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ZrO2 is so much brighter than the other phases because
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Sample B - Unetched and Thermally Etched 96% Liquid Phase Sintered Alumina
96% aluminas are used in many mechanical and electrical insulation applications including seals
and bearings, shafts, thermostat washers and tap plates. Oxide liquid forming additives include
MnO and TiO2. They are fired at 1420 oC which is above the MnTiO3 eutectic temperature at which
melting occurs. This low temperature makes them cheap to produce. They are brown due to the
MnO. Unetched the microstructure reveals porosity at low magnification. A 15 minute thermal etch
at 1350 oC enables the individual angular grains of alumina to be seen.
Images
Unetched Alumina.20X
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Angular porosity similar in size to the grains often arises in an optical micrograph of a ceramic
because of
a. grain pullout during the grinding and polishing procedure
b. incomplete sintering resulting in condensation of voids at grain boundaries
c. the volatilisation of some of Al2O3 during high temperature sintering
What is the approximate grain size of the Al2O3?
a. 1 micron
b. 10 microns
c. 100 microns
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The particles are angular because...
a. the material is only lightly sintered; therefore there are only necks between particles that
essentially have a geometry residual from grinding
b. the material has fractured during grinding
c. the particles naturally grow with sharp points due to their crystal growth habit
There are so few contact points between the silica particle because
a. the ceramic has fractured during grinding
b. the material is only lightly sintered so there is insufficient time to form many bonds
c. the polymer resin has expanded and forced the particles apart
Which of the following is not an important consequence of the light sintering process in the
context of the application?
a. It maintains the net shape.
b. The pores allow out-gassing.
c. The resin/silica composite is easy to machine.
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Aligned Ferrite. 5X
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Non-aligned Ferrite. 5X
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Questions
Approximately how large are the granules?
a. 0.3 microns
b. 3 microns
c. 30 microns
Porosity surrounds each granule because
a. the pores are interfaces between the individual granules
b. pores align to reduce free energy
c. fracture occurs between each granule
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Questions
The ceramic layers are approximately
a. 10 microns thick
b. 100 microns thick
c. 1000 microns thick
The electrode layers are approximately
a. 10 microns thick
b. 100 microns thick
c. 1000 microns thick
The alternate electrode layers increase
a. the area between electrodes
b. the distance between electrodes
c. the relative permittivity
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20X Zoom.
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Which of the following is a second phases in Macor Glass ceramics?
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a. MgF2
b. residual glass
c. fluorophlogopite
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