24937 Avenue Tibbitts

Valencia, California 91355

Industrial Gauging Laboratory


1800 North Keystone Street

Burbank, California 91504

QUALITY CONTROL PROGRAM


MP..009

Rev.8; 1/10/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATEI .
11/9/2012 0:001
SOLUTION REFERENCE #r.:IIP::-:-L-=-86~7~~5:-:-4~
... -.. -.. .,....-.,....,..._..
SOLUTION #~I.,..,.,....;-:;T~h-~18;:-,;:..;;,:>.,;....;..;..,. ~~
Principal Radionuclide

Half Life, Years


7.34oi=+o3l

Radlonuclidol '

Half Life, Days


2.681 E+o6l

Z;Z8:"Ch 1

1!'ili:, ,

Reference Datel :

1/15/2002 o:ooj

Certified Activity . , f.013E+oo J.t.CI


Certified Concentration :' > - ' J.t.Ci per gram
Ampoule /Solution Gross
Empty Ampoule
Solution Net
Total Activity In Ampoule

Dilution Instructions:

. 8.7752 Weight, Grams


. 3. 7591 Weight, Grams
5.0161 Weight, Grams
1.0130 J.t.CI

Dilution Solvent Used

Dilute to a volume of I , 1000.00 <.I milliliters

Certified Total Activity ofl -: 1.0130lJ.lCi

Which Eauals

2~249E+06Idpm at the date listed above


This activity concentration is based on the original
All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

And after dilution the activity of this solution is 1 2.249E+03ldpmlml reference date listed above.

Expiration Date:

October 9, 2013 ]

Date: _ _1.;...1~/9~/2;;.;0...;.12--..0:...;.o_o
Date:

--:.14-,,J,z/tz_
__,,..o.;;..,_ __

~~E"'~~~ QUALITY CONTROL PROGRAM


MP.009

Rev.7; 9129199

Title: Radioactive Reference Standards Solutions & RecordS

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
Date I
Solution #I

MP~09

Solution Reference #IIPL867~54


Principal Radionucllde
Half Life, Years
~9Th

Radionucllde of lnteresj . ~
Parent Solution Cone. 2.25E+03 ldpmiml

Reference Date

Chemical Come2sition of Standard Solution


'. . ..... .. >> .. . . ... ..
jTH(N03)4 in0.1MHNOs

Dilution Instructions:

Th~tsa

Halt Life, oar

I . 7.34oe+o31

11/9/2012 O:OOJ

. . .

. 2.~81E+06l

l .111si2oo2 o:oo I

I
j0.1MHNO.
. . . . . . 3.

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution:
Total Activity:
Final Volume:

10.0000 ml
2.2490E+04 dpm
1000.00 ml

Final Activity Concentration:!

2.2490E+01ldpmlml

This activity concentration Is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:l October 9, 2013

Verified & Approved By

~~

'
QC Approval~)'~') ~L.
,,.

~~
'-.,...!_

Date:

11/9/2012 0:00

Date:

llt~f~-z_
i r

J}ational 3Jn(titute of j,tanbatb( & m;ecbnologp

-,1).
'.

'l.-
.
i
\.

~ ~ ~,/

; ..

.4

/
-~

.F

.,,_

.1'

.;

C!tertificate
.

..

.:

. .j_ ~ ~-,,

Standard Reference Material 4251C


Barium-133 Radioactivity .Standard

This Standard Reference M,ate.rial(SRM) consists of radioactive barium-133. c~loride,_ non~~adioactive barium
chloride, and hydrochloric acid diSsolved in 5 mL of distilled water. The solution is contain in a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization thambers and
solid-state
gamma-ray,,spectrometry
.systems.
.
... .
.
.
Radiological Hazard

SRM

'a

The
ampoule contains bariuni-133 with total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during tl:te decay process X-rays and gaiilllla;rays with energies from 4. tp 400 keV are
emitted. Most of these photons escape from the SRM ampoule and can represent a radl.atipn hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be 11$ed to minimize. ~rsonnel exposure... The. ,SRM $hould be
}~Sed only by persons qUalified to' han~e radioactiv~ materiaL
'
.
Chemical Hazard

The SRM ampoule.c~ntain~.hydr~hloric acid (HCl) with a concentration qf 1 mole per Iite:r;.o(.water. 'Jhe
solution is corrosive and represents a health hazard if it comes in contact with, eyes or skin~ -If. the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened. only by persons qualified to handle, both radioactive material and strong a,cid solution.

Storage and Handling


The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.

Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.

The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standarc! Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994

SR1144251C, ~ge l.of 6.

Thomas E. Gills, Chief


Standard Reference Materials Program

*Notes and references are. on pages.~ and 6.

8641

QUALITY CONTROL PROGRAM


QCP-G09
Rev.a; 11/10103
TIUe: Radioactive Reference standards Solutions & Records

EBERLINE SERVICES -OAK RIDGE LABORATORY


RADI()ACTIVE REFERENCE SOLUTIONS
PmMARYD~UTIONRECERTIRCATION

QCP009-1

CURRENT DATE!'
'9/2012012 0:001
SOLUTION REFERENCE #r."N:o:-:.ls=:r="':;s="=R::"M~4~25~1~C~'_,
:".
~-:~:>...,.i~l SOLUTION #l';'~'/.0>.;:r;::sa':;Q.:t<>i:~;\':::r1
Principal Radlonuclide
Half Life, Years
Half Life, Days

:J~a~ri'(Jm'?l

j:;:,1:04e~ro11

:;3.s2ee+o:;3l

1.,,.:. .... .

Radionuclide .yJ~aariUro.i;:
Certified Activity ji:C::;t;F;~ J.LCI
Certified Concentration \'41';3teE.01; J.LCi per gram
Ampoule /Solution Gross }':?,'.;g;.3Q8.t Weight, Grams
Empty Ampoule ;;;.t';i'4i:2$32 Weight, Grams
Solution Net . $0499 Weight, Grams
Total Activity in Ampoule 66~5577 J.LCi
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofh:.:.::.tOOO:OO . :<!milliliters


Certified Total Activity otl:

66.5577IJ.LCi

Which Eauals

l 1A78E+08)dpm at the date listed above

And after dilution the activity of this solution is I 1o478E+05 Idpm/ml

This activity concentration is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date: S#taniber 20; 20131

,..
Verified & Approved By
QC Approval

~
.~JAW\UI
\

___. ---.l

\\
._.,

Date:

9127/12

Date:

I-z.rtft 'Z.

Rev.8; 11/10/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
QCP.0091-A
Solution Reference# NISTSRM4251 C
Half Life, Years
1.048E+01l

Reference Date

I ... 9/1/1993 0:00 I

Chemical Composition of Standard Solution

Dilution Instructions:

. . I

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: . .. ~25:0000 ml
Total Activity:
3.6950E+06. dpm
Final Volume: 1000;00 ml

NOTES:

Final Activity Concentration:!

3.6950E+03Idprnlml

This activity concentration Is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Oate:l September 20, 2013

Date: ___9;.;./;;;.;27~/1.2..____
Date: _ _'t_.{_t'7-t/-"tZ......___

Radionuclide:
Half Life:
Catalog No.:

1600

Source No.:

7 years

P~O.No.:

Reference Date:.
February 1 1994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 J.'Ci.
Contained Radioactivity: (Ra-226)
37.0 kBq.

7'126

453-26

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:

d. Density:

TMAEBERUNE
VH1888

Customer.

Ra-226

5.1864 g (in a 5 ml Flame Sealed Ampoule)


Ra(N03)2 in 1 N HN03
None added
1.0318

g/ml @20C.

None detected(other tha:il daughters)

Radioimpurities

Radioactive Daughters
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuelide Concentration
(Ra-226) . 0.1929

, . p.Cilg.

Method of Calibration
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Brancbitlg ratio(s) used:
0.0351
gamma rays per decay.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:

3.4%
3.1%
0.2%
4.6%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.

Leak Test(s)
See reverse side for Leak Test(s) applied to this source.

Notes
1. Nuclear data were taken ftom "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability fur a num~r of nuclides,
based oinne blincrassay(aiiillater NIST'certificationrorstaiidiiro ReferenoeMateriiils\Ai'in NRC'RegulitOryomdn:; 15): ---

QUALITY CONTROL

/iA,. ;

199 If

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

QUALITY CONTROL PROGRAM


MP009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
M

PRIMARY DILUTION RECERTIFICATION


MP009
CURRENT DATEI
SOLUTION REFERENCE #r:::IP::':'L~4:o::5'="3.:.':'26=-.......
. .......
:. .~
. -~.......,,
SOLUTION ~1_
Principal Radionuclide

Ra.:.5

'

Half Life, Days

Half Life, Years

. .
I
. Radium..

I . 1.600E+031

~26.

11/9/2012 O:OOJ
<

Radionucllde ~~Radium
Certified Activity .1;001E+OO J.(Ci
Certified Concentration 1... ... .. . . J.t.CI per gram

1/_19_94_._o_:o__,o)
Reference Date.._l_-'--2_1....

Ampoule /Solution GrosS~


. .... .. . We~ght, Grams
Empty Ampoule .. . : Wetght, Grams
Solution Net
.
Weight, Grams
Total Activity in Ampoule
1.0010 J.I.CI
Chemical Composition of Standard Solution

Dilution Instructions:

jtMHN03

Dilution Solvent Used

Dilute to a volume ofl . 1000.00

Certified Total Activity otl

1;0010IJ.1.CI

.. .

!milliliters

Which Eauals

. 2.222E+06ldpm at the date listed above

And after dilution the activity of this solution isf 2.222E+03ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:! November 9, 2013

~-~----t-...,.....,.~-~-~-

Verified &Approved By __
QC

Approval_~~;::::::::;.o.aA~w.
.;lo~~l..;::.;...J....--=--~\J..;;;,..___

Date:

------1119/2012

Date:---''~
f,t+-./ulf?....__
I ,

Rev.8; 11101103
TrUe: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES- OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP009
Solution Reference #IIPL~53+26i ,_,,c,.;)
PrinciPal Radionuclide
Half Life, Years

::.~RadiUrnn

DateL 1119/2012 O:OOJ


Solution #lC::~:;>/x9R~5b::"-i:: d

>il

j;::1:Ceoo6+o31

Radlonucllde of Interest !F~RadiunE/1


Parent Solution Cone. r:~:~2:~E:t03h/ldpm/ml

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solve.nt Used


SECONDARY VOLUMETRIC DILUTION

:2o:nooo

Vol. Parent Solution: /;<


ml
Total Activity: : '4i4440E+04 dpm
Final Volume: :::::<.<AOOO!OO. ml

NOTES:

Final Activity Concentration:! . . . 4.4440E+01Idpm/ml


This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date: November 9, 20131

Date:

Date:

,,

11/9/2012 0:00

ftz J,lr '

RA- \\
ANALYTICS

1380 Seaboard Industrial Blvd.


Atlanta, Georgia 30318 U.S.A.
Phone (404) 352-8677
Fax (404) 352-2837

CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:

Ra-228

ACTIVITY (dps) :

2.585 E3

HALF-LIFE:

5.75 years

CALIBRATION DATE:

November 7, 2001 12:00 EST

TOTAL UNCERTAINTY*:

4.0%

SYSTEMATIC:

3.0%

RANDOM:

1. 0%

*99% Confidence Level


Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.1M HCl solution with 50 ~g/g Ba carrier.
P 0 NUMBER

9508, Item 1 (Part #4339A)

SOURCE PREPARED BY:

Q A APPROVED:

M:i~mist

QUALITY CONTROL PROGRAM


MP-009

Rev.S; 1/10/03
Title:

Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
RECERTIFICATION
MP009

Half Life, Days

1.> :

::2:100Eo~l

Reference DateF1tiitW!.M:3;1?t7i2.1X{O!dbl

Ampoule /Solution Gross \t~::;~DKS~4aaz Weight, Grams


Empty Ampoule ;;';''?N~;i;~r4$~5. Weight, Grams
Solution Net Y ~ :5?.07 Weight, Grams
Total Activity in Ampoule
:<.OS0699 p.Ci
Chemical Com

sition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume otl;e{;;;tQQO;'O().i).:i:'lmllllllters

Certified Total Activity otl> . Oi0699IJJ.Ci

Which Eauals

I :.} :1:5StE+Qqfdpm at the date listed above

And after dilution the activity of this solution isi<J~55tE+02 Idprnlml

This activity concentration is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:l ;e.pril12;''20l3>

Date:

__

4116/12

__

....;;....;,...;.;...;.;;;,_

Date:------Date: ---44~}. ./W;z;;;.;/"""'


. . 1.-h-;:;;,.._

SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY

Eberline Services
Analysis Control Chart

Printed: 4/2212013 S:59 AM


Page 1 of 2

WO

Analysis

13-04051

UUISO

+---Run
I

Aliquot Units

Activity Units
-

Client Name

Engineering Management Support, Inc.

pCi

Laboratory Control Sample


Analyte

U-234

Normalized
Difference

0.4S

U-23S

0.12

LCS
Measured

csu
Measured

LCS
Expected

Uncert_
Expected

Known

Known
Error

~.33%

15.42%

100.95%

15.36%

Standard

csu

Result

Standard
ACT(dpm)

Standard
Error

Standard
Added (g)

U-Sa

3.52E+01

3.60E+OO

i 5.13E-01

U-Sa

3.44E+01

I 3.60E+OO

5.13E-01

10

I
100.00%

3.60%
--

100.00%

3.60%

S.15E+OO

2.93E-01

I 7.S5E+OO I 1.21E+OO
I

'

~------~--------j--------r
7.94E+OO

2.S6E-01

S.02E+OO

1.23E+OO

Matrix Spike
Analyte

Normalized
Difference

MSActual
%Rec

Expected
MSResult

Expected
MS Uncert

Actual
MSResult

Actual
MSCSU

Replicate Sample
Analyte

U-234
U-23S
U-235

Q,
Gil'
1;.,.11
It'~)

Version

Normalized
Difference

RPD

0.05

0.73

0.67
0.03

10.30
1.91

Original
Result

Original

csu

Replicate
Result

Replicate

2.62E+OO

4.92E-01

2.60E+OO

4.97E-01

csu

Sample
Result

Sample

I
I
I

Sample
Aliquot

csu

Standard
ID

Standard
Error%

Standard
ACT(dpm)

Standard
Added(g)

QCSummary

LCS Relative
Bias

LCS%R

0.96

OK

LCSND

OK

-+--:;

OK

3.52E-01

1.S2E+OO

3.S4E-01t--~~-1

S.73E-02

1.11 E-01

S.56E-02

MS%R

MSND

II
I

RepRPD

RepND

OK

OK
--

OK
OK

OK

OK

NA

OK

Printed: 4/22/2013 8:59AM


Page 2 of 2

Eberline Services
Analysis Control Chart

wo

Analysis

Run

13-04051

UUISO

-+---" Acti~nits

Client Name

Aliquot Units

Engineering Management Support, Inc.

pCi

Replicate Sample RPD

LCS% Recovery
130.00

40.00
120 00

35.00
110.00

30.00

100.00

25.00
20.00

90 00

15.00
80.00

10.00
70.00

+--------------------,---------------------,
U-234
U-238

Lower Error I
-

_Uf>er Error

77"31

81.99

115"34

119.91
100%
80
100

00~

80
100
-

-UCL

120

5.00

0.00 t--------,~':-c------,-----~=c-----,-------:-:-:

U-L:.:S4

-CL

0"80
0"66
0"73
35

"-

u-238
11.40
9.20
10.30
35

Normalized Difference
3"50 - , - - - - - - - - - - - - - - - - - - - - - 3.001

- - - -

- - - -

2"50+---2"00

-----"

1"50+---------------------------------1"00 + - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

;::,

llli!,
u~
!~-'

Version

No Matrix Spike

U-235
2"66
U6
1"91
35

Eberline Services
Analysis Control Chart

Printed: 4/22/2013 8:57 AM


Page 1 of 2

WO

Analysis

Run

Activity Units

13-04051

ThiSO

pCi

Client Name

-----~ig_tJ_~I_lj_nJ~-----------------

Engineering Management Support, Inc.

