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# Refractory:

## Apparent porosity & Bulk Density:Apparent porosity:

This is the amount of the total closed and open pores in the refractory materials in
percentage.The good refractory material should have a minimum
porosity vale except in the case of the insulation bricks.
Bulk Density:
This is the ration of weight to the volume of the refractory materials in gram/cc.The
good refractory material shouls have a high bulk density value for its better
performance.
Remove the outer layer of the bricks by sample cutting machine.Take the sample size
oe 65x65x40mm and remove the moisture by putting them in air oven at 120 deg.
C.Take out and allowed to cool.Take the dry weight in gm(D).Put the samples in the
vessel containing water.Boil for about one hour.Take out and vipe out the excess water
by a wet cloth.Take the wet weight(W).The the suspended weight while the sample is
immersing in the water.(S)
(W D)
AP%

x 100
(W-S)
W

BD gm/cc =
(W S)

## under specified conditions of

Take the sample size of 50 mm diameter and 50 mm height(+ / - 0.5 mm) by a RUL
sample cutting machine.Calculate the area in cm2.Put the sample in the RUL testing
machine .Apply the of 2 kg per cm2.Set the dial gauge of 0.01 mm accuracy.Switch on
the RUL furnace to heta the sample.RUL temperature(t 0 C) is the temperature at
which 0.3 mm deformatation take place ie. Measure the temperature when the dedle of
the dial gauge is at 30th division after deformation taking place.
Pyrometric cone equivalent:This is the resistance of the refractory material to soften during service temperature.

Take the composite sample of the refractory material in 150 micron size.Remove the
iron by a magnet.Make the PCE sample of a regular tetrahedron of base in 8 mm and
height in 25 mm by using a PCE mould with the help of water and dextrose as a
binder.
Place the sample on a refractory flake along with the standard cone(Ortan/Sekher
cone).Put the flake with the samples in a PCE furnace and raise the temperature.
Standard
Sample

PCE temperature is the temperature at which the sample bend and its tip just tough the
plane of the flake and can measure by a optical pyrometer. This is the comparison test
and can compare with the standard sample. ie. if the standard bends first and the
sample is intact
then the PCE value is + of the standard cone PCE number. If the sample bends first
and the standard is intact then the PCE value is minus of the standard cone number or
if both the sample and standard are bend simultaneously then the PCE value is the
same value of the standard cone number.

Cold Crushing Strength:This is the ratio of the breaking load to the area in cm 2 of the refractor materials. The
good refractory material should have high value of the cold crushing strength.
Make the sample of size of 75 mm3 by sample cutting machine.Remove the moisture
the moisture by putting them in a air oven.After air cooling measure the area of the
sample and place the sample in to the ccs machine with the cushion above and below
of the sample.Apply the load and note the crushing load in kg and calculate the CCS
value.

CCS kg/cm2 =

kg/cm2
Area of cross section.

Permanent linear change:The expansion of the refractory during service temperature in percentage is called as
permanent linear change.

Cut the sample of size 125x40 mm by a sample cutting machine and try in an air oven
to remove the moisture. Measure the length of the specimen in mm. Place the sample
in a PLC furnace and switch on the furnace. soak the samples in the specified
temperature for the specified period. Allow the samples to cool in the furnace itself.
After cooling to the room temperature measure the final length of the specimens in the
same location and calculate the PLC value in %
Initial length Final length
PLC%

=.

X 100
Initial length

War page:This is the bend of the refractory material. The good refractory material should free
from war page.
Place the war page gauge on the bigger area ie. On the surface of 230x115 mm2 of the
ladle brick and measure the bend/war page in mm.

P h y s i c a l:
Tensile test:This is the ratio of the maximum load per area of the cross section on the tensile test
piece.
Make the tensile sample as per IS-1608/latest.Measure the diameter of the sample and
make two dots apart 5 times of diameter of the test piece. Place the sample in to the
and measure the reduced diameter of the broken sample.Calculate the tensile
strength.The sampling frequency shall be one per cast for axles and 1 for 1000,1 for
500 and 1 foro 250 for Box-N,Carriage and loco wheels respectively.

Tensile strength

Kg/mm2
Area of cross section

## Final length - Initial length

Elongation%
=
(GL-5.64 root A0 )

Initial length

## Initial area Final area

Reduction area %

x 100
Initial area

Micro grain size:This is the number of grains per square inch at 100x.
Take the micro sample and grind wheel by a grinding machine. Use the emery papers
of various grades from rough to fine and while changing the next emery paper the
polishing direction should be perpendicular to the previous paper. Use the diamond
paste for final polishing .Clean well by alcohol/dish paper and etch the polished
specimen in 1:1 HCl.After drying check the micro grain size under metallurgical
microscope at 100 magnification. This is the comparison test and compare the grain
size with the standard chart as per IS-2853/latest.

Inclusion content:This also the comparison test and compare the inclusion rating with the stand chart as
per IS-1463/latest and report as follows. Carry out the test before etching.

Type
Sulphide(A type)
Alumina(B type)
Silicate(C type)
Oxide(D type)

Thin

Thick

Macro examination.
Take the vertical slice of wheel or axle. Mill it and heat in 1:1 HCl to the temperature
75 - 80 degree centigrade for about half an hour. Take out the etched sample clean by
water and dry. Examine with the naked eye or low magnifying glass of less than
10x.This also a comparison test and compare the macro piece with the standard chart
as per Astm-381/latest.The etched sample should free from crack, non-metallic
inclusion, flake, lap mark, segregation, pipe, pin holes, cavity and any other defects.

Hardness survey:
Take a vertical slice of one inch thickness, mill it and take the indentation by 10 mm
hardened steel ball in presence of 3000 kg load. Measure the diameter of the
indentation by a Brinel microscope and find out the value from the chart of clculate the
values by the following formulae.The sample frequency shall be one in 1000 for BoxN,one in 500 for Carriage and one in 250 for loco wheels.The hardness values should
be in desending in nature from flange to the hub of the wheel.

