Professional Documents
Culture Documents
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04051-0R
May 6, 2013
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
II
Sample Acknowledgement
III
Case Narrative
0012
IV
0015
Analytical Standards
0019
VI
0025
VII
0049
VIII
0088
IX
0202
0318
XI
0428
XII
0447
0523
0004
00
MP-001, Rev. 12
Effective. 10131112
Page 14 of 14
Sample Receiving
MP-001-3
1_3_-_0_4_0_5_1_____
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials
Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
Sampl~lyzed
Yes? LX:
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Date/Initials
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Date package approved by:
~~
Laboratory Manager
CJ
Copy No. _ _ __
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Date
Radiochemistry Services
-5&63
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
13-04051
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EBERLINE
SERViCES
Internal
Work Order#
13-04051
Chain of
Lab Deadline
4/30/2013
Custody
UUISO - Level 4
Analysis
Water
Sample Matrix
Sample
Fraction
Comments
HP 210/270
Detector Activity
Storage
Location
Initials
Date
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
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Chain of
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Work Order#
Lab Deadline
ThiSO- Level4
Sample
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Comments
HP 210 I 270
Detector Activity
Storage
Location
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EBERLINE
SERVICES
Internal
Work Order#
13-04051
Chain of
Custody
Lab Deadline
4/30/2013
Ra226 - Level 4
Analysis
Water
Sample Matrix
HP 210 I 270
Detector Activity
Sample
Fraction
Comments
Storage
Location
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
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Ra228 - Level 4
Comments
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04
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Page 1 of 1
13-04051
Received By
SERVICES
KCOULSTON
FR
01
02
03
04
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WA
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container Number
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MP-001, Rev 5
Effective: 11/22/02
iii iii i l
SECTION II
SAMPLE ACKNOWLEDGEMENT
Client Name
..
~--
ou-11
:
ClientWO
Contract/PO
..
Client ID
Project Type
Date Received
Environmental
04/09/2013
28
Sample Disp
Lab Deadline
Internal Deadline
04/30/2013
05/06/2013
West Lake
ou-11
Sample Date
Matrix
Storage
. ...
,.
13-04051
--.
05/07/2013
IJ
:C
1-
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..
(I)
01
LCS
04/09/13
WA
Ul.O
02
BLANK
04/09/13
WA
Ul.O
03
DUP
04/09/13
WA
Ul.O
04
PZ-105-SS TOT
04/04/13 15:06
WA
Ul.O
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PZ-105-SS DIS
04/04/13 15:06
WA
Ul.O
06
S-10 TOT
04/04/13 15:25
WA
Ul.O
07
S-10 DIS
04/04/13 15:25
WA
Ul.O
08
LR-104 TOT
04/04/13 15:52
WA
Ul.O
09
LR-104 DIS
04/04/13 15:52
WA
Ul.O
10
DUP 01 TOT
04/04/13 00:00
WA
Ul.O
11
DUP 01 DIS
04/04/13 00:00
WA
Ul.O
12
DUP 02 TOT
04/04/13 00:00
WA
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13
DUP 02 DIS
04/04/13 00:00
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14
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04/04/13 09:30
WA
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15
FB at PZ-110-SS DIS
04/04/13 09:30
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16
MW-103 TOT
04/05/13 09:50
WA
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17
MW-103 DIS
04/05/13 09:50
WA
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18
PZ-200-SS TOT
04/05/13 11:10
WA
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19
PZ-200-SS DIS
04/05/13 11:10
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16
16
Invoice
~
"
EeERLI. NE
SERVICES
Voice
16
16
Paul V. Rosasco, P. E.
Report Data
Lakewood. CO 80235
Lakewood, CO 80235
303-640-3426
Voice
303-940-3426
Fax
Fax
Contact
Lyn Fitzgerald
Voice
303-601-4255
Fax
G',
II-
(.,;~
MP-001, Rev. 12
Effective. 10131112
Page 13 of 14
Sample Receiving
1 3- 0 4 0 5
1MP-001-2
WORK ORDER# ___________________
SAMPLE MATRIX/MATRICES:
NON-AQUEOUS
krJ
N/A
r0
10
N
N
Unbroken on samples?
IM
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: __________________________________________________________
DATE:
Copy No. _ _ __
'i/q_/IJ
Radiochemistry Services
SECTION III
CASE NARRATIVE
EBS-OR-35526
May 7, 2013
Paul V. Rosasco, P.E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 8023 5
CASE NARRATIVE
Work Order# 13-04051-0R
SAMPLE RECEIPT
This work order contains eight water samples received 04/09/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID
LABID
CLIENT ID
LABID
13-04051-04
13-04051-05
13-04051-06
13-04051-07
13-04051-08
13-04051-09
13-04051-10
13-04051-11
DUP02TOT
DUP 02 DIS
FB at PZ-110-SS TOT
FB at PZ-11 0-SS DIS
MW-103 TOT
MW-103 DIS
PZ-200-SS TOT
PZ-200-SS DIS
13-04051-12
13-04051-13
13-04051-14
13-04051-15
13-04051-16
13-04051-17
13-04051-18
13-04051-19
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using EPA Method 903.0. Radium-228 was analyzed using EPA Method 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page 1 of3
Page 2 of3
M.R. McDougall
Laboratory Manag
Date: 5/7/2013
Ebcrlinc Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.cbcrlincscrviccs.com/clicnt.htm to provide us with feedback on our services.
Page 3 of3
5Hi18
SECTION IV
ANALYTICAL RESULTS SUMMARY
Client Sample ID
c;,
Q)
ft.ll
Q~
Lab Sample ID
Analysis Date/Time
Analvte
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
LCS13-04051-01
13-04051-01
13-04051-01
13-04051-01
13-04051-0 1
13-04051-01
13-04051-01
13-04051-01
13-04051-01
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
14:39:26
08:17:44
13:48:50
13:48:50
13:48:50
11:36:31
11:36:31
11 :36:31
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02
8 LANK 13-04051-02
BLANK13-04051-02
BLANK13-04051-02
BLANK13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
13-04051-02
04/19/2013 14:39:27
04/29(2013 08:17:45
04/20/2013 13:48:51
04/20/2013 13:48:51
04/20/2013 13:48:51
04/19/201311:36:32
04/19/201311:36:32
04/19/2013 11:36:32
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
13-04051-03
04/19/2013 14:39:28
04/29/2013 08:17:45
04/20/2013 13:48:52
04/20/2013 13:48:52
04/20/2013 13:48:52
04/19/201311:36:33
04/19/2013 11:36:33
04/19/2013 11 :36:33
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
PZ-1 05-SS TOT
PZ-105-SS TOT
PZ-105-SS TOT
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
13-04051-04
04/19/2013 14:39:28
04/29/2013 08:17:45
04/20/2013 13:48:53
04/20/2013 13:48:53
04/20/2013 13:48:53
04/19/201311:36:34
04/19/2013 11:36:34
04/19/2013 11 :36:34
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
2J
~EBER~I ..... E
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
10.63
9.72
5.19
5.36
5.22
7.85
0.43
8.02
1.15
0.89
0.81
0.83
0.81
1.07
0.17
1.09
0.17
1.04
0.14
0.08
0.08
0.09
0.08
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.12
0.59
0.00
0.10
0.00
0.05
0.04
0.02
0.12
0.39
0.03
0.07
0.02
0.05
0.06
0.05
0.17
0.76
0.09
0.05
0.05
0.07
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
-0.03
0.13
-0.02
0.13
0.01
2.60
0.11
1.82
0.04
0.43
0.06
0.09
0.04
0.46
0.09
0.36
0.15
0.91
0.15
0.08
0.09
0.09
0.07
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.79
0.87
0.04
0.08
0.01
2.62
0.11
1.64
0.40
0.46
0.06
0.07
0.02
0.45
0.09
0.33
0.14
0.88
0.10
0.08
0.06
0.08
0.09
0.06
Method
FAX
0.09
865/483-4621
Qualifier
Units
pC~
~~
pC~
pC~
~~
pC~
pC~
pC~
~~
pC~
pC~
pC~
u
u
u
u
~~
~~
pC~
pC~
pC~
pC~
~~
pC~
~~
~~
pC~
~~
~~
pC~
pC~
~~
~~
pC~
pC~
~~
Client Sample 10
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
PZ-105-SS
~lt
I'\)
~~-
Analvte
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
14:39:29
09:09:03
13:50:08
13:50:08
13:50:08
11 :36:35
11 :36:35
11 :36:35
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
S-10 TOT
S-10TOT
S-10 TOT
S-10 TOT
S-10 TOT
S-10TOT
S-10 TOT
S-10 TOT
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
13-04051-06
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
14:39:30
09:09:03
13:50:09
13:50:09
13:50:09
11 :36:36
11 :36:36
11 :36:36
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
S-10
S-10
S-10
S-10
S-10
S-10
S-10
S-10
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
13-04051-07
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
15:00:27
09:09:03
13:50:10
13:50:10
13:50:10
11 :57:43
11 :57:43
11 :57:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
13-04051-08
04/19/2013 15:00:29
04/29/2013 09:09:03
04/20/2013 13:50:11
04/20/201313:50:11
04/20/2013 13:50:11
04/19/2013 11 :57:45
04/19/2013 11 :57:45
04/19/2013 11 :57:45
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
EBERLINE'
SERVICES
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.22
1.03
0.01
0.24
0.03
2.58
0.08
1.42
0.33
0.42
0.05
0.12
0.05
0.44
0.07
0.30
0.17
0.77
0.12
0.08
0.08
0.07
0.09
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.03
0.06
0.03
0.26
0.12
0.23
0.03
0.24
0.05
0.51
0.09
0.15
0.10
0.11
0.05
0.12
0.10
1.09
0.18
0.11
0.10
0.08
0.08
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.01
0.37
0.05
0.10
0.01
0.13
0.02
0.09
0.04
0.36
0.11
0.12
0.05
0.10
0.04
0.09
0.09
0.73
0.21
0.16
0.12
0.11
0.09
0.11
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.63
1.58
0.08
0.16
0.05
2.60
0.16
2.11
0.25
0.46
0.08
0.10
0.06
0.44
0.10
0.38
0.12
0.80
0.09
0.08
0.07
0.05
0.09
0.06
Method
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
13-04051-05
LR-104
LR-104
LR-104
LR-104
LR-104
LR-104
LR-104
LR-104
G'll
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
865/481-0683
FAX 865/483-4621
Qualifier
u
u
J
u
u
u
J
u
u
J
u
u
u
J
u
u
u
J
u
J
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------,
Client Sample ID
~,
lil,
W<,)
,.,,,
Lab Sample ID
Analysis Date/Time
Analyte
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
LR-104 DIS
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
13-04051-09
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
15:00:31
09:09:07
13:50:12
13:50:12
13:50:12
11 :57:40
11 :57:40
11 :57:40
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP01TOT
DUP01TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP 01 TOT
DUP01 TOT
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
13-04051-10
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
15:00:32
09:09:07
13:50:13
13:50:13
13:50:13
11 :57:41
11 :57:41
11 :57:41
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP
01
01
01
01
01
01
01
01
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
13-04051-11
04/19/2013 15:00:35
04/29/2013 09:09:07
04/20/201314:11:33
04/20/201314:11:33
04/20/2013 14:11:33
04/19/2013 11 :57:49
04/19/2013 11 :57:49
04/19/2013 11 :57:49
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP
02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02 TOT
02TOT
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
13-04051-12
04/19/2013 15:00:37
04/29/2013 09:09:08
04/20/2013 14:11 :34
04/20/201314:11:34
04/20/2013 14:11:34
04/19/2013 11 :57:46
04/19/2013 11 :57:46
04/19/2013 11 :57:46
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
r2J
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
~EBER!,-I ...... E
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.39
1.00
0.03
0.06
-0.01
2.72
0.16
1.94
0.18
0.47
0.07
0.07
0.03
0.45
0.10
0.36
0.10
0.88
0.12
0.10
0.11
0.06
0.09
0.05
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.32
0.89
0.08
0.19
0.05
0.26
0.01
0.12
0.17
0.43
0.09
0.12
0.06
0.11
0.03
0.07
0.12
0.81
0.13
0.10
0.10
0.05
0.06
0.05
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.19
0.65
0.01
0.10
-0.04
0.20
0.03
0.14
0.13
0.45
0.03
0.08
0.03
0.11
0.06
0.09
0.11
0.89
0.07
0.09
0.12
0.07
0.10
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.45
1.61
0.10
0.17
0.07
0.16
0.01
0.10
0.21
0.48
0.12
0.14
0.09
0.10
0.04
0.09
0.17
0.85
0.16
0.11
0.12
0.08
0.10
0.12
Method
FAX
865/483-4621
Qualifier
Units
~~
~~
~~
u
u
u
pC~
pC~
~~
~~
~~
~~
~~
~~
~~
pC~
~~
~~
J
J
~~
pC~
~~
~~
pC~
~~
~~
pC~
pC~
u
u
~~
~~
~~
~~
~~
pC~
~~
~~
Client Sample ID
Lab Sample ID
Analvsis Date/Time
Analvte
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
13-04051-13
04/19/2013 15:00:40
04/29/2013 10:21:09
04/20/2013 14:11 :30
04/20/201314:11:30
04/20/201314:11:30
04/19/2013 11:57:47
04/19/2013 11 :57:4 7
04/19/2013 11:57:47
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-11 0-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
FB at PZ-110-SS TOT
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
13-04051-14
04/19/2013 15:00:42
04/29/201310:21:09
04/20/2013 14:11:31
04/20/201314:11:31
04/20/201314:11:31
04/19/2013 14:33:37
04/19/2013 14:33:37
04/19/2013 14:33:37
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
FB
FB
FB
FB
FB
FB
FB
FB
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
13-04051-15
04/19/2013 15:00:44
04/29/2013 10:21:09
04/20/2013 14:11 :27
04/20/201314:11:27
04/20/2013 14:11:27
04/19/2013 14:33:38
04/19/2013 14:33:38
04/19/2013 14:33:38
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
13-04051-16
04/19/2013
04/29/2013
04/20/2013
04/20/2013
04/20/2013
04/19/2013
04/19/2013
04/19/2013
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
DUP 02
at
at
at
at
at
at
at
at
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-11 0-SS
PZ-11 0-SS
PZ-110-SS
PZ-110-SS
MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103 TOT
MW-103TOT
MW-103TOT
MW-103 TOT
t:U
Q)
~"\.)
(,.~
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
EBERLINE
SERVICES
15:00:47
10:21:09
14:11:28
14:11 :28
14:11 :28
14:33:33
14:33:33
14:33:33
Result
Error
MDA
Qualifier
Units
0.11
0.50
0.03
0.10
0.04
0.10
0.09
0.09
0.13
0.97
0.06
0.09
0.09
0.07
0.07
0.07
J
J
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.12
0.85
0.01
0.15
0.00
0.18
0.12
0.13
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.12
1.16
0.15
0.15
0.04
0.02
0.03
-0.01
0.09
0.57
0.13
0.13
0.07
0.03
0.04
0.02
0.06
1.08
0.11
0.11
0.13
0.06
0.06
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.03
0.45
0.02
0.25
-0.01
0.04
0.00
-0.01
0.05
0.59
0.04
0.14
0.04
0.07
0.04
0.03
0.07
1.22
0.08
0.09
0.09
0.12
0.12
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.78
0.88
1.38
1.22
1.19
4.07
0.37
3.72
0.25
0.49
0.36
0.32
0.32
0.67
0.17
0.63
0.12
0.96
0.09
0.06
0.06
0.12
0.10
0.09
865/481-0683
FAX 865/483-4621
Method
u
J
u
J
J
J
J
J
J
u
u
u
u
u
u
u
u
u
u
u
J
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
Client Sample ID
tn
ili'J!)