Laboratory Control Sample


Measured

LCS
Expected

Uncert.
Expected

Known

Known
Error

Result

csu

107.62%

18.25%

100.00%

3.60%

4.82E+OO

1.73E-01

5.19E+OO

9.46E-01

Th-8b

1.04E+02

3.60E+OO

1.03E-01

97.59%

19.82%

100.00%

2.70%

5.49E+OO

1.48E-01

5.36E+OO

1.06E+OO

Th-1b

i 2.35E+01

I 2.70E+OO

5.18E-01

I 108.41%

17.89%

100.00%

3.60%

4.82E+OO I 1.73E-01 I 5.22E+OO I 9.35E-01 I

Th-8b

11.04E+02

3.60E+OO

1.03E-01

TH-228

TH-230

TH-232

0.24
0.84

csu

LCS
Measured

Analyte

Standard
ACT(dpm)

Standard
10

Standard
Error

Standard
Added (g)

Matrix Spike
Normalized
Difference

Analyte

Sample
Result

Actual

MSCSU

Sample

Sample
Aliquot

csu

Replicate Sample
Analyte

Normalized
Difference

RPD

Standarc/
ID

Standard
ACT(dpm)

Standard
Error%

Standard
Added(g)

RepRPD

RepND

QCSummary

Original
Resun

Replicate
Result

Original

csu

Replicate

csu

LCS Relative

Bias

LCS%R

LCSND

OK

OK

NA

OK

OK

NA

OK

OK

NA

OK

MS%R

MSND

TH-228

1.53

584.85

4.21E-02

TH-230

0.95

52.45

TH-232

0.37

87.36

C&1

c;)

Ul

.... ~

Version

5.82E-02

-2.07E-02 ; 5.54E-02

7.81E-02

6.61E-02

1.34E-01

9.37E-02

0.98

5.61E-03

2.34E-02

1.43E-02

3.98E-02

1.08

1.08

I
I

OK
OK

I
I

Printed: 4/22/2013 8:57 AM


Page 2 of 2

Eberline Services
Analysis Control Chart
_____________ _!._n_<~!~~is

WO

ThiSO

13-04051

Run

Activity Units

pCi

Client Nam.e
00_ _ _ __

Aliquot Units

Engineering Management Support, Inc.

Replicate Sample RPD

LCS % Recovery
130.00

-------+---

40.00

UCL

120 00

35.00

110.00

30.00

25.00

100.00

20 00

90.00

15.00
80.00

- - - - - - - LCL
10.00

70.00

%R

-LCL
---Mean
-

-UCL

+--------------.-------------,-------------.
TH-232
TH-230
TH-228
85.77
7507
86.92
-----12947
129.90
120.11
107.62
97.59
108.41
80
80
80
100
100
100
120
120
120

5.00
0.00

+------=:c-=c::c:------,-----==-:-=::-----,--------c=-1::::::------,

Lower Error

!JEeer Error
RPD
-CL

TH-228
2131.74
-962.05
-:::~ :::
584.85

:35--

TH-<!;;u
72.24
32.65
: : ~:
52.45
35

Normalized Difference
No Matrix Spike

3.50 , - - - - - 3.00 1

U1
t ... ~

+---------------

2.00

+-------~

G!,
;i;f

2.50

Version

----------

IH-L;,jL

:~ ; :

Eberline Services
Analysis Control Chart

Printed: 4/22/2013 9:00AM


Page 1 of 2

wo

Analysis

Run

Activity Units

13-04051

Ra226

pCi

Aliquot Units

Client Name

Engineering Management Support, Inc.

Laboratory Control Sample


csu

Analyte

RA-226

Measured

Measured

102.89%

23.73%

LCS
Expected

100.00%

Uncert.
Expected

4.60%

Known

1.03E+01

I
I
I

Known
Error

Result

4.75E-01 ! 1.06E+01

Standard
10

csu

I
1

Standard
ACT(dpm)

Standard
Error

Standard
Added (g)

5.21E-01

2.52E+OO

Ra-5b

4.41E+01

4.60E+OO

Matrix Spike
Analyte

Normalized
Difference

MSActual
%Rec

Expected
MSResult

Expected
MS Uncert

Actual
MSResult

Actual
MSCSU

Sample
Result

Sample

csu

Replicate Sample
Analyte

RA-226

Q)

GJ:)
u~

.t::r.t

Version

2.88

Sample
Aliquot

Standard
ID

Standard
ACT(dpm)

Standard
Error%

Standard
Added(g)

RepRPD

RepND

INV

OK

QCSummary

RPD

Original
Result

Original

csu

Replicate
Result

Replicate

csu

LCS Relative
Bias

LCS%R

LCSND

305.90

1.21 E-01

8.98E-02

-2.54E-02

4.31E-02

1.03

OK

OK

MS%R

MSND

Printed: 4/22/2013 9:00AM


Page 2 of 2

Eberline Services
Analysis Control Chart

wo

Analysis

Run

Activity Units

13-04051

Ra226

pCi

__ _).____

Aliquot Units

Client Name

Engineering Management Support, Inc.

Replicate Sample RPD

LCS % Recovery
130.00

40.00
120.00

35.00
110.00
30.00

100.00

25.00
20.00

90.00

15.00
80 00

10.00

7o_oo

RA-226

=-._h_ower Error

74_55

102_89

Upper Error
%R
I

-::__::-_t,<::L_ ----1----

5.00

o_oo

a_o_

120

~----

---Mean

-UCL

Lower Error
Upper Error
RPD
-CL

RA-226
517_94
93_86
305_90
35
---

Normalized Difference
3_50~---------------------------------------------------------------

3.001

----

2_50 +---------------------------1
2_00 +--------------------------j
1_50 + - - - - - - - - - - - - - - - 1

1_00 +--------------------------1

o_5o + - - - - - - - - - - - - - - - - - - 1

Q;)

tn

U1
U1

Version

------

--

No Matrix Spike

Eberline Services
Analysis Control Chart

Printed: 4/30/2013 12:17 PM


Page 1 of 2

WO

Analysis

Run

Activity Units

13-04051

Ra228

pCi

---+--~Aliquot_ I.Jnits_ __

_ __,_ _ _ ___________________ _ Client Name


j

Engineering Management Support, Inc.

Laboratory Control Sample


Ana lyle

RA-228

Normalized
Difference

LCS

csu

LCS

Measured

Measured

Expected

Uncert.
Expected

0.53

107.19%

24.41%

100.00%

5.10%

Known

Known
Error

9.06E+OO I 4.62E-01

9.72E+OO

standard
ACT(dpm)

csu

Result

2.37E+OO

Ra-11

Sample
Aliquot

Standard
ID

3.91E+01

Standard
Error

5.10E+OO

Standard
Added(g)

5.15E-01

Matrix Spike
Analyte

Normalized
Difference

MSActual
%Rec

Expected
MSResult

Expected
MSUncert

Actual
MSResult

Actual
MSCSU

Sample
Result

Sample

csu

Replicate Sample
Analyle

RA-228

Gl!~

~'

Version

Standard
ACT(dpm)

Error%

Standard
Added(g)

RepRPD

RepND

NA

OK

Standard

QCSummary

Normalized
Difference

RPD

Original
Result

Original

csu

Replicate
Result

Replicate

csu

LCS Relative
Bias

LCS%R

LCSND

2.65

158.56

1.16E+OO

6.25E-01

1.34E-01

4.33E-01

1.07

OK

OK

MS%R

MSND

Eberline Services
Analysis Control Chart

Printed: 4/30/201312:17 PM
Page 2 of 2

wo

Analysis

13-04051

Ra228

. _R_LJn~~~-

Activity Units

Aliquot Units

--~-

Name
---- ------ Client
-----------------

Engineering Management Support, Inc.

pCi

Replicate Sample RPD

LCS % Recovery
130.00
40.00
120.00
35.00
110.00

30.00
100.00

25.00

20.00

90.00

15.00
80.00

10.00

7o.oo

RA228

Lower Error

77.68
136.70
107.19

Uooer Error

%R

5 DO

0.00

-LCL

---Mean
-

-UCL

Lower Error
Upper Error

RPD
CL

RA-228
223.29
93.83
158.56
35

Normalized Difference
No Matrix Spike

3.50 ,---------

3.00~----

2.50 + - - - - - - - - - - - - - - 1
2.00 i - - - - - - - - - - - - - - - 1
1.50

+--~-----~-----1

1.001----

~'!l'll

tll!:'

U1

.... ~

Version

-~---

SECTION VII
LABORATORY TECHNICIAN'S NOTES

ISOUNOTES

5553

Printed: 4/16/2013 8:36AM

Page 1 of 1

Oak Ridge Laboratory

}!;EBERI,..,.INE

SERVICES

Work Order Analysis Notes

Date

Dept

04/16/13 08:36

PREP

User
JBARNARD

lnternaiiNork Order

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

13-04051

Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

Printed: 4/18/2013 6:21PM

Page 1 of 1

~EBERI,...INE
~

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

Ii

Internal Work Order

Analysis Code
Run Number

13-04051
UUISO
1

Date

Dept

04/16/13 08:36

PREP

JBARNARD

ALIQUOT ED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

04/18/13 18:21

CHEM

JDEMELAS

Addedconcentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.

User

Notes

tiii61

Page 1 of 1

Printed: 4/19/2013 5:57AM

4:EB!O;R~\,~~

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridae, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Work Order Analysis Notes

lnte~nai\Nork Order I
Run Number

13-04051
1

Date

Dept

04/16/13 08:36

PREP

JBARNARD

ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

04/18/13 18:21

CHEM

JDEMELAS

Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 mi8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 10C
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred
to new, labeled C-Tubes with Dl H20. Set samples aside for later orecioitation and filtering.
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SEl
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.

User

I
3

04/19/13 05:57

CHEM

RMARTZ

Notes

Eberline Analytical
Oak Ridge Laboratory

Printed: 4/19/2013 5:59AM


Page 1 of 1
Internal Work Otder

SERVICES

Analysis Code

Run

UUISO

Reagents Used in an Analysis

Reagent
ID

13-04051

EE;JER.L....lNE

Reagent
Name

1
"

Reagent
concentration

Analyst
ID"

Date
Recor

013624P

Nitric Acid

Reagent Grade

JBARNARD

~/1 l=\l?n1 ~

013666P

Anion Exchange Resin

Reagent Grade

JDEMELAS

4/18/2013

8N-0.1M

JDEMELAS

4/18/2013

- 0.1M

JDEMELAS

~~.8/2013

JDEMELAS

4/18/2013

6.5N

JDEMELAS

4/18/2013

8N

JDEMELAS

4/18/2013
4/18/2013

0137725

- HF

0137785

- NH41

01357300

lyd

Acid

0137125

lyd

Acid

0137705

/('"rochloric Acid

---

013675P

Hydrochloric Acid

Reagent Grade

JDEMELAS

0132465

Carbon substrate

Solution

RMARTZ

14/19/2013

Ethyl Alcohol

Reagent Grade

RMARTZ

14/19/2013

D \111\DTZ

4/19/2013

~RTZ

4/19/2013

RTZ

4/19/2013

012809P
013221P

drofluoric Acid
1

0131915
f--------013434P

odymium Carrier
nous Chloride

Reagent Grade

1 mg/ml

Reagent Grade

~-----~--J~----------~-----1-------------- --!-------------+~------ -------f-~---------1----lr


~----~------+---~----------------------1-- ------- --------------~----1- ----------1- ------------~---- -1--------------~--+--~-

I.e_______--------~--------------------l---------------------ll------------l-----------~-----+-------+-----81
r--~ -----~1~--~-------------lL---------~--

--------f-------------~--~-~------l~---~----~-------+----------~-~1--~- - - - - - - - -+-------------+---~

'l

1 Q

J..LJ

- ------

/_

_'f(l""llrJ_

--------

~~~~-

~:(")

{_01.-

/-"JD Lj

___ 'iu

....... .(2 ...:/4ff.PttY-

-... l.fll f:Ja

L?_l?'.l "~AJ I)
___ 1 '1 ~-t.tQ&f~(.~-r:~
l ~~i ()~~A 4--~)

____ l(_IJttn

~1\.,h~~
Y\l~\(3 l~o\,1 O"\~ A(cil-1-l_
--- --~ ---.. .i1J9li1__ t:~Q~~~-1!-(f~~!~).
4 hi li"J
0~~{~ 4)
.. e.,'l 't4 ~
---------- ________ (((I

_/7 0 ~)l~t?J-")ti.f}

----------.. -----~f.il.

--- -)ec... .CAC... ..

_ ---------. __ flurta

{7~)

'&...ltHIU'II

__ I?Jot(<>JJ/1(.

o/1 to

rA'"-->
lA-L-~~c,.y\..:7 l.

0570

~-~k'-~\.

0531

v.,)e:)~

ll.-1--\

PtL
1\I'UV..IIL.._

t:;:;?--'/

s \.l

I'N.N:t>~ s~

t 9"2-Of
I~<....,

u.~'

Dr'--\'
0f)1"

v--;,

. 07oo

,A-/

'51>~~)

2. ~,. ~-=--

/1/l.?

[-

..

-~--

--------

----

iHi65

ISOTHNOTES

liii67

Printed: 4/16/2013 8:36AM

~
E;~~E3 E R
~

Page 1 of 1

Oak Ridge Laboratory

L,. .1 N

E::

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

#
1

Date

Dept

04/16/13 08:36

PREP

User

JBARNARD

Internal Work Order

Analysis Code
Run Number

13-04051
ThiSO
1

Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

6868

Printed: 4/18/2013 6:21 PM

Page 1 of 1

Oak Ridge Laboratory

j!JEBER,l,.,.IN.E

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

Date

Dept

04/16/13 08:36

PREP

04/18/13 18:21

-'--~~

CHEM

User

Internal Work Order

Analysis Code
Run Number

13-04051
ThiSO
1

Notes

JBARNARD

ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

JDEMELAS

AddedCon-centrated-HN03 to-sample beakers and heatedtodryness; Added 20 ml 8N HN03 to samples and


transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15m I. Set samples aside for later orecioitation and filterinq.

Printed: 4/19/2013 5:58AM

Page 1 of 1

~
E B E;:Rb-1.-.....~E;:
~

SERVICES

Work Order Analysis Notes

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridae. TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

13-04051

Analysis Code
Run Number

Date

Dept

04/16/13 08:36

PREP

JBARNARD

ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN

04/18/13 18:21

CHEM

JDEMELAS

04/19/13 05:58

CHEM

RMARTZ

Added concentrated HN03 to sample beakers and heated io dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15ml. Set samf:>les aside for later precipitation and filtering.
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.

User

Notes

Eberline Analytical
Oak Ridge Laboratory

Printed: 4/19/2013 5:59AM


Page 1 of 1
...

Internal Work Order

}!J E E;IE~LI_N E

13-04051
Analysis C:ode

SERVICES

Reagent
ID
I

013624P

I 013666P
013675P

ThiSO

Reagents Used in an Analysis


Reagent
Name

.Reagent
Concentration

Nitric Acid

Reagent Grade

Anion Exchange Resin

Reagent Grade

Hydrochloric Acid

Reagent Grade

Analyst [ Date
ID ..
Recorded

JBARNARD

4/16/2013

JDEMELA5

4/18/2013

JDE_MELA5

4/18/2013

JDEMELA5

4/18/2013

------------4-------------+------~

---r

~0_1_3_7_3_3_5_ _~-N_i_tr_ic_A_c_id_ _ _ _ _ _ _ _~~8_N_______-_-_~1-J-~ME~


013624P

J Nitric Acid

Reagent Grade

~1~2013

,._.._.~-~-~-:-:-~-:-----[ c:~~:~h~-:~-i:-t-r:-~~--=======----=~~----~--58-,~-~-u--t-i_o_n______=-----+~-~D-M-:M-R-~LA-z-5----r-:-~-~-:-~~-~-~-~-;
0130175

Cerrium Carrier

0 12809P

Ethyl Alcohol

0.1~g/ml

RMARTZ

! 4/19/2013

=Reagent Grad_e_____--+__R_M_A__R_T_z_ _ _ 4_/_1_


9,/_2__0_1_3
t-1

013221P

Hydrofluoric Acid

Reagent Grade

RMARTZ

4/19/2013

ii671

~----- --'--+~-

{OJA..~v

-~~-- ----'f~-+-"~~~__!_.~="---"-~-~_L-~J----.f~~.!o'-\-1:__:~'!_~f!-'---~....,_ ll~~.~.c:_c=::::_-'~----t a.Jf_{!~~ ~f~~-~-'-""---"-1--'---------

----

------- ------

---

---------

------

----+-------~--------l~-----~-~ -------~--8-------~-

---~----- +-----~---~~------1--- -~---~-~---~--l--------~- -~~

--~---

-~-----~----------~------

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--

--~-----------

+-----~~--t--

'

------------------~~raw~~~~.w:t;,::~.:::~:::?;::":~;::;~~------,
x_

\--

'119

1.-L-Y~ -/t~':l!Q____ e-__ _

l{tt"11t7 _ _ _ 11 olto JS'Il <"1 r) ~.(...


L(ff1lt?
_ .. .{ J of.( /)ol~
vC:OA-ll -.\
I r -...~
(I
~
V'l - - '111~11-:>

....,,~~
11,4 otCJ.A <.

'it,IYt

P-.''-1( ft;.t-

II

-........,

LflliJO __ l?o'{ ,c;y 4 t l)

l{ftftn ...

l)cJL.(08fALIf~

whn,?J

\ ~o~ o~SA Lt-u)

'-4\t~\1'3

\_~o'-lo"\~~{o1-"l)

l_\ \ lli lll \'3Q'toso .rC ~~~ \q)


4 hi b'J ,~., '1 c'S') 1'\ (a-~)

~: -C(/~11~

p4,'l~fJHy;--

or

()

--~-- _.Lffl)J/2 . _/7 ,,,..t~


,vJ
t{ ll )IJ
) ~ c_ CAL.

__ l-

_________ lfllfto --- !?;oct~ Jl~l J.,r,_

l..t

vt..-1'---: _. ~~ -~--

. . - - }ll!_u_
.... .~~
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<-

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--- _Y\..
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r~t.-'1'

l91-"f

r'Sl>..,...,.>

I ~'--,
Dr""'L

1.. \v ~-=-

r-

/c..__ __

orr~

~ t-.r-~-

. Oleo

-z..t-2

/II~

~.....-.-

--~-: ~\~~~~i ~~~:~~~~ t.-<a~.s~ 1~~ ~:- --~-. ~


=: w~\r~ p~~~~~~)

e.,; ';.;~ ~

to'l-V"

/3 so

'{'(\}""~--- ___ N_fr___


;l.f+IL ~,....
i sa;TJ.__

U)

Y2_

{;"J
'

7'

ol---l-----'/"-""t,.---~-- - ~~- -~
-J--+--I------1J..J_____ --~- ~-~'1--~~~-~----~

~===1-___l<c!_J_Jf':___t---I ..J .-r

.--f.-J...Lr__:V':.._j __ :z_. k r

,~~~~---~-~_:

---~_$

-~--

_ k~~

-~

---

_/Y~-:!:7r _c_____

-~~~

_u

tG6
--~---~~---~ L\)_ ~. ~-- - =-~~-- fJ -C4'-IJ

h.rvs

=--r::--LC.__:_-+--'--'-_::::_:::---+-'-1-=Co~<(c_o------~-1~-~- V\

-1--_!__L_'-=--~~=If_:._:_:flJ=-;{)---',.~---[~~- ~~ ~-

RA-226 NOTES

Page 1 of 1

Printed: 4/16/2013 8:35AM

Oak Ridge Laboratory

EBE::RLINE
SERVICES

~
I

Work Order Analysis Notes I

I
#

Date
04/16/13 08:35

Dept

'

PREP

User
JBARNARD

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Anal __ _____
Run Number

13-04051
Ra226
1

Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS

_if- Hf,tJ ~

~\llD\~~

ii&76

Printed: 4/18/2013 2:57PM

}!J E
~

Page 1 of 1

Oak Ridge Laboratory

B.I:::R.-=1N .E
SERVICES

Work Order Analysis Notes

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-04051
Ra226
1

Date

Dept

04/16/13 08:35

PREP

JBARNARD

ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS

04/17/13 17:19

PREP

LWALKER

ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.

04/18/13 14:57

PREP

LWALKER

FOLLOWED STEPS 12.1 TO 12.81N AP-006 REV12 FOR RA 226 ANALYSIS (SYRINGE FILTERED
SAMPLES-PRECIP-FILTERED-DRIED-OBTAIN FINAL WEIGHT) SUBMIT TO COUNT ROOM.

User

Notes

Printed: 4/19/2013 12:55 PM


Page 1 of 1

Eberline Analytical
Oak Ridge Laboratory

Reagents Used in an Analysis

JBARNARD
JBARNARD

Lead Carrier
013624P

JBARNARD

0137545

LWALKER

011383P

Acetic Acid

013377001

Ammonium Sulfate

eagent Grade
200 mg/ml

LWALKER
LWALKER

4/18/2013

iiii78

1J.t7

--~.~

~lUJ~2-~-L~~~~~-~c~~~--~~~~~-~-~~~ . .~~---

-~--~-_:_:__:_.~-=----~..N'~-----1

t-"-"'-'--'-'-------t-----1

l<:-6.
19'2_ __

1--~...;..:_,_..,_~ . J((?__
~~~-1--.~~----1 &_ __