2P
BHN =
3.14xD(10 ( Root D2 - d2)
Where P
D
d

Diameter of the indenter and
diameter of the indentation

Closer test:
This is the indication of the wheel contains a residual compressive stress after
quenching. Mark two points between 100 mm on the flange and the back rim. Take out
a slice of one thickness of a vertical slice by two radial saw cuts in a Do all machine

and after taking out the slice for the hardness survey measurer the distance between the
two points. The wheel should close and the minimum closer value should be +1 mm.
Closer test of wheel:
Puch 2 points apart 100mm on the flange
Takeout a wheel slice of 1 thickness by radial saw cut machine(Do all)
Take the final measurement and it shols be +1mm minium.

Hardness of wheel:
Mill both sides of the vertical wheel slice taken out during closer test.
Take BHN indentations by I gap fron flange to hub of the wheel by a
BHN machine containing 10mm hardened steel ball&3000kgs load.
The hardness value should decreasing in trend from flange to the hub.

Axle.
Ultrasonic testing of axles.
Purposes :
To evaluate the quality of the axles by detecting the discontinuities which are harmful
to the axle service.
Principle:
Pass the ultrasonic sound in to the axle under test from one end face of better surface
finishing of 3.2 micron. The sound rays will penetrate through out the axle and after
reaching the opposite end the sound rays will reflect back t o the home position by the
reflection of the air medium.
Method
Equipment used
Normal probe
frequency

## Low angle probe

Couplant
Stage of inspection

## Pulse echo method

USD-15S,Khruatkrammer,German make or equivalent.
PZT typeof 20-26 mm diameter and 2 2.5 MHz
of Kruatkrammer,German make or eqivallent.
Gun assembly contains 1.3,19.3&24.3 degree probes to
detect the the discontinuities in body,up to inner wheel
seat fillet and up to the outer wheel seat fillet
respectively.
Grease dissolved in oil
Surface finish shall be better than 3.2 micron

Standardization:
406

Probe

25
381

Initial echo

Back wall
Flaw echo (12.5%)

Place the normal probe just opposite to the 3.2 mm dia artifishal made flat bottom hole
and adjust the gain to get 12.% of the flaw height. Not the gain and is called as FBH
standard gain.
Standardization for Gun assembly:

Probe
6mm saw cut
Gun assembly

Initial echo
wall

## Flaw echo(75% height)

Back

Place the gun assembly on the standard axle containing 6 mm artifishal saw cut and
adjust the flaw height to 75% and note the gain.It is the standard gain for
Gunassembly scanning.

Fax No.0343-2546625
Kind attn to Shri.ChandrasekharRao,CMT,RWF Inspection cell
C/o. R & C Lab. /ASP.

## Standardization for radial scanning(As per R-16/95):

200
3.2
252

150

Initial echo

Range =

Flaw echo(60%)

back wall

250 mm

Place the probe exactly opposite to the artificial flaw of 3.2 mm diameter and adjust
the gain to get 60% flaw height and note the gain. This is called as FBH standard gain
for radial scanning of R-16 / 95 axles.

Fax No.0343-2546625
Kind attn to Shri.ChandrasekharRao,CMT,RWF Inspection cell
C/o. R & C Lab. / ASP.

## Standardization for radial scanning(As per R-43/92):

260
3.2
252

150

Initial echo

Range =

Flaw echo(60%)

back wall

400 mm

Place the probe exactly opposite to the artificial flaw of 3.2 mm diameter and adjust
the gain to get 60% flaw height and note the gain. This is called as FBH standard gain
for radial scanning of R-43 / 92 axles.

10

Fax No.0343-2546625
Kind attn to Shri.ChandrasekharRao,CMT,RWF Inspection cell
C/o. R & C Lab./ASP.

## Standardization for End End scanning: (As per R-1695&R-43/92)

406

Probe

25
381

Initial echo

Back wall
Flaw echo (12.5%)

Place the normal probe just opposite to the 3.2 mm dia artificial made flat bottom hole
and adjust the gain to get 12.5% of the flaw height. Note the gain and is called as FBH
standard gain.
(All dimensions are in mm)

11

Fax No.0343-2546625
Kind attn to Shri.ChandrasekharRao,CMT,RWF Inspection cell
C/o. R & C Lab./ASP.

Gun assembly
6mm saw cut
Gun assembly

Initial echo
wall

## Flaw echo(75% height)

Back

Place the gun assembly on the standard axle containing 6 mm depth artificial saw cut
and adjust the flaw height to 75% and note the gain.It is the standard gain for
Gunassembly scanning.

12

Fax No.0343-2546625
Kind attn to Shri.ChandrasekharRao,CMT,RWF Inspection cell
C/o. R & C Lab./ASP.

DAC blocks for drawing DAC curve: As per IRS specifications R-16/95&R-43/92)

Zone
I

## Length of DAC block in mm

101.6

Diameter of FBH in mm
3.2

177.8

3.2

279.4

3.2

406.4

## 3.2,6.4(Use for II zone also

as a first block)