W\)
.11:::::
Lab Sample ID
Analvsis Date/Time
Analvte
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
MW-103 DIS
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
13-04051-17
04/19/2013 15:00:50
04/29/2013 13:17:02
04/21/201314:27:41
04/21/201314:27:41
04/21/2013 14:27:41
04/19/2013 14:33:34
04/19/2013 14:33:34
04/19/2013 14:33:34
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
PZ-200-SS TOT
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
13-04051-18
04/20/2013
04/29/2013
04/21/2013
04/21/2013
04/21/2013
04/19/2013
04/19/2013
04/19/2013
13:48:54
13:17:02
14:27:42
14:27:42
14:27:42
14:33:35
14:33:35
14:33:35
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
13-04051-19
04/20/2013 13:48:55
04/29/201313:17:02
04/21/2013 14:27:40
04/21/2013 14:27:40
04/21/2013 14:27:40
04/19/2013 14:33:36
04/19/2013 14:33:36
04/19/2013 14:33:36
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
EBERLINE
SERVICES
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.24
1.08
-0.02
0.12
0.07
3.17
0.27
3.00
0.15
0.57
0.06
0.10
0.08
0.55
0.14
0.53
0.09
1.09
0.18
0.12
0.09
0.06
0.11
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.44
1.38
0.00
0.14
0.01
0.54
0.06
0.52
0.58
0.88
0.06
0.10
0.04
0.18
0.07
0.17
0.25
1.73
0.15
0.11
0.10
0.08
0.07
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.84
1.37
0.03
0.10
-0.01
0.53
0.04
0.58
0.45
0.60
0.07
0.08
0.03
0.18
0.06
0.18
0.22
1.12
0.13
0.07
0.08
0.09
0.09
0.06
Method
fAX
865/483-4621
Qualifier
u
J
u
J
u
u
J
u
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
LL-8
7338
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
TMAEBERLINE
Customer:
OR2778
P.O.No.:
12:00 PST.
Reference Date:
January 11995
Contained Radioactivity: (Total U) 8.016 p,Ci
Contained Radioactivity: (Total U) 297 k:Bq
U-238NAT
0.005) x IOA9 years
..
,.
:~:
'
d. Density:
,....~. .
Radioimpurities
Radioactive Daughters
..
Radionuclide Concentration
':
(fotal U) 0.1228
pCi/g.
Method of Calibration
.........
.'-;
.:,
..... -
-Activity calculations are based upon known specific activity and mass .
..... .,
.:
.,.
.-.:;
-:
::>:. .... ;
:-.!
. .. . ' .
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibrntion:
b. Random uncertainty in assay:
3.0%
0.0%
2.0%
3.6%
.: ...
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
\~
. .
. :.;.::.
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986 .
2. IPL participates in an NIST measurement assurance program to et.tablish and maintain implicit traceability for a number of nuclides,
based on the blind aSBlly (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
EEftlvAuA7
YCONTROL
-p;/
...,,_.
,:'
<
91504
8188437000
8188436168
FAX
,.. . '
:-!
........
, .. ..
.:.:
,,
. .
;: .. i
-~
... -
<:.;
..
:"'!.
;;.'
._.:<::""::::-;'!"
. '""
.'
~.
-v
..
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
I~
\ :4.466e.+osl
. . , .....
Dilution Instructions:
j1MHNO
. ....... 3 ...:
. ..
...........
Imilliliters
Which Eauals
And after dilution the activity of this solution is 1.77955E+04ldpm/ml-eterence date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
o:....o....o
Date: _ _9.;;.;./2;;.;6:.;.;/2;;;;.;0;..;.1-..2....
Date:
--'~/.;;;..u.~/-t~--
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solution$ & Records
:~;2~.2381J
9/6/2012 0:001
Date I
u~aa
1
Solution#!
Half Life1 Dals
. .. 1.632E+12I
0
. .
,..... . I
I< '4;4sae+osl
Reference Date
HN03
. . ...
I'
..., ...
'-11111995 o:oo I
. I
<\
Dilution Instructions:
.. ..
j1MHNOd
0
0
'
>I
> ..
7.1182E+01Jdpmlml
NOTES:
Isotopic Distribution as:
U-238 Atom % 48.239
U-235 Atom % "' 2.25
U-234 Atom o/o = 49.501
All values +/- 3.6%
f\.
~~.
QCApproval
Date:
9/26/2012 0:00
Date:
r4ZbJrz. .
RECORD COPY
Tracer Solution for Environmental Analysis & Disequililirium Studies
Product Description & Measurement Certificate
Description
Principal radionuclide:
Daughter Nuclide:
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
Volume of solution
Total activity ofU-232
which is equivalent to
Accuracy
Radionuclidic
Purity
Isotopic
Purity
...,....ne isotopic composition, exprP.ssed as atom per cent at the reference date .
!~Ot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Physical
Data
Remarks
For safety information and notes to ensure correct usage by all persons handling this radioqctive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 9001.
Approved
Signatory
Roger Wiltshire
Prepared and characterised in the UK, for world wide distribution by lsotrak, AEA Technology, QSA.
Trkcert.wps 10/03/00
~623
Rev.8; 11/01/03
1itle: Radioactive Reference Standards Solutions & Records
Ce~lon,.:::,9.~E~11~CI
Certified Concentration . . . .. . . .. . . JJ.CI per gram
>
Dilution Instructions:
Dilute to a volume ofl'
1000.00
I ... 0.9760IJ1CI
Imilliliters
Which Eauals
And after dilution the activity of this solution Is j 2.167E+03Idpmfml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Date:
Date:
12113/2012 0:00
1~
~E ...
EF<LINE
--~ ---seftv~
Rev.6; 11/01103
Title: Radioactive Reference Standanls Solutions & Records
1217/2012 0:001
U~10a
< I
Half Life, Dal!
2.630E+04I
I .. . . .
R~~~nn~c~i:~:~!~n~=1.~~.1=~~~' ldpm/ml
lm . .. . . . .
Dilution Instructions:
DateI
Solution #I
:o:oo I
I
I2MHN03
:: ... ...
.'.
.. ;._.'
:,
. 10.0000 ml
2.1670E+04 dpm
. 1000~00 ml
2.1e70E+01Idprnlml
NOTES:
c~
l\
~~
ac Approval6~a
~
.kJJJ j( ~\
Date:
Date:
12/13/2012 0:00
t~lta:
I
RTIFICATE OF CALffiRATI~t~
q\
PHA STANDARD SOLUTION" oe' ft_~~t\\\\\\
TMA EBmull\t.V.\\\~\\ \.'0
Th-230
Customer:
(7 .54 0.03) x 10"4 years
P.O.No.:
TT4944
\\\\l
Catalog No.:
7230
Reference Date:
November 1 1991
Contained Radioactivity:
1.036
Source No.:
Desaiption of Solution
a.
b.
c.
d.
Mass of solution:
Chemical form:
Carrier content:
Density:
5.0042
Th(N03)4 in O.lN HN03
None added
1.0016
12:00 PST.
grams.
Radioimpurities
See attached technical data sheet
Radioactive Daughters
I'Cilgnun.
Method of Calibration
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
Uncertainty of Measurement
a. Systematic uncertainty in iustruinent calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
2.0%
0.5%
0.2%
2.7%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes
1. Nuclear data were taken from Table of Isotopes", Seventh Edition, edited by Vi.Iginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintaiu implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatoty Guide 4.15)
$&32
~
E EJ E RLI hll;; I QUALITY CONTROL PROGRAM
~
MP-009
SERVICI!$
Rev.8; 11101(03
Title: Radioactive Reference Standards Solutions & Records
MP-009
Solution Reference# IPL ~.116 ;: .
Half Life, Years
I 7054oE+b41
Reference DateV
/11/111~1J>:ool
Dilution Instructions:
2.2999E+01Jdpmlml
NOTES:
Expiration Date:
Recertified
Date:
Date:
QCApproval
Date:
March 4, 2014
312112013 0:00
j~l'~
~r~
..\ {"
> ~h
:7:540E~..041
Radionuclide ~;,P:rhe>riurn;
Certified Activity 'J:.036E+()O ~-tCI
Certified Concentration I_ / . > ; :. <: \' ~-tCi per gram
Reference Datel
: ':''11I1/199l:o:bol
Dilution Instructions:
Dilute to a volume of
I 10oo;oo:
>1.0360lllCI
>!milliliters
Which Eauals
And after dilution the activity of this solution Is I 2.300E+03ldpm/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date:
Date:
'March 4, 2014 .
3/21/2013 0:00
----'-----
Date: ___.,.,.../:u
.....,..,f.....
r 3...___ _
1h-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Half Life:
Catalog No.:
Source No.:
TMAEBERLINE
Customer:
VH1632
P.O.No.:
Reference Date:
November 11993
12:00 PST.
Contained Radioactivity:
(Th-232) 0.0933
~i.
Contained Radioactivity:
(Th-232) 3.45
kBq.
Th-232
(1.~5 0.006) x 10" 10 years
7232
435-104-2
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:
Radioimpurities
g/ml @ZOc.
Radioactive Daughters
.
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Po-212, TI-208
Radionuclide Concentration
(Th-232) 0.00779
p.Ci/g.
Method of Calibration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data '\Yete .lakCn from "'!:able of Radioactive Isotopes", edited by Virginia S. Shirley,.l986.
2. IPL participines ill an NIST mc-ment assurance program 1o establish and maintain implicit traceability for a number of nucJi~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (Aa in NRC Regulatory Guide 4.15).
QUALITY CONI'ROL
Al,zv.
<6' I
I 1 9>
Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000
fiUi35
~EBERLINE I
~
SEAVIC:I!:S
Rev.B; 1/10/03
Title: Radioactive Reference Standards Solutions & Records
I'H'/~:tjS4o5gt:1'ol
Weight, Grams
Weight, Grams
Weight, Grams
J.LCI
Dilution Instructions:
Which Eauals
Date: _ _10/9/2012
0:00
.:.:::.:::..=.;::..:.=...::.:.;;..;;..
SttRVICE$
Rev.8; 1/10103
Title: Radioactive Reference Standards Solutions & RecordS
DataL
MP-Q09
Solution Reference #IIPL 435~1 ~2
Principal Radionuclide
Half Llfe1 Years
.228&232Th l
Solution#!
Th;.;sb . I
I 1.4o5E.1o!
Reference Date j
228 "'~Th
2;07E+02 dpm/ml
Radionucllde of lnteresd
Parent Solution Cone. I
11/9/2012 O:OOj
<
5.132E12I
. 111111ses:o:oo 1
Dilution Instructions:
I
11% NitrieAeid
NOTES:
Expiration Date:
Verifted &
1.0366E.+02Idpm/ml
Approved~ ~
QCAppraval
"9
~v
Date:
Date:
I . October 9, 2013 I
1119/2012 0:00
1\
,..,_I 1'1..
I
f!Hi
1 f Isotope Products
lh-18
Laboratories
An Eckert &Ziegler Company
Tel 6613091010
Fax 6612578303
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radio nuclide:
Half-life:
Catalog No.:
Source No.:
Th-229
7340 160 years
Customer:
P.O. No.:
Reference Date:
Contained Radioactivity:
(Th-229 only}
7229
867-54
Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. Density:
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
~-tCi
37.48
kBq
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration:
0.2020
lJCi/g,
kBqfg
7.474
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in !JCifg was determined
Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type 8 (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence revel:
0.7%
3.0%
0.0%
3.1%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
Quality 'Control
Date Signed
867-54
- - - - - - - - - - - - - - - - - - 1509001 CERTIFIED - - - - - - - - - - - - - - - - - -
Rev.8; 1/10/03
Title: Radioactive Reference Standards Solutions & Records
Radlonuclidol '
Z;Z8:"Ch 1
1!'ili:, ,
Reference Datel :
1/15/2002 o:ooj
Dilution Instructions:
Which Eauals
And after dilution the activity of this solution is 1 2.249E+03ldpmlml reference date listed above.
Expiration Date:
October 9, 2013 ]
Date: _ _1.;...1~/9~/2;;.;0...;.12--..0:...;.o_o
Date:
--:.14-,,J,z/tz_
__,,..o.;;..,_ __
Rev.7; 9129199
MP~09
Radionucllde of lnteresj . ~
Parent Solution Cone. 2.25E+03 ldpmiml
Reference Date
Dilution Instructions:
Th~tsa
I . 7.34oe+o31
11/9/2012 O:OOJ
. . .
. 2.~81E+06l
l .111si2oo2 o:oo I
I
j0.1MHNO.
. . . . . . 3.
10.0000 ml
2.2490E+04 dpm
1000.00 ml
2.2490E+01ldpmlml
NOTES:
~~
'
QC Approval~)'~') ~L.
,,.
~~
'-.,...!_
Date:
11/9/2012 0:00
Date:
llt~f~-z_
i r
-,1).
'.
'l.-
.
i
\.
~ ~ ~,/
; ..
.4
/
-~
.F
.,,_
.1'
.;
C!tertificate
.
..
.:
. .j_ ~ ~-,,
This Standard Reference M,ate.rial(SRM) consists of radioactive barium-133. c~loride,_ non~~adioactive barium
chloride, and hydrochloric acid diSsolved in 5 mL of distilled water. The solution is contain in a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization thambers and
solid-state
gamma-ray,,spectrometry
.systems.
.
... .
.
.
Radiological Hazard
SRM
'a
The
ampoule contains bariuni-133 with total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during tl:te decay process X-rays and gaiilllla;rays with energies from 4. tp 400 keV are
emitted. Most of these photons escape from the SRM ampoule and can represent a radl.atipn hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be 11$ed to minimize. ~rsonnel exposure... The. ,SRM $hould be
}~Sed only by persons qUalified to' han~e radioactiv~ materiaL
'
.
Chemical Hazard
The SRM ampoule.c~ntain~.hydr~hloric acid (HCl) with a concentration qf 1 mole per Iite:r;.o(.water. 'Jhe
solution is corrosive and represents a health hazard if it comes in contact with, eyes or skin~ -If. the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened. only by persons qualified to handle, both radioactive material and strong a,cid solution.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standarc! Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
8641
QCP009-1
CURRENT DATE!'
'9/2012012 0:001
SOLUTION REFERENCE #r."N:o:-:.ls=:r="':;s="=R::"M~4~25~1~C~'_,
:".
~-:~:>...,.i~l SOLUTION #l';'~'/.0>.;:r;::sa':;Q.:t<>i:~;\':::r1
Principal Radlonuclide
Half Life, Years
Half Life, Days
:J~a~ri'(Jm'?l
j:;:,1:04e~ro11
:;3.s2ee+o:;3l
1.,,.:. .... .
Radionuclide .yJ~aariUro.i;:
Certified Activity ji:C::;t;F;~ J.LCI
Certified Concentration \'41';3teE.01; J.LCi per gram
Ampoule /Solution Gross }':?,'.;g;.3Q8.t Weight, Grams
Empty Ampoule ;;;.t';i'4i:2$32 Weight, Grams
Solution Net . $0499 Weight, Grams
Total Activity in Ampoule 66~5577 J.LCi
Chemical Composition of Standard Solution
Dilution Instructions:
66.5577IJ.LCi
Which Eauals
,..
Verified & Approved By
QC Approval
~
.~JAW\UI
\
___. ---.l
\\
._.,
Date:
9127/12
Date:
I-z.rtft 'Z.
Rev.8; 11/10/03
Title: Radioactive Reference Standards Solutions & Records
Reference Date
Dilution Instructions:
. . I
NOTES:
3.6950E+03Idprnlml
Date: ___9;.;./;;;.;27~/1.2..____
Date: _ _'t_.{_t'7-t/-"tZ......___
Radionuclide:
Half Life:
Catalog No.:
1600
Source No.:
7 years
P~O.No.:
Reference Date:.
February 1 1994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 J.'Ci.
Contained Radioactivity: (Ra-226)
37.0 kBq.
7'126
453-26
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:
TMAEBERUNE
VH1888
Customer.
Ra-226
g/ml @20C.
Radioimpurities
Radioactive Daughters
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuelide Concentration
(Ra-226) . 0.1929
, . p.Cilg.
Method of Calibration
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Brancbitlg ratio(s) used:
0.0351
gamma rays per decay.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
3.4%
3.1%
0.2%
4.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken ftom "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability fur a num~r of nuclides,
based oinne blincrassay(aiiillater NIST'certificationrorstaiidiiro ReferenoeMateriiils\Ai'in NRC'RegulitOryomdn:; 15): ---
QUALITY CONTROL
/iA,. ;
199 If
Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
Ra.:.5
'
. .
I
. Radium..
I . 1.600E+031
~26.
11/9/2012 O:OOJ
<
Radionucllde ~~Radium
Certified Activity .1;001E+OO J.(Ci
Certified Concentration 1... ... .. . . J.t.CI per gram
1/_19_94_._o_:o__,o)
Reference Date.._l_-'--2_1....
Dilution Instructions:
jtMHN03
1;0010IJ.1.CI
.. .
!milliliters
Which Eauals
~-~----t-...,.....,.~-~-~-
Verified &Approved By __
QC
Approval_~~;::::::::;.o.aA~w.