- ----~-------

iG79

t117lrJ

l.frm,?
t{II~IJ

'iUCJt
'itt~Ja

_ J1o~to "'1S'Il< '1.-rJ ~~,

['7ol.(ot~,..u,~

_t""l,Yo~~

p . . .'4f f~:-.ty.-

t?t.?Lt ,'irA l l)

t..t~

..-L-Y~ 4-~:t-'1..2

lot.."""-'

~ W~v-

{IL-)

&A-'>

ortro

lA-t..-\~ .....~ l.

077~

L(ltttn
_lJoL-tQ&fALr~ ~~~'-<;.D\. ..
05J/
_, ~ h\k?J l ~oi q<i'S"_A 6-t.) We:>~
tz...t..\
___ 4\t'l\l3 l~C>~-Q~~)1 (~-1-)
Pc.L
l ??.,'f
, L\_ \l9 t,) _\'?>o~os-o ~( ~~~ lq)
-~) s'-l
t9 2-or

\db'?
l( ~~~~7

[f(I)Jl2

- - , _ t( ll )A

--"

Lftt_fto

1~<1'f o~ ~ ( - 4)

--rz,., ~1!4 ~

f?_Q'f/t~dlltl.f}
-) g'__L CAL.
l)o'l->_f"_f&l J.,r,

.l'V\&~d-s"l.
1/V'?

t-v>'-

v-'7

hA

- ~ _1..\ltotl r2 _ \3)o '-lo-s L~ (J- \D) ~ca, ~ ~"'

c:::-____

-vt-rc---~: -~~ -~-- -1... t...


- _/J/!__~2 -~~ .
/~

.... -~ --~

"1.-t..... -r

~~~ --~~

,q~,

orl.."
0jJ7

_O~co
/1/ (&?
li~

;c...._
-z_ l._r1.---

/L _,__iL___

~-.
---~~ __-::--__

l.-1-7 ___ -----

-L

/yA=_

-- ~ ~--1~--- -- ---

----~--~-1-

----------- - - - - - t -

------ ~---~--

------------

~~JI---

~---~-

f.

_,

----~-----------+----------~-----b------~----~

! -.
-

----

-,

--

.-:~--

RA-228 NOTES

Printed: 4/16/2013 8:35AM

~
1;:: B
~

Page 1 of 1

Oak Ridge Laboratory

1;: R l,....j_N E

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

#
1

Date

Dept

04/16/13 08:35

PREP

User
JBARNARD

Internal Work Order

Analysis Code

13-04051
Ra228
1

Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS

Printed: 4/25/2013 6:25PM

Page 1 of 1

~
EBERI,...,IN-=:
~

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

#
1

Date
04/16/13 08:35

I
I

Dept
PREP

Ii

User
JBARNARD

~
3

LWALKER

I
04/25/13 18:2SrPREP -- -LWALKER

Analysis Code
Run Number

13-04051
Ra228
1

Notes
ALIQUOT ED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS

-------!-04/22/13 12:14 1 PREP

lntemal Work Order

--------------

..
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.

-----~~-----

-~OLLOWED STEPS 12.1 TO 12.71N AP-ooiREV 17 (CHEMr'CAL CLEANUP FOR RA 228)

--

Printed: 4/29/2013 7:52 AM

j!J E
~

Page 1 of 1

Oak Ridge Laboratory

BE;:RJ,...,I NE
SERVICES

Work Order Analysis Notes

Date

Dept

04/16/13 08:35

PREP

JBARNARD

04/22/13 12:14

PREP

LWALKER

=3

04/25/13 18:25

PREP

LWALKER

User

__

I
04/29/13 07:52

,n-~--~--

CHEM- TSMITH-

13-04051

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Analysis Code
Run Number

Ra228
1

Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS

--~REcEivEo-~FIL fE:R"ssAcR-fRoiXcouNT Roo!Vi:-F>uTsAcK INrc5c:rusEs:.A:o-oE:-6"EbTA AND


SWIRLED-LET SIT OVERNIGHT TO DIGEST.
F'oCCowED STEPs-12.1T0~12.iiN ,t\p:-oo7 RE\Ti7-(cHEMICALCLEANUP FOR RA 228)

--

---~-'"

Followed steps 12.7 to 12.15 in AP-007 rev. 17 . ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil. and took to count room l

ii85

Eberline Analytical
Oak Ridge Laboratory

r
I

Printed: 4/29/2013 8:38AM


Page 1 of 1

Internal Work Order

e::. . e . e:e ~~ ..-. . e:

SERVICES

Run

Ra228

Reagents Used in an Analysis

1
c

Reagent
ID

Reagent
Name

Reagent
Concentration

Analyst
ID

' CWl

Date
Recorded

I
1

4/16/20l3"i
~~

4/16/2013
i
........
...... '"'""!
Barium Carrier

JBARNARD

cwvw'i

.. .....

JBARNARD~r4/16/.2o131

i Lead Carrier
--r~-N.itric Acid
'''(""'

4/16/2013

.. -~~-~--~~)
JBARNARD
I 4/16/2013 I

...

~.-

4/25/2013 I
................................ ~

Ammonium Sulfide

LWALKER

...........

4/25/2013 I
T4/2s;2o13

.......... ... ..-..4 .. ... .................1

~~

LWALKER

4/25/2013

' 4/25/2013

TSMITH
J 4/29/20l3:
TSMITH ............. 1..
. ~~~ ~-..-~~""T~~-~-1
TSMITH
14/29/2013 :

4/29/20131

...... y

18M

.. L..

TSMITH

TSMITH

!:.4/29/2013
I
...J
l 4/29/2013 I

j"'"""~~"m~VV'~~~~m~~M,lm.~"''"

vn Ah''""'"">

Lf) 4Uo

Q~

~CJ...C.-'-11) 0 ~

0 C. ~.

.*

r\0

'--k_.t~ Q '1 o'iv-. 1 A~~ C/kJ.-,... ~


tL\~ -:2.. d- ~~ fb'"l-W> I~-~

~=---~=v~IJkJr)_JC3P':lJ~~f_bu.~j)_ -----L4~4:
____ -~---l(h..tt'-12 _ _ G-~ __ -----~---1---cr ri;:L
------- ~---- VrJ.JtJn .. _.ll_\.~_ -----~------- o(ttf.t,
_________ ~---- <:it::tWt: ___ L:J~kJti.PU-4-lJ.!(' __ _{2 ~. ~" '~4..r1
__ ____ .-- 'f t\.11~ ____ _l_ l_p_!l_f&~~ (~~ Q~~ 0'-t \l
-----~L1.k'JO _. L')...c::.~L~'6-i~.U~'1 ____Li.l.l?l~-- D YC"'YI""UID L
-L 2D'l~YII!II. .:.1- _J.d. t.-ot--- _ nK1?

o""

f-..

J,(L'"":\.~ ,.,____ __L]. 0'1_~tiM-~ 1.-1)_.~ ~

..--- ,__

------ -- lfL1.ul/fL ____ _j_'2_e''!Jlt~AAt.


______ r--'-1 l2~ll}

79

( oo l,

'.t.~uJ_~ l 0 2L

"?D-

1~ _

--v~...-

:1,..-L.-

-(.._~..-

L-~

~.A--

e-.

I<-_f

c._:

L,
/h

~~YLf {)/y.
SA.f_~
S/37:;-7_
'>It-rD7

L--

,.

C- _

-j

'-' _

c._._.,, ~

f1..A-tl
flA-V-

'--'-.~

.,u2

~ _. ~ ..

J~P~_t_':f1_.e_~(_Z:~'')_ -- ---~~ ~____ _I v, 0


"2--h-.~ {l~~ :
)
_______t.-iWtlt~-'~t?~~-~~~1.\)-~.~~._____t}J\L
U~C) _
_
_____ -. __'{Ll-i+ll'2 __we~~- t2\CfA __ ____ ~~----- .-lb'32.~- f---1~ ~:>
t>Lp i ~ _ .
---- .CII-dt/2 -- (ff~ - - ___ _.!A::-7_ ____~ ~12f1'1' 1--oL d'}_
c
c

_________ __lff'l9J[J. _____ 01L~~------ ---~

~
- ______ . f((l)p? - JJ:O!to2LD!J~-~ .~~t=----- tL!fltt- __ t.-

() ll-r

l/11

L- ./

__________ Lft"\..'u~ ___L"J_o!i.o_(\..ll.k'-l=--~ ---~ ........._....

n '<t'5

f2./Pr c......-

-------- _'tGJ.II-:> ____ t'?_\2.'iJlfU1~.!-~t~-~t---

fJSJ'O
-l \ o'2-

~
'1.---

fl-+-y-

---~ .l11:t:2~o _______f2'?_'fVJJI~.... l1n_- L~.)__~~"'"'-f!

_____ --~(z.,~lt~ i"o=t~Ltttlto~~t~}~~ ---ll&.~


------~--

----- ---- -- ---

-----------------~-~----

------

--- --- ------ ---- ------------ ---

------~

----- -- .. ---- -- __ ......._

_ . . . .--.-~

c_ .

~ c....--L

~1

_\C .J . [
. . ..

---~--------------t----------t------1-----l-------

----------~--+--------+----+-~----+--.

----------------- - - - - - . 1 - - - - - - - - - . 1 - - - - - - f - - - - o / '

-.----- ------------ ----------.... ----..-- ----


--------- ------- -.-.---------.-- ----

-~

- -

---~

-------------f----+------t--------1---~if~

-- --- -------- ---------- ..--- - ---- - - - - - - - - - - - - - - - - t - - - - 1 - - - - - - + - - - - - - - t - - - ; L : :

; .

- -

... --~---

...:;:<

--- ------ ....--.--- ---- ----- --------~-------~---1-------il---------t----~r:<::

"'<:

-----

; f

--------t

- -------t -------- ------------------------ ---

... __ ... ---------- ----~----.J-----+--------1------tb<i


r.. :.f

----------------1----

______j - ....... _______ ------- ------------------ -

=---1

. - - ------------ - -----

!-...:

----------+-------t---~-+--------+---r!J

-~ - - ~= ~~-~- _-_ ~-=- -~

J-q

'_;,

. . . ___L-

SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 4/19/2013 5:59AM


Page 1 of 3

13-04051
UUISO
Run 1
Internal

Work Order
Analysis Code

Sample
Desc

Client
ID

Login
CPM

LCS

LCS

04/09/13 00:00

MBL

BLANK

04/09/13 00:00

Sample
Aliquot

Sample
Date

1.0000E+00

-~------

--------

03

Date Received

PZ-105-SS TOT

DUP

-----

~------

Lab Deadline
Client

4/30/2013

04

DO

Engineering Management Support, Inc.

05

TRG

--------

Project

West Lake OU-1

PZ-105-SS TOT
PZ-105-SS DIS

06

TRG

04/04/13 15:06

1.0000E+OO

46

j 04/04/13 15:06

1.0000E+OO

46

--04/04/13 15:06

-------

42

S-10 TOT

07

TRG

S-10 DIS

pCi

08

TRG

42

09

TRG

LR-104 DIS

WA

10

TRG

DUP 01 TOT

NAS NS-3050 Mod

11

TRG

DUP 01 DIS

45

Alpha Spectroscopy

12

TRG

U-232

13

TRG

----------

Radiometric Tracer

------------+-------------

Radiometric Sol#

U-10a

14

TRG

1.0000E+OO

48

04/04/13 00:00

1.0000E+OO

04/04/13 00:00

1.0000E+OO

04/04/13 00:00

1.0000E+OO

04/04/13 09:30

1.0000E+OO

04/04/13 OB:30!

1.0000E+OO

------~------+----------------

43

DUP 02 DIS

43

FB at PZ-110-SS TOT

04/04/13 00:00

------------

-----

1.0000E+OO

48

DUP 02 TOT

+----------------

-----

04/04/13 15:52

----~-------

Instrument Type

1.0000E+OO

-~--

-------------- - - - - - -

Method

-~---

04/04/13 15:52

45

-----

Matrix

1.0000E+OO

04/04/13 15:25N.OOOOE+OO

--~-

1.0000E+OO
-----------

-~-----

-~-~-

LR-104 TOT

-----~

Aliquot Units

04/04/13 15:25

----

Activity Units

----

~----~

Report Level

46

------------+---~-

---------------

1.0000E+OO

~~~-------~

42

--------~----~-

1-----------------~--~---------

-~----

Tracer Act (dpm/g)


----~-----

19.098

15

Carrier Cone (mg/ml)

FB at PZ-110-SS DIS

42

TRG

MW-103 TOT

-----------

--------~-

Carrier
-----

TRG

- - - - - -

48

04/05/13 09:50

1.0000E+OO

------~

-----~-----

17

TRG

MW-103 DIS

48

04/05/13 09:50

1.0000E+OO

18

TRG

PZ-200-SS TOT

37

04/05/13 11 :1 0

1.0000E+OO'

19

TRG

PZ-200-SS DIS

37

04/05/13 11:1 0

1.0000E+OO

-----!