II

533.4

6.4

660.4

6.4

787.4

## 6.4,9.5(Use for III zone

also as a first block

II

914.4

9.5

1041.4

9.5

1168.4

3.2,6.4,9.5

13

Visual inspection:
Check the face, CTA, Journal, wheel seat and body of the axle visually by naked
eye/low magnifying lens etc. If the axle contains gouge mark, end crack of the defects
due to the RWFs process make it as defective non-source(S).If the axle is getting
rejected ultrasonically made as UT rejected and if contains inclusion crack of any
other defects due to the manufacturer of the bloom make it as defective Source(S) and
enter in LAN record.If the defect may go by further machining make it as others(O) or
if it is free from any defects carry out the ultrasonic testing.
Penetrability test:Clean the face of the axle and apply the couplant.Do the preliminary adjustments of
the UFD and scan with normal probe.If the wack wall at FBH gain is mere than 25%
further carry out the testing and the penetrability test is ok..If it is <25% mark it for
RHTMore than two RHT is not permitted and the axle is rejected.
Far end scanning:Clean the face of the axle and apply the couplant.Do the preliminary adjustments of
the UFD and scan with normal probe&observe any signal between initial and back
wall.If it is due to the shape/geometry of the axle it is ok.If it is due to flaw, reduce the
gain in the setting FBH gain and if it is more the 12.5% amplitude height it is cause for
rejection and enter in LAN as ut rejected.
Testing by Gun assembly:Place the gun assembly on the axle face and rotate slowly at least twice in clock and
another twice in the anti clock directions and observed the ut screen. If there is no flaw
signal the axle is ok and if there is a flaw signal with more than 75% of the amplitude
height at FBH gain is a cause for the rejection.
Manual radial scanning:Do the preliminary adjustments and apply the couplant on the axle laterally. Scan and
if the axle is free from the flaw signal it is ok. Otherwise follow the following rejection
norms for the radial scanning of the axle.
a)

Flaw signal with more than 60% at FBH gain and more than 2 probe length
on Journal & Wheel seat and more than three probe length on body is cause
for rejection.
b)
If the distance between two isolated signals is lesser than 200 mm is a
cause for rejection.
c)
More than three isolated signals throughout the axle is a cause for rejection.
d)
Flaw signal with 60% of amplitude height provided the location is between
and mod-radius & surface f the axle is cause for rejection.
Manufacture of Box-N axle:
Billet cutting:Cut the bloom in 975 +/- 5 mm by saw/gas cutting carefully
Preheating in RHW:-

14

Charge the billets in the RHW and heat to 1150 1200 deg C for about 6 hours
Forging:Forge the preheated billets by long forging machine
End cutting:Remove sufficient discards by gas cutting
Number stamping:Stamp the serial number of the axle by automatic stamp punching machine in hot
condition
Intermediate cooling:
Allow the hot axle to cool to 200 - 250 deg. C through the intermediate cooling bed
Heat treatment:
Normalizing:Charge the cooled axles at 200 250 deg. C in to Normalizing furnace and heat to 840
- 860 deg C for about 6 hours.
Intermediate cooling:
Allow the normalized axles to cool to 200 deg. C through the intermediated cooling
bed.
Tempering:Charge the air cooled axles to 200 deg. C in to the Tempering furnace at the
temperature of 550 - 640 deg. C for about 8 hours 45 minutes.
Air cooling:After tempering allow the tempered axles to air cool for about 24 hours.
Lab. Test:
Take two samples of size 250x25x25 mm size from the center portion of the prolonged
journal portion of the heat treated axle and conduct all the required tests to conform
following requirements as per R-16-/1995.
Physical properties:-

Sl.No.

Characteristics

1
2
3

## Yield strength N/mm2 Min.

Tensile strength N/mm2
Elongation% Min.

320
550 650
22

15

4
5

## (Gl-5.65 root A0 ) Where, Ao - area of

cross section of test piece.
Micro grain size @ 100x
Not coarser than ASTM
grain size No.5
Macro examination
Should not reveal any
defects and central

Micro structure

segregation should be
better than C2
Uniform fine pearlitic
structure

Chemical composition:Sl.No.

Elements

C%

Mn%

Si%

P%

S%

Cr%

7
8
9

Ni%
Cu%
Mo%

10

V%

0.37 + 0.03
- 0.00
1.12 + 0.06
- 0.00
0.46 + 0.04
- 0.00
0.04 + 0.005
- 0.000
0.04 + 0.005
- 0.000
0.3 + 0.05
- 0.00
0.3 + 0.02
- 0.00
0.05 + 0.00
- 0.00
0.05 + 0.00
- 0.00

## Machining of the axle:a.

Cup turn,end mill and make the lathe center bore.
Number stamping:Punch the serial No. and Cast No. of the axle manually on the axle face.
Ultrasonic testing:Scan the axle ultrasonically thoroughly and if the axle is passing allow to further
machining by putting the UT stamp on the axle number face.

16

Further machining:b.
Rough turn the axle
c.
Semi finishing of the axle except body
d.
Body finishing
e.
Finishing of the axle except body
f.
Drilling, tapping and recentering of the axle
g.
Furnishing of wheel seat
h.
Centreless grinding of journal, dust guard etc.
Magnetic particle testing of axle:Conduct the MPT of the axle and if it is passed allow the passed axle for pressing by
putting the MPT stamp on the axle face opposite to the UT stamp.

## Magnetic Particle Testing of axle:(MPT)

Equipment used:
Magnaflux,USA make of DH 5455 model.
Current used:
Half wave DC for coil&Contact magnetization
AC for Demagnetisation
Current used for
Coil magnetization = 1200 Amps.
Contact magnetization = 1800 Amps.
Demagnetization = 3000 Amps.
Bath oil = MX-MG Carrier Oil-II supplied by M/s.ITW Signode,Hyderabad.
MPT Powder = Magnaflux-14A supplied by M/s.ITW Signode,Hydreabad.
Amount of powder per litre = 1.25 gram/litre.
Concentration of the bath = 0.2 - 0.30 ml/100 ml after half an hour.
Watt of the UV lamp = 100 watt.
Intensity of the UV lamp = 525 micro watt/centimeter square.
Principle:
Magnetize the axle under test.Magnetic force of lines will develop.Spray the bath containing containing
iron particle coated with flourescent material.If there is a defect,the magnetic force of lines will leak
i.e. leakage of magnetic flux arround the defect and attract more particle around the defect and can seen
under UV lamp.
Coil magnetization:
Place the coil over wheel seat and pass the current through the coil to develop longitudinal field.Spray the.
bath and after few seconds inspect under UV lamp to detect the verticle discontinuities.The discontinuity
will develop polority and will attract more powder arround the defect and can seen under UV lamp.If the defect
may go by re work mark for rework.
Contact magnetization:
Press the contact pad and pass the current through the axle to develop circular magnetic field to detect the
longitidinal discontinuities.Spray the bath and inspect under UV lamp as above.
Demagnetization:
Press the contact pad and pass the AC current through the axle to demagnetize the magnetized axle.The
residual magnetic field shall be plu or minus 5 gauss.
Imperfections not permisciple:
1. Any type of verticle,circumferential discontinuities any where on the axle not permitted.
2 Any type of discontinuities on the fillet not permitted.