.;lo~~l..;::.;...J....--=--~\J..;;;,..___
Date:
------1119/2012
Date:---''~
f,t+-./ulf?....__
I ,
Rev.8; 11101103
TrUe: Radioactive Reference Standards Solutions & Records
::.~RadiUrnn
>il
j;::1:Ceoo6+o31
Dilution Instructions:
:2o:nooo
NOTES:
Date:
Date:
,,
11/9/2012 0:00
RA- \\
ANALYTICS
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
Ra-228
ACTIVITY (dps) :
2.585 E3
HALF-LIFE:
5.75 years
CALIBRATION DATE:
TOTAL UNCERTAINTY*:
4.0%
SYSTEMATIC:
3.0%
RANDOM:
1. 0%
Q A APPROVED:
M:i~mist
Rev.S; 1/10/03
Title:
1.> :
::2:100Eo~l
Reference DateF1tiitW!.M:3;1?t7i2.1X{O!dbl
Dilution Instructions:
Which Eauals
Date:
__
4116/12
__
....;;....;,...;.;...;.;;;,_
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
WO
Analysis
13-04051
UUISO
+---Run
I
Aliquot Units
Activity Units
-
Client Name
pCi
U-234
Normalized
Difference
0.4S
U-23S
0.12
LCS
Measured
csu
Measured
LCS
Expected
Uncert_
Expected
Known
Known
Error
~.33%
15.42%
100.95%
15.36%
Standard
csu
Result
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
U-Sa
3.52E+01
3.60E+OO
i 5.13E-01
U-Sa
3.44E+01
I 3.60E+OO
5.13E-01
10
I
100.00%
3.60%
--
100.00%
3.60%
S.15E+OO
2.93E-01
I 7.S5E+OO I 1.21E+OO
I
'
~------~--------j--------r
7.94E+OO
2.S6E-01
S.02E+OO
1.23E+OO
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MSResult
Expected
MS Uncert
Actual
MSResult
Actual
MSCSU
Replicate Sample
Analyte
U-234
U-23S
U-235
Q,
Gil'
1;.,.11
It'~)
Version
Normalized
Difference
RPD
0.05
0.73
0.67
0.03
10.30
1.91
Original
Result
Original
csu
Replicate
Result
Replicate
2.62E+OO
4.92E-01
2.60E+OO
4.97E-01
csu
Sample
Result
Sample
I
I
I
Sample
Aliquot
csu
Standard
ID
Standard
Error%
Standard
ACT(dpm)
Standard
Added(g)
QCSummary
LCS Relative
Bias
LCS%R
0.96
OK
LCSND
OK
-+--:;
OK
3.52E-01
1.S2E+OO
3.S4E-01t--~~-1
S.73E-02
1.11 E-01
S.56E-02
MS%R
MSND
II
I
RepRPD
RepND
OK
OK
--
OK
OK
OK
OK
NA
OK
Eberline Services
Analysis Control Chart
wo
Analysis
Run
13-04051
UUISO
-+---" Acti~nits
Client Name
Aliquot Units
pCi
LCS% Recovery
130.00
40.00
120 00
35.00
110.00
30.00
100.00
25.00
20.00
90 00
15.00
80.00
10.00
70.00
+--------------------,---------------------,
U-234
U-238
Lower Error I
-
_Uf>er Error
77"31
81.99
115"34
119.91
100%
80
100
00~
80
100
-
-UCL
120
5.00
0.00 t--------,~':-c------,-----~=c-----,-------:-:-:
U-L:.:S4
-CL
0"80
0"66
0"73
35
"-
u-238
11.40
9.20
10.30
35
Normalized Difference
3"50 - , - - - - - - - - - - - - - - - - - - - - - 3.001
- - - -
- - - -
2"50+---2"00
-----"
1"50+---------------------------------1"00 + - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
;::,
llli!,
u~
!~-'
Version
No Matrix Spike
U-235
2"66
U6
1"91
35
Eberline Services
Analysis Control Chart
WO
Analysis
Run
Activity Units
13-04051
ThiSO
pCi
Client Name
-----~ig_tJ_~I_lj_nJ~-----------------
LCS
Expected
Uncert.
Expected
Known
Known
Error
Result
csu
107.62%
18.25%
100.00%
3.60%
4.82E+OO
1.73E-01
5.19E+OO
9.46E-01
Th-8b
1.04E+02
3.60E+OO
1.03E-01
97.59%
19.82%
100.00%
2.70%
5.49E+OO
1.48E-01
5.36E+OO
1.06E+OO
Th-1b
i 2.35E+01
I 2.70E+OO
5.18E-01
I 108.41%
17.89%
100.00%
3.60%
Th-8b
11.04E+02
3.60E+OO
1.03E-01
TH-228
TH-230
TH-232
0.24
0.84
csu
LCS
Measured
Analyte
Standard
ACT(dpm)
Standard
10
Standard
Error
Standard
Added (g)
Matrix Spike
Normalized
Difference
Analyte
Sample
Result
Actual
MSCSU
Sample
Sample
Aliquot
csu
Replicate Sample
Analyte
Normalized
Difference
RPD
Standarc/
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
RepND
QCSummary
Original
Resun
Replicate
Result
Original
csu
Replicate
csu
LCS Relative
Bias
LCS%R
LCSND
OK
OK
NA
OK
OK
NA
OK
OK
NA
OK
MS%R
MSND
TH-228
1.53
584.85
4.21E-02
TH-230
0.95
52.45
TH-232
0.37
87.36
C&1
c;)
Ul
.... ~
Version
5.82E-02
-2.07E-02 ; 5.54E-02
7.81E-02
6.61E-02
1.34E-01
9.37E-02
0.98
5.61E-03
2.34E-02
1.43E-02
3.98E-02
1.08
1.08
I
I
OK
OK
I
I
Eberline Services
Analysis Control Chart
_____________ _!._n_<~!~~is
WO
ThiSO
13-04051
Run
Activity Units
pCi
Client Nam.e
00_ _ _ __
Aliquot Units
LCS % Recovery
130.00
-------+---
40.00
UCL
120 00
35.00
110.00
30.00
25.00
100.00
20 00
90.00
15.00
80.00
- - - - - - - LCL
10.00
70.00
%R
-LCL
---Mean
-
-UCL
+--------------.-------------,-------------.
TH-232
TH-230
TH-228
85.77
7507
86.92
-----12947
129.90
120.11
107.62
97.59
108.41
80
80
80
100
100
100
120
120
120
5.00
0.00
+------=:c-=c::c:------,-----==-:-=::-----,--------c=-1::::::------,
Lower Error
!JEeer Error
RPD
-CL
TH-228
2131.74
-962.05
-:::~ :::
584.85
:35--
TH-<!;;u
72.24
32.65
: : ~:
52.45
35
Normalized Difference
No Matrix Spike
3.50 , - - - - - 3.00 1
U1
t ... ~
+---------------
2.00
+-------~
G!,
;i;f
2.50
Version
----------
IH-L;,jL
:~ ; :
Eberline Services
Analysis Control Chart
wo
Analysis
Run
Activity Units
13-04051
Ra226
pCi
Aliquot Units
Client Name
Analyte
RA-226
Measured
Measured
102.89%
23.73%
LCS
Expected
100.00%
Uncert.
Expected
4.60%
Known
1.03E+01
I
I
I
Known
Error
Result
4.75E-01 ! 1.06E+01
Standard
10
csu
I
1
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
5.21E-01
2.52E+OO
Ra-5b
4.41E+01
4.60E+OO
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MSResult
Expected
MS Uncert
Actual
MSResult
Actual
MSCSU
Sample
Result
Sample
csu
Replicate Sample
Analyte
RA-226
Q)
GJ:)
u~
.t::r.t
Version
2.88
Sample
Aliquot
Standard
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
RepND
INV
OK
QCSummary
RPD
Original
Result
Original
csu
Replicate
Result
Replicate
csu
LCS Relative
Bias
LCS%R
LCSND
305.90
1.21 E-01
8.98E-02
-2.54E-02
4.31E-02
1.03
OK
OK
MS%R
MSND
Eberline Services
Analysis Control Chart
wo
Analysis
Run
Activity Units
13-04051
Ra226
pCi
__ _).____
Aliquot Units
Client Name
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80 00
10.00
7o_oo
RA-226
=-._h_ower Error
74_55
102_89
Upper Error
%R
I
-::__::-_t,<::L_ ----1----
5.00
o_oo
a_o_
120
~----
---Mean
-UCL
Lower Error
Upper Error
RPD
-CL
RA-226
517_94
93_86
305_90
35
---
Normalized Difference
3_50~---------------------------------------------------------------
3.001
----
2_50 +---------------------------1
2_00 +--------------------------j
1_50 + - - - - - - - - - - - - - - - 1
1_00 +--------------------------1
o_5o + - - - - - - - - - - - - - - - - - - 1
Q;)
tn
U1
U1
Version
------
--
No Matrix Spike
Eberline Services
Analysis Control Chart
WO
Analysis
Run
Activity Units
13-04051
Ra228
pCi
---+--~Aliquot_ I.Jnits_ __
RA-228
Normalized
Difference
LCS
csu
LCS
Measured
Measured
Expected
Uncert.
Expected
0.53
107.19%
24.41%
100.00%
5.10%
Known
Known
Error
9.06E+OO I 4.62E-01
9.72E+OO
standard
ACT(dpm)
csu
Result
2.37E+OO
Ra-11
Sample
Aliquot
Standard
ID
3.91E+01
Standard
Error
5.10E+OO
Standard
Added(g)
5.15E-01
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MSResult
Expected
MSUncert
Actual
MSResult
Actual
MSCSU
Sample
Result
Sample
csu
Replicate Sample
Analyle
RA-228
Gl!~
~'
Version
Standard
ACT(dpm)
Error%
Standard
Added(g)
RepRPD
RepND
NA
OK
Standard
QCSummary
Normalized
Difference
RPD
Original
Result
Original
csu
Replicate
Result
Replicate
csu
LCS Relative
Bias
LCS%R
LCSND
2.65
158.56
1.16E+OO
6.25E-01
1.34E-01
4.33E-01
1.07
OK
OK
MS%R
MSND
Eberline Services
Analysis Control Chart
Printed: 4/30/201312:17 PM
Page 2 of 2
wo
Analysis
13-04051
Ra228
. _R_LJn~~~-
Activity Units
Aliquot Units
--~-
Name
---- ------ Client
-----------------
pCi
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
7o.oo
RA228
Lower Error
77.68
136.70
107.19
Uooer Error
%R
5 DO
0.00
-LCL
---Mean
-
-UCL
Lower Error
Upper Error
RPD
CL
RA-228
223.29
93.83
158.56
35
Normalized Difference
No Matrix Spike
3.50 ,---------
3.00~----
2.50 + - - - - - - - - - - - - - - 1
2.00 i - - - - - - - - - - - - - - - 1
1.50
+--~-----~-----1
1.001----
~'!l'll
tll!:'
U1
.... ~
Version
-~---
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
5553
Page 1 of 1
}!;EBERI,..,.INE
SERVICES
Date
Dept
04/16/13 08:36
PREP
User
JBARNARD
lnternaiiNork Order
13-04051
Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Page 1 of 1
~EBERI,...INE
~
SERVICES
Ii
Analysis Code
Run Number
13-04051
UUISO
1
Date
Dept
04/16/13 08:36
PREP
JBARNARD
ALIQUOT ED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/18/13 18:21
CHEM
JDEMELAS
Addedconcentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
User
Notes
tiii61
Page 1 of 1
4:EB!O;R~\,~~
lnte~nai\Nork Order I
Run Number
13-04051
1
Date
Dept
04/16/13 08:36
PREP
JBARNARD
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/18/13 18:21
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 mi8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 10C
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred
to new, labeled C-Tubes with Dl H20. Set samples aside for later orecioitation and filtering.
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SEl
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
User
I
3
04/19/13 05:57
CHEM
RMARTZ
Notes
Eberline Analytical
Oak Ridge Laboratory
SERVICES
Analysis Code
Run
UUISO
Reagent
ID
13-04051
EE;JER.L....lNE
Reagent
Name
1
"
Reagent
concentration
Analyst
ID"
Date
Recor
013624P
Nitric Acid
Reagent Grade
JBARNARD
~/1 l=\l?n1 ~
013666P
Reagent Grade
JDEMELAS
4/18/2013
8N-0.1M
JDEMELAS
4/18/2013
- 0.1M
JDEMELAS
~~.8/2013
JDEMELAS
4/18/2013
6.5N
JDEMELAS
4/18/2013
8N
JDEMELAS
4/18/2013
4/18/2013
0137725
- HF
0137785
- NH41
01357300
lyd
Acid
0137125
lyd
Acid
0137705
/('"rochloric Acid
---
013675P
Hydrochloric Acid
Reagent Grade
JDEMELAS
0132465
Carbon substrate
Solution
RMARTZ
14/19/2013
Ethyl Alcohol
Reagent Grade
RMARTZ
14/19/2013
D \111\DTZ
4/19/2013
~RTZ
4/19/2013
RTZ
4/19/2013
012809P
013221P
drofluoric Acid
1
0131915
f--------013434P
odymium Carrier
nous Chloride
Reagent Grade
1 mg/ml
Reagent Grade
I.e_______--------~--------------------l---------------------ll------------l-----------~-----+-------+-----81
r--~ -----~1~--~-------------lL---------~--
--------f-------------~--~-~------l~---~----~-------+----------~-~1--~- - - - - - - - -+-------------+---~
'l
1 Q
J..LJ
- ------
/_
_'f(l""llrJ_
--------
~~~~-
~:(")
{_01.-
/-"JD Lj
___ 'iu
L?_l?'.l "~AJ I)
___ 1 '1 ~-t.tQ&f~(.~-r:~
l ~~i ()~~A 4--~)
____ l(_IJttn
~1\.,h~~
Y\l~\(3 l~o\,1 O"\~ A(cil-1-l_
--- --~ ---.. .i1J9li1__ t:~Q~~~-1!-(f~~!~).
4 hi li"J
0~~{~ 4)
.. e.,'l 't4 ~
---------- ________ (((I
_/7 0 ~)l~t?J-")ti.f}
----------.. -----~f.il.
_ ---------. __ flurta
{7~)
'&...ltHIU'II
__ I?Jot(<>JJ/1(.
o/1 to
rA'"-->
lA-L-~~c,.y\..:7 l.
0570
~-~k'-~\.
0531
v.,)e:)~
ll.-1--\
PtL
1\I'UV..IIL.._
t:;:;?--'/
s \.l
I'N.N:t>~ s~
t 9"2-Of
I~<....,
u.~'
Dr'--\'
0f)1"
v--;,
. 07oo
,A-/
'51>~~)
2. ~,. ~-=--
/1/l.?
[-
..
-~--
--------
----
iHi65
ISOTHNOTES
liii67
~
E;~~E3 E R
~
Page 1 of 1
L,. .1 N
E::
SERVICES
#
1
Date
Dept
04/16/13 08:36
PREP
User
JBARNARD
Analysis Code
Run Number
13-04051
ThiSO
1
Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
6868
Page 1 of 1
j!JEBER,l,.,.IN.E
SERVICES
Date
Dept
04/16/13 08:36
PREP
04/18/13 18:21
-'--~~
CHEM
User
Analysis Code
Run Number
13-04051
ThiSO
1
Notes
JBARNARD
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
JDEMELAS
Page 1 of 1
~
E B E;:Rb-1.-.....~E;:
~
SERVICES
13-04051
Analysis Code
Run Number
Date
Dept
04/16/13 08:36
PREP
JBARNARD
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/18/13 18:21
CHEM
JDEMELAS
04/19/13 05:58
CHEM
RMARTZ
Added concentrated HN03 to sample beakers and heated io dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15ml. Set samf:>les aside for later precipitation and filtering.
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
User
Notes
Eberline Analytical
Oak Ridge Laboratory
}!J E E;IE~LI_N E
13-04051
Analysis C:ode
SERVICES
Reagent
ID
I
013624P
I 013666P
013675P
ThiSO
.Reagent
Concentration
Nitric Acid
Reagent Grade
Reagent Grade
Hydrochloric Acid
Reagent Grade
Analyst [ Date
ID ..
Recorded
JBARNARD
4/16/2013
JDEMELA5
4/18/2013
JDE_MELA5
4/18/2013
JDEMELA5
4/18/2013
------------4-------------+------~
---r
J Nitric Acid
Reagent Grade
~1~2013
,._.._.~-~-~-:-:-~-:-----[ c:~~:~h~-:~-i:-t-r:-~~--=======----=~~----~--58-,~-~-u--t-i_o_n______=-----+~-~D-M-:M-R-~LA-z-5----r-:-~-~-:-~~-~-~-~-;
0130175
Cerrium Carrier
0 12809P
Ethyl Alcohol
0.1~g/ml
RMARTZ
! 4/19/2013
013221P
Hydrofluoric Acid
Reagent Grade
RMARTZ
4/19/2013
ii671
~----- --'--+~-
{OJA..~v
----
------- ------
---
---------
------
----+-------~--------l~-----~-~ -------~--8-------~-
--~---
-~-----~----------~------
--~----
--
--~-----------
+-----~~--t--
'
------------------~~raw~~~~.w:t;,::~.:::~:::?;::":~;::;~~------,
x_
\--
'119
....,,~~
11,4 otCJ.A <.