~----

g:)

g;
Ul

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 411912013 5:59AM


Page 2 of3

13-04051
UUISO
Run 1

Internal
Fraction

Sample
Desc

LCS

-~
I

Tracer Total
ACT(dpm)

Radiometric
Tracer (pCi)

o.6104

11.1

MBL I

0.6068

11.6 r - - l o o o

DUP I

0.6050

DO I

0.5980

TRG

0.6003

I .

TRG

o.6041

TRG I

0.5~ 11.4

11.6

11.5

oooj

0.6002 I

TRG

0.5998

TRG

o.6012

TRG

0.5945

1
I

11.5

; ;

:1

0.00

0.001

0.00

:::

--'1

-0~~~J-~
-~-

~oo,

11.3 I_

0.00

TRG

0.5965 !

11.4

0.00

0.5962

---~

11.3

r-

I ---

-t'
,

-t---__j
l

0.5933

TRG

o.ool

TRG

0.5933 I

~-

11.5 [

2*

+
+-----1

!_

SAF

--

0.00

SAF
1*

Mean
% Rec

11.4

TRG

-~-

ID.OOf

o.5956 .

~-

11.5

11.4

Grav

% Rec

0.00

TRG

Grav Filter
Net(g)
I

~00
'

Grav Filter
Final (g)

o.ooi

I
11 ~

0.6016j_~_
_ : : : : :

11.4

TRG i

: : :

Grav Filter
Tare (g)

Radiometric I Grav Carrier


% Rec
Added (ml)

~G
I

Tracer
Aliquot (g)

--f

-----+----

~--______

--i-

I
1

-+----1

0.00

11.4 I

0.00

l
c;n
~!)
t~

II!~

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

L~ ~

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 4/19/2013 5:59AM


Page 3 of3

13-04051
UUISO
Run 1

Internal
Fraction

Sample
Desc

01

LCS

02

MBL

03

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

04/16/13 08:25

JBARNARD

04/16/13 08:25

JBARNARD

DO
--------+--- ---

JBARNARD

04/16/13 08:25

JBARNARD I

I o4t16/13 08:25

JBARNARD I

Sep tO
By

--------

04/16/13 08:25

DUP

04

Sep tO
Date/Time

_os

I TRG

06

TRG

07

TRG

04/16/13 08:25 , JBARNARD

08

TRG

04/16/13 08:25

JBARNARD I

TRG

04/16/13 08:25

JBARNARD

TRG

04/16/13 08:25 I JBARNARD

t-

--

r-j

+-I

Sep t1
By

I
I
I

JBARNARD

I 04/16/13 o8:25

Sep t1
Date/Time

---

09

f----

10
r-----

11

I
I

TRG

04/16/13 08:251 JBARNARD

12

i TRG

__?4/16/13 08:25 I JBARNARD

13

I TRG

----------

04/16/13 08:25

JBARNARD

-- --

14

04/16/13 08:25

-----.-

JBARNARD
-----

15

II : : :

l- 04/16/13 08:25

JBARNARD

16

TRG

I 04/16/13 08:25

JBARNARD

17

TRG

18

TRG

I 04/16/13 08:25

19

TRG

-L-~---

-----

--

--

JBARNARD i

04/16/13 08:25

04/16/13 08:25
--

JBARNARD
JBARNARD
--r--

tl!'
lldl;,

lO
~~-

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory

~
0

.!I!
~

ca
~

OK

MDA
Flag

01

U-234

LCS

LCS

pCi/1

7.85E+OO

1.07E+OO

8.92E-02

02

U-234

MBL

BLANK

pCi/1

4.51E-02

5.14E-02

6.78E-02

03

U-234

DUP

PZ-105-SS TOT

pCi/1

2.60E+OO

4.61E-01

9.02E-02

04

U-234

DO

PZ-105-SS TOT

pCi/1

2.62E+OO

4.55E-01

7.94E-02

OK

en

05

U-234

TRG

PZ-105-SS DIS

pCi/1

2.58E+OO

4.43E-01

6.90E-02

OK

::l
::l

06

U-234

TRG

S-10 TOT

pCi/1

2.29E-01

1.15E-01

8.09E-02

OK

07

U-234

TRG

S-10 DIS

pCi/1

1.25E-01

1.00E-01

1.07E-01

OK

08

U-234

TRG

LR-104 TOT

pCi/1

2.60E+OO

4.42E-01

5.07E-02

OK

09

U-234

TRG

LR-104 DIS

pCi/1

2.72E+OO

4.51E-01

5.62E-02

OK

10

U-234

TRG

DUP 01 TOT

pCi/1

2.55E-01

1.09E-01

5.38E-02

OK

11

U-234

TRG

DUP 01 DIS

pCi/1

2.04E-01

1.08E-01

6.66E-02

OK

12

U-234

TRG

DUP 02 TOT

pCi/1

1.59E-01

9.76E-02

7.93E-02

OK

13

U-234

TRG

DUP 02 DIS

pCi/1

1.77E-01

1.01E-01

6.69E-02

OK

14

U-234

TRG

FB

at PZ-110-SS TOT

pCi/1

1.57E-02

2.98E-02

5.52E-02

OK

15

U-234

TRG

FB

at PZ-110-SS DIS

pCi/1

4.42E-02

6.79E-02

1.16E-01

OK

16

U-234

TRG

MW-103 TOT

pCI/1

4.07E+OO

6.75E-01

1.19E-01

OK

17

U-234

TRG

MW-103 DIS

pCi/1

3.17E+OO

5.52E-01

5.99E-02

OK

C"l

18

U-234

TRG

PZ-200-SS TOT

pCi/1

5.42E-01

1.80E-01

8.08E-02

OK

19

U-234

TRG

PZ-200-SS DIS

pCi/1

5.32E-01

1.77E-01

9.34E-02

OK

or-

(/)

....c
Q)

E
Q)
C"l
Ill

~
c

;:
Q)
Q)

a,
c
w

I'~)

96.33

RPD
Flag

Activity
Units

Q..
Q..

I;~

LCS
Flag

Client
Identification

:I

LCS
%R

Sample
Desc

g~

LCS
Known

Nuclide

.E

ujl

Work Order: 13-04051-UUIS0-1

Lab
Fraction

"

Printed: 4/22/2013 8:59AM


Page 1 of 3

Preliminary Data Report & Analytical Calculations

Results

Error Estimate

MDA

8.15E+OO

Blank
Flag

OK
OK
OK

OK

OK

~
~
.g
0

.!!!
~

ct

01

U-234

LCS

04/09/13 00:00

1.00E+OO

110.41

0.00

0.00

02

U-234

MBL

04/09/13 00:00

1.00E+OO

134.21

0.00

0.00

03

U-234

DUP

04/04/13 15:06

1.00E+OO

117.95

0.00

0.00

04

U-234

DO

04/04/13 15:06

1.00E+OO

121.42

0.00

0.00

en

05

U-234

TRG

04/04/13 15:06

1.00E+OO

125.70

0.00

0.00

~
~

06

U-234

TRG

04/04/13 15:25

1.00E+OO

101.21

0.00

0.00

07

U-234

TRG

04/04/13 15:25

1.00E+OO

81.32

0.00

0.00

08

U-234

TRG

04/04/13 15:52

1.00E+OO

117.88

0.00

0.00

09

U-234

TRG

04/04/13 15:52

1.00E+OO

123.81

0.00

0.00

10

U-234

TRG

04/04/13 00:00

1.00E+OO

132.22

0.00

0.00

11

U-234

TRG

04/04/13 00:00

1.00E+OO

100.34

0.00

0.00

12

U-234

TRG

04/04/13 00:00

1.00E+OO

95.45

0.00

0.00

13

U-234

TRG

04/04/13 00:00

1.00E+OO

102.84

0.00

0.00

t!

14

U-234

TRG

04/04/13 09:30

1.00E+OO

144.40

0.00

0.00

...c

15

U-234

TRG

04/04/13 09:30

1.00E+OO

91.62

0.00

0.00

16

U-234

TRG

04/05/13 09:50

1.00E+OO

90.80

0.00

0.00

17

U-234

TRG

04/05/13 09:50

1.00E+OO

93.69

0.00

0.00

18

U-234

TRG

04/05/13 11:10

1.00E+OO

105.27

0.00

0.00

19

U-234

TRG

04/05/1311:10

1.00E+OO

109.45

0.00

0.00

SAF

SeptO
Date/Time

Sep t1
Date/Time

:::1

CD
CD

Cl
I'll

I'll

:IE
Cl

;::
CD
CD

.E
Cl
c

[,;,~

Mean
%Rec

Grav
%Rec

Sample
Date

U)

tO

Radiometric
%Rec

Sample
Desc

Q.
Q.

~'1l

Sample
Aliquot

Nuclide

~,

Work Order: 13-04051-UUIS0-1

Lab
Fraction

.E

~I

Printed: 4/22/2013 8:59 AM


Page 2 of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory


a::

..:-

Printed: 4/22/2013 8:59AM


Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-04051-UUIS0-1

Lab
Fraction

Nuclide

Sample
Desc

Counting
Date/Time

01

U-234

LCS

02

U-234

MBL

03

U-234

Halflife
(days)

Count
Time

Counts

Bkg
CPM

Eff

Detect

Carrier

04/19/13 11:36

A_Spec

Alpha_018

170 5.80 E+02

7.00 E-03

17.8

04/19/13 11:36

A_Spec

Alpha_022

170 3.49 E+OO

3.00 E-03

15.3

I
I

DUP

04/19/1311:36

A_Spec

Alpha_024

170 1.98 E+02

8.00 E-03

17.1

--- - -

0
(.)
.~

~
.,
s::

"'(

04

U-234

DO

04/19/13 11:36

A_Spec

Alpha_025

170 2.08 E+02

6.00 E-03

17.4

tn

05

U-234

TRG

04/19/1311:36

A_Spec

Alpha_027

170 2.11 E+02

4.00 E-03

17.3

::;:)
::;:)

06

U-234

TRG

04/19/13 11:36

A_Spec

Alpha_029

170 1.70 E+01

0.00 E+OO

19.5

07

U-234

TRG

04/19/13 11:57

A_Spec

Alpha_033

170 7.00 E+OO

0.00 E+OO

18.2

08

U-234

TRG

04/19/13 11:57

A_Spec

Alpha_034

170 2.14 E+02

1.00 E-03

18.6

09

U-234

TRG

04/19/13 11 :57

A_Spec

Alpha_035

170 2.32 E+02

2.00 E-03

18.3

10

U-234

TRG

04/19/13 11:57

A_Spec

Alpha_037

170 2.27 E+01

2.00 E-03

17.8

11

U-234

TRG

04/19/13 11:57

A_Spec

Alpha_040

170 1.47 E+01

2.00 E-03

19

12

U-234

TRG

04/19/13 11:57

A_Spec

Alpha_041

170 1.13 E+01

4.00 E-03

19.8

13

U-234

TRG

04/19/13 11 :57

A_Spec

Alpha_042

170 1.27 E+01

2.00 E-03

18.5

t:

14

U-234

TRG

04/19/13 14:33

A_Spec

Alpha_003

170.02 1.49 E+OO

3.00 E-03

17.5

.E
0

c.
c.
:I

...

15

U-234

TRG

04/19/13 14:33

A_Spec

Alpha_004

170 2.96 E+OO

1.20 E-02

19.4

Cl)

16

U-234

TRG

04/19/13 14:33

A_Spec

Alpha_010

170.02 2.74 E+02

1.30 E-02

19.7

17

U-234

TRG

04/19/13 14:33

A_Spec

Alpha_011

170 2.21 E+02

1.00 E-03

19.7

18

U-234

TRG

04/19/13 14:33

A_Spec

Alpha_013

170 4.02 E+01

5.00 E-03

18.7

19

U-234

TRG

04/19/13 14:33

Alpha_014

170 4.05 E+01

9.00 E-03

18.5

tJ)

s::::

~I

E
Cl)
Cl

I'll

s::::

I'll

==Cl
s::::

;:
Cll
Cl)

.5

Cl
s::::

m
CilU

if.J(~

t:~

'
.

A_Spec
-

L___

----

--

a:

Printed: 4/22/2013 8:59 AM


Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-04051-UUIS0-1

LCS
Known

LCS
%R

LCS
Flag

100.95

OK

RPD
Flag

MDA
Flag

Lab
Fraction

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

U-238

LCS

LCS

pCi/1

8.02E+OO

1.09E+OO

8.88E-02

02

U-238

MBL

BLANK

pCi/1

2.11E-02

4.54E-02

8.82E-02

03

U-238

DUP

PZ-105-SS TOT

pCi/1

1.82E+OO

3.62E-01

6.27E-02

04

U-238

DO

PZ-105-SS TOT

pCi/1

1.64E+OO

3.32E-01

S.OOE-02

OK

05

U-238

TRG

PZ-105-SS DIS

pCi/1

1.42E+OO

3.00E-01

8.65E-02

OK

06

U-238

TRG

S-10 TOT

pCI/1

2.41E-01

1.18E-01

8.46E-02

OK

07

U-238

TRG

S-10 DIS

pCi/1

8.91E-02

8.62E-02

1.07E-01

OK

08

U-238

TRG

LR-104 TOT

pCi/1

2.11E+OO

3.84E-01

5.78E-02

OK

09

U-238

TRG

LR-104 DIS

pCi/1

1.94E+OO

3.58E-01

4.88E-02

OK

10

U-238

TRG

DUP 01 TOT

pCi/1

1.21E-01

7.40E-02

4.68E-02

OK

11

U-238

TRG

DUP 01 DIS

pCI/1

1.43E-01

9.20E-02

7.82E-02

OK

12

U-238

TRG

DUP 02TOT

pCi/1

1.04E-01

8.94E-02

1.17E-01

OK

13

U-238

TRG

DUP 02 DIS

pCi/1

1.32E-01

8.79E-02

7.31E-02

OK

14

U-238

TRG

FB

at PZ-110-SS TOT

pCI/1

-7.13E-03

2.17E-02

5.91E-02

OK

15

U-238

TRG

FB

at PZ-110-SS DIS

pCi/1

-1.26E-02

3.12E-02

8.90E-02

OK

16

U-238

TRG

MW-103 TOT

pCi/1

3.72E+OO

6.30E-01

8.86E-02

OK

co
co

17

U-238

TRG

MW-103 DIS

pCI/1

3.00E+OO

5.31E-01

9.01E-02

OK

Cl

18

U-238

TRG

PZ-200-SS TOT

pCi/1

5.22E-01

1.74E-01

5.61E-02

OK

19

U-238

TRG

PZ-200-SS DIS

pCi/1

5.84E-01

1.84E-01

6.26E-02

OK

Results

Error Estimate

MDA

7.94E+OO

Blank
Flag

OK
OK

OK
I

OK

OK

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%Rec

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%Rec

Grav
%Rec

Sample
Desc

Sample
Date

01

U-238

LCS

04/09/13 00:00

1.00E+OO

110.41

0.00

0.00

U-238

MBL

04/09/13 00:00

1.00E+OO

134.21

0.00

0.00

DUP

04/04/13 15:06

1.00E+OO

117.95

0.00

DO

04/04/13 15:06

1.00E+OO

121.42

0.00

0.00

------

03

U-238

04

U-238

SAF

05

U-238

TRG

04/04/13 15:06

1.00E+OO

125.70

0.00

0.00

::J
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06

U-238

TRG

04/04/13 15:25

1.00E+OO

101.21

0.00

0.00

07

U-238

TRG

04/04/13 15:25

1.00E+OO

81.32

0.00

0.00

08

U-238

TRG

04/04/13 15:52

1.00E+OO

117.88

0.00

0.00

09

U-238

TRG

04/04/13 15:52

1.00E+OO

123.81

0.00

0.00

10

U-238

TRG

04/04/13 00:00

1.00E+OO

132.22

0.00

0.00

11

U-238

TRG

04/04/13 00:00

1.00E+OO

100.34

0.00

0.00

12

U-238

TRG

04/04/13 00:00

1.00E+OO

95.45

0.00

0.00

13

U-238

TRG

04/04/13 00:00

1.00E+OO

102.84

0.00

0.00

14

U-238

TRG

04/04/13 09:30

1.00E+OO

144.40

0.00

0.00

...c::