17

Imperfection permiciple:
Journal:

18

## Iron - Carbon System

1600
Liquid
Delta iron
1539
Delta iron + Liquid
0.53%
Austenite

0.08%

Liquid
+
Cemintite

1490
Austenite+Liquid
1400
Liquid+
Austenite

Austenite+
Delta

T
e
m
p
e
r

1146 oC

Austenite+Ferrite
910
768

Austenite
+
Aus+ Ledeburite
Cemin
+
tite
Cemintite

Cemintite
+
Ledeburite
727 oC

19

Iron-Carbon System:
t
u
r
e

0.02%

Ferrite
Pearlite +
Ferrite

P
e
a
r
l
i Pearlt ite +
e Fe3C

Pearlite
+
Transformed Ledeburite +
Cementite

0.8
2
4.3
Steel
Cast Iron
Hypo
Hyper
Hypo
Eutectoid
Eutectoid Euectic

Cemintite
+
Ledeburite

6.67
Hyper
Eutectic

Carbon% wt

## Fe-C system is a graphic representation of various transformation of carbon % weight at various

temperatures.
Phases:
Ferrite:It is an interistial solid solution in which carbon in BCC iron .The maximum solubility is 0.02%
Austenite:
It is an interstitial solid solution of carbon in FCC iron. The maximum solibility is 2.1 % at 1146
Delta iron:
It is an interstitial solid solution of carbon in BCC iron. The maximum solibility is 0.08 %
It is from 1539 degree centigrade which is the melting point of iron to 1400 degree centigrade.
Pearlite:
This an alternative arrangement of parallel plates of ferrite and cemintite
Cemintite:
It is an intermetalic compound represented by the formula Fe3O4.the structure is
orthorhombic and the number of
atom is 25% but the C weight % is 6.67.Hence after 6.67% of carbon the Fe-c system is
not extended.
Transformations:

20

## The various transformations place in Fe-C system is as follows.

1.Feritectic reaction:
Reaction
Structure
C% wt.

Delta iron
BCC
0.08

Liquid
-0.53

Gama iron
FCC
2.1

Liquid and delta irons react together and forms austenite at 1400 degree centigrade
temperature.
2.Eutectic reaction:
Reaction
Structure
C% wt.

Austenit
e
FCC
2.1

Liquid
-4.3

Cemintite
Ortorhombic
6.67

Liquid iron will become austenite and cemitite on cooling at 1146 degree centigrade
temperature.
3.Eutectic reaction:
Reaction
Structure
C% wt.

Austenite
FCC
0.80

Ferrrite
BCC
0.02

Cemintite
Orthorhombi
c
6.67

Critical temperatures:
These are the temperatures at which various transformations tking place and are as follows.
1.Gama iron will become ferrite and cemintite on cooling at 727 degree centigrate and represened
by the symbols A,c,r etc.,
On slow cooling Ac1=Acr=727 degree centigrade.
On normal cooling there is thermal hysterisis and Ac1>Acr.
2.The next higher is curie temperature of ferrite iron & represented by the symbol A2 and is 768
frrrite will undergo magnetic transition from ferro to para magnetic stage.
3.The temperature corresponds to the phases Gama+ferrite/gama iron is A3 and it is steeper
degreses from 910 degree
centigrade to 727 degree centigrade.Unlike A1 this is function of carbon % weight.
4.The temperature corresponds to the phase Gama iron+cemintite/gama iron is ACM and is increased
from 727 to 1146 degree
centigrades.This also a function of carbon % weight.
5.The curie temperature of ferrite is A0 and is 210 degree centigrade.
Micro structure of steel:

21

1.Eutectiod steel:
The structure is pearlite and the chemical composition is '0.80% C weight. The amount of ferrite &
cementite can be calculated
By lever rule and is as follows.

Ferrite% =
88.3

x 100 =

6.67 - 0.80
6.67 - 0.02

Cementite=
11.7

x 100 =

0.80 -

0.02

6.67 - 0.02
or
100 - 88.3 = 11.7%
2.Hypo eutectoid steel:
The chemistry is < 0.80 % c weight.For example in 0.2% C steel the amount of
consitituents in 0.2 % C weight are
'0.80 - 0.2
Ferrite% =
x 100 =
76.9
0.80 - 0.02
'0.20 - 0.02
Pearlite % =
x 100 =
23.1
'0.80 - 0.02
3.Hyper eutectic steel:
The chemistry is '0.80 - 2.1 % C weight.In 1.2% Carbon steel the amont of consistituents are
Pearlie % =

'

6.67 - 1.2
x 100 =

93.2

6.67 - 0.80
Cemintite = 100 - 93.2 = 6.8

## Wheel defects:Defect Code

3
8
9
10
12
13
15
16

Description
Off analysis
Low Brinell
Tramp elements
Crack&Checks
Ceramic-Metal-Refractory
Slag
Pin holes
Ultrasonic

22

20
30
31
32
33
35
38
39
40
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
70
71
72
73
90
91
92
93
94

## Rabit ears(Sand expansion)

Off center hub cut
Wrong hub cut
Gough bore
Hole in bore
Goughed riser
Damaged stampimg
Unknown heat number
Thin flange
Wrong mould machining
Insufficient spray
Hole in riser
Pocker
Eroded mould
Pin at apex
Mould shift
Poured short
LAP
Clusters of small holes on rim
Gas holes in rim
Hollow sprue
Shrinkage riser stubs
Hollow hub face
Run out
Closed down wrong
Stopper broken
Run back
Mould inclusions
Defective tube
Porous sprue
Hollow hub feeding
Defective core
Dela processing
War page
Spoiled normalizing
Spoiled handling
Spoiled mounting
Spoiled grinding
Spoiled machining
Spoiled mechanical
Spoiled power
23