'it,IYt
P-.''-1( ft;.t-
II
-........,
l{ftftn ...
l)cJL.(08fALIf~
whn,?J
'-4\t~\1'3
\_~o'-lo"\~~{o1-"l)
~: -C(/~11~
p4,'l~fJHy;--
or
()
__ l-
l..t
vt..-1'---: _. ~~ -~--
. . - - }ll!_u_
.... .~~
-----~""'~-
l-4c--
tA-'}
f)f( (o
LAA...-\~o....\,:H.
0'77~
l.AA'~~'-~\..
0531
We.!>~
PC..C...
~) sl.l.
. ~~ s\;\.
(/4'/
~-v> c -
v-'7
~A
.-
<- -
----~-----
<-
'-c,.~
--- _Y\..
__ ~-- --------
lt,1)'\
r~t.-'1'
l91-"f
r'Sl>..,...,.>
I ~'--,
Dr""'L
1.. \v ~-=-
r-
/c..__ __
orr~
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. Oleo
-z..t-2
/II~
~.....-.-
e.,; ';.;~ ~
to'l-V"
/3 so
U)
Y2_
{;"J
'
7'
ol---l-----'/"-""t,.---~-- - ~~- -~
-J--+--I------1J..J_____ --~- ~-~'1--~~~-~----~
.--f.-J...Lr__:V':.._j __ :z_. k r
,~~~~---~-~_:
---~_$
-~--
_ k~~
-~
---
_/Y~-:!:7r _c_____
-~~~
_u
tG6
--~---~~---~ L\)_ ~. ~-- - =-~~-- fJ -C4'-IJ
h.rvs
=--r::--LC.__:_-+--'--'-_::::_:::---+-'-1-=Co~<(c_o------~-1~-~- V\
-1--_!__L_'-=--~~=If_:._:_:flJ=-;{)---',.~---[~~- ~~ ~-
RA-226 NOTES
Page 1 of 1
EBE::RLINE
SERVICES
~
I
I
#
Date
04/16/13 08:35
Dept
'
PREP
User
JBARNARD
Anal __ _____
Run Number
13-04051
Ra226
1
Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
_if- Hf,tJ ~
~\llD\~~
ii&76
}!J E
~
Page 1 of 1
B.I:::R.-=1N .E
SERVICES
Analysis Code
Run Number
13-04051
Ra226
1
Date
Dept
04/16/13 08:35
PREP
JBARNARD
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
04/17/13 17:19
PREP
LWALKER
04/18/13 14:57
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.81N AP-006 REV12 FOR RA 226 ANALYSIS (SYRINGE FILTERED
SAMPLES-PRECIP-FILTERED-DRIED-OBTAIN FINAL WEIGHT) SUBMIT TO COUNT ROOM.
User
Notes
Eberline Analytical
Oak Ridge Laboratory
JBARNARD
JBARNARD
Lead Carrier
013624P
JBARNARD
0137545
LWALKER
011383P
Acetic Acid
013377001
Ammonium Sulfate
eagent Grade
200 mg/ml
LWALKER
LWALKER
4/18/2013
iiii78
1J.t7
--~.~
~lUJ~2-~-L~~~~~-~c~~~--~~~~~-~-~~~ . .~~---
-~--~-_:_:__:_.~-=----~..N'~-----1
t-"-"'-'--'-'-------t-----1
l<:-6.
19'2_ __
1--~...;..:_,_..,_~ . J((?__
~~~-1--.~~----1 &_ __
- ----~-------
iG79
t117lrJ
l.frm,?
t{II~IJ
'iUCJt
'itt~Ja
['7ol.(ot~,..u,~
_t""l,Yo~~
p . . .'4f f~:-.ty.-
t?t.?Lt ,'irA l l)
t..t~
..-L-Y~ 4-~:t-'1..2
lot.."""-'
~ W~v-
{IL-)
&A-'>
ortro
lA-t..-\~ .....~ l.
077~
L(ltttn
_lJoL-tQ&fALr~ ~~~'-<;.D\. ..
05J/
_, ~ h\k?J l ~oi q<i'S"_A 6-t.) We:>~
tz...t..\
___ 4\t'l\l3 l~C>~-Q~~)1 (~-1-)
Pc.L
l ??.,'f
, L\_ \l9 t,) _\'?>o~os-o ~( ~~~ lq)
-~) s'-l
t9 2-or
\db'?
l( ~~~~7
[f(I)Jl2
- - , _ t( ll )A
--"
Lftt_fto
1~<1'f o~ ~ ( - 4)
--rz,., ~1!4 ~
f?_Q'f/t~dlltl.f}
-) g'__L CAL.
l)o'l->_f"_f&l J.,r,
.l'V\&~d-s"l.
1/V'?
t-v>'-
v-'7
hA
c:::-____
.... -~ --~
"1.-t..... -r
~~~ --~~
,q~,
orl.."
0jJ7
_O~co
/1/ (&?
li~
;c...._
-z_ l._r1.---
/L _,__iL___
~-.
---~~ __-::--__
-L
/yA=_
-- ~ ~--1~--- -- ---
----~--~-1-
----------- - - - - - t -
------ ~---~--
------------
~~JI---
~---~-
f.
_,
----~-----------+----------~-----b------~----~
! -.
-
----
-,
--
.-:~--
RA-228 NOTES
~
1;:: B
~
Page 1 of 1
1;: R l,....j_N E
SERVICES
#
1
Date
Dept
04/16/13 08:35
PREP
User
JBARNARD
Analysis Code
13-04051
Ra228
1
Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
Page 1 of 1
~
EBERI,...,IN-=:
~
SERVICES
#
1
Date
04/16/13 08:35
I
I
Dept
PREP
Ii
User
JBARNARD
~
3
LWALKER
I
04/25/13 18:2SrPREP -- -LWALKER
Analysis Code
Run Number
13-04051
Ra228
1
Notes
ALIQUOT ED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
--------------
..
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
-----~~-----
--
j!J E
~
Page 1 of 1
BE;:RJ,...,I NE
SERVICES
Date
Dept
04/16/13 08:35
PREP
JBARNARD
04/22/13 12:14
PREP
LWALKER
=3
04/25/13 18:25
PREP
LWALKER
User
__
I
04/29/13 07:52
,n-~--~--
CHEM- TSMITH-
13-04051
Analysis Code
Run Number
Ra228
1
Notes
ALIQUOTED ALL SAMPLES AND FILTERED SUSPENDED FRACTIONS- ADDED SPIKES AND TRACERSPH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
--
---~-'"
Followed steps 12.7 to 12.15 in AP-007 rev. 17 . ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil. and took to count room l
ii85
Eberline Analytical
Oak Ridge Laboratory
r
I
SERVICES
Run
Ra228
1
c
Reagent
ID
Reagent
Name
Reagent
Concentration
Analyst
ID
' CWl
Date
Recorded
I
1
4/16/20l3"i
~~
4/16/2013
i
........
...... '"'""!
Barium Carrier
JBARNARD
cwvw'i
.. .....
JBARNARD~r4/16/.2o131
i Lead Carrier
--r~-N.itric Acid
'''(""'
4/16/2013
.. -~~-~--~~)
JBARNARD
I 4/16/2013 I
...
~.-
4/25/2013 I
................................ ~
Ammonium Sulfide
LWALKER
...........
4/25/2013 I
T4/2s;2o13
~~
LWALKER
4/25/2013
' 4/25/2013
TSMITH
J 4/29/20l3:
TSMITH ............. 1..
. ~~~ ~-..-~~""T~~-~-1
TSMITH
14/29/2013 :
4/29/20131
...... y
18M
.. L..
TSMITH
TSMITH
!:.4/29/2013
I
...J
l 4/29/2013 I
j"'"""~~"m~VV'~~~~m~~M,lm.~"''"
vn Ah''""'"">
Lf) 4Uo
Q~
~CJ...C.-'-11) 0 ~
0 C. ~.
.*
r\0
~=---~=v~IJkJr)_JC3P':lJ~~f_bu.~j)_ -----L4~4:
____ -~---l(h..tt'-12 _ _ G-~ __ -----~---1---cr ri;:L
------- ~---- VrJ.JtJn .. _.ll_\.~_ -----~------- o(ttf.t,
_________ ~---- <:it::tWt: ___ L:J~kJti.PU-4-lJ.!(' __ _{2 ~. ~" '~4..r1
__ ____ .-- 'f t\.11~ ____ _l_ l_p_!l_f&~~ (~~ Q~~ 0'-t \l
-----~L1.k'JO _. L')...c::.~L~'6-i~.U~'1 ____Li.l.l?l~-- D YC"'YI""UID L
-L 2D'l~YII!II. .:.1- _J.d. t.-ot--- _ nK1?
o""
f-..
..--- ,__
79
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'.t.~uJ_~ l 0 2L
"?D-
1~ _
--v~...-
:1,..-L.-
-(.._~..-
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c._:
L,
/h
~~YLf {)/y.
SA.f_~
S/37:;-7_
'>It-rD7
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,.
C- _
-j
'-' _
c._._.,, ~
f1..A-tl
flA-V-
'--'-.~
.,u2
~ _. ~ ..
~
- ______ . f((l)p? - JJ:O!to2LD!J~-~ .~~t=----- tL!fltt- __ t.-
() ll-r
l/11
L- ./
n '<t'5
f2./Pr c......-
fJSJ'O
-l \ o'2-
~
'1.---
fl-+-y-
-----------------~-~----
------
------~
_ . . . .--.-~
c_ .
~ c....--L
~1
_\C .J . [
. . ..
---~--------------t----------t------1-----l-------
----------~--+--------+----+-~----+--.
----------------- - - - - - . 1 - - - - - - - - - . 1 - - - - - - f - - - - o / '
-~
- -
---~
-------------f----+------t--------1---~if~
; .
- -
... --~---
...:;:<
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-----
; f
--------t
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. - - ------------ - -----
!-...:
----------+-------t---~-+--------+---r!J
J-q
'_;,
. . . ___L-
SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
13-04051
UUISO
Run 1
Internal
Work Order
Analysis Code
Sample
Desc
Client
ID
Login
CPM
LCS
LCS
04/09/13 00:00
MBL
BLANK
04/09/13 00:00
Sample
Aliquot
Sample
Date
1.0000E+00
-~------
--------
03
Date Received
PZ-105-SS TOT
DUP
-----
~------
Lab Deadline
Client
4/30/2013
04
DO
05
TRG
--------
Project
PZ-105-SS TOT
PZ-105-SS DIS
06
TRG
04/04/13 15:06
1.0000E+OO
46
j 04/04/13 15:06
1.0000E+OO
46
--04/04/13 15:06
-------
42
S-10 TOT
07
TRG
S-10 DIS
pCi
08
TRG
42
09
TRG
LR-104 DIS
WA
10
TRG
DUP 01 TOT
11
TRG
DUP 01 DIS
45
Alpha Spectroscopy
12
TRG
U-232
13
TRG
----------
Radiometric Tracer
------------+-------------
Radiometric Sol#
U-10a
14
TRG
1.0000E+OO
48
04/04/13 00:00
1.0000E+OO
04/04/13 00:00
1.0000E+OO
04/04/13 00:00
1.0000E+OO
04/04/13 09:30
1.0000E+OO
04/04/13 OB:30!
1.0000E+OO
------~------+----------------
43
DUP 02 DIS
43
FB at PZ-110-SS TOT
04/04/13 00:00
------------
-----
1.0000E+OO
48
DUP 02 TOT
+----------------
-----
04/04/13 15:52
----~-------
Instrument Type
1.0000E+OO
-~--
-------------- - - - - - -
Method
-~---
04/04/13 15:52
45
-----
Matrix
1.0000E+OO
04/04/13 15:25N.OOOOE+OO
--~-
1.0000E+OO
-----------
-~-----
-~-~-
LR-104 TOT
-----~
Aliquot Units
04/04/13 15:25
----
Activity Units
----
~----~
Report Level
46
------------+---~-
---------------
1.0000E+OO
~~~-------~
42
--------~----~-
1-----------------~--~---------
-~----
19.098
15
FB at PZ-110-SS DIS
42
TRG
MW-103 TOT
-----------
--------~-
Carrier
-----
TRG
- - - - - -
48
04/05/13 09:50
1.0000E+OO
------~
-----~-----
17
TRG
MW-103 DIS
48
04/05/13 09:50
1.0000E+OO
18
TRG
PZ-200-SS TOT
37
04/05/13 11 :1 0
1.0000E+OO'
19
TRG
PZ-200-SS DIS
37
04/05/13 11:1 0
1.0000E+OO
-----!
~----
g:)
g;
Ul
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
13-04051
UUISO
Run 1
Internal
Fraction
Sample
Desc
LCS
-~
I
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
o.6104
11.1
MBL I
0.6068
11.6 r - - l o o o
DUP I
0.6050
DO I
0.5980
TRG
0.6003
I .
TRG
o.6041
TRG I
0.5~ 11.4
11.6
11.5
oooj
0.6002 I
TRG
0.5998
TRG
o.6012
TRG
0.5945
1
I
11.5
; ;
:1
0.00
0.001
0.00
:::
--'1
-0~~~J-~
-~-
~oo,
11.3 I_
0.00
TRG
0.5965 !
11.4
0.00
0.5962
---~
11.3
r-
I ---
-t'
,
-t---__j
l
0.5933
TRG
o.ool
TRG
0.5933 I
~-
11.5 [
2*
+
+-----1
!_
SAF
--
0.00
SAF
1*
Mean
% Rec
11.4
TRG
-~-
ID.OOf
o.5956 .
~-
11.5
11.4
Grav
% Rec
0.00
TRG
Grav Filter
Net(g)
I
~00
'
Grav Filter
Final (g)
o.ooi
I
11 ~
0.6016j_~_
_ : : : : :
11.4
TRG i
: : :
Grav Filter
Tare (g)
~G
I
Tracer
Aliquot (g)
--f
-----+----
~--______
--i-
I
1
-+----1
0.00
11.4 I
0.00
l
c;n
~!)
t~
II!~
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
L~ ~
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
13-04051
UUISO
Run 1
Internal
Fraction
Sample
Desc
01
LCS
02
MBL
03
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
04/16/13 08:25
JBARNARD
04/16/13 08:25
JBARNARD
DO
--------+--- ---
JBARNARD
04/16/13 08:25
JBARNARD I
I o4t16/13 08:25
JBARNARD I
Sep tO
By
--------
04/16/13 08:25
DUP
04
Sep tO
Date/Time
_os
I TRG
06
TRG
07
TRG
08
TRG
04/16/13 08:25
JBARNARD I
TRG
04/16/13 08:25
JBARNARD
TRG
t-
--
r-j
+-I
Sep t1
By
I
I
I
JBARNARD
I 04/16/13 o8:25
Sep t1
Date/Time
---
09
f----
10
r-----
11
I
I
TRG
12
i TRG
13
I TRG
----------
04/16/13 08:25
JBARNARD
-- --
14
04/16/13 08:25
-----.-
JBARNARD
-----
15
II : : :
l- 04/16/13 08:25
JBARNARD
16
TRG
I 04/16/13 08:25
JBARNARD
17
TRG
18
TRG
I 04/16/13 08:25
19
TRG
-L-~---
-----
--
--
JBARNARD i
04/16/13 08:25
04/16/13 08:25
--
JBARNARD
JBARNARD
--r--
tl!'
lldl;,
lO
~~-
SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Oak Ridge Laboratory
~
0
.!I!