15

U-238

TRG

04/04/13 09:30

1.00E+OO

91.62

0.00

0.00

16

U-238

TRG

04/05/13 09:50

1.00E+OO

90.80

0.00

0.00

17

U-238

TRG

04/05/13 09:50

1.00E+OO

93.69

0.00

0.00

18

U-238

TRG

04/05/13 11 :10

1.00E+OO

105.27

0.00

0.00

19

U-238

TRG

04/05/13 11:10

1.00E+OO

109.45

0.00

0.00

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02

Work Order: 13-04051-UUIS0-1

Lab
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Printed: 4/22/2013 8:59 AM


Page 2 of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

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Oak Ridge Laboratory

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Printed: 4/22/2013 8:59 AM


Page 3 of 3

Preliminary Data Report & Analytical Calculations

Work Order: 13-04051-UUIS0-1

Lab
Fraction

Nuclide

Sample
Desc

Counting
Date/Time

01

U-238

LCS

02

U-238

03

U-238

04

U-238

DO

05

U-238

06

Halflife
(days)

Count
Time

Counts

Bkg
CPM

Eff

Detect

Carrier

04/19/13 11:36

A_Spec

Alpha_018

170 5.95 E+02

7.00 E-03

17.8

MBL

04/19/13 11 :36

A_Spec

Alpha_022

170 1.64 E+OO

8.00 E-03

15.3

DUP

04/19/13 11 :36

A_Spec

Alpha_024

170 1.39 E+02

2.00 E-03

17.1

04/19/13 11 :36

A_Spec

Alpha_025

170 1.31 E+02

2.00 E-03

17.4

TRG

04/19/13 11:36

A_Spec

Alpha_027

170 1.16 E+02

9.00 E-03

17.3

U-238

TRG

04/19/13 11:36

A_Spec

Alpha_029

170 1.80 E+01

6.00 E-03

19.5

07

U-238

TRG

04/19/13 11 :57

A_Spec

Alpha_033

170 5.00 E+OO

0.00 E+OO

18.2

08

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_034

170 1.75 E+02

2.00 E-03

18.6

09

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_035

170 1.66 E+02

1.00 E-03

18.3

10

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_037

170 1.08 E+01

1.00 E-03

17.8

11

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_040

170 1.03 E+01

4.00 E-03

19

12

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_041

170 7.45 E+OO

1.50 E-02

19.8

13

U-238

TRG

04/19/13 11:57

A_Spec

Alpha_042

170 9.49 E+OO

3.00 E-03

18.5

14

U-238

TRG

04/19/13 14:33

A..,Spec

Alpha_003

170.02 -6.80 E-01

4.00 E-03

17.5

...c

15

U-238

TRG

04/19/13 14:33

A_Spec

Alpha_004

170 -8.50 E-01

5.00 E-03

19.4

16

U-238

TRG

04/19/13 14:33

A_Spec

Alpha_010

170.02 2.51 E+02

5.00 E-03

19.7

17

U-238

TRG

04/19/13 14:33

A_Spec

Alpha_011

170 2.10 E+02

6.00 E-03

19.7

18

U-238

TRG

04/19/13 14:33

A_Spec

Alpha_013

170 3.88 E+01

1.00 E-03

18.7

19

U-238

TRG

04/19/13 14:33

A_Spec

Alpha_014

170 4.47 E+01

2.00 E-03

18.5

or-

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Client
Identification

Activity
Units

LCS

LCS

pCi/1

Results

IError Estimate I

4.29E-011

1.74E-011

MDA

7.98E-02

LCS
Known

LCS
%R

LCS
Flag

RPD
Flag

MDA
Flag

U-235

r----

DO

PZ-105-SS TOT

pCi/1

1.09E-011

8.69E-021

9.32E-02

OK

-----~--+--~--------r---~---+---~--+---~---+------r---~-----+----~

U-235

TRG

PZ-105-5S DIS

pCi/1

8.02E-021

7.36E-021

8.51E-02

OK

06

U-235

TRG

S-10 TOT

pCi/1

2.76E-021

4.69E-021

7.95E-02

OK

07

U-235

TRG

S-10 DIS

pCi/1

1.83E-021

4.39E-021

9.21E-02

OK

08

U-235

TRG

LR-104 TOT

pCi/1

1.65E-011

1.03E-011

8.98E-02

OK

09

U-235

TRG

LR-104 DIS

pCi/1

1.59E-011

9.98E-021

8.69E-02

OK

10

U-235

TRG

DUP 01 TOT

pCI/1

1.15E-021

2.76E-021

5.80E-02

OK

11

U-235

TRG

DUP 01 DIS

pCi/1

3.44E-021

5.84E-021

1.03E-01

OK

12

U-235

TRG

DUP 02 TOT

pCI/1

5.55E-031

3.59E-02I

9. 78E-02

OK

13

U-235

TRG

DUP 02 DIS

pCi/1

1.18E-011

9.06E-021

7 .20E-02

OK

t:

14

U-235

TRG

FB at PZ-110-SS TOT

pCi/1

3.45E-021

4.46E-021

6.21E-02

OK

15

U-235

TRG

FB at PZ-110-SS DIS

pCi/1

-3.50E-031

3.96E-021

1.21E-01

OK

16

U-235

TRG

MW-103 TOT

pCi/1

3.73E-011

1.71E-011

1.03E-01

OK

17

U-235

TRG

MW-103 DIS

pCi/1

2.66E-011

1.42E-011

1.06E-01

OK

::J
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Cll

E
Cll

Blank
Flag

OK

(3

Sample
Desc

05

a.
a.

...s::

Work Order: 13-04051-UUIS0-1

OK
3.70E-021
5.53E-021
8.99E-02
OK
MBL
BLANK
pCi/1
U-235
02
1-----j-~~---~
-T----------t-----+-~ -r----~---~~--~---4----~--4---~--_j
03
1.11E-011 8.52E-021
6.78E-02
NA
OK
U-235
DUP
PZ-105-SS TOT
pCI/1

04

.E

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U-235

Printed: 4/22/2013 8:59AM


Page 1 of 3

Preliminary Data Report & Analytical Calculations

Cl

ns

1:

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U-235

TRG

PZ-200-5S TOT

pCi/1

6.38E-021

6.59E-021

6.95E-02

OK

U-235

TRG

PZ-200-SS DIS

pCi/1

3.76E-021

5.62E-021

9.15E-02

OK

~
c::

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8
.!Q

Sample
Date

01

U-235

LCS

04/09/13 00:00

1.00E+OO

110.41

0.00

0.00

02

U-235

MBL

04/09/13 00:00

1.00E+OO

134.21

0.00

0.00

03

U-235

DUP

04/04/13 15:06

1.00E+OO

117.95

0.00

0.00

04

U-235

DO

04/04/13 15:06

1.00E+OO

121.42

0.00

0.00

en

05

U-235

TRG

04/04/13 15:06

1.00E+OO

125.70

0.00

0.00

::J
::J

06

U-235

TRG

04/04/13 15:25

1.00E+OO

101.21

0.00

0.00

07

U-235

TRG

04/04/13 15:25

1.00E+OO

81.32

0.00

0.00

08

U-235

TRG

04/04/13 15:52

1.00E+OO

117.88

0.00

0.00

09

U-235

TRG

04/04/13 15:52

1.00E+OO

123.81

0.00

0.00

10

U-235

TRG

04/04/13 00:00

1.00E+OO

132.22

0.00

0.00

11

U-235

TRG

04/04/13 00:00

1.00E+OO

100.34

0.00

0.00

12

U-235

TRG

04/04/13 00:00

1.00E+OO

95.45

0.00

0.00

..5

13

U-235

TRG

04/04/13 00:00

1.00E+OO

102.84

0.00

0.00

t::
0

14

U-235

TRG

04/04/13 09:30

1.00E+OO

144.40

0.00

0.00

15

U-235

TRG

04/04/13 09:30

1.00E+OO

91.62

0.00

0.00

16

U-235

TRG

04/05/13 09:50

1.00E+OO

90.80

0.00

0.00

17

U-235

TRG

04/05/13 09:50

1.00E+OO

93.69

0.00

0.00

18

U-235

TRG

04/05/1311:10

1.00E+OO

105.27

0.00

0.00

19

U-235

TRG

04/05/1311:10

1.00E+OO

109.45

0.00

0.00

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Grav
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Sample
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Nuclide

a.
a.

Work Order: 13-04051-UUIS0-1

Lab
Fraction

Printed: 4/22/2013 8:59AM


Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Eberline Services
Oak Ridge Laboratory

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Work Order: 13-04051-UUIS0-1

Halflife
(days)

Count
Time

Bkg
CPM

Sample
Desc

Counting
Date/Time

U-235

LCS

04/19/13 11:36

A_Spec

Alpha_018

170 2.57 E+01

2.00 E-03

17.8

U-235

MBL

04/19/13 11:36

A_Spec

Alpha_022

170 2.32 E+OO

4.00 E-03

15.3

03

U-235

DUP

04/19/13 11:36

A_Spec

Alpha_024

170 6.83 E+OO

1.00 E-03

17.1

04

U-235

DO

04/19/13 11:36

A_Spec

Alpha_025

170 7.00 E+OO

0.00 E+OO

17.4

en

05

U-235

TRG

04/19/1311:36

A_Spec

Alpha_027

170 5.32 E+OO

4.00 E-03

17.3

::J
::J

06

U-235

TRG

04/19/13 11 :36

A_Spec

Alpha_029

170 1.66 E+OO

2.00 E-03

19.5

07

U-235

TRG

04/19/1311:57

A_Spec

Alpha_033

170 8.30 E-01

1.00 E-03

18.2

08

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_034

170 1.10 E+01

0.00 E+OO

18.6

09

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_035

170 1.10 E+01

0.00 E+OO

18.3

10

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_037

170 8.30 E-01

1.00 E-03

17.8

11

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_040

170 2.00 E+OO

0.00 E+OO

19

12

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_041

170 3.20 E-01

4.00 E-03

19.8

13

U-235

TRG

04/19/13 11:57

A_Spec

Alpha_042

170 6.83 E+OO

1.00 E-03

18.5

14

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_003

170.02 2.66 E+OO

2.00 E-03

17.5

...

15

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_004

170 -1.90 E-01

7.00 E-03

19.4

Cl)

16

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_010

170.02 2.03 E+01

4.00 E-03

19.7

17

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_011

170 1.50 E+01

0.00 E+OO

19.7

18

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_013

170 3.83 E+OO

1.00 E-03

18.7

19

U-235

TRG

04/19/13 14:33

A_Spec

Alpha_014

170 2.32 E+OO

4.00 E-03

18.5

Lab
Fraction

Nuclide

01
02
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Printed: 4/22/2013 8:59 AM


Page 3 of 3

Preliminary Data Report & Analytical Calculations

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Counts

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Printed: 4/19/2013 5:59AM


Page 1 of 1

13-04051-UUIS0-1 (pCi/1) in WA
Tracer ID: U-1 Oa

Count Room Report


Client: Engineering Management Su

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Internal
Fraction

Sample
Desc

Client
ID

,
i

Sample
Aliquot

11.5887

1.0000

0.6050

11.5543

o.598o

11.4206

o.oo

11.4645

o.oo

07 ...-'\?TRG I

S-10 DIS

1.0000

TRG

LR-104 TOT

09

TRG

LR-104 DIS

10

TRG-t

DUP 01 TOT

11

TRG

-~uP_~~-~~2"-

TRG

FBatPZ-110-SSTOT

TRG
I

FB at PZ-110-SS DIS

=~~-TR~I _____ MW-103 TOT


TR~[

17

TR~--

18

~.1 TRG
I

Q,
ftwn.J,

I
I

PZ-200-SS DIS

_1

II

11.5371

0.5991

11.4416

+--~:~~~61

0.00

0.6012

11.4817

1-------+---

0.00

--+-

----=

-t--

0.00
0.00

1-.
-+--~__j____o.o~----1-~-0.00

0.00

1
0.00 i

11.35381

04/04/13 09:30

1.0000

0.5956 I

11.3748 I

04/05/13 09:5o

1.oooo

o.5933 :

11.33081

0. 4/05/13 09:50

1.0000

0.5965

11.39~0 ------ I ~~~~~~

04/05/13 11:1 o

1.0000

1.0000

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1

I
i

0.5933

11.3308
-11.3862

SAF
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11.4454
11.4550

SAF
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I

11.4894 I

0.5998

1.0000 --1---~_:_5945

04/04/1309:30

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I
I

0.6041

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04/04/13 00:00 11.0000

MW-103 DIS
PZ-200-SS TOT

1.0000

04/04/130o:oo __T_1.000C>__j

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04/04/13 15:52 I

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%Rec

0.6068 I

1.0000

08

Radiometric
Tracer (pCi)

1.0000

1.0~0.6003

TRG

11.6574

S-10 TOT

Tracer
ACT(dpm)

II

0.61~~-

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12

Tracer
Aliquot(g)

1.0000

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Eberline Services
Oak Ridge Laboratory

Isotope

Sol#

U-234

U-8a

U-238

Activity
dpmlg

U-8a

Solution
Date

Approx
Addition

35.24~~201_3

0.500

34.350,

0.500

4/16/2013

LCS

MS

LCSD

MSO~

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

0.5133

JBARNARD
-LCS

--

---~MS

Known
pCi

I----

1----

Sol#

0.293

7.94

0.5133

0.286

a.~m~g

Solution
Date

Volume
Used(g)

I
1

Approx
Addition

U-10a

19.098 4/16/2013

0.6104

0.6300

--0.

02

U-232

U-10a

19.098 4/16/2013

0.6068

0.6300

-'.:'1 .. 59:;~~'~ 9

03

U-232

U-10a

19.098 4/16/2013

0.6050

04

U-232

-----

05

U-232

06

U-232

07

U-232

U-10a

08

U-232

U-10a

09

U-232

10

U-232

11

U-232

U-232

13
14

I
!

U-232

U-232

U-10a
U-10a

0.6041

0.6300

19.098 4/16/2013

0.5991

19.098 4/16/2013

0.6016

0.6300

U-1 ,,

_j_

19.098 4/16/2013

0.6002

0.6300

U-1 Oa

19.098 4/16/2013

0.5979

0.6300

U-10a

19 098

4/16/2013

0.5993

0.6300

--(1'

l:.fi02 q

U-10a

19.098 4/16/2013

0.5998

0.6300

~~0 ll

597

U-10a

U-10a

19 098

4/16/2013

0.5945

0.6300
0.6300

19.098 4/16/2013

0.6012

0.6300

0.6300
-------

U-232

U-10a

19.0981 4/16/2013

0.5956

16

U-232

U-10a

19.0981 4/16/2013

0.5933

=~:

Printer Tapes

Matrix Spike

:3

-(i" 599:::~ -~J

-0.

-~-~~&2

0.6300

17

U-232

U-10a

19.098 4/16/2013

0.5965

0.6300

18

U-232

U-10a

19.098 4/16/2013

0;5933

0.6300

19

U-232

U-10a

1--
---

19.098 4/16/2013

0.5962

-R0

59~:+5

-0 .. 595t:.

'~

II

0.6300
-~

-~3" 5::.-~~;:~::

-0.5965

-0.5933 9

li'";li

0.000

lb ~~

1
:::;

-~:1=

596:?

Error
Estimate

0.00

0.000

0.00

0.000

~-

':l

---~--

Version 2.0 08/99

--

!~i ~5 J..3.3 ':::i

6 ~Ji~f3:
. . . o. 6fJ4 ~i.
- [1 ~

g:,

0.000

....

f--~-

m:'
.......

0.000

o.ool
o.ool

15

1 - - - - - -\--

0.001

Estimate

------

19.0981 4/16/2013

0.000

+---~f---

0.6300

0.5980

0.6300

u~

OOOi

pCi

MSD
Added
pCi

------

0.6003

i-----

i Estimate
Error

----

LCSD
Known I
Error

-;

6~).50

19.098 4/16/2013

I
I

--

0.6300

19.098 4/16/2013

1-

..