95
96
97
98
99
121
122
123
124
125
126
128
129
131
135
138
139
621
622
623
624
625
626
627
628
629

Spoiled electrical
Experimental
Obsolete
Missing
New design
Black, gray tube inclusion
Small,irregula,combined brown
Splatter of 122
Refractory
Defective tube
Unknown
Small red orange
Blowing tube
Pin in slag
Furnace slag
Slag splatter
Spray
Asbestos
Rat tail(Seams in throat)
Graphite or sand
Spray or sand
Graphite
Fused sand
Raw sand
Sand splatter

24

Specifications:
Specn. Analysis H2

N2

P%

## S+P% Cr% Ni% Cu% Mo% V%

UTS

YS E%(GL= GS @
Min. 5.65 root 100x

Macro

A0

RLA
16/95

3
70 2-1/Ingot 0.37 1.12 0.46 0.04 0.04 0.07
PPM PPM - Bloom Max. Max. Max. Max. Max. Max.
Max. Max. 1.5-1/
Ingotbloom
provided
5-1/ ingot
axle
3-1/
Ingot-axle
3-1/
Concast
bloomaxle
PA(Over
--- 2-1/Ingot +0.03 +0.06 +0.04 +0.005 +0.005 -LA the
- Bloom - 0 - 0 - 0 - 0
-0
following
1.5-1/
shall be
Ingotpermitted)
bloom
provided
5-1/ ingot
axle
3-1/
Ingot-axle
3-1/
Concast
bloomaxle
RLA /
2
70 2-1/Ingot 0.40- 0.60- 0.15 0.05 0.045
-43/92 Ctategory- PPM PPM - Bloom 0.55 0.90 Min. Max. Max.
A
Max. Max. 3-1/
Ingot-axle
1.5-1/
Ingotbloom
provided
5-1/ ingot
axle
PA(Over
--- 2-1/Ingot +/- +/- +0.0 +0.005 +0.005 -LA the
- Bloom 0.03 0.03 -0.15
following
3-1/
Max. Max.
shall be
Ingot-axle
permitted)
1.5-1/
Ingotbloom
provided
5-1/ ingot
axle
RLA
3
70
-0.57- 0.60- 0.40 0.03 0.03
-19(III)
PPM PPM
0.67 0.80 Max. Max. Max.
/1995

PA

--

--

--

+0.03 0.01
0.02

0 +0.005 +0.005
-0
-0

--

## 0.3 0.3 0.3 0.05 0.05 550- 320 22 %

Max. Max. Max. Max. Max. 650 N/ N/ Min.
2
2
mm
mm

-0
-0

-0

-do-

--

--

--

--

685
of
N/mm2 UTS
Min.

--

--

--

--

--

0.06 -Max.

0.05 0.05 --

+0.02

-do- -do-

-do-

930
50% 4.5 Min.
N/mm2 of
Min./ UTS
Rim
Min.
--

--

--

Not
coarser
than 5
@100x

--

25

6-8
@100x

Better
than
C2&No
any
other
defects

-do-

-do-

-do-

-do-

--

-do-

--

-do-

Body
Inner
W/s fillet
Wheel
seat
CTA
LCB
Face
Journal
Outer
w/s
fillet

## Axle flow chart.

Billet cutting
by Gas/Saw
cutting)
Air
cooling

Lab.
testing

Preheating
at RHF (1150

Forging by
LFM(1100
-900)

Cooling

Cooling

Normalizing
(1150-1200

-1200)

Tempering(550640)

CTA,
LCB&End
Milling

deg. C

UT

Assembly

Further
machining

MPT

## ON LINE ULTRASONIC TESTING OF CAST STEEL WHEELS MANUFACTURED

AT RWF
Introduction
All the cast wheels shall be ultrasonically tested with minimum of 6 transducers in two
directions (radially and axially) through rim section in accordance with IRS R-19/1993
(Part III). The Calibration reference standard and rejection level of each wheel design is
established by making test set-up wheel. Procedure for ultrasonic testing of cast steel
wheels are followed as laid down in the relevant specification.
Standardization of Ultrasonic testing system is carried out in the beginning of each shift
or whenever there is a break down or any change of component in on line system or
change in wheel design under process.
The custom built ultrasonic system is in compliment with the production process to detect
all possible casting defects in rim section of the wheel.
Ultrasonic scanning system
In casting of wheels by controlled pressure pouring technique, defects like shrinkage
porosity, gas holes etc., which occur during solidification within the rim section. In RWF
the ultrasonic testing methodology employed is automatic on line immersion technique in
water medium incorporating 6 transducers connected to a microprocessor based multichannel computer controlled scanning system.

## Convergent beam Transducers of 2.25MHz & 5.0MHz frequency and 20 mm crystal

diameter are employed. Each transducer is identified as 1A, 2A, 3A, 1B, 2B & 3B.
Transducer 1A(2.25MHz) is focused axially closer to tread for detecting defects
like gas holes below the front rim face and closer to tread.
Transducer 1B(2.25MHz) is adjusted axially for detecting gas holes that may
occur below the front rim face farther away from tread and for cavities below the
sprue area.
defects at the central line.
defects at 1/8 away from the central line towards back rim.
Transducer 3A(5.0MHz) is adjusted axially through front rim for detecting
defects at the central line.
defects below the sprue.
All above 6 transducers are assembled in manipulator probe assembly immersed in tank
containing continuous flow of water.
Test Set Up
An ultrasonic standard test wheel of each design is fabricated by saw cutting the rim
cross-section and artificial reference holes of 1/8dia length are introduced at
shrinkage co-ordinates of the respective locations. Slices are welded back to match the
original profile of the wheel.
The above wheel is used as a standard-set-up-wheel for setting up probes so as to achieve
maximum response from the artificially drilled holes in the wheel rim.
Sensitivity of the equipment is set by using UT standard manufactured from the same
design wheel with 1/8 flat bottom hole, which will not be disturbed during the normal
testing process.
Testing System
RWF has employed microprocessor based computer controlled automatic on-line
ultrasonic system, which consists of basic ultrasonic machine, multiplxer, oscilloscope,
and computer with dedicated custom built software. The whole system is inter-linked
with PLC for communication and control. The Speed of the wheel is kept at 4 rpm and
minimum of 2 revolutions for a complete test cycle is ensured for every wheel. All the
testing parameters are displayed on screen and reference location is measured by the help
of an encoder. During the test, any signal from the defect location exceeding the set level
will be indicated on the screen as REJECTED and wheel stops automatically.
Inspectors ensure the defect & location manually and send the wheel to the scrap line.
28