~
ca
~
OK
MDA
Flag
01
U-234
LCS
LCS
pCi/1
7.85E+OO
1.07E+OO
8.92E-02
02
U-234
MBL
BLANK
pCi/1
4.51E-02
5.14E-02
6.78E-02
03
U-234
DUP
PZ-105-SS TOT
pCi/1
2.60E+OO
4.61E-01
9.02E-02
04
U-234
DO
PZ-105-SS TOT
pCi/1
2.62E+OO
4.55E-01
7.94E-02
OK
en
05
U-234
TRG
PZ-105-SS DIS
pCi/1
2.58E+OO
4.43E-01
6.90E-02
OK
::l
::l
06
U-234
TRG
S-10 TOT
pCi/1
2.29E-01
1.15E-01
8.09E-02
OK
07
U-234
TRG
S-10 DIS
pCi/1
1.25E-01
1.00E-01
1.07E-01
OK
08
U-234
TRG
LR-104 TOT
pCi/1
2.60E+OO
4.42E-01
5.07E-02
OK
09
U-234
TRG
LR-104 DIS
pCi/1
2.72E+OO
4.51E-01
5.62E-02
OK
10
U-234
TRG
DUP 01 TOT
pCi/1
2.55E-01
1.09E-01
5.38E-02
OK
11
U-234
TRG
DUP 01 DIS
pCi/1
2.04E-01
1.08E-01
6.66E-02
OK
12
U-234
TRG
DUP 02 TOT
pCi/1
1.59E-01
9.76E-02
7.93E-02
OK
13
U-234
TRG
DUP 02 DIS
pCi/1
1.77E-01
1.01E-01
6.69E-02
OK
14
U-234
TRG
FB
at PZ-110-SS TOT
pCi/1
1.57E-02
2.98E-02
5.52E-02
OK
15
U-234
TRG
FB
at PZ-110-SS DIS
pCi/1
4.42E-02
6.79E-02
1.16E-01
OK
16
U-234
TRG
MW-103 TOT
pCI/1
4.07E+OO
6.75E-01
1.19E-01
OK
17
U-234
TRG
MW-103 DIS
pCi/1
3.17E+OO
5.52E-01
5.99E-02
OK
C"l
18
U-234
TRG
PZ-200-SS TOT
pCi/1
5.42E-01
1.80E-01
8.08E-02
OK
19
U-234
TRG
PZ-200-SS DIS
pCi/1
5.32E-01
1.77E-01
9.34E-02
OK
or-
(/)
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Q)
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Q)
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Ill
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Q)
Q)
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96.33
RPD
Flag
Activity
Units
Q..
Q..
I;~
LCS
Flag
Client
Identification
:I
LCS
%R
Sample
Desc
g~
LCS
Known
Nuclide
.E
ujl
Lab
Fraction
"
Results
Error Estimate
MDA
8.15E+OO
Blank
Flag
OK
OK
OK
OK
OK
~
~
.g
0
.!!!
~
ct
01
U-234
LCS
04/09/13 00:00
1.00E+OO
110.41
0.00
0.00
02
U-234
MBL
04/09/13 00:00
1.00E+OO
134.21
0.00
0.00
03
U-234
DUP
04/04/13 15:06
1.00E+OO
117.95
0.00
0.00
04
U-234
DO
04/04/13 15:06
1.00E+OO
121.42
0.00
0.00
en
05
U-234
TRG
04/04/13 15:06
1.00E+OO
125.70
0.00
0.00
~
~
06
U-234
TRG
04/04/13 15:25
1.00E+OO
101.21
0.00
0.00
07
U-234
TRG
04/04/13 15:25
1.00E+OO
81.32
0.00
0.00
08
U-234
TRG
04/04/13 15:52
1.00E+OO
117.88
0.00
0.00
09
U-234
TRG
04/04/13 15:52
1.00E+OO
123.81
0.00
0.00
10
U-234
TRG
04/04/13 00:00
1.00E+OO
132.22
0.00
0.00
11
U-234
TRG
04/04/13 00:00
1.00E+OO
100.34
0.00
0.00
12
U-234
TRG
04/04/13 00:00
1.00E+OO
95.45
0.00
0.00
13
U-234
TRG
04/04/13 00:00
1.00E+OO
102.84
0.00
0.00
t!
14
U-234
TRG
04/04/13 09:30
1.00E+OO
144.40
0.00
0.00
...c
15
U-234
TRG
04/04/13 09:30
1.00E+OO
91.62
0.00
0.00
16
U-234
TRG
04/05/13 09:50
1.00E+OO
90.80
0.00
0.00
17
U-234
TRG
04/05/13 09:50
1.00E+OO
93.69
0.00
0.00
18
U-234
TRG
04/05/13 11:10
1.00E+OO
105.27
0.00
0.00
19
U-234
TRG
04/05/1311:10
1.00E+OO
109.45
0.00
0.00
SAF
SeptO
Date/Time
Sep t1
Date/Time
:::1
CD
CD
Cl
I'll
I'll
:IE
Cl
;::
CD
CD
.E
Cl
c
[,;,~
Mean
%Rec
Grav
%Rec
Sample
Date
U)
tO
Radiometric
%Rec
Sample
Desc
Q.
Q.
~'1l
Sample
Aliquot
Nuclide
~,
Lab
Fraction
.E
~I
Eberline Services
Oak Ridge Laboratory
a::
..:-
Eberline Services
Oak Ridge Laboratory
Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
U-234
LCS
02
U-234
MBL
03
U-234
Halflife
(days)
Count
Time
Counts
Bkg
CPM
Eff
Detect
Carrier
04/19/13 11:36
A_Spec
Alpha_018
7.00 E-03
17.8
04/19/13 11:36
A_Spec
Alpha_022
3.00 E-03
15.3
I
I
DUP
04/19/1311:36
A_Spec
Alpha_024
8.00 E-03
17.1
--- - -
0
(.)
.~
~
.,
s::
"'(
04
U-234
DO
04/19/13 11:36
A_Spec
Alpha_025
6.00 E-03
17.4
tn
05
U-234
TRG
04/19/1311:36
A_Spec
Alpha_027
4.00 E-03
17.3
::;:)
::;:)
06
U-234
TRG
04/19/13 11:36
A_Spec
Alpha_029
0.00 E+OO
19.5
07
U-234
TRG
04/19/13 11:57
A_Spec
Alpha_033
0.00 E+OO
18.2
08
U-234
TRG
04/19/13 11:57
A_Spec
Alpha_034
1.00 E-03
18.6
09
U-234
TRG
04/19/13 11 :57
A_Spec
Alpha_035
2.00 E-03
18.3
10
U-234
TRG
04/19/13 11:57
A_Spec
Alpha_037
2.00 E-03
17.8
11
U-234
TRG
04/19/13 11:57
A_Spec
Alpha_040
2.00 E-03
19
12
U-234
TRG
04/19/13 11:57
A_Spec
Alpha_041
4.00 E-03
19.8
13
U-234
TRG
04/19/13 11 :57
A_Spec
Alpha_042
2.00 E-03
18.5
t:
14
U-234
TRG
04/19/13 14:33
A_Spec
Alpha_003
3.00 E-03
17.5
.E
0
c.
c.
:I
...
15
U-234
TRG
04/19/13 14:33
A_Spec
Alpha_004
1.20 E-02
19.4
Cl)
16
U-234
TRG
04/19/13 14:33
A_Spec
Alpha_010
1.30 E-02
19.7
17
U-234
TRG
04/19/13 14:33
A_Spec
Alpha_011
1.00 E-03
19.7
18
U-234
TRG
04/19/13 14:33
A_Spec
Alpha_013
5.00 E-03
18.7
19
U-234
TRG
04/19/13 14:33
Alpha_014
9.00 E-03
18.5
tJ)
s::::
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E
Cl)
Cl
I'll
s::::
I'll
==Cl
s::::
;:
Cll
Cl)
.5
Cl
s::::
m
CilU
if.J(~
t:~
'
.
A_Spec
-
L___
----
--
a:
Eberline Services
Oak Ridge Laboratory
LCS
Known
LCS
%R
LCS
Flag
100.95
OK
RPD
Flag
MDA
Flag
Lab
Fraction
Nuclide
Sample
Desc
Client
Identification
Activity
Units
01
U-238
LCS
LCS
pCi/1
8.02E+OO
1.09E+OO
8.88E-02
02
U-238
MBL
BLANK
pCi/1
2.11E-02
4.54E-02
8.82E-02
03
U-238
DUP
PZ-105-SS TOT
pCi/1
1.82E+OO
3.62E-01
6.27E-02
04
U-238
DO
PZ-105-SS TOT
pCi/1
1.64E+OO
3.32E-01
S.OOE-02
OK
05
U-238
TRG
PZ-105-SS DIS
pCi/1
1.42E+OO
3.00E-01
8.65E-02
OK
06
U-238
TRG
S-10 TOT
pCI/1
2.41E-01
1.18E-01
8.46E-02
OK
07
U-238
TRG
S-10 DIS
pCi/1
8.91E-02
8.62E-02
1.07E-01
OK
08
U-238
TRG
LR-104 TOT
pCi/1
2.11E+OO
3.84E-01
5.78E-02
OK
09
U-238
TRG
LR-104 DIS
pCi/1
1.94E+OO
3.58E-01
4.88E-02
OK
10
U-238
TRG
DUP 01 TOT
pCi/1
1.21E-01
7.40E-02
4.68E-02
OK
11
U-238
TRG
DUP 01 DIS
pCI/1
1.43E-01
9.20E-02
7.82E-02
OK
12
U-238
TRG
DUP 02TOT
pCi/1
1.04E-01
8.94E-02
1.17E-01
OK
13
U-238
TRG
DUP 02 DIS
pCi/1
1.32E-01
8.79E-02
7.31E-02
OK
14
U-238
TRG
FB
at PZ-110-SS TOT
pCI/1
-7.13E-03
2.17E-02
5.91E-02
OK
15
U-238
TRG
FB
at PZ-110-SS DIS
pCi/1
-1.26E-02
3.12E-02
8.90E-02
OK
16
U-238
TRG
MW-103 TOT
pCi/1
3.72E+OO
6.30E-01
8.86E-02
OK
co
co
17
U-238
TRG
MW-103 DIS
pCI/1
3.00E+OO
5.31E-01
9.01E-02
OK
Cl
18
U-238
TRG
PZ-200-SS TOT
pCi/1
5.22E-01
1.74E-01
5.61E-02
OK
19
U-238
TRG
PZ-200-SS DIS
pCi/1
5.84E-01
1.84E-01
6.26E-02
OK
Results
Error Estimate
MDA
7.94E+OO
Blank
Flag
OK
OK
OK
I
OK
OK
~
0
.!(!
~
CQ
~I
en
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0
c.
c.
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111
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Radiometric
%Rec
Mean
%Rec
Grav
%Rec
Sample
Desc
Sample
Date
01
U-238
LCS
04/09/13 00:00
1.00E+OO
110.41
0.00
0.00
U-238
MBL
04/09/13 00:00
1.00E+OO
134.21
0.00
0.00
DUP
04/04/13 15:06
1.00E+OO
117.95
0.00
DO
04/04/13 15:06
1.00E+OO
121.42
0.00
0.00
------
03
U-238
04
U-238
SAF
05
U-238
TRG
04/04/13 15:06
1.00E+OO
125.70
0.00
0.00
::J
::J
06
U-238
TRG
04/04/13 15:25
1.00E+OO
101.21
0.00
0.00
07
U-238
TRG
04/04/13 15:25
1.00E+OO
81.32
0.00
0.00
08
U-238
TRG
04/04/13 15:52
1.00E+OO
117.88
0.00
0.00
09
U-238
TRG
04/04/13 15:52
1.00E+OO
123.81
0.00
0.00
10
U-238
TRG
04/04/13 00:00
1.00E+OO
132.22
0.00
0.00
11
U-238
TRG
04/04/13 00:00
1.00E+OO
100.34
0.00
0.00
12
U-238
TRG
04/04/13 00:00
1.00E+OO
95.45
0.00
0.00
13
U-238
TRG
04/04/13 00:00
1.00E+OO
102.84
0.00
0.00
14
U-238
TRG
04/04/13 09:30
1.00E+OO
144.40
0.00
0.00
...c::
15
U-238
TRG
04/04/13 09:30
1.00E+OO
91.62
0.00
0.00
16
U-238
TRG
04/05/13 09:50
1.00E+OO
90.80
0.00
0.00
17
U-238
TRG
04/05/13 09:50
1.00E+OO
93.69
0.00
0.00
18
U-238
TRG
04/05/13 11 :10
1.00E+OO
105.27
0.00
0.00
19
U-238
TRG
04/05/13 11:10
1.00E+OO
109.45
0.00
0.00
:I
(/)
Ill
Ill
Cl
I'll
c::
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Cl
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Ill
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Sep t1
Date/Time
0.00
en
Q.
Q.
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Date/Time
-- ---
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Sample
Aliquot
Nuclide
02
Lab
Fraction
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Oak Ridge Laboratory
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Oak Ridge Laboratory
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0
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Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
U-238
LCS
02
U-238
03
U-238
04
U-238
DO
05
U-238
06
Halflife
(days)
Count
Time
Counts
Bkg
CPM
Eff
Detect
Carrier
04/19/13 11:36
A_Spec
Alpha_018
7.00 E-03
17.8
MBL
04/19/13 11 :36
A_Spec
Alpha_022
8.00 E-03
15.3
DUP
04/19/13 11 :36
A_Spec
Alpha_024
2.00 E-03
17.1
04/19/13 11 :36
A_Spec
Alpha_025
2.00 E-03
17.4
TRG
04/19/13 11:36
A_Spec
Alpha_027
9.00 E-03
17.3
U-238
TRG
04/19/13 11:36
A_Spec
Alpha_029
6.00 E-03
19.5
07
U-238
TRG
04/19/13 11 :57
A_Spec
Alpha_033
0.00 E+OO
18.2
08
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_034
2.00 E-03
18.6
09
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_035
1.00 E-03
18.3
10
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_037
1.00 E-03
17.8
11
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_040
4.00 E-03
19
12
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_041
1.50 E-02
19.8
13
U-238
TRG
04/19/13 11:57
A_Spec
Alpha_042
3.00 E-03
18.5
14
U-238
TRG
04/19/13 14:33
A..,Spec
Alpha_003
4.00 E-03
17.5
...c
15
U-238
TRG
04/19/13 14:33
A_Spec
Alpha_004
5.00 E-03
19.4
16
U-238
TRG
04/19/13 14:33
A_Spec
Alpha_010
5.00 E-03
19.7
17
U-238
TRG
04/19/13 14:33
A_Spec
Alpha_011
6.00 E-03
19.7
18
U-238
TRG
04/19/13 14:33
A_Spec
Alpha_013
1.00 E-03
18.7
19
U-238
TRG
04/19/13 14:33
A_Spec
Alpha_014
2.00 E-03
18.5
or-
en
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:::J
II
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Q.
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CD
CD
Cl
I'll
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Cl
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CD
CD
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Cl
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Oak Ridge Laboratory
Lab
Fraction
Nuclide
" r-----x=---01
f5
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iii
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q:
en
Client
Identification
Activity
Units
LCS
LCS
pCi/1
Results
IError Estimate I
4.29E-011
1.74E-011
MDA
7.98E-02
LCS
Known
LCS
%R
LCS
Flag
RPD
Flag
MDA
Flag
U-235
r----
DO
PZ-105-SS TOT
pCi/1
1.09E-011
8.69E-021
9.32E-02
OK
-----~--+--~--------r---~---+---~--+---~---+------r---~-----+----~
U-235
TRG
PZ-105-5S DIS
pCi/1
8.02E-021
7.36E-021
8.51E-02
OK
06
U-235
TRG
S-10 TOT
pCi/1
2.76E-021
4.69E-021
7.95E-02
OK
07
U-235
TRG
S-10 DIS
pCi/1
1.83E-021
4.39E-021
9.21E-02
OK
08
U-235
TRG
LR-104 TOT
pCi/1
1.65E-011
1.03E-011
8.98E-02
OK
09
U-235
TRG
LR-104 DIS
pCi/1
1.59E-011
9.98E-021
8.69E-02
OK
10
U-235
TRG
DUP 01 TOT
pCI/1
1.15E-021
2.76E-021
5.80E-02
OK
11
U-235
TRG
DUP 01 DIS
pCi/1
3.44E-021
5.84E-021
1.03E-01
OK
12
U-235
TRG
DUP 02 TOT
pCI/1
5.55E-031
3.59E-02I
9. 78E-02
OK
13
U-235
TRG
DUP 02 DIS
pCi/1
1.18E-011
9.06E-021
7 .20E-02
OK
t:
14
U-235
TRG
FB at PZ-110-SS TOT
pCi/1
3.45E-021
4.46E-021
6.21E-02
OK
15
U-235
TRG
FB at PZ-110-SS DIS
pCi/1
-3.50E-031
3.96E-021
1.21E-01
OK
16
U-235
TRG
MW-103 TOT
pCi/1
3.73E-011
1.71E-011
1.03E-01
OK
17
U-235
TRG
MW-103 DIS
pCi/1
2.66E-011
1.42E-011
1.06E-01
OK
::J
::J
:I
(/)
.....1:
Cll
E
Cll
Blank
Flag
OK
(3
Sample
Desc
05
a.
a.
...s::
OK
3.70E-021
5.53E-021
8.99E-02
OK
MBL
BLANK
pCi/1
U-235
02
1-----j-~~---~
-T----------t-----+-~ -r----~---~~--~---4----~--4---~--_j
03
1.11E-011 8.52E-021
6.78E-02
NA
OK
U-235
DUP
PZ-105-SS TOT
pCI/1
04
.E
.!!:!