LCS

U-~

Added
pCi

'

0.6104 g

01

12

Isotope

Activity
dpm/g

Error
Estimate

8.15

Tracers -
fraction

Page 1 of 1
Printed: 4/16/2013 8:25AM

Spike and Tracer Worksheet

Eberline Analytical
Oak Ridge Laboratory

Printed: 4/16/2013 8:25AM


Page 1 of 1

Aliquot Worksheet

JBARNARD
Engineering Management Support, Inc.

Lab
Fraction
01
02

-----o3
04
_05
06
07
08
09
10
11
12
13
14
15
16
17
18
19

~-

I
....

ClientiD
LCS
BLANK
1----PZ-105-SS TOT

(..,)

Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG

PZ-105-SS TOT
PZ-105-SS DIS
S-10 TOT
S-10 DIS
LR-104 TOT
--LR-104 DIS
-DUP 01 TOT
DUP 01 DIS
DUP 02 TOT
DUP 02 DIS
FB at PZ-110-SS TOT
FB at PZ-110-SS DIS
MW-103 TOT
MW-103 DIS
PZ-200-SS TOT
PZ-200-SS DIS
---~--

Comments

Ci)~)

~~;,~,

Sample

Technician:

Dilution Data

Muffle Data
Ratio
Post/Pre

NoofDils ..

Aliquot Data

Oil Factor

Aliquot

Ratio

NetEquiv

1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.00008+00
1.0000E+OO
1.0QOOE+OO
1.0000E+OO
1:QOOOE+OO
1.0000E+OO
1.ooooe+oo
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OQ
1.0000E+OO
t.OOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO
1.00QOE+OO
1.0000E+OO
1.0000Et00
1.0000E+OO
1.ooooe+oo
1.0000E+OO
1.QOOOE+OO
1.0000E+OO
1.0000E+O.O
1.0000E+OO __-1 :.OOOOE;f.OO
1.0000E+OO
1,QQOOE+OO

H-3 Solids Only

MS Aliquot Data
Aliquot

Water Added
(ml)

NetEquiv

H3 Dist
Aliq

-----

!
-~-~-~-----

----

- -------

- -

--

I
I
--~----

-------

----- ----- ------------

---~----

---------

I
~

Date:

4j /(u, J3
I

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
01
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_018
18
System Bkgd 54576
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/19/2013
7:30:32 AM
4/19/2013 11:36:31 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.610 mL
0.1961 +/- 0.0110
0.1776 +/- 0.0033 on 12/15/2012
1.1041 +/- 0.0651

Control Certificate Name: NatU U-SA


Chern. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.271
4.726
4.406
4.151

Net
Pk Area
386.47
579.81
25.66
594.81

0.984027 +/-

AREA

0.074385

REPORT

Pk Area
Error %
9.99
8.15
38.99
8.05

1:57:26 PM

Ambient
Backgnd
1. 53
1.19
0.34
1.19

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

20.9
25.5
3.9
8.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
0.993
5302.50*
5.23E+000 +I- 5.74E-001
9.62E-002 +I- 1.05E-002
U-234
0.991
4761.50*
7.85E+000 +I- 1.07E+000
8.92E-002 +I- 9.78E-003
U-235
0.997
4385.50*
4.29E-001 +I- 1.74E-001
7.98E-002 +!- 8.75E-003
U-238
0.992
4184.40*
8.02E+000 +!- 1.09E+000
8.88E-002 +I- 9.74E-003

ftc;

t~/:1~

0000055915.CNF
Live Time :10200.000 sec
Rea1 Time :10201.000 sec
start:
1:3404.1(kev)
stop : 1024:6604.2(kev)
Acq. Start :Fri Apr 19 11:36:31 2013

60
55
50
45
40
35
V)

.j..J

s::::

:::::s

8 30

25
20
I

Oil

r,[;

15

'f

10

5
0
3500

4500

4000

5000
Energy(kev)

6000

5500

II-
~,

[.n

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

Page

5:26tl)

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10200
10201

Channell------l-------l-------l-------l-------l-------l-------1-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
3
1
1
3
4
8
9
20
21
15
0
0
0
0
0
1
1
1
0
1
0
0
0

10200
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
1
0
1
0
0
2
1
4
1
7
9
18
18
18
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
3
0
1
4
0
5
4
8
16
12
17
13
0
0
0
0
1
0
0
1
0
0
0
1
0

0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
1
0
0
1
2
0
7
4
14
21
22
7
0
0
0
0
0
0
2
0
1
2
0
2
1

1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
1
1
0
1
3
4
1
5
9
7
15
7
18
5
0
1
0
0
1
1
1
0
0
0
0
0
1

0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
2
0
1
3
3
11
4
18
24
12
4
0
0
0
0
0
0
1
0
0
0
0
2
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
2
2
5
8
4
13
16
16
3
1
0
0
0
0
1
2
0
0
1
0
1
1

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
2
2
1
0
0
1
1
2
1
1
1
0
4
8
17
12
10
3
0
1
1
0
2
0
0
0
0
3
0
0
1
~..;;

.......

~J.~C

Channel Data Report


369:

4/19/2013
0

Sample Title:

5:2~:.:1~

..,
0

Page
1

01

Channell------1-------l-------l-------l-------l-------l-------l-------l
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

3
1
2
8
6
11
13
18
17
0
0
0
0
0
0
0
1
0
0
1
0
0
0
2
4
1
9
8
12
15
4
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

2
4
1
2
11
10
15
13
13
1
0
0
0
0
0
1
0
0
0
0
0
0
1
3
0
5
3
7
8
7
9
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

4
1
2
2
8
12
21
12
13
0
0
0
0
1
0
0
0
0
0
0
0
1
0
2
1
3
6
8
7
13
11
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
2

5
6
9
13
10
13
7
0
0
0
0
0
1
0
0
0
1
0
0
3
0
2
4
5
10
13
9
10
4
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

3
5
5
2
11
15
11
24
5
0
0
0
0
0
0
0
1
0
1
1
2
1
1
2
1
6
5
7
12
4
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0

0
5
6
5
9
12
8
18
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
3
7
9
11
7
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
4
7
5
8
14
19
20
1
0
0
0
0
1
0
0
0
0
0
0
1
1
1
4
0
5
12
7
10
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
6
9
11
11
16
20
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
3
5
6
7
13
11
12
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
...,..

..

jFOoP"'!iii

tlLU!U'

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:26:33
0

Page
0

01

Channell------l-------l-------l-------l-------l-------l-------1-------l
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

BLANK
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
02
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_022
22
System Bkgd 54577
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/19/2013
7:30:32 AM
4/19/2013 11:36:32 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

0232 UU-10A
0.607 mL
0.2055 +/0. 0113
0.0029 on 12/15/2012
0.1531 +/1. 3421 +/- 0.0781

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.273
4.751
4.381
4.189

Net
Pk Area

AREA

REPORT

Pk Area
Error %

402.64
3.49
2.32
1.64

1:57:26 PM

9.79
113.53
149.12
214.83

Ambient
Backgnd
1.36
0.51
0.68
1.36

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

17.1
3.1
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.994
0.999
1. 000
1. 000

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.20E+000
4.51E-002
3.70E-002
2 .llE- 002

+1+I+1+I-

5.60E-001
5.14E-002
5.53E-002
4.54E-002

AG
tf(J.f)--/(J

MDA
(pCi/liter
8.86E-002
6.78E-002
8.99E-002
8.82E-002

+I+I+I+I-

9.54E-003
7.30E-003
9.69E-003
9.50E-003

0000055916.CNF
Live Time :10200.000 sec
Real Time :10201.000 sec
Start:
1: 3421.5 (kev)
stop : 1024:6608.8(kev)
Acq. Start :Fri Apr 19 11:36:32 2013

60
55
50
45
40
35
V)

+-'

I::
:::3

8 30

25
20
15
10
5
0
3500

4000

4500

(;tlf

....

5000
Energy(kev)

5500

6000

li'-~

fill

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

s:at~:tf

Page

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10200
10201

Channell------l-------1-------l-------l-------l-------l-------l-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
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129:
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145:
153:
161:
169:
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185:
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249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
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1
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0
0
0
0
0
0
0
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0
0
0
0

10200
0
0
0
0
0
0
0
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0
1
0
0
0
0
0
0
0
0
0
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0
0
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0
1
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0
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0
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0

G111

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Sample Title:

Page

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0

02

Channell------l-------l-------l-------l-------l-------l-------l-------1
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457:
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681:
689:
697:
705:
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721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

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11
16
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1
0
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0
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1
2
0
0
1
3
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1
3
5
16
11
11
1
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0
0
0

ii 112

Channel Data Report


801:

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Sample Title:

Page

5:26:41 tiN
0

02

Channell------l-------l-------1-------l-------l-------l-------l-------l
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-105-SS TOT-DUP
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
03
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_024
24
System Bkgd 54578
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


7:30:32 AM
4/4/2013
4/19/2013 11:36:33 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.605 mL
0. 0112
0.2017 +/0.0032 on 12/15/2012
0.1710 +/1.1795 +/0.0690

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.243
4.703
4.387
4.137
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

393.98
197.64
6.83
138.66

2:02:15 PM

Ambient
Backgnd
1. 02
1. 36
0.17
0.34

9.89
14.00
76.08
16.67

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

9.3
4.7
3.1
5.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.975
0.976
1. 000
0.984

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.19E+000
2.60E+000
1.11E-001
1.82E+000

+I+I+I+I-

5.64E-001
4.61E-001
8.52E-002
3.62E-001

MDA
(pCi/liter
8.30E-002 +/- 9.02E-003
9.02E-002 +1- 9.81E-003
6.78E-002 +I- 7.37E-003
6.27E-002 +I- 6.81E-003

1\C

'f{~r3

6114

0000055917.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
1:3411.6(kev)
Stop : 1024:6597 .O(kev)
Acq. Start : Fri Apr 19 11: 36: 33 2013

60
55
50
45
40
35
Vl

......
r:::
:::::s

8 30

25
20
15
10
5
0
3500

4000

4500

G)

5000
Energy(kev)

6000

5500

l!ln.!l-i.
J.o~~l.

Ul

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

Page

5:2fi:~'f

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------l-------l-------l-------l-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
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273:
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305:
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361:

10200
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6
3
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10200
0
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1
4
4
5
1
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1
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0
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0
1

0
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4
1
2
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0
1
0

0
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1
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9
8
3
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0
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2
3
4
3
1
3
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1
1
0
0
0
0
0
0
0
0

0
0
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1
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1
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3
1
3
4
1
0
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1
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0
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0
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0
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1
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0
1

0
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3
3
2
5
0
1
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0
1
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0
0
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1
0
0
0
1

0
0
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0
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0
oilp!;o--

.. ,-r=;,

l!i!J.J.O

Channel Data Report


369:

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0

Sample Title:

5:26;if
1

Page
1

03

Channell------l-------l-------l-------l-------l-------l-------l-------1
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569:
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601:
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633:
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681:
689:
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705:
713:
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729:
737:
745:
753:
761:
769:
777:
785:
793:

0
2
2
5
4
3
5
1
1
0
0
0
0
0
0
0
0
0
0
2
0
0
1
4
6
3
7
10
15
3
0
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1
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0
0
0
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0
1
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0
0
0
0
0
0
0
0
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0
0
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7
8
5
12
5
0
0
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0
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1
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3
3
11
11
20
11
5
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0
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0
0
0
0
0
0
0
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0

0
0
1
1
7
3
3
3
0
0
0
0
1
0
0
0
0
0
0
0
0
1
2
4
1
14
10
12
9
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
3
7
8
4
3
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
4
4
2
14
10
8
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

1
1
2
2
5
4
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
2
3
12
14
12
9
1
0
0
0
0
0
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0
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0
0
0
1
0
0
0
0
0
0
0
0
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0
1
2
3
3
9
9
3
0
0
0
0
1
0
0
0
0
0
1
0
2
1
3
3
10
8
12
10
5
0
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0
0
0
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1
1
4
6
8
5
5
1
0
0
0
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0
0
0
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1
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0
0
3
1
2
3
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4
12
5
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1
2
3
2
0
5
3
0
0
0
0
0
1
1
0
0
0
0
0
0
1
0
1
4
7
6
9
14
6
0
0
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0
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0
0
.A. .,;i

..!"~'a

t\U l. l

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801:

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Sample Title:

5:26:51
0

Page
0

03

Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
817:
825:
833:
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849:
857:
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881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
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0
0
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0
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0
0
0
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0
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0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

tillS

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-105-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
04
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_025
25
System Bkgd 54579
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:36:34 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.598 mL
0.2107 +/- 0. 0115
0.1736 +/- 0.0032 on 12/15/2012
1.2142 +/- 0.0702

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.287
4.736
4.362
4.166
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

406.81
207.98
7.00
130.66

9.73
13.63
79.20
17.17

1:57:27 PM

Ambient
Backgnd
1.19
1. 02
0.00
0.34

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

4.8
10.4
3.1
13.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.995
0.996
0.998

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.13E+000 +I- 5.50E-001
2.62E+000 +/- 4.55E-001
1.09E-001 +I- 8.69E-002
1.64E+000 +I- 3.32E-001

MDA
(pCi/liter
8.30E-002 +!- 8.91E-003
7.94E-002 +/- 8.52E-003
9.32E-002 +I- 1. OOE- 002
6.00E-002 +I- 6.43E-003

AG
tf(JJ/t!;

8119

0000055918.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
start:
1 3405.9(kev)
stop : 1024 6615.8(kev)
Acq. start Fri Apr 19 11:36:34 2013

60
55
50
45
40
35
VI
.j-J

c:

::::s

8 30

25
20
15
10
5
0
3500

4000

4500

Q;)

5000
Energy(kev)

5500

6000

......
M

(i)

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

Page

4/19/2013

*******************************************************
S P E C T R A L
R E P 0 R T
*****
DATA
*****
*******************************************************
Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
9:
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10200
0
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0
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5
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0
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1

Channel Data Report


369:

4/19/2013
0

Sample Title:

Page

5:~&ti~-

04

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1
1
0
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3
9
12
17
4
0
0
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0
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0
0
0
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1
0
0
2
0
4
10
6
2
0
0
0
0
0
0
0
0
0
0
0
0
1
2
2
1
3
5
9
11
18
0
0
0
0
0
1
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0
0
1
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0
0
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0
0
0
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0
0

0
2
2
1
0
4
6
7
4
0
0
0
0
0
1
0
0
0
0
0
1
0
1
2
0
1
3
14
7
9
0
0
0
0
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0
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0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

1
0
1
2
1
5
5
8
1
0
1
0
0
0
0
0
0
0
0
0
1
0
1
2
2
3
8
14
15
29
0
0
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1
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0
0
0
0
0
0
1
0
1
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0
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0
1
0
1
3
5
5
13
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
1
4
2
10
19
11
0
0
0
0
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0
0
0
0
0
0
0
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0
0
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0
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0
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0

1
1
1
1
5
9
5
5
0
0
0
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0
0
0
0
1
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0
0
0
0
2
2
1
2
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16
21
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1
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0
1
3
3
3
5
6
11
1
0
0
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0
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24
9
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0
fl-Mi

,t=;;.~

~ll:L

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:2itl~

Page
0

04

Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
817:
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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
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0
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0
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0
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0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
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0
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0
0
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0
0
0
0
0
0
0
0
0
0

i123

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-105-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
05
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_027
27
System Bkgd 54580
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:36:35 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.600 mL
0.2171 +/- 0.0117
0.1728 +/- 0.0032 on 12/15/2012
1.2570 +/- 0.0718

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.290
4.740
4.394
4.158
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

420.81
211.32
5.32
116.47

2:27:41 PM

Ambient
Backgnd
1.19
0.68
0.68
1.53

9.57
13.51
91.11
18.30

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

23.5
22.0
3.2
5.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.999
0.997
0.999
0.995

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+000
2.58E+000
8.02E-002
1.42E+000

+I+I+I+I-

5.45E-001
4.43E-001
7.36E-002
3.00E-001

ftG

'f/.J~/13

MDA
(pCi/liter
8.06E-002 +/- 8.53E-003
6.90E-002 +I- 7.30E-003
8.51E-002 +I- 9.00E-003
8.65E-002 +/- 9.16E-003

0000055919.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
1:3402 .4(kev)
stop : 1024:6658 .l(kev)
Acq. Start :Fri Apr 19 11:36:35 2013

60
55
50
45
40

35
Vl

......
s::::
::::s

8 30

25
20
15
10
5
0

3500

4000

4500

(;i!J

......