Other wise, wheel automatically deemed as PASSED by the system and moves for
further processing. Ultrasonic status of the all the wheels tested is entered into the LAN
for record.
Equipment in use
Presently RWF is using 2 customized ultrasonic testing system designed and supplied by
M/s ULTRASONIC SCIENCES LIMITED
Unit 4-Spring Lakes Industrial Estate
GU-12 4 UH, Dead brook lane, Aldershot
Hampshire, ENGLAND
Tel: +44(0) 1252350550
Fax: +44(0) 1252350445
E-mail:info@ultrasonic-sciences.co.uk
Website:http://www.ultrasonic-sciences.co.uk

## Points to be added x Tonnage of liquid metal x 10

-------------------------------------------------------------Efficiency of alloy

35 pts x 20 x 10
7000
-------------------------------------- = ------------70%
70

= 100 kgs
100 kg of ferro
alloy to be added to raise 35 pts with 70 % efficiency
Conversely for 35 pts recovery (Recovery is 100%)
Accordingly recovery can be calculated.

29

## Spray Mix 100 lb. Batch 35O Baume.

Ingredients:
CMC 0.1% of the weight of fused Silica, 2 bags weighing 22.7 grams etch.
Veegum-T 1.0% of the weight of Fused Silica, 3 bags weighing 152 grams each.
30 Micron Fuses Silica 100 lbs (45,400 gms)
Formaldehyde 120 ml (optional, depending on bacteria levels
Hot water used with initial CMC or Veegum mixture, allows materials to go into solution more
Mixing Instructions:
a)

To a clean mixing tank add 8 gallons of water. A permanent mark shall bemade on a rod
that relates 8 known gallons of water to a certain depth in the mixing tank. Turn mixer
on.
It is imperative that the mixing tank be thoroughly clean and completely empty.
Absolutely no spray mixture should remain in the tank from a previous batch.

b)

Add 1 gallon of water to the specified mixing bucket. Turn waring blender on and add 1
bag (22.7 grams) of CMC powder slowly and uniformly to the water, while the agitator is
continuously in operation. Mix fore a minimum of 2 minutes, making sure that the CMC
is completely dissolved and free of lumps. Add this mixture to the larger mixing tank.

c)

Repeat the above operation (b), using one gallon of water and 22.7 grams of CMC.

d)

To the appropriate mixing bucket add 1 gallon of water and 1 bag (152 grams) of
Veegum-T, Mix for a minimum of 1 minute or until the Veegum-T is completely
dissolved and free of lumps.

e)

Repeat the above operation (d), using one gallon of water and 1 bag (152 grams) of
Veegum T.
f)
Repeat the above operation (d), using one gallon of water and 1 bag (152
grams) of Veegum-T.

g)

After all the premixed CMC and Veegum-T has been added to the large mixing tank, wait
5 additional minutes before adding the fused silica. Each of the two 50 lb. Bags shall be
added separately and not until the prior bag has gone into solution. The lightening mixer
must be in operation at all times. Any paper from the bags that falls into the tank must be
removed.
h)
After above solution has been mixed for 5 minutes, add 120 ml of
formaldehyde.
30

i)
With the Baume instrument, measure the density of the spray
mixture. Adjust the consistency of the solution to 35O - 40O Baume. (Baume may
be different from plant to plant depending non gun distance from mold and other
variables. This difference shall be verified through the Operating Department). If
the Baume is too high, add water slowly, and carefully bring down the Baume
within limits. If the Baume is too low, add Fused Silica slowly and carefully bring
up the Baume within limits. Determine the proper amount of water to add to the
mixing tank (in part (a)) in order to obtain a consistent Baume on the final spray
mixtures from batch to batch.
j) The Baume shall be recorded on the 302s for the molds being sprayed.
6B. Mold Spray mix 100 lb. Batch 36O Baume (Alternate method).
Ingredients:
CMC 0.1% OF THE WEIGHT OF fuses Silica, 1 bag weighing 45.4 grams.
Veegum T 1.0% of the weight of Fused Silica, 1 bag weighing 454 grams.
30 Micron Fuses Silica 100 lbs. (45,400 gms).
Formaldehyde 120 ml (optional depending on

bacteria levels).

