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added dropwise with agitation until a brown color of the solution persist for 2
minutes. Then the test tube was placed in a water bath for another 5 minutes and
then the reaction was observed. For the Jones test, 4 drops of chromic acid solution
were added wit agitation after each drop. Then it is allowed to stand for 10 minutes
and the reaction was observed. Lastly the unknown samples were identified by
comparing their solubility and reaction profile against that of the known compounds.
Results and Discussion
Table 1.1 Solubility and Reaction Profile
http://www.chemhaven.org/che102/lab/CHE102_E23_S12.pdf
and Jones Test while it gives a negative result on Solubility in H 2O, Solubility in
NaOH and Iodoform Test. Lastly, for the cyclohexanone it gives a positive result on
2,4-DNP test while it gives a negative result on Solubility in H2O, Solubility in NaOH,
Tollens test, Iodoform test and Jones test.
ReferencesT
Purdue Chemistry Department [1] (retrieved Sep 2006). Includes water solubility data.