U-235
Cl
ns
1:
fl ~~: ~~~~-;;;;~--t~S~~~t-+--+--l-=I~CJ
1:
w
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tit~
(U
U-235
TRG
PZ-200-5S TOT
pCi/1
6.38E-021
6.59E-021
6.95E-02
OK
U-235
TRG
PZ-200-SS DIS
pCi/1
3.76E-021
5.62E-021
9.15E-02
OK
~
c::
~I
.g
8
.!Q
Sample
Date
01
U-235
LCS
04/09/13 00:00
1.00E+OO
110.41
0.00
0.00
02
U-235
MBL
04/09/13 00:00
1.00E+OO
134.21
0.00
0.00
03
U-235
DUP
04/04/13 15:06
1.00E+OO
117.95
0.00
0.00
04
U-235
DO
04/04/13 15:06
1.00E+OO
121.42
0.00
0.00
en
05
U-235
TRG
04/04/13 15:06
1.00E+OO
125.70
0.00
0.00
::J
::J
06
U-235
TRG
04/04/13 15:25
1.00E+OO
101.21
0.00
0.00
07
U-235
TRG
04/04/13 15:25
1.00E+OO
81.32
0.00
0.00
08
U-235
TRG
04/04/13 15:52
1.00E+OO
117.88
0.00
0.00
09
U-235
TRG
04/04/13 15:52
1.00E+OO
123.81
0.00
0.00
10
U-235
TRG
04/04/13 00:00
1.00E+OO
132.22
0.00
0.00
11
U-235
TRG
04/04/13 00:00
1.00E+OO
100.34
0.00
0.00
12
U-235
TRG
04/04/13 00:00
1.00E+OO
95.45
0.00
0.00
..5
13
U-235
TRG
04/04/13 00:00
1.00E+OO
102.84
0.00
0.00
t::
0
14
U-235
TRG
04/04/13 09:30
1.00E+OO
144.40
0.00
0.00
15
U-235
TRG
04/04/13 09:30
1.00E+OO
91.62
0.00
0.00
16
U-235
TRG
04/05/13 09:50
1.00E+OO
90.80
0.00
0.00
17
U-235
TRG
04/05/13 09:50
1.00E+OO
93.69
0.00
0.00
18
U-235
TRG
04/05/1311:10
1.00E+OO
105.27
0.00
0.00
19
U-235
TRG
04/05/1311:10
1.00E+OO
109.45
0.00
0.00
::I
....c
G)
E
G)
Ol
I'CI
I'CI
:E
Ol
;:
G)
G)
c
c
w
a,
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G,
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SAF
SeptO
Date/Time
Sept1
Datemme
U)
~I
Mean
%Rec
Grav
%Rec
Sample
Desc
Sample
Aliquot
Radiometric
%Rec
Nuclide
a.
a.
Lab
Fraction
Eberline Services
Oak Ridge Laboratory
Eberline Services
Oak Ridge Laboratory
c::
::s
a:
.!!!
~
.,
c::
oq;
Halflife
(days)
Count
Time
Bkg
CPM
Sample
Desc
Counting
Date/Time
U-235
LCS
04/19/13 11:36
A_Spec
Alpha_018
2.00 E-03
17.8
U-235
MBL
04/19/13 11:36
A_Spec
Alpha_022
4.00 E-03
15.3
03
U-235
DUP
04/19/13 11:36
A_Spec
Alpha_024
1.00 E-03
17.1
04
U-235
DO
04/19/13 11:36
A_Spec
Alpha_025
0.00 E+OO
17.4
en
05
U-235
TRG
04/19/1311:36
A_Spec
Alpha_027
4.00 E-03
17.3
::J
::J
06
U-235
TRG
04/19/13 11 :36
A_Spec
Alpha_029
2.00 E-03
19.5
07
U-235
TRG
04/19/1311:57
A_Spec
Alpha_033
1.00 E-03
18.2
08
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_034
0.00 E+OO
18.6
09
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_035
0.00 E+OO
18.3
10
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_037
1.00 E-03
17.8
11
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_040
0.00 E+OO
19
12
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_041
4.00 E-03
19.8
13
U-235
TRG
04/19/13 11:57
A_Spec
Alpha_042
1.00 E-03
18.5
14
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_003
2.00 E-03
17.5
...
15
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_004
7.00 E-03
19.4
Cl)
16
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_010
4.00 E-03
19.7
17
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_011
0.00 E+OO
19.7
18
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_013
1.00 E-03
18.7
19
U-235
TRG
04/19/13 14:33
A_Spec
Alpha_014
4.00 E-03
18.5
Lab
Fraction
Nuclide
01
02
~
1------
r---
.g
.E
0
Q.
Q.
:::1
en
Detect
Carrier
Counts
Eff
'
~-
r::::
~I
E
Cl)
Cl
CG
r::::
CG
:E
Cl
r::::
;:
Cl)
Cl)
.5
Cl
r::::
w
Gilt)
Uw-1,
ll:r.!'
~*
13-04051-UUIS0-1 (pCi/1) in WA
Tracer ID: U-1 Oa
/'\.- \) L-"
Internal
Fraction
Sample
Desc
Client
ID
,
i
Sample
Aliquot
11.5887
1.0000
0.6050
11.5543
o.598o
11.4206
o.oo
11.4645
o.oo
07 ...-'\?TRG I
S-10 DIS
1.0000
TRG
LR-104 TOT
09
TRG
LR-104 DIS
10
TRG-t
DUP 01 TOT
11
TRG
-~uP_~~-~~2"-
TRG
FBatPZ-110-SSTOT
TRG
I
FB at PZ-110-SS DIS
17
TR~--
18
~.1 TRG
I
Q,
ftwn.J,
I
I
PZ-200-SS DIS
_1
II
11.5371
0.5991
11.4416
+--~:~~~61
0.00
0.6012
11.4817
1-------+---
0.00
--+-
----=
-t--
0.00
0.00
1-.
-+--~__j____o.o~----1-~-0.00
0.00
1
0.00 i
11.35381
04/04/13 09:30
1.0000
0.5956 I
11.3748 I
04/05/13 09:5o
1.oooo
o.5933 :
11.33081
0. 4/05/13 09:50
1.0000
0.5965
04/05/13 11:1 o
1.0000
1.0000
J__o.~:~--~
1
I
i
0.5933
11.3308
-11.3862
SAF
2*
11.4454
11.4550
SAF
1*
~-~'
0.00 I
I
11.4894 I
0.5998
1.0000 --1---~_:_5945
04/04/1309:30
~05/13 11:10
I
I
0.6041
OOO~=r-- 0.599-3 -~
MW-103 DIS
PZ-200-SS TOT
1.0000
04/04/130o:oo __T_1.000C>__j
~TRG
G'
DUP 02 DIS
-"'1---=--:_--ri
04/04/13 15:52 I
13\i
~"<
Radiometric
%Rec
0.6068 I
1.0000
08
Radiometric
Tracer (pCi)
1.0000
1.0~0.6003
TRG
11.6574
S-10 TOT
Tracer
ACT(dpm)
II
0.61~~-
os-t~TRG
12
Tracer
Aliquot(g)
1.0000
1.oooo
05
I
I
~~---i
0.00
=f
____J_o:oo_J_
~--
0.00
-- I
O.Oa~---r=~~~
I
Eberline Services
Oak Ridge Laboratory
Isotope
Sol#
U-234
U-8a
U-238
Activity
dpmlg
U-8a
Solution
Date
Approx
Addition
35.24~~201_3
0.500
34.350,
0.500
4/16/2013
LCS
MS
LCSD
MSO~
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
0.5133
JBARNARD
-LCS
--
---~MS
Known
pCi
I----
1----
Sol#
0.293
7.94
0.5133
0.286
a.~m~g
Solution
Date
Volume
Used(g)
I
1
Approx
Addition
U-10a
19.098 4/16/2013
0.6104
0.6300
--0.
02
U-232
U-10a
19.098 4/16/2013
0.6068
0.6300
-'.:'1 .. 59:;~~'~ 9
03
U-232
U-10a
19.098 4/16/2013
0.6050
04
U-232
-----
05
U-232
06
U-232
07
U-232
U-10a
08
U-232
U-10a
09
U-232
10
U-232
11
U-232
U-232
13
14
I
!
U-232
U-232
U-10a
U-10a
0.6041
0.6300
19.098 4/16/2013
0.5991
19.098 4/16/2013
0.6016
0.6300
U-1 ,,
_j_
19.098 4/16/2013
0.6002
0.6300
U-1 Oa
19.098 4/16/2013
0.5979
0.6300
U-10a
19 098
4/16/2013
0.5993
0.6300
--(1'
l:.fi02 q
U-10a
19.098 4/16/2013
0.5998
0.6300
~~0 ll
597
U-10a
U-10a
19 098
4/16/2013
0.5945
0.6300
0.6300
19.098 4/16/2013
0.6012
0.6300
0.6300
-------
U-232
U-10a
19.0981 4/16/2013
0.5956
16
U-232
U-10a
19.0981 4/16/2013
0.5933
=~:
Printer Tapes
Matrix Spike
:3
-0.
-~-~~&2
0.6300
17
U-232
U-10a
19.098 4/16/2013
0.5965
0.6300
18
U-232
U-10a
19.098 4/16/2013
0;5933
0.6300
19
U-232
U-10a
1--
---
19.098 4/16/2013
0.5962
-R0
59~:+5
-0 .. 595t:.
'~
II
0.6300
-~
-~3" 5::.-~~;:~::
-0.5965
-0.5933 9
li'";li
0.000
lb ~~
1
:::;
-~:1=
596:?
Error
Estimate
0.00
0.000
0.00
0.000
~-
':l
---~--
--
6 ~Ji~f3:
. . . o. 6fJ4 ~i.
- [1 ~
g:,
0.000
....
f--~-
m:'
.......
0.000
o.ool
o.ool
15
1 - - - - - -\--
0.001
Estimate
------
19.0981 4/16/2013
0.000
+---~f---
0.6300
0.5980
0.6300
u~
OOOi
pCi
MSD
Added
pCi
------
0.6003
i-----
i Estimate
Error
----
LCSD
Known I
Error
-;
6~).50
19.098 4/16/2013
I
I
--
0.6300
19.098 4/16/2013
1-
..
LCS
U-~
Added
pCi
'
0.6104 g
01
12
Isotope
Activity
dpm/g
Error
Estimate
8.15
Tracers -
fraction
Page 1 of 1
Printed: 4/16/2013 8:25AM
Eberline Analytical
Oak Ridge Laboratory
Aliquot Worksheet
JBARNARD
Engineering Management Support, Inc.
Lab
Fraction
01
02
-----o3
04
_05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
~-
I
....
ClientiD
LCS
BLANK
1----PZ-105-SS TOT
(..,)
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
PZ-105-SS TOT
PZ-105-SS DIS
S-10 TOT
S-10 DIS
LR-104 TOT
--LR-104 DIS
-DUP 01 TOT
DUP 01 DIS
DUP 02 TOT
DUP 02 DIS
FB at PZ-110-SS TOT
FB at PZ-110-SS DIS
MW-103 TOT
MW-103 DIS
PZ-200-SS TOT
PZ-200-SS DIS
---~--
Comments
Ci)~)
~~;,~,
Sample
Technician:
Dilution Data
Muffle Data
Ratio
Post/Pre
NoofDils ..
Aliquot Data
Oil Factor
Aliquot
Ratio
NetEquiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.00008+00
1.0000E+OO
1.0QOOE+OO
1.0000E+OO
1:QOOOE+OO
1.0000E+OO
1.ooooe+oo
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OQ
1.0000E+OO
t.OOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO
1.00QOE+OO
1.0000E+OO
1.0000Et00
1.0000E+OO
1.ooooe+oo
1.0000E+OO
1.QOOOE+OO
1.0000E+OO
1.0000E+O.O
1.0000E+OO __-1 :.OOOOE;f.OO
1.0000E+OO
1,QQOOE+OO
MS Aliquot Data
Aliquot
Water Added
(ml)
NetEquiv
H3 Dist
Aliq
-----
!
-~-~-~-----
----
- -------
- -
--
I
I
--~----
-------
---~----
---------
I
~
Date:
4j /(u, J3
I
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
01
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 54576
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.610 mL
0.1961 +/- 0.0110
0.1776 +/- 0.0033 on 12/15/2012
1.1041 +/- 0.0651
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.271
4.726
4.406
4.151
Net
Pk Area
386.47
579.81
25.66
594.81
0.984027 +/-
AREA
0.074385
REPORT
Pk Area
Error %
9.99
8.15
38.99
8.05
1:57:26 PM
Ambient
Backgnd
1. 53
1.19
0.34
1.19
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
20.9
25.5
3.9
8.5
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
0.993
5302.50*
5.23E+000 +I- 5.74E-001
9.62E-002 +I- 1.05E-002
U-234
0.991
4761.50*
7.85E+000 +I- 1.07E+000
8.92E-002 +I- 9.78E-003
U-235
0.997
4385.50*
4.29E-001 +I- 1.74E-001
7.98E-002 +!- 8.75E-003
U-238
0.992
4184.40*
8.02E+000 +!- 1.09E+000
8.88E-002 +I- 9.74E-003
ftc;
t~/:1~
0000055915.CNF
Live Time :10200.000 sec
Rea1 Time :10201.000 sec
start:
1:3404.1(kev)
stop : 1024:6604.2(kev)
Acq. Start :Fri Apr 19 11:36:31 2013
60
55
50
45
40
35
V)
.j..J
s::::
:::::s
8 30
25
20
I
Oil
r,[;
15
'f
10
5
0
3500
4500
4000
5000
Energy(kev)
6000
5500
II-
~,
[.n
ROI Type: 1
ROI Type: 3
6500
4/19/2013
Page
5:26tl)
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
01
10200
10201
Channell------l-------l-------l-------l-------l-------l-------1-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10201
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
3
1
1
3
4
8
9
20
21
15
0
0
0
0
0
1
1
1
0
1
0
0
0
10200
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
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0
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2
1
4
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18
18
18
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0
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0
0
0
1
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1
4
0
5
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8
16
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17
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7
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14
21
22
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1
1
1
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1
3
4
1
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9
7
15
7
18
5
0
1
0
0
1
1
1
0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
2
0
1
3
3
11
4
18
24
12
4
0
0
0
0
0
0
1
0
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
2
2
5
8
4
13
16
16
3
1
0
0
0
0
1
2
0
0
1
0
1
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
2
2
1
0
0
1
1
2
1
1
1
0
4
8
17
12
10
3
0
1
1
0
2
0
0
0
0
3
0
0
1
~..;;
.......
~J.~C
4/19/2013
0
Sample Title:
5:2~:.:1~
..,
0
Page
1
01
Channell------1-------l-------l-------l-------l-------l-------l-------l
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
3
1
2
8
6
11
13
18
17
0
0
0
0
0
0
0
1
0
0
1
0
0
0
2
4
1
9
8
12
15
4
0
0
1
0
0
0
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0
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0
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0
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0
0
0
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0
0
1
0
2
4
1
2
11
10
15
13
13
1
0
0
0
0
0
1
0
0
0
0
0
0
1
3
0
5
3
7
8
7
9
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4
1
2
2
8
12
21
12
13
0
0
0
0
1
0
0
0
0
0
0
0
1
0
2
1
3
6
8
7
13
11
0
0
0
0
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...,..
..
jFOoP"'!iii
tlLU!U'
4/19/2013
0
Sample Title:
5:26:33
0
Page
0
01
Channell------l-------l-------l-------l-------l-------l-------1-------l
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
BLANK
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
02
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_022
22
System Bkgd 54577
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
0232 UU-10A
0.607 mL
0.2055 +/0. 0113
0.0029 on 12/15/2012
0.1531 +/1. 3421 +/- 0.0781
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.273
4.751
4.381
4.189
Net
Pk Area
AREA
REPORT
Pk Area
Error %
402.64
3.49
2.32
1.64
1:57:26 PM
9.79
113.53
149.12
214.83
Ambient
Backgnd
1.36
0.51
0.68
1.36
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
17.1
3.1
3.1
3.1
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.999
1. 000
1. 000
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.20E+000
4.51E-002
3.70E-002
2 .llE- 002
+1+I+1+I-
5.60E-001
5.14E-002
5.53E-002
4.54E-002
AG
tf(J.f)--/(J
MDA
(pCi/liter
8.86E-002
6.78E-002
8.99E-002
8.82E-002
+I+I+I+I-
9.54E-003
7.30E-003
9.69E-003
9.50E-003
0000055916.CNF
Live Time :10200.000 sec
Real Time :10201.000 sec
Start:
1: 3421.5 (kev)
stop : 1024:6608.8(kev)
Acq. Start :Fri Apr 19 11:36:32 2013
60
55
50
45
40
35
V)
+-'
I::
:::3
8 30
25
20
15
10
5
0
3500
4000
4500
(;tlf
....