## Hot water used with initial CMC and Veegum Solution.

Mixing Instructions:
a) To a large clean mixing tank add 7 gallons of water. A permanent mark shall be made on
rod that relates 7 known gallons of water to a certain depth in the mixing tank. Turn
mixer on.
It is imperative that the mixing tank be thoroughly clean and completely empty.
Absolutely no spray mixtures should remain in the tank from a previous hatch.
a)
Add 3 gallons of water to a mixing bucket (Detail-D) or sufficient water to bring
water level upto a known marker. Turn Waring Blender on and add 1 bag (45.4 grams) of
CMC powder slowly and uniformly to the water while the agitator is continuously in
operation. Mix for a minimum of 5 minutes making sure that the CMC is completely
dissolved and free of lumps. Add this mixture to the larger mixing tank.
a)
To the mixing bucket add 3 gallons of water (or sufficient water to bring water
level upto a known marker) and add 1 bag (456 grams) of Veegum-T. Mix for a
minimum of 5 minutes or until the veegum-T is completely dissolved and free of lumps.
Again the mixer should be turning prior to adding the Veegum-T in a slow and uniform
manner. Add this mixture to the larger mixing tank.
a)
After all the premixed CMC and Veegum-T have been added to the large mixing tank,
wait 5 additional minutes before adding the Fused Silica. Each of the two 50 lb. Bags
shall be added separately and not until the prior bag has gone into solution. The lightning
mixer must be in operation at all times. Any paper from the bags that fall into the tank
must be removed.
31

a)

After above solution has mixed for 5 minutes, add 120 ml of formaldehyde.

b) With Baume instrument, measure the density of the spray mixtures. Adjust
the consistency of the solution to 35O - 40O Baume. (Baume may be different
from plant to plant depending on gun distance from mold and other variables.
This difference shall be verified through the Operating Department). If the
Baume is too high, add water slowly and carefully bring down the Baume
within limits. If the Baume is too low, add Fused Silica slowly and carefully
bring up the Baume within limits. Determine the proper amount of water to
add to the mixing tank (in part (a)) in order to obtain a consistent Baume on
the final spray mixture from batch to batch.
c)

The Baume shall be recorded on the 302s for the molds being sprayed.

7A.

## CMC 0.1% OF THE WEIGHT OF fuses Silica, 2 bags

weighing 28.4 grams.
Veegum T 1.0% of the weight of Fused Silica, 3 bags
weighing 190.0 grams each.
30 Micron Fuses Silica 125 lbs. (56,800 gms).
Formaldehyde 150 ml (optional depending on bacteria
levels).
Hot water used with initial CMC and Veegum Solution.
Mixing Instructions:
a)
To a large clean mixing tank add 11.25gallons of water. A
permanent mark shall be made on rod that relates 11.25 known
gallons of water to a certain depth in the mixing tank. Turn mixer
on.
It is imperative that the mixing tank be thoroughly clean and completely
empty. Absolutely no spray mixtures should remain in the tank from a
previous hatch.
a)

## Add 1 gallons of water to a appropriate mixing bucket. Turn Waring Blender

on and add 1 bag (28.4 grams) of CMC powder slowly and uniformly to the
water while the agitator is continuously in operation. Mix for a minimum of 2
minutes making sure that the CMC is completely dissolved and free of lumps.
Add this mixture to the larger mixing tank.

c) Repeat the above operation (b), using 1 gallon of water and 1 bag (28.4 grams) of
CMC.
d) To the small mixing bucket add 1 gallons of water and add
1 bag ( 190.0 grams) of Veegum-T. Mix for a minimum of 1
32

## minute or until the veegum-T is completely dissolved and free of

lumps. Again the mixer should be turning prior to adding the
Veegum-T in a slow and uniform manner. Add this mixture to the
larger mixing tank.
a)

Repeat operation (d), using 1 gallon of water and 1 bag (190.0 grams) of
Veegum-T.

b) Repeat operation (d), using 1 gallon of water and 1 bag (190.0 grams) of
Veegum-T.
g)
After all the premixed CMC and Veegum-T have
before adding the Fused Silica. Each of the two 50 lb. Bags shall
be added separately and not until the prior bag has gone into
solution. The lightning mixer must be in operation at all times.
Any paper from the bags that fall into the tank must be removed.
d) After above solution has mixed for 5 minutes, add 150 ml of formaldehyde.
e)

With Baume instrument, measure the density of the spray mixtures. Adjust
the consistency of the solution to 35O - 40O Baume. (Baume may be different
from plant to plant depending on gun distance from mold and other variables.
This difference shall be verified through the Operating Department). If the
Baume is too high, add water slowly and carefully bring down the Baume
within limits. If the Baume is too low, add Fused Silica slowly and carefully
bring up the Baume within limits. Determine the proper amount of water to
add to the mixing tank (in part (a)) in order to obtain a consistent Baume on
the final spray mixture from batch to batch.

f)

The Baume shall be recorded on the 302s for the molds being sprayed.

33

7B.

## CMC 0.1% OF THE WEIGHT OF fuses Silica, 2 bags

weighing 56.8 grams.
Veegum T 1.0% of the weight of Fused Silica, 3 bags
weighing 568 grams each.
30 Micron Fuses Silica 125 lbs. (56,800 gms).
Formaldehyde 150 ml (optional depending on bacteria
levels).
Hot water used with initial CMC and Veegum Solution.
Mixing Instructions:
a)
To a large clean mixing tank add 10.25 gallons of water. A
permanent mark shall be made on rod that relates 10.25 known
gallons of water to a certain depth in the mixing tank. Turn mixer
on.
It is imperative that the mixing tank be thoroughly clean and completely
empty. Absolutely no spray mixtures should remain in the tank from a
previous hatch.
b)
Add 1 gallons of water to a appropriate mixing bucket
(Detail-D) or sufficient water to bring water level upto a known
marker. Turn Waring Blender on and add 1 bag (56.8 grams) of
CMC powder slowly and uniformly to the water while the agitator
is continuously in operation. Mix for a minimum of 2 minutes
making sure that the CMC is completely dissolved and free of
lumps. Add this mixture to the larger mixing tank.
c) To the mixing bucket add 3 gallonss of water are sufficient
water to bring water level upto a known marker)and add 1 bag (
568.0 grams) of Veegum-T. Mix for a minimum of 5 minute or
until the veegum-T is completely dissolved and free of lumps.
Again the mixer should be turning prior to adding the Veegum-T in
a slow and uniform manner. Add this mixture to the larger mixing
tank.
d)
After all the premixed CMC and Veegum-T have
before adding the Fused Silica. Each of the two 50 lb. Bags shall
be added separately and not until the prior bag has gone into
solution. The lightning mixer must be in operation at all times.
Any paper from the bags that fall into the tank must be removed.
e)

After above solution has mixed for 5 minutes, add 150 ml of formaldehyde.

