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AWS A4.2_ Standard Procedures for Calibrating Magnetic Instruments to Measure to the Delta Ferrite Content of Austentie and Duplex Austenitic-Ferritic Stainless Steel Weld Metal
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HOT CRACKING
Hot cracking
Referring to cracking that occurs during welding, casting, hot working at temp. close to the melting point Not completely understood, but generally accepted as following ;
Segregation during solidification & form low-melting-point liquid films on GB Tensile stresses(building up during solidification & cooling) cause cracking along the liquid films
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Liquation cracking
Liquation cracking
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1979
1988
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Less than 3 FN
3 45 FN
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From Welding Metallurgy and Weldability of Stainless Steels / John C. Lippold From Welding Metallurgy / Sindo Kou
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Constitution Diagram
Magnetic Instrumentation
Experimental Trials
Ferrite Austenite
X600
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Metallurgical sections shall be polished and etched to clearly reveal the two-phase Examining and photographing under a microscope at a sufficient magnification (Recommending X400 for parent plate & weld metal, X700-1000 for HAZ) Overlaying with a grid of at least 100 points Calculating ferrite % by counting the number of points that fall on the ferrite phase and the total number of points
Limitation
Destructive : Requiring sections to be removed from an actual weldment Time consuming & inherently inaccurate unless many sections in various locations & orientations are examined Poor reproducibility : Among a number of laboratories shown to be poor
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Still retaining because of reasonably accurate predictions martensite in lean stainless steel
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Being modified to show FN after the adoption of a standardized method in AWS A4.2 : 1974
Effect of N on ferrite content in TIG welds of DSS / Welding metallurgy, Sindo Kou
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1,000 measurements based on AWS A4.2 from manufacturers, research institutes, fabricators Expanding FN range : 0-18 0-100
Schaeffler Creq Nieq Delong WRC
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Magnetic Instrumentation
Severn Gage
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Requiring the measurement of higher FN(e.g., duplex stainless steel) Acc. many standard, FN = Ferrite volume 0-8(or 10) % Acc. to Welding Journal 61
Conversion
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FERRITE OPTIMIZATION
Ferrite in ASS
Should contain a small but controlled amount of ferrite Too much -ferrite(10 vol%) : Reducing the ductility, toughness, corrosion resistance Too little -ferrite(5 vol%) : hot cracking
7075 Al
SS310
From Welding Metallurgy / Sindo Kou
Ferrite in DSS
Phase balance is important to optimize their mechanical & corrosion properties Too much -ferrite(>70 vol%) : Low ductility, loss of corrosion resistance, HE susceptability Too less -ferrite(<20 vol%) : Low strength, low SCC resistance
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High temp. service(above 538) with FCAW weld material : < 9FN Final layer overlay : 3-10FN(except 347 : 511FN) Base metal, HAZ and weld metal : 30-65% Weld deposit : 3-15FN Acceptable corrosion resistance : 30-100FN, Delayed cracking can be formed : >110FN No FN for ASS welding DSS Welding : 35-65% by ASTM E562 for each PQR
API 582, Austenitic SS overlay API 582/938-C, Duplex stainless steel welding(P10H) BS EN 1011-3:2000, Standard austenitic stainless steels BS EN 1011-3:2000, Duplex stainless steels NACE 0103-2010, Appendix D
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And others,
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DISCUSSION
Dilution
In general, arc welding dilution : 15%(cladding) 40%(thin plate), 60%(GTAW root) How can we calculate or expect the dilution in field?
4 5
1 3 2
FN limitation
Any more FN limitation by spec. from this presentation
1 5
More questions??
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REFERENCES
Welding Metallurgy / Sindo Kou Solidification and Liquation Cracking Issues in Welding / Sindo Kou Welding Metallurgy and Weldability of Stainless Steels / John C.Lippold, Damian J.Kotecki Welding integrity and performance : Chapter 14 / ASM International Metallurgy of welding(Sixth Edition) / J.F.Lancaster A new constitution diagram for predicting ferrite content of stainless steel weld metals Ferrite Measurement in Austenitic and Duplex Stainless Steel Castings / C.D.Lundin Stainless Steel Castings Improved Ferrite Number Prediction Model / Welding Research BS EN 1011-3:2000, Welding Recommendations for welding of metallic materials, Part 3 : Arc welding of stainless steels ASM Metal HandBook Vol.6 Welding, Brazing, and Soldering / ASM International AWS 4.2 Standard Procedures for Calibrating Magnetic Instruments to Measure to the Delta Ferrite Content of Austentie and Duplex Austenitic-Ferritic Stainless Steel Weld Metal ISO 8249 : 2000, Welding Determination of Ferrite Number(FN) in austenitic and duplex ferriticaustenitic CR-Ni stainless steel weld metals / ISO ASTM E562, Standard Practice for Determining Volume Fraction by Systematic Manual Point Count. / ASTM ASME Section II, Part C, ASME Section IX API582, 938, NACE 0103
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