5000
Energy(kev)
5500
6000
li'-~
fill
ROI Type: 1
ROI Type: 3
6500
4/19/2013
s:at~:tf
Page
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
02
10200
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G111
4/19/2013
0
Sample Title:
Page
S:2iltf
0
02
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ii 112
4/19/2013
0
Sample Title:
Page
5:26:41 tiN
0
02
Channell------l-------l-------1-------l-------l-------l-------l-------l
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889:
897:
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953:
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969:
977:
985:
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
PZ-105-SS TOT-DUP
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
03
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 54578
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.605 mL
0. 0112
0.2017 +/0.0032 on 12/15/2012
0.1710 +/1.1795 +/0.0690
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.243
4.703
4.387
4.137
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
393.98
197.64
6.83
138.66
2:02:15 PM
Ambient
Backgnd
1. 02
1. 36
0.17
0.34
9.89
14.00
76.08
16.67
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.3
4.7
3.1
5.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.975
0.976
1. 000
0.984
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.19E+000
2.60E+000
1.11E-001
1.82E+000
+I+I+I+I-
5.64E-001
4.61E-001
8.52E-002
3.62E-001
MDA
(pCi/liter
8.30E-002 +/- 9.02E-003
9.02E-002 +1- 9.81E-003
6.78E-002 +I- 7.37E-003
6.27E-002 +I- 6.81E-003
1\C
'f{~r3
6114
0000055917.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
1:3411.6(kev)
Stop : 1024:6597 .O(kev)
Acq. Start : Fri Apr 19 11: 36: 33 2013
60
55
50
45
40
35
Vl
......
r:::
:::::s
8 30
25
20
15
10
5
0
3500
4000
4500
G)
5000
Energy(kev)
6000
5500
l!ln.!l-i.
J.o~~l.
Ul
ROI Type: 1
ROI Type: 3
6500
4/19/2013
Page
5:2fi:~'f
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
03
10200
10200
Channell------l-------l-------1-------l-------l-------l-------l-------l
1:
9:
17:
25:
33:
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49:
57:
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113:
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129:
137:
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161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
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oilp!;o--
.. ,-r=;,
l!i!J.J.O
4/19/2013
0
Sample Title:
5:26;if
1
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1
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.A. .,;i
..!"~'a
t\U l. l
4/19/2013
0
Sample Title:
5:26:51
0
Page
0
03
Channell------l-------l-------l-------l-------l-------l-------l-------1
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929:
937:
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953:
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tillS
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
PZ-105-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
04
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_025
25
System Bkgd 54579
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.598 mL
0.2107 +/- 0. 0115
0.1736 +/- 0.0032 on 12/15/2012
1.2142 +/- 0.0702
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.287
4.736
4.362
4.166
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
406.81
207.98
7.00
130.66
9.73
13.63
79.20
17.17
1:57:27 PM
Ambient
Backgnd
1.19
1. 02
0.00
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.8
10.4
3.1
13.2
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.995
0.996
0.998
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+000 +I- 5.50E-001
2.62E+000 +/- 4.55E-001
1.09E-001 +I- 8.69E-002
1.64E+000 +I- 3.32E-001
MDA
(pCi/liter
8.30E-002 +!- 8.91E-003
7.94E-002 +/- 8.52E-003
9.32E-002 +I- 1. OOE- 002
6.00E-002 +I- 6.43E-003
AG
tf(JJ/t!;
8119
0000055918.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
start:
1 3405.9(kev)
stop : 1024 6615.8(kev)
Acq. start Fri Apr 19 11:36:34 2013
60
55
50
45
40
35
VI
.j-J
c:
::::s
8 30
25
20
15
10
5
0
3500
4000
4500
Q;)
5000
Energy(kev)
5500
6000
......
M
(i)
ROI Type: 1
ROI Type: 3
6500
Page
4/19/2013
*******************************************************
S P E C T R A L
R E P 0 R T
*****
DATA
*****
*******************************************************
Sample Title:
04
10200
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4/19/2013
0
Sample Title:
Page
5:~&ti~-
04
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fl-Mi
,t=;;.~
~ll:L
4/19/2013
0
Sample Title:
5:2itl~
Page
0
04
Channell------l-------l-------l-------l-------l-------l-------l-------1
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i123
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
PZ-105-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
05
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_027
27
System Bkgd 54580
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.600 mL
0.2171 +/- 0.0117
0.1728 +/- 0.0032 on 12/15/2012
1.2570 +/- 0.0718
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.290
4.740
4.394
4.158
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
420.81
211.32
5.32
116.47
2:27:41 PM
Ambient
Backgnd
1.19
0.68
0.68
1.53
9.57
13.51
91.11
18.30
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
23.5
22.0
3.2
5.4
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
0.997
0.999
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000
2.58E+000
8.02E-002
1.42E+000
+I+I+I+I-
5.45E-001
4.43E-001
7.36E-002
3.00E-001
ftG
'f/.J~/13
MDA
(pCi/liter
8.06E-002 +/- 8.53E-003
6.90E-002 +I- 7.30E-003
8.51E-002 +I- 9.00E-003
8.65E-002 +/- 9.16E-003
0000055919.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
1:3402 .4(kev)
stop : 1024:6658 .l(kev)
Acq. Start :Fri Apr 19 11:36:35 2013
60
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Vl
......
s::::
::::s
8 30
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0
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......
M
Ul
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
4/19/2013
Page
5:27:0.,. Wf
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
05
10200
10200
Channell------1-------l-------l-------l-------l-------l-------l-------l
1:
9:
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10200
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6126
4/19/2013
0
Sample Title:
5:2"1': ...
0
..,
0
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0
05
Channell------l-------l-------l-------l-------l-------l-------l-------1
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0
~..-_,.,.,.l="'lll;
ali/
4/19/2013
0
Sample Title:
5: 3"JJ ...
0
Page
0
05
Channell------l-------l-------l-------l-------1-------l-------l-------l
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i12S
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
S-10 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
06
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 54581
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.604 mL
0.1969 +/- 0. OllO
0.1945 +/- 0.0036 on 12/15/2012
1.0121 +/- 0.0597
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.287
4.741
4.408
4.178
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
383.98
17.00
1. 66
17.98
2:30:02 PM
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
1. 02
0.00
0.34
1. 02
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
10.02
48.92
169.38
47.73
19.0
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.997
0.996
1. 000
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.18E+000
2.29E-001
2.76E-002
2.41E-001
+1+I+I+1-
5.69E-001
1.15E-001
4.69E-002
1.18E- 001
ltG
1//J3
MDA
(pCi/liter
8.50E-002
8.09E-002
7.95E-002
8.46E-002
+I+I+I+I-
9.34E-003
8.88E-003
8.74E-003
9.29E-003
0000055920.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
start:
1: 3413 .5 (kev)
stop : 1024:6597. S(kev)
Acq. Start :Fri Apr 19 11:36:36 2013
60
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V'l
+-'
s::::
:::J
8 30
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Jl<l!)
......
w
~)
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
4/19/2013
s:27t41
11
Page
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
06
10200
10200
Channell------l-------1-------l-------l-------l-------l-------l-------l
1:
9:
17:
25:
33:
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49:
57:
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313:
321:
329:
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345:
353:
361:
10200
0
0
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1
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0
0
.......
-rq, ...
lJLL:U
4/19/2013
0
Sample Title:
5:2'7;J.
0
Page
0
06
Channell------l-------l-------l-------l-------l-------l-------l-------1
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793:
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6132
4/19/2013
0
Sample Title:
Page
5:27:2. tliM
0
06
Channell------l-------l-------l-------l-------l-------l-------l-------1
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849:
857:
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5133
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
S-10 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
07
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 54582
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.599 mL
0.1484 +/- 0.0094
0.1825 +/- 0.0032 on 12/16/2012
0.8132 +/0.0535
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.292
4.757
4.356
4.163
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
287.00
7.00
0.83
5.00
5:49:18 PM
Ambient
Backgnd
11.59
79.20
239.53
96.02
0.00
0.00
0.17
0.00
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
23.8
4.5
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
1. 000
0.994
0.997
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+000
1.25E-001
1.83E-002
8.91E-002
+I+!+I+I-
6.39E-001
1. OOE-001
4.39E-002
8.62E-002
A(,
~;)){tJ
MDA
(pCi/liter
1.07E-001
1.07E-001
9.21E-002
1. 07E-001
+I+I+I+!-
1.33E-002
1.33E-002
1.15E-002
1.33E-002
0000055930.CNF
Live Time 10200.000 sec
Rea1 Time 10215 .400 sec
Start:
1 3465.6(kev)
stop : 1024 6503.3(kev)
Acq. Start Fri Apr 19 11:57:43 2013
60
55
50
45
40
35
Vl
.......
r::::
::::s
8 30
25
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15
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5
0
3500
4000
4500
~,
......
Jl,.)
!.J~
ROI Type: 1
5000
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5500
6000
ROI Type: 3
6500
4/19/2013
5:27:31
..
Page
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
07
10200
10215
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4/19/2013
0
Sample Title:
Page
0
07
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4/19/2013
0
Sample Title:
5:2?:)f
Page
!
0
07
Channell------l-------l-------l-------l-------l-------l-------l-------1
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
LR-104 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
08
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 54583
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.602 mL
0.2188 +/- 0. 0117
0.1856 +/- 0.0032 on 12/16/2012
1.1788 +/- 0.0666
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.728
4.415
4.155
Net
Pk Area
424.83
213.83
11.00
174.66
AREA
5:49:43 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
9.51
13.41
61.72
14.85
0.17
0.17
0.00
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
32.2
15.1
5.9
7.4
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.992
0.994
0.994
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.16E+000
2.60E+000
1.65E-001
2 .11E+000
+!+!+I+I-
5.43E-001
4.42E-001
1.03E-001
3.84E-001
MDA
(pCi/liter
5.07E-002
5.07E-002
8.98E-002
5.78E-002
+I+I+!+I-
5.33E-003
5.33E-003
9.45E-003
6.08E-003
AG
1/)J/13
6135
0000055931.CNF
Live Time :10200.000 sec
Real Time :10215.400 sec
start:
1:3439.1(kev)
stop : 1024:6479.9(kev)
Acq. Start :Fri Apr 19 11:57:45 2013
60
55
50
45
40
35
VI
.......
c
:::3
8 30
25
20
15
10
5
0
3500
4000
4500
t~)
5000
Energy(kev)
6000
5500
jiw;o~i.
,g:~
r.:u
ROI Type: 1
ROI Type: 3
4/19/2013
5:2?Jfj
..
Page
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
08
10200
10215
Channell------l-------l-------l-------l-------l-------1-------l-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
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129:
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145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
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345:
353:
361:
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51d1
4/19/2013
0
Sample Title:
S:3!7;i4
0
"
0
Page
1
08
Channell------l-------l-------l-------1-------l-------l-------l-------l
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569:
577:
585:
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641:
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4/19/2013
0
Sample Title:
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0
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Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
LR-104 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
09
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_035
04026477A
58771
System Bkgd 54584
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.600 mL
0.2261 +/0.0120
0.1826 +/- 0.0032 on 12/16/2012
1. 2381 +I- 0.0692
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.308
4.757
4.391
4.186
T
Net
Pk Area
438.00
231.66
11.00
165.83
AREA
5:49:42 PM
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
9.38
12.89
61.72
15.23
0.00
0.34
0.00
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
30.0
5.9
2.9
7.4
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
1. 000
1. 000
1.000
1. 000
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000 +I- 5.35E-001
2.72E+000 +I- 4.51E-001
1.59E-001 +/- 9.98E-002
1.94E+000 +I- 3.58E-001
AG
til :J)-/13
MDA
(pCi/liter
7.05E-002
5.62E-002
8.69E-002
4.88E-002
+I+I+I+I-
7.33E-003
5.84E-003
9.04E-003
5.08E-003
0000055932.CNF
Live Time 10200.000 sec
Real Time 10215.300 sec
Start:
1 3463 .4(kev)
stop : 1024 6473.5(kev)
Acq. start Fri Apr 19 11:57:40 2013
60
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Vl
......
s::::
:::s
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5500
6000
~-~
til
Ul
ROI Type: 1
ROI Type: 3
4/19/2013
Page
5:27:52 PM
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
09
10200
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4/19/2013
0
Sample Title:
S:i'iiiJ
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*'"''"" -~
WliJI
4/19/2013
0
Sample Title:
s~t~'''
0
Page
W
0
09
Channell------l-------l-------l-------l-------l-------l-------l-------1
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fii148
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
DUP 01 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
10
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_037
04026478A
91133
System Bkgd 54585
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.598 mL
0.2357 +/- 0.0123
0.1783 +/- 0.0033 on 1/26/2013
1.3222 +/- 0.0733
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.749
4.406
4.165
Net
Pk Area
AREA
REPORT
Pk Area
Error %
455.00
22.66
0.83
10.83
3:28:25 PM
9.20
41.53
239.53
60.10
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
0.00
0.34
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
38.2
2.9
2.9
2.9
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.999
0.997
0.997
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+000
2.55E-001
1.15E-002
1.21E-001
+I+I+!+!-
5.25E-001
1. 09E-001
2.76E-002
7.40E-002
MDA
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6.92E-003
5.52E-003
5.94E-003
4.79E-003
JICi
t!/J~/3
6149
0000055933.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
start:
1 3463. 5(kev)
stop : 1024 6468.S(kev)
Acq. start Fri Apr 19 11:57:41 2013
60
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.f-1
s:::::
::::s
8 30
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4000
4500
5000
Energy(kev)
5500
6000
u~
c:n
ROI Type: 1
ROI Type: 3
4/19/2013
Page
5:28: tit
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
10
10200
10215
Channell------l-------l-------l-------l-------l-------l-------l-------1
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9:
17:
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281:
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353:
361:
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4/19/2013
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4/19/2013
0
Sample Title:
5:28s81
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DUP 01 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
11
Shelf 2
U iso
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Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 54586
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.599 mL
0.1906 +/- 0.0109
0.1900 +/- 0.0033 on 12/16/2012
1. 0034 +I- 0.0597
0.150 MeV
PEAK
Energy
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Nuclide
U-232
U-234
U-235
U-238
5.274
4.732
4.365
4.142
T
Net
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AREA
REPORT
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368.83
14.66
2.00
10.32
5:49:33 PM
10.21
51.88
169.74
63.32
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0.34
0.00
0.68
O.OOE+OOO
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O.OOE+OOO
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0.994
0.997
0.987
5302.50*
4761.50*
4385.50*
4184.40*
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3.44E-002
1.43E-001
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5.74E-001
1.08E-001
5.84E-002
9.20E-002
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6.66E-002
1. 03E-001
7.82E-002
+!+1+I+I-
6.49E-003
7.43E-003
1.15E-002
8.73E-003
N;
1(~/t!J
ii15ii
0000055934.CNF
Live Time :10200.000 sec
Rea1 Time :10215. 400 sec
start:
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stop : 1024:6497.3(kev)
Acq. Start :Fri Apr 19 11:57:49 2013
60
55
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VI
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c:
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4/19/2013
Page
5:28:J.). WI
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
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11
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Sample Title:
Page
5:28:1!.. JIM
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
DUP 02 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
12
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 54587
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.600 mL
0.1888 +/- 0.0108
0.1978 +/- 0.0034 on 12/16/2012
0.9545 +/- 0.0570
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.287
4.733
4.411
4.166
Net
Pk Area
AREA
REPORT
Pk Area
Error %
365.66
11.32
0.32
7.45
5:49:31 PM
10.26
60.27
646.93
84.98
Ambient
Backgnd
0.34
0.68
0.68
2.55
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
24.3
3.0
3.0
4.5
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.994
0.995
0.998
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+000
1.59E-001
5.55E-003
1.04E-001
+I+!+I+!-
5.76E-001
9.76E-002
3.59E-002
8.94E-002
AG
l(/JJ/13
MDA
(pCi/liter
6.72E-002
7.93E-002
9.78E-002
1.17E-001
+!+I+!+I-
7.53E-003
8.88E-003
1.10E-002
1.32E-002
0000055936.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
start:
1 3452.7(kev)
stop : 1024 6506.6(kev)
Acq. Start Fri Apr 19 11:57:46 2013
60
55
50
45
40
35
V)
.......