M
Ul

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

4/19/2013

Page

5:27:0.,. Wf

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------1-------l-------l-------l-------l-------l-------l-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
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153:
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249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
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10200
0
0
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2
3
2
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1

10200
0
0
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0
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0
0
0
0
0
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1
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2
0
2
4
6
0
0
1
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0
0
0
1
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0
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0
0
1

0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
2
1
0
1
8
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
3
6
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
4
5
1
0
0
0
0
0
0
1
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
3
5
2
11
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
2
4
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
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0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
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0
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2
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0
0
0
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0
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0
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0
0
0

6126

Channel Data Report


369:

4/19/2013
0

Sample Title:

5:2"1': ...
0

..,
0

Page
0

05

Channell------l-------l-------l-------l-------l-------l-------l-------1
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649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
1
4
4
6
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
3
4
5
13
20
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
3
5
2
9
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
13
8
16
7
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
1
1
7
10
4
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
1
1
3
13
7
16
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
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0

0
1
1
3
4
4
14
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
7
14
9
22
1
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0
0
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5
12
0
0
0
0
0
0
0
0
0
0
0
1
1
0
2
0
1
2
7
11
23
28
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
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0
0
1
3
6
11
16
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
2
9
1
19
21
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
5
9
9
11
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
4
1
12
8
13
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
1
2
3
4
12
0
0
0
0
0
0
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7
5
5
20
13
0
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1
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
~..-_,.,.,.l="'lll;

ali/

Channel Data Report


801:

4/19/2013
0

Sample Title:

5: 3"JJ ...
0

Page
0

05

Channell------l-------l-------l-------l-------1-------l-------l-------l
809:
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897:
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921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
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1
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0
0
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0
0
0

i12S

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

S-10 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
06
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_029
29
System Bkgd 54581
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +I- O.OOOE+OOO liter


7:30:32 AM
4/4/2013
4/19/2013 11:36:36 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.604 mL
0.1969 +/- 0. OllO
0.1945 +/- 0.0036 on 12/15/2012
1.0121 +/- 0.0597

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.287
4.741
4.408
4.178
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

383.98
17.00
1. 66
17.98

2:30:02 PM

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

1. 02
0.00
0.34
1. 02

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

10.02
48.92
169.38
47.73

19.0
3.1
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.997
0.996
1. 000

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.18E+000
2.29E-001
2.76E-002
2.41E-001

+1+I+I+1-

5.69E-001
1.15E-001
4.69E-002
1.18E- 001

ltG

1//J3

MDA
(pCi/liter
8.50E-002
8.09E-002
7.95E-002
8.46E-002

+I+I+I+I-

9.34E-003
8.88E-003
8.74E-003
9.29E-003

0000055920.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
start:
1: 3413 .5 (kev)
stop : 1024:6597. S(kev)
Acq. Start :Fri Apr 19 11:36:36 2013

60
55
50
45
40
35
V'l

+-'
s::::
:::J

8 30

25
20
15
10
5
0
3500

4000

4500

Jl<l!)

......
w

~)

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

4/19/2013

s:27t41

11

Page

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

06

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------l-------l-------l-------l-------l-------l
1:
9:
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10200
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10200
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0
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0
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0
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0
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0
.......

-rq, ...

lJLL:U

Channel Data Report


369:

4/19/2013
0

Sample Title:

5:2'7;J.
0

Page
0

06

Channell------l-------l-------l-------l-------l-------l-------l-------1
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721:
729:
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769:
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793:

0
0
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1
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1
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0
0
2
4
7
13
14
15
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
1
0
1
0
1
1
1
0
0
1
0
0
0
2
3
6
9
11
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
2
5
10
8
7
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
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1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
3
0
5
7
12
21
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0
0
0
0
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0
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1
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0
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1
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1
3
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8
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20
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1
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1
0
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1
1
1
7
11
15
23
0
0
0
1
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0
0
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1
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9
11
6
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0
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22
13
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1
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0
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0
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0
0
0
0
0

6132

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:27:2. tliM
0

06

Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
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857:
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897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
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0
0
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0
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0
0
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0
0
0
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0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
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0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

5133

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

S-10 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
07
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_033
04026479A
91132
System Bkgd 54582
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +!- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:43 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.599 mL
0.1484 +/- 0.0094
0.1825 +/- 0.0032 on 12/16/2012
0.8132 +/0.0535

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.292
4.757
4.356
4.163
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

287.00
7.00
0.83
5.00

5:49:18 PM

Ambient
Backgnd

11.59
79.20
239.53
96.02

0.00
0.00
0.17
0.00

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

23.8
4.5
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.999
1. 000
0.994
0.997

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.14E+000
1.25E-001
1.83E-002
8.91E-002

+I+!+I+I-

6.39E-001
1. OOE-001
4.39E-002
8.62E-002

A(,

~;)){tJ

MDA
(pCi/liter
1.07E-001
1.07E-001
9.21E-002
1. 07E-001

+I+I+I+!-

1.33E-002
1.33E-002
1.15E-002
1.33E-002

0000055930.CNF
Live Time 10200.000 sec
Rea1 Time 10215 .400 sec
Start:
1 3465.6(kev)
stop : 1024 6503.3(kev)
Acq. Start Fri Apr 19 11:57:43 2013

60
55
50
45
40
35
Vl

.......
r::::
::::s

8 30

25
20
15
10
5
0

3500

4000

4500

~,

......
Jl,.)
!.J~

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

4/19/2013

5:27:31

..

Page

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10200
10215

Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
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1
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"" .

~.!.

Channel Data Report


369:

4/19/2013
0

Sample Title:

5: 2,t); ' '


0

Page
0

07

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Channel Data Report


801:

4/19/2013
0

Sample Title:

5:2?:)f

Page

!
0

07

Channell------l-------l-------l-------l-------l-------l-------l-------1
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937:
945:
953:
961:
969:
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985:
993:
1001:
1009:
1017:

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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-104 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
08
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_034
04026479B
91136
System Bkgd 54583
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:45 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.602 mL
0.2188 +/- 0. 0117
0.1856 +/- 0.0032 on 12/16/2012
1.1788 +/- 0.0666

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.274
4.728
4.415
4.155

Net
Pk Area
424.83
213.83
11.00
174.66

AREA

5:49:43 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

9.51
13.41
61.72
14.85

0.17
0.17
0.00
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

32.2
15.1
5.9
7.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.994
0.992
0.994
0.994

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.16E+000
2.60E+000
1.65E-001
2 .11E+000

+!+!+I+I-

5.43E-001
4.42E-001
1.03E-001
3.84E-001

MDA
(pCi/liter
5.07E-002
5.07E-002
8.98E-002
5.78E-002

+I+I+!+I-

5.33E-003
5.33E-003
9.45E-003
6.08E-003

AG
1/)J/13

6135

0000055931.CNF
Live Time :10200.000 sec
Real Time :10215.400 sec
start:
1:3439.1(kev)
stop : 1024:6479.9(kev)
Acq. Start :Fri Apr 19 11:57:45 2013

60
55
50
45
40
35
VI

.......
c

:::3

8 30

25
20
15
10
5
0

3500

4000

4500

t~)

5000
Energy(kev)

6000

5500

jiw;o~i.

,g:~

r.:u

ROI Type: 1

ROI Type: 3

Channel Data Report

4/19/2013

5:2?Jfj

..

Page

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

10200
10215

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51d1

Channel Data Report


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Sample Title:

S:3!7;i4
0

"
0

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1

ild2

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:27:jf
0

Page

i!tf
0

08

Channell------l-------l-------l-------l-------l-------l-------l-------1
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0
0
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0
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0
0
0
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0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-104 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
09
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_035
04026477A
58771
System Bkgd 54584
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


7:30:32 AM
4/4/2013
4/19/2013 11:57:40 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.600 mL
0.2261 +/0.0120
0.1826 +/- 0.0032 on 12/16/2012
1. 2381 +I- 0.0692

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.308
4.757
4.391
4.186
T

Net
Pk Area
438.00
231.66
11.00
165.83

AREA

5:49:42 PM

REPORT
FWHM
(keV)

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

9.38
12.89
61.72
15.23

0.00
0.34
0.00
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

30.0
5.9
2.9
7.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

1. 000
1. 000
1.000
1. 000

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+000 +I- 5.35E-001
2.72E+000 +I- 4.51E-001
1.59E-001 +/- 9.98E-002
1.94E+000 +I- 3.58E-001

AG

til :J)-/13

MDA
(pCi/liter
7.05E-002
5.62E-002
8.69E-002
4.88E-002

+I+I+I+I-

7.33E-003
5.84E-003
9.04E-003
5.08E-003

0000055932.CNF
Live Time 10200.000 sec
Real Time 10215.300 sec
Start:
1 3463 .4(kev)
stop : 1024 6473.5(kev)
Acq. start Fri Apr 19 11:57:40 2013

60
55
50
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40
35
Vl

......
s::::

:::s

8 30

25
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15
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5
0

3500

4000

4500

caa

5000
Energy(kev)

5500

6000

~-~

til
Ul

ROI Type: 1

ROI Type: 3

Channel Data Report

4/19/2013

Page

5:27:52 PM

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10200
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-*""*

~i4b

Channel Data Report


369:

4/19/2013
0

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S:i'iiiJ
0

..
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*'"''"" -~
WliJI

Channel Data Report


801:

4/19/2013
0

Sample Title:

s~t~'''
0

Page

W
0

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fii148

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

DUP 01 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
10
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_037
04026478A
91133
System Bkgd 54585
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:41 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.598 mL
0.2357 +/- 0.0123
0.1783 +/- 0.0033 on 1/26/2013
1.3222 +/- 0.0733

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.284
4.749
4.406
4.165

Net
Pk Area

AREA

REPORT

Pk Area
Error %

455.00
22.66
0.83
10.83

3:28:25 PM

9.20
41.53
239.53
60.10

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.00
0.34
0.17
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

38.2
2.9
2.9
2.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.999
0.997
0.997

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.13E+000
2.55E-001
1.15E-002
1.21E-001

+I+I+!+!-

5.25E-001
1. 09E-001
2.76E-002
7.40E-002

MDA
(pCi/liter
6.76E-002 +I5.38E-002 +I5.80E-002 +I4.68E-002 +/-

6.92E-003
5.52E-003
5.94E-003
4.79E-003

JICi
t!/J~/3

6149

0000055933.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
start:
1 3463. 5(kev)
stop : 1024 6468.S(kev)
Acq. start Fri Apr 19 11:57:41 2013

60
55
50
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40
35
V)

.f-1

s:::::

::::s

8 30

25
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3500

...c:n

4000

4500

5000
Energy(kev)

5500

6000

u~

c:n

ROI Type: 1

ROI Type: 3

Channel Data Report

4/19/2013

Page

5:28: tit

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10200
10215

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OR<

..

~-""

~l.::li

Channel Data Report


369:

4/19/2013
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5:28:00
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PM
0

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1
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0
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9
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0
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6
5
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16
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0
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19
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~_,.;;~~

!lLl :l

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:28s81
0

ttl
0

Page
0

10

Channell------l-------l-------l-------l-------l-------l-------l-------1
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84 9:
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93 7:
94 5:
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0
1
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8153

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

DUP 01 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
11
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_040
06027396B
91135
System Bkgd 54586
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:49 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.599 mL
0.1906 +/- 0.0109
0.1900 +/- 0.0033 on 12/16/2012
1. 0034 +I- 0.0597

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.274
4.732
4.365
4.142
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

368.83
14.66
2.00
10.32

5:49:33 PM

10.21
51.88
169.74
63.32

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

0.17
0.34
0.00
0.68

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

70.0
3.0
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.994
0.994
0.997
0.987

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.14E+000
2.04E-001
3.44E-002
1.43E-001

+1+1+I+I-

5.74E-001
1.08E-001
5.84E-002
9.20E-002

MDA
(pCi/liter
5.81E-002
6.66E-002
1. 03E-001
7.82E-002

+!+1+I+I-

6.49E-003
7.43E-003
1.15E-002
8.73E-003

N;

1(~/t!J

ii15ii

0000055934.CNF
Live Time :10200.000 sec
Rea1 Time :10215. 400 sec
start:
1:3459.0(kev)
stop : 1024:6497.3(kev)
Acq. Start :Fri Apr 19 11:57:49 2013

60
55
50
45
40
35
VI
.j...J

c:

::::l

8 30

25
20

15
10
5

0 ~3~50~0~-L~~~~~ll__L~~~~~JL-L:~~L_~~~_L~~L-~4--L-L~--~
6500
4000
4500
5000
5500
6000
Energy(kev)

l<J!)
II-

01

01

ROI Type: 1

ROI Type: 3

Channel Data Report

4/19/2013

Page

5:28:J.). WI

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

10200
10215

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....

~1

Channel Data Report


369:

4/19/2013
0

Sample Title:

Page

5:28:11 Wl
0

11

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6157

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:28:1!.. JIM
0

11

Channell------l-------l-------l-------l-------l-------l-------l-------1
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817:
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889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
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0
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0
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0
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-6158

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

DUP 02 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
12
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_041
05026930A
91087
System Bkgd 54587
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:46 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.600 mL
0.1888 +/- 0.0108
0.1978 +/- 0.0034 on 12/16/2012
0.9545 +/- 0.0570

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.287
4.733
4.411
4.166

Net
Pk Area

AREA

REPORT

Pk Area
Error %

365.66
11.32
0.32
7.45

5:49:31 PM

10.26
60.27
646.93
84.98

Ambient
Backgnd
0.34
0.68
0.68
2.55

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

24.3
3.0
3.0
4.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.994
0.995
0.998

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.14E+000
1.59E-001
5.55E-003
1.04E-001

+I+!+I+!-

5.76E-001
9.76E-002
3.59E-002
8.94E-002

AG

l(/JJ/13

MDA
(pCi/liter
6.72E-002
7.93E-002
9.78E-002
1.17E-001

+!+I+!+I-

7.53E-003
8.88E-003
1.10E-002
1.32E-002

0000055936.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
start:
1 3452.7(kev)
stop : 1024 6506.6(kev)
Acq. Start Fri Apr 19 11:57:46 2013

60
55
50
45
40
35
V)

.......
s:::

:::s

8 30

25
20
15
10
5
0

3500

4000

4500

~,

5000
Energy(kev)

5500

6000

....t

tn

tn

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

Page

"S:!I:2e PM

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

12

Elapsed Live time:


Elapsed Real Time:

10200
10215

Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
9:
17:
25:
33:
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49:
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257:
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281:
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297:
305:
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361:

0
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6161

Channel Data Report


369:

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0

Sample Title:

5:2SsH
0

Page

ttt
0

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,;11#:;. -IIi

..,...... -F'

UI !bi

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:28:28 tiN
0

12

Channell------l-------l-------l-------l-------l-------l-------l-------1
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rii 163

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

DUP 02 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
13
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_042
05026930B
84185
System Bkgd 54588
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013 11:57:47 AM
170.0 minutes
170.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.601 mL
0.1899 +/- 0.0108
0.1846 +/- 0.0032 on 12/16/2012
1.0284 +/- 0.0613

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.283
4.731
4.435
4.164
T

Net
Pk Area
368.49
12.66
6.83
9.49

AREA

5:49:29 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

10.22
55.94
76.08
65.59

0.51
0.34
0.17
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

4.6
3.0
3.0
4.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.997
0.993
0.983
0.997

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+000
1. 77E-001
1.18E-001
1.32E-001

+1+1+I+I-

5.76E-001
1. 01E-001
9.06E-002
8.79E-002

k;

1(/13>

MDA
(pCi/liter
7.34E-002
6.69E-002
7.20E-002
7.31E-002

+I+I+I+I-

8.20E-003
7.47E-003
8.04E-003
8.16E-003

0000055937.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
1 3450.2(kev)
Start:
stop : 1024 6505. 5(kev)
Acq. Start Fri Apr 19 11:57:47 2013

60+
55

50
45
40
35
VI
.j...J

c:

::::s

8 30

25
20
15
10
5
0

3500

4000

4500

~)

5000
Energy(kev)

5500

6000

il'~~

till

Ul

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

5:lliii

Page

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10200
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9166

Channel Data Report


369:

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Sample Title:

5:2!1:26
0

Page

PM
0

13

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~""~~

U!.iD/

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:29:26
1

Page

13

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8168

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

FB AT PZ-110-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000560
1304051A-UU
14
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_003
3

System Bkgd 54570


<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013
2:33:37 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.595 mL
0.2522 +!- 0.0129
0.1746 +/0.0033 on 12/15/2012 11:26:47 AM
1.4440 +/- 0.0784

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.286
4.750
4. 396
4.149
T

Net
Pk Area
483.98
1.49
2.66
-0.68

AREA

REPORT

Pk Area
Error %
8.92
190.03
128.85
304.42

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

1. 02
0.51
0.34
0.68

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

31.9
3.0
3.0
0.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.998
0.999
0.999
0.991

5302.50*
4761.50*
4385.50*
4184.40*

5.10E+000
1.57E-002
3.45E-002
-7.13E-003

+!+I+I+I-

5.10E-001
2.98E-002
4.46E-002
2.17E-002

AG
tt!J~/f!>

6.64E-002
5.52E-002
6.21E-002
5.91E-002

+!+!+I+!-

6.63E-003
5.52E-003
6.21E-003
5.91E-003

0000056095.CNF
Live Time 10201.000 sec
Real Time 10201. 000 sec
start:
1 3498.4~kev~
stop : 1024 6549.5 kev
Acq. Start Fri Apr 19 14:33:37 2013

60+
55

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Vl

......
c

8 30
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...