s:::
:::s
8 30
25
20
15
10
5
0
3500
4000
4500
~,
5000
Energy(kev)
5500
6000
....t
tn
tn
ROI Type: 1
ROI Type: 3
6500
4/19/2013
Page
"S:!I:2e PM
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
12
10200
10215
Channell------l-------l-------l-------l-------l-------l-------l-------1
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6161
4/19/2013
0
Sample Title:
5:2SsH
0
Page
ttt
0
12
Channell------l-------l-------l-------l-------l-------l-------l-------1
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,;11#:;. -IIi
..,...... -F'
UI !bi
4/19/2013
0
Sample Title:
Page
5:28:28 tiN
0
12
Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
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825:
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841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
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rii 163
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
DUP 02 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
13
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_042
05026930B
84185
System Bkgd 54588
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.601 mL
0.1899 +/- 0.0108
0.1846 +/- 0.0032 on 12/16/2012
1.0284 +/- 0.0613
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.283
4.731
4.435
4.164
T
Net
Pk Area
368.49
12.66
6.83
9.49
AREA
5:49:29 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
10.22
55.94
76.08
65.59
0.51
0.34
0.17
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.6
3.0
3.0
4.5
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.993
0.983
0.997
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000
1. 77E-001
1.18E-001
1.32E-001
+1+1+I+I-
5.76E-001
1. 01E-001
9.06E-002
8.79E-002
k;
1(/13>
MDA
(pCi/liter
7.34E-002
6.69E-002
7.20E-002
7.31E-002
+I+I+I+I-
8.20E-003
7.47E-003
8.04E-003
8.16E-003
0000055937.CNF
Live Time 10200.000 sec
Real Time 10215.400 sec
1 3450.2(kev)
Start:
stop : 1024 6505. 5(kev)
Acq. Start Fri Apr 19 11:57:47 2013
60+
55
50
45
40
35
VI
.j...J
c:
::::s
8 30
25
20
15
10
5
0
3500
4000
4500
~)
5000
Energy(kev)
5500
6000
il'~~
till
Ul
ROI Type: 1
ROI Type: 3
6500
4/19/2013
5:lliii
Page
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
13
10200
10215
Channell------l-------l-------l-------l-------l-------1-------l-------l
1:
9:
17:
25:
33:
41:
49:
57:
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137:
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153:
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169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
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0
9166
4/19/2013
0
Sample Title:
5:2!1:26
0
Page
PM
0
13
Channell------l-------l-------l-------l-------l-------1-------l-------l
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641:
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681:
689:
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705:
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769:
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793:
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~""~~
U!.iD/
4/19/2013
0
Sample Title:
5:29:26
1
Page
13
Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
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857:
865:
873:
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889:
897:
905:
913:
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8168
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
FB AT PZ-110-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000560
1304051A-UU
14
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_003
3
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.595 mL
0.2522 +!- 0.0129
0.1746 +/0.0033 on 12/15/2012 11:26:47 AM
1.4440 +/- 0.0784
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.286
4.750
4. 396
4.149
T
Net
Pk Area
483.98
1.49
2.66
-0.68
AREA
REPORT
Pk Area
Error %
8.92
190.03
128.85
304.42
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Backgnd
Reagent
Backgnd
FWHM
(keV)
1. 02
0.51
0.34
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
31.9
3.0
3.0
0.0
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Conf.
Energy
(keV)
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(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.998
0.999
0.999
0.991
5302.50*
4761.50*
4385.50*
4184.40*
5.10E+000
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3.45E-002
-7.13E-003
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2.98E-002
4.46E-002
2.17E-002
AG
tt!J~/f!>
6.64E-002
5.52E-002
6.21E-002
5.91E-002
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6.63E-003
5.52E-003
6.21E-003
5.91E-003
0000056095.CNF
Live Time 10201.000 sec
Real Time 10201. 000 sec
start:
1 3498.4~kev~
stop : 1024 6549.5 kev
Acq. Start Fri Apr 19 14:33:37 2013
60+
55
50
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35
Vl
......
c
8 30
25
20
15
10
5
0
3500
I
...
1!:'0:~
~
~~~
(!~
4000
4500
ROI Type: 1
5000
Energy(kev)
5500
ROI Type: 3
6000
6500
4/19/2013
s:29;U
Page
*******************************************************
S P E C T R A L
R E P 0 R T
*****
DATA
*****
*******************************************************
Sample Title:
14
10201
10201
Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
9:
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1
81 1
4/19/2013
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Sample Title:
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8172
4/19/2013
0
Sample Title:
5:29:1,
0
Page
0
14
Channell------l-------l-------l-------l-------l-------1-------l-------l
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
FB AT PZ-110-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
15
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_004
4
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.596 mL
0.1778 +/- 0.0105
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
0.9162 +/- 0.0565
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.286
4.692
4.324
4.134
Net
Pk Area
341.81
2.96
-0.19
-0.85
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
10.62
153 .11
1131.2
246.69
1.19
2.04
1.19
0.85
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
21.8
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2.9
0.0
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Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.967
0.974
0.982
5302.50*
4761.50*
4385.50*
4184.40*
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4.42E-002
-3.50E-003
-1.26E-002
+I+I+1+I-
5.89E-001
6.79E-002
3.96E-002
3.12E-002
MDA
(pCi/liter
9.84E-002
1.16E-001
1.21E-001
8.90E-002
+!+I+I+I-
1.14E-002
1.34E-002
1.40E-002
1.03E-002
/:JZ/13
fi17ii
0000055943.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
Start:
1 3493 .1(kev)
stop : 1024 6486. 9(kev)
Acq. Start Fri Apr 19 14:33:38 2013
55
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35
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.j..J
r::::
::::l
8 30
25
20
15
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5
0
3500
I
4000
4500
~,
5000
Energy(kev)
5500
6000
~~>~~
"'"'J
U1
ROI Type: 1
ROI Type: 3
6500
4/19/2013
s:a9i
Page
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
15
10200
10200
Channell------l-------l-------l-------l-------l-------l-------1-------l
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
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113:
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129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
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G176
4/19/2013
0
Sample Title:
Page
5:29:52 PM
0
15
Channell------l-------l-------l-------l-------l-------l-------l-------1
377:
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44 9:
457:
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4 97:
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54 5:
553:
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569:
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4/19/2013
0
Sample Title:
Page
5:29:52 PM
0
15
Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
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969:
977:
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993:
1001:
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1017:
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
MW-103 TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
16
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_010
10
System Bkgd 54572
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.593 mL
0.1786 +/- 0.0105
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
0.9080 +!- 0.0560
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4.730
4.398
4.145
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
342.13
273.79
20.32
251.15
Ambient
Backgnd
10.63
11.90
44.32
12.39
1. 87
2.21
0.68
0.85
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
17.1
23.8
2.9
15.3
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------'
U-232
U-234
U-235
U-238
0.997
0.993
0.999
0.989
5302.50*
4761.50*
4385.50*
4184.40*
5.09E+000
4.07E+000
3. 73E-001
3.72E+000
+I+I+I+!-
5.87E-001
6.75E-001
1.71E-001
6.30E-001
1.13E-001
1.19E- 001
1. 03E- 001
8.86E-002
+I+I+I+I-
1.30E-002
1.37E-002
1.19E-002
1.02E-002
A6.
'f/:J:>/13
i179
0000055938.CNF
Live Time :10201.000 sec
Rea1 Time :10201.000 sec
start:
1:3505.7(kev)
stop : 1024:6498.0(kev)
Acq. Start :Fri Apr 19 14:33:33 2013
60
55
50
45
40
35
V'l
........
s:::
:::s
8 30
25
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15
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ROI Type: 1
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ROI Type: 3
!!
I II!!
'
6500
4/19/2013
5:31:8C
Page
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
16
10201
10201
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9:
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25:
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iil1H
4/19/2013
0
Sample Title:
5:31:0~
Page
9M
1
16
Channell------l-------l-------1-------l-------l-------l-------l-------l
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545:
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i1
4/19/2013
0
Sample Title:
Page
5:3l:OC tiN
0
16
Channell------l-------l-------l-------l-------l-------l-------l-------1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
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ii183
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
MW-103 DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\OOOO 559
1304051A-UU
17
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_Oll
11
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.596 mL
0.1849 +/- 0.0107
0.1973 +/- 0.0042 on 12/15/2012 11:28:06
0.9369 +1- 0.0577
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
10.41
13.20
52.27
13.56
1. 02
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.277
4.731
4.407
4.150
355.98
220.83
15.00
209.98
0.17
0.00
1. 02
17.3
15.
2.
9.4
Id
------;~~~~~------------~~~~~~~~------------------
'
MDA
-~~;;;~~---~~;;~----~;~;:~~:---~:~~~:~~~~~~~~~=~~~=~~~---;:~~~~~~~~~~~~;-~~;;=~~;
U-234
U-235
U-238
0.993
0.997
0.992
4761.50*
4385.50*
4184.40*
iiSA.
0000055939.CNF
Live Time :10200.000 sec
Rea1 Time :10201.000 sec
start:
1:3645. S(kev)
stop : 1024:6374.2(kev)
Acq. Start :Fri Apr 19 14:33:34 2013
60
55
50
45
40
35
Vl
.j..J
s::::
::::l
8 30
25
20
15
10
5
0
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!!
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6000
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ROI Type: 1
ROI Type: 3
!I
!Jl!
4/19/2013
5:3l.:Jj
,.
Page
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
17
10200
10201
Channell------l-------l-------l-------1-------l-------l-------l1:
9:
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41:
49:
57:
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10201
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6185
4/19/2013
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Sample Title:
5:31:25
1
Page
PM
1
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Channell------l-------1-------l-------l-------l-------l-------l377:
385:
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465:
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&187
4/19/2013
0
Sample Title:
Page
5:31~"
0
17
Channell------l-------l-------1-------l-------l-------l-------l- -----1
809:
817:
825:
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849:
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865:
873:
881:
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897:
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913:
921:
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6188
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
PZ-200-SS TOT
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\OOOO 559
1304051A-UU
18
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_013
13
System Bkgd 54574
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.593 mL
0.1967 +/- 0.0111
0.1869 +/- 0.0035 on 12/15/2012 11:26:45
1.0527 +/- 0.0626
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1.19
0.85
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.282
4.738
4.435
4.160
376.81
40.15
3.83
38.83
10.12
31.31
102.72
31.53
5.2
4.7
2.8
3.3
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.997
0.996
0.983
0.996
5302.50*
4761.50*
4385.50*
4184.40*
5.09E+000
5.42E-001
6.38E-002
5.22E-001
+I+I+I+I-
5.63E-001
1.80E-001
6.59E-002
1. 74E-001
8.89E-002
8.08E-002
6.95E-002
5.61E-002
+I+!+!+I-
9.85E-003
8.95E-003
7.70E-003
6.21E-003
fr;
1/dJ((J
ii18S
0000055940.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
Start:
1 3547.5(kev)
stop : 1024 6438.1(kev)
Acq. Start Fri Apr 19 14:33:35 2013
60
55
50
45
40
35
V)
+-'
s:::::
::J
8 30
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20
15
10
5
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10
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4/19/2013
~'
Page
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
18
10200
10200
Channell------l-------l-------l-------l-------l-------1-------l-- -----1
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
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10200
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0
"'""-
...
~l::IJ.
4/19/2013
1
Sample Title:
5:3JJJi
0
...
0
Page
0
18
Channell------l-------1-------l-------l-------l-------l-------l809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
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1
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0
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
PZ-200-SS DIS
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000559
1304051A-UU
19
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 54575
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
0232 UU-10A
0.596 mL
0.2020 +!- 0.0113
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.0945 +/- 0.0644
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4.724
4.364
4.160
Net
Pk Area
AREA
REPORT
Pk Area
Error %
388.79
40.47
2.32
44.66
9.97
31.48
149.12
29.46
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
2.21
1.53
0.68
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
11.2
3.7
2.9
3.9
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.996
0.990
0.997
0.996
5302.50*
4761.50*
4385.50*
4184.40*
5.11E+000
5.32E-001
3.76E-002
5.84E-001
+I+!+!+1-
5.60E-001
1. 77E-001
5.62E-002
1.84E-001
1\-(i
J/1~13
1. 05E-001
9.34E-002
9.15E-002
6.26E-002
+!+!+!+I-
1.15E-002
1.02E-002
1.00E-002
6.85E-003
0000055941.CNF
Live Time 10200.000 sec
Rea1 Time 10200.000 sec
1 3507. 9(kev)
Start:
stop : 1024 6512.2(kev)
Acq. Start Fri Apr 19 14:33:36 2013
60+
55
50
45
40
35
V)
.j-1
c::
:::::s
8 30
25
20
15
10
5
0
4000
4500
II:!~
5000
Energy(kev)
5500
6000
6500
j!.o>IDi>
lj;J)
Ul
ROI Type: 1
ROI Type: 3
4/19/2013
5:32:43
Page
PM
*******************************************************
s p E C T R A L DATA R E P 0 R T
*****
*****
*******************************************************
Sample Title:
19
10200
10200
Channell------l-------l-------l-------l-------l-------l-------l-------1
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
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177:
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201:
209:
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249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
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0
1
0
0
0
4
1
0
0
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0
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0
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0
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10200
0
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1
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0
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1
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1
0
1
3
1
1
0
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0
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0
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0
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0
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1
0
1
0
0
0
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0
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0
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0
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0
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0
1
0
0
0
0
0
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0
0
1
0
2
0
2
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
1
0
0
0
0
0
0
0
0
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0
0
0
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0
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0
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1
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0
1
2
1
1
0
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1
1
0
0
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1
4
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
u.t;:,tJ
W1'lo ..
""""""
4/19/2013
1
Sample Title:
5:32:43
0
Page
19
Channell------l-------1-------l-------l-------l-------l-------l-------l
377:
385:
393:
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433:
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457:
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0
0
0
0
2
1
3
0
0
0
0
0
0
0
1
0
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1
2
0
1
1
0
2
0
9
10
11
14
2
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1
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0
0
0
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0
0
0
0
0
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1
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0
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0
1
0
2
0
0
0
0
0
0
0
1
1
0
0
1
1
1
1
2
3
1
3
5
5
11
18
0
0
0
0
0
0
0
0
0
0
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2
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0
0
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0
1
1
1
2
3
1
3
8
16
10
0
0
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0
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1
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1
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1
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4
1
2
2
14
4
17
13
1
0
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0
0
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1
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1
2
3
1
0
0
0
0
0
0
0
0
0
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1
0
0
1
0
2
2
7
5
8
17
13
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
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1
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0
3
1
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
1
1
5
1
9
7
12
6
0
0
0
0
0
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0
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0
1
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1
2
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3
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21
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1
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0
0
0
0
0
0
0
0
0
0
0
6197
4/19/2013
0
Sample Title:
5:32;4;t
0
Page
0
19
Channell------l-------l-------l-------1-------l-------l-------l-------l
809:
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889:
897:
905:
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921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
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1
1
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0
ii1SS
Page 1 of 2
4/19/2013 5:45:48 AM
QA SUMMARY REPORT
: 4/19/2013
: 5:45:48 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
21f
2lf
21f
21f
21f
21f
2lf
2lf
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha Analyst!OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Not Done
Not Done
Passed
Passed
Passed
DATE
4/19/2013 5:25:30 AM
4119/2013 5:25:31 AM
4/19/2013 5:25:31 AM
4/19/2013 5:25:32 AM
4/19/2013 5:25:33 AM
4/19/2013 5:25:34 AM
4119/2013 5:25:35 AM
4119/2013 5:25:35 AM
4/19/2013 5:25:36 AM
4/19/2013 5:25:37 AM
4119/2013 5:25:38 AM
4119/2013 5:25:39 AM
4119/2013 5:25:40 AM
4/19/2013 5:25:41 AM
4/19/2013 5:25:43 AM
4119/2013 5:25:44 AM
4119/2013 5:25:46 AM
4/19/2013 5:25:47 AM
4/19/2013 5:25:49 AM
Page 2 of 2
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst100DC
Alpha Analyst 1OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Not Done
Passed
Not Done
Passed
Passed
Passed
DATE
4119/2013 5:25:50 AM
4/19/2013 5:25:52 AM
4/19/2013 5:25:53 AM
4119/2013 5:25:55 AM
6/12/12
Page
12:17:04 PM
*************************************************************************
*****
LIBRARY LISTING REPORT
*****
*************************************************************************
Nuclide Library Title:
Uranium
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1. 410E+017
* =
Energy
(keV )
U-232,-234,-235,-238
Energy
uncert. {keV
0.000
0.000
0.000
0.000
5302.500*
4761. 500*
4385.500*
4184.400*
Yield
( %)
99.8000
99.8000
80.9000
100.2300
Yield
uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
key line
TOTALS:
Nuclides
Energy Lines
52&1