1!:'0:~
~

~~~
(!~

4000

4500
ROI Type: 1

5000
Energy(kev)

5500
ROI Type: 3

6000

6500

Channel Data Report

4/19/2013

s:29;U

Page

*******************************************************
S P E C T R A L
R E P 0 R T
*****
DATA
*****
*******************************************************
Sample Title:

14

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Elapsed Real Time:

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8172

Channel Data Report


801:

4/19/2013
0

Sample Title:

5:29:1,
0

Page
0

14

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1
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0
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1
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0
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

FB AT PZ-110-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
15
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_004
4

System Bkgd 54571


<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/4/2013
7:30:32 AM
4/19/2013
2:33:38 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.596 mL
0.1778 +/- 0.0105
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
0.9162 +/- 0.0565

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.286
4.692
4.324
4.134

Net
Pk Area
341.81
2.96
-0.19
-0.85

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

10.62
153 .11
1131.2
246.69

1.19
2.04
1.19
0.85

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

21.8
2.9
2.9
0.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.967
0.974
0.982

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.11E+000
4.42E-002
-3.50E-003
-1.26E-002

+I+I+1+I-

5.89E-001
6.79E-002
3.96E-002
3.12E-002

MDA
(pCi/liter
9.84E-002
1.16E-001
1.21E-001
8.90E-002

+!+I+I+I-

1.14E-002
1.34E-002
1.40E-002
1.03E-002

/:JZ/13

fi17ii

0000055943.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
Start:
1 3493 .1(kev)
stop : 1024 6486. 9(kev)
Acq. Start Fri Apr 19 14:33:38 2013

55
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40
35
VI
.j..J

r::::

::::l

8 30

25
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0
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I

4000

4500

~,

5000
Energy(kev)

5500

6000

~~>~~

"'"'J

U1

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

4/19/2013

s:a9i

Page

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

15

Elapsed Live time:


Elapsed Real Time:

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10200

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G176

Channel Data Report


369:

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5:29:52 PM
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15

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1
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1
2
8
5
12
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0
0
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1
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5
9
15
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0
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0
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1
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11
7
22
0
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0
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1
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0

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:29:52 PM
0

15

Channell------l-------l-------l-------l-------l-------l-------l-------1
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0
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0
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0
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0
0
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0
0
0
0
1
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

MW-103 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
16
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_010
10
System Bkgd 54572
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/5/2013
7:30:32 AM
4/19/2013
2:33:33 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.593 mL
0.1786 +/- 0.0105
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
0.9080 +!- 0.0560

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.282
4.730
4.398
4.145
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

342.13
273.79
20.32
251.15

Ambient
Backgnd

10.63
11.90
44.32
12.39

1. 87
2.21
0.68
0.85

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

17.1
23.8
2.9
15.3

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------'
U-232
U-234
U-235
U-238

0.997
0.993
0.999
0.989

5302.50*
4761.50*
4385.50*
4184.40*

5.09E+000
4.07E+000
3. 73E-001
3.72E+000

+I+I+I+!-

5.87E-001
6.75E-001
1.71E-001
6.30E-001

1.13E-001
1.19E- 001
1. 03E- 001
8.86E-002

+I+I+I+I-

1.30E-002
1.37E-002
1.19E-002
1.02E-002

A6.
'f/:J:>/13

i179

0000055938.CNF
Live Time :10201.000 sec
Rea1 Time :10201.000 sec
start:
1:3505.7(kev)
stop : 1024:6498.0(kev)
Acq. Start :Fri Apr 19 14:33:33 2013

60
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V'l

........
s:::
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8 30

25
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10
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5500

6000

!!-~~o4l

(0

G)

ROI Type: 1

!l

ROI Type: 3

!!

I II!!

'

6500

Channel Data Report

4/19/2013

5:31:8C

Page

*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

16

Elapsed Live time:


Elapsed Real Time:

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iil1H

Channel Data Report


369:

4/19/2013
0

Sample Title:

5:31:0~

Page

9M
1

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2
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2
2
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2
6
5
11
1
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5
12
9
9
3
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4
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3
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9
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5
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i1

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:3l:OC tiN
0

16

Channell------l-------l-------l-------l-------l-------l-------l-------1
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0
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0
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0
0
0
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0
0
0
0
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0
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0
0
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0
0
1
0
0
0
0
0
0
0

ii183

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

MW-103 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\OOOO 559
1304051A-UU
17
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_Oll
11

System Bkgd 54573


<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/5/2013
7:30:32 AM
4/19/2013
2:33:34 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.596 mL
0.1849 +/- 0.0107
0.1973 +/- 0.0042 on 12/15/2012 11:28:06
0.9369 +1- 0.0577

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

10.41
13.20
52.27
13.56

1. 02

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

FWHM
(keV)

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.277
4.731
4.407
4.150

355.98
220.83
15.00
209.98

0.17
0.00
1. 02

17.3
15.
2.
9.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Id

------;~~~~~------------~~~~~~~~------------------

'
MDA

-~~;;;~~---~~;;~----~;~;:~~:---~:~~~:~~~~~~~~~=~~~=~~~---;:~~~~~~~~~~~~;-~~;;=~~;
U-234
U-235
U-238

0.993
0.997
0.992

4761.50*
4385.50*
4184.40*

3.17E+000 +/- 5.52E-001


2.66E-001 +/- 1.42E-001
3.00E+000 +/- 5.31E-001

5.99E-002 +/- 6.80E-003


1.06E-001 +/- 1.20E-002
9.01E-002 +/- 1.02E-002

iiSA.

0000055939.CNF
Live Time :10200.000 sec
Rea1 Time :10201.000 sec
start:
1:3645. S(kev)
stop : 1024:6374.2(kev)
Acq. Start :Fri Apr 19 14:33:34 2013

60
55
50
45
40
35
Vl
.j..J

s::::

::::l

8 30

25
20

15
10
5
0

II

!!

Ill

O!!l!!lr~;\o!ll'"!lld!

!\

ll"'l it"i'

1'1"

4000

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4500

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5000
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'I

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fl!

5500

6000

~~--

c:o
m

ROI Type: 1

ROI Type: 3

!I

!Jl!

Channel Data Report

4/19/2013

5:3l.:Jj

,.

Page

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

17

Elapsed Live time:


Elapsed Real Time:

10200
10201

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6
3
7
4
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
1
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
1
2
1
8
4
5
5
3
1
0
0
0
1
0
1
0
0
0
0
0
1
0
0
0
0
1
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
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2
1
2
1
3
3
4
1
8
2
2
0
1
1
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0

0
0
0
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0
0
0
0
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0
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0
0
0
0
1
0
1
0
1
5
1
5
9
2
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
1
0
2
3
5
3
0
0
0
0
1
1
1
0
0
0
0
0
0
0
0
1
0
2
1

-----1
0
0
0
0
1
0
0
0
0
0
0
0
0
2
0
0
0
1
1
0
0
3
2
6
6
8
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
1
0

6185

Channel Data Report


369:

4/19/2013
0

Sample Title:

5:31:25
1

Page

PM
1

0
2
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9
12
4
0
0
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0
1
0
0
0
0
0
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0
0
0
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0
0
0
0
0

4
2
4
2
9
4
4
0
0
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0
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2
0
0
0
0
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0
0
0
1
4
2
2
3
6
9
10
11
5
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0

17

Channell------l-------1-------l-------l-------l-------l-------l377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
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545:
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569:
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721:
729:
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761:
769:
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793:

1
1
3
0
3
6
8
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
3
2
6
11
8
13
1
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
3
3
5
7
5
1
1
0
0
0
0
0
0
1
1
0
0
0
0
0
1
0
0
0
4
1
3
3
7
6
11
2
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
4
3
4
8
4
2
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
2
1
2
1
0
4
3
6
8
8
3
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0

2
2
4
4
6
4
2
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
1
5
3
8
7
4
4
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
2
2
7
11
3
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
2
1
2
0
5
3
9
13
18
5
2
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

-----1
0
2
3
5
7
5
3
0
0
0
0
0
0
0
0
1
0
0
1
0
0
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1
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0
0
0
0
1
0
0
0
0

&187

Channel Data Report


801:

4/19/2013
0

Sample Title:

Page

5:31~"
0

17

Channell------l-------l-------1-------l-------l-------l-------l- -----1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
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0
0
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0
0
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0
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0
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0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
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0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
0
0
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0
0
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0
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0
0
0
0
0
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0
0
0
0

6188

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-200-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\OOOO 559
1304051A-UU
18
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_013
13
System Bkgd 54574
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/5/2013
7:30:32 AM
4/19/2013
2:33:35 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

U232 UU-10A
0.593 mL
0.1967 +/- 0.0111
0.1869 +/- 0.0035 on 12/15/2012 11:26:45
1.0527 +/- 0.0626

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

1.19
0.85
0.17
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.282
4.738
4.435
4.160

376.81
40.15
3.83
38.83

10.12
31.31
102.72
31.53

5.2
4.7
2.8
3.3

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.997
0.996
0.983
0.996

5302.50*
4761.50*
4385.50*
4184.40*

5.09E+000
5.42E-001
6.38E-002
5.22E-001

+I+I+I+I-

5.63E-001
1.80E-001
6.59E-002
1. 74E-001

8.89E-002
8.08E-002
6.95E-002
5.61E-002

+I+!+!+I-

9.85E-003
8.95E-003
7.70E-003
6.21E-003

fr;

1/dJ((J
ii18S

0000055940.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
Start:
1 3547.5(kev)
stop : 1024 6438.1(kev)
Acq. Start Fri Apr 19 14:33:35 2013

60
55
50
45
40
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V)

+-'
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8 30
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10

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Channel Data Report

4/19/2013

~'

Page

*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:

18

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------l-------1-------l-- -----1
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
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185:
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257:
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281:
289:
297:
305:
313:
321:
329:
337:
345:
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361:

10200
0
0
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0
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0
2
2
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10200
0
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0
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2
1
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0
0
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0
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0
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0
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"'""-

...

~l::IJ.

Channel Data Report


801:

4/19/2013
1

Sample Title:

5:3JJJi
0

...
0

Page
0

18

Channell------l-------1-------l-------l-------l-------l-------l809:
817:
825:
833:
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897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
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0
0
0
0
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1
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0

0
0
0
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0
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0
0
0
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0
0
0
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0

0
0
0
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0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

-----1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-200-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
19
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_014
14
System Bkgd 54575
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+000 +/- O.OOOE+OOO liter


4/5/2013
7:30:32 AM
4/19/2013
2:33:36 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:

0232 UU-10A
0.596 mL
0.2020 +!- 0.0113
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.0945 +/- 0.0644

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.280
4.724
4.364
4.160

Net
Pk Area

AREA

REPORT

Pk Area
Error %

388.79
40.47
2.32
44.66

9.97
31.48
149.12
29.46

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

2.21
1.53
0.68
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

11.2
3.7
2.9
3.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.996
0.990
0.997
0.996

5302.50*
4761.50*
4385.50*
4184.40*

5.11E+000
5.32E-001
3.76E-002
5.84E-001

+I+!+!+1-

5.60E-001
1. 77E-001
5.62E-002
1.84E-001

1\-(i

J/1~13

1. 05E-001
9.34E-002
9.15E-002
6.26E-002

+!+!+!+I-

1.15E-002
1.02E-002
1.00E-002
6.85E-003

0000055941.CNF
Live Time 10200.000 sec
Rea1 Time 10200.000 sec
1 3507. 9(kev)
Start:
stop : 1024 6512.2(kev)
Acq. Start Fri Apr 19 14:33:36 2013

60+
55

50
45
40

35
V)

.j-1

c::

:::::s

8 30

25
20
15
10
5
0

4000

4500

II:!~

5000
Energy(kev)

5500

6000

6500

j!.o>IDi>

lj;J)

Ul

ROI Type: 1

ROI Type: 3

Channel Data Report

4/19/2013

5:32:43

Page

PM

*******************************************************
s p E C T R A L DATA R E P 0 R T
*****
*****
*******************************************************
Sample Title:

19

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
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17:
25:
33:
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49:
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65:
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185:
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257:
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289:
297:
305:
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10200
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4
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10200
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
3
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
2
0
2
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
2
1
1
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
u.t;:,tJ
W1'lo ..

""""""

Channel Data Report


369:

4/19/2013
1

Sample Title:

5:32:43
0

Page

19

Channell------l-------1-------l-------l-------l-------l-------l-------l
377:
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705:
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737:
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769:
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785:
793:

0
0
0
0
2
1
3
0
0
0
0
0
0
0
1
0
0
0
0
1
2
0
1
1
0
2
0
9
10
11
14
2
0
0
0
0
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1
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

1
0
0
0
0
1
0
2
0
0
0
0
0
0
0
1
1
0
0
1
1
1
1
2
3
1
3
5
5
11
18
0
0
0
0
0
0
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0
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0
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0
0
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1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
2
3
1
3
8
16
10
0
0
0
0
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0
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0
0
0
0
0
0
0
0
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0
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1
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1
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1
2
2
14
4
17
13
1
0
0
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0
0
0
0
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0
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0
0
0
0
0
0
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0
2
1
0
1
2
3
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
2
2
7
5
8
17
13
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
3
1
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
1
1
5
1
9
7
12
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

1
2
1
0
0
0
3
0
0
0
0
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0
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0
0
0
0
0
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1
2
0
2
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2
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14
5
9
7
0
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0
0
2
1
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2
0
1
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4
8
6
21
2
0
0
1
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0
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0
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0
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0
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0

6197

Channel Data Report


801:

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0

Sample Title:

5:32;4;t
0

Page
0

19

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1017:

0
0
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1
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0
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0
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1
1
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0

ii1SS

Page 1 of 2
4/19/2013 5:45:48 AM

QA SUMMARY REPORT

Review Of QA Results - Pulser Check


Date
Time

: 4/19/2013
: 5:45:48 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042

DEVICE
2lf
2lf
2lf
21f
2lf
21f
21f
21f
21f
2lf
2lf
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha Analyst!OODC
Alpha Analyst!OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Not Done
Not Done
Passed
Passed
Passed

DATE

4/19/2013 5:25:30 AM
4119/2013 5:25:31 AM

4/19/2013 5:25:31 AM
4/19/2013 5:25:32 AM
4/19/2013 5:25:33 AM
4/19/2013 5:25:34 AM

4119/2013 5:25:35 AM

4119/2013 5:25:35 AM
4/19/2013 5:25:36 AM
4/19/2013 5:25:37 AM
4119/2013 5:25:38 AM
4119/2013 5:25:39 AM

4119/2013 5:25:40 AM
4/19/2013 5:25:41 AM
4/19/2013 5:25:43 AM
4119/2013 5:25:44 AM

4119/2013 5:25:46 AM
4/19/2013 5:25:47 AM
4/19/2013 5:25:49 AM

Page 2 of 2

Review of QA Results - Pulser Check


4/19/2013 5:45:48 AM

CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

DEVICE
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst100DC
Alpha Analyst 1OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL

APPROVED BY:

APPROVAL DATE:

FLAG
Not Done
Passed
Not Done
Passed
Passed
Passed

DATE
4119/2013 5:25:50 AM
4/19/2013 5:25:52 AM
4/19/2013 5:25:53 AM
4119/2013 5:25:55 AM

6/12/12

Library Listing Report

Page

12:17:04 PM

*************************************************************************
*****
LIBRARY LISTING REPORT
*****
*************************************************************************
Nuclide Library Title:

Uranium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

U-232
U-234
U-235
U-238

2.174E+009
7.731E+012
2.221E+016
1. 410E+017

* =

Energy
(keV )

U-232,-234,-235,-238
Energy
uncert. {keV
0.000
0.000
0.000
0.000

5302.500*
4761. 500*
4385.500*
4184.400*

Yield
( %)

99.8000
99.8000
80.9000
100.2300

Yield
uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000

key line

TOTALS:

Nuclides

Energy Lines

52&1

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