34

f)
With Baume instrument, measure the density of the spray mixtures. Adjust the
consistency of the solution to 35O - 40O Baume. (Baume may be different from plant to plant
depending on gun distance from mold and other variables. This difference shall be verified
through the Operating Department). If the Baume is too high, add water slowly and carefully
bring down the Baume within limits. If the Baume is too low, add Fused Silica slowly and
carefully bring up the Baume within limits. Determine the proper amount of water to add to the
mixing tank (in part (a)) in order to obtain a consistent Baume on the final spray mixture from
batch to batch.
g)

The Baume shall be recorded on the 302s for the molds being sprayed.

35

8A.

## Mold Spray mix 200 lb Batch 36O Baume

Ingredients:
CMC 0.1% OF THE WEIGHT OF fuses Silica, 4 bags weighing 22.7 grams.
Veegum T 1.0% of the weight of Fused Silica, 3 bags weighing 152 grams each.
30 Micron Fuses Silica 4 bags weighing 50 lbs each or a total weight of 200 lbs. (90,800 gms).
Formaldehyde 240 ml (optional depending on bacteria levels).
Hot water used with initial CMC and Veegum Solution.
Mixing Instructions:
a)
To a large clean mixing tank add 16 gallons of water. A permanent mark shall be made
on rod that relates 16 known gallons of water to a certain depth in the mixing tank. Turn mixer
on.
It is imperative that the mixing tank be thoroughly clean and completely empty. Absolutely no
spray mixtures should remain in the tank from a previous hatch.
b)
Add 1 gallons of water to a appropriate mixing bucket. Turn Waring Blender on and add
1 bag (22.7 grams) of CMC powder slowly and uniformly to the water while the agitator is
continuously in operation. Mix for a minimum of 2 minutes making sure that the CMC is
completely dissolved and free of lumps. Add this mixture to the larger mixing tanks.
b)

Repeat the above operation (b), using 1 gallon of water and 22.7 grams of CMC.
b)

Repeat the above operation (b), using 1 gallon of water and 22.7 grams of CMC.

c)

Repeat the above operation (b), using 1 gallon of water and 22.7 grams of CMC.

d)

To the appropriate mixing bucket add 1 gallons of water and add 1 bag ( 152.0
grams) of Veegum-T. Mix for a minimum of 1 minute or until the veegum-T is
completely dissolved and free of lumps.
c)

Repeat operation (f), using 1 gallon of water and 1 bag (152.0 grams) of
Veegum-T.

d) Repeat operation (d), using 1 gallon of water and 1 bag (152.0 grams) of
Veegum-T.
e)

Repeat operation (d), using 1 gallon of water and 1 bag (152.0 grams) of
Veegum-T.

f)

Repeat operation (d), using 1 gallon of water and 1 bag (152.0 grams) of
Veegum-T.

g) Repeat operation (d), using 1 gallon of water and 1 bag (152.0 grams) of
Veegum-T.
36

l)
After all the premixed CMC and Veegum-T have
before adding the Fused Silica. Each of the two 50 lb. Bags shall
be added separately and not until the prior bag has gone into
solution. The lightning mixer must be in operation at all times.
Any paper from the bags that fall into the tank must be removed.
m)
After above solution has mixed for 5 minutes, add
240 ml of formaldehyde.
n)
With Baume instrument, measure the density of the
spray mixtures. Adjust the consistency of the solution to 35O - 40O
Baume. (Baume may be different from plant to plant depending on
gun distance from mold and other variables. This difference shall
be verified through the Operating Department). If the Baume is too
high, add water slowly and carefully bring down the Baume within
limits. If the Baume is too low, add Fused Silica slowly and
carefully bring up the Baume within limits. Determine the proper
amount of water to add to the mixing tank (in part (a)) in order to
obtain a consistent Baume on the final spray mixture from batch to
batch.
o)

8B.

The Baume shall be recorded on the 302s for the molds being sprayed.

## Mold Spray mix 200 lb Batch 36O Baume(Alternate method)

Ingredients
CMC 0.1% OF THE WEIGHT OF fuses Silica, 4 bags
weighing 45.4 grams.
Veegum T 1.0% of the weight of Fused Silica, 2 bags
weighing 454 grams each.
30 Micron Fuses Silica 4 bags weighing 50 lbs each or a total
weight of 200 lbs. (90,800 gms).
Formaldehyde 240 ml (optional depending on bacteria
levels).
Hot water used with initial CMC and Veegum Solution.
Mixing Instructions:
a)
To a large clean mixing tank add 16 gallons of water. A
permanent mark shall be made on rod that relates 14 known gallons
of water to a certain depth in the mixing tank. Turn mixer on.
It is imperative that the mixing tank be thoroughly clean and completely
empty. Absolutely no spray mixtures should remain in the tank from a
previous hatch.
37

a)

b)
Add 3 gallons of water to a appropriate mixing bucket or
sufficient water to bring water level upto a known marker. Turn
Waring Blender on and add 1 bag (45.5 grams) of CMC powder
slowly and uniformly to the water while the agitator is continuously
in operation. Mix for a minimum of 5 minutes making sure that the
CMC is completely dissolved and free of lumps. Add this mixture
to the larger mixing tank.
Repeat the above operation (b), using 1 gallon of water and 45.5 grams of CMC.
d) To the mixing bucket add 3 gallons of water or sufficient
water to bring water level upto a known maker and add 1 bag (
454.0 grams) of Veegum-T. Mix for a minimum of 1 minute or
until the veegum-T is completely dissolved and free of lumps.
Again the mixer should be turning in a slow and uniform manner
mixing tank.
e)
Repeat operation (f), using 1 gallon of water and 1 bag
(152.0 grams) of Veegum-T.
f)
After all the premixed CMC and Veegum-T have been
adding the Fused Silica. Each of the two 50 lb. Bags shall be added
separately and not until the prior bag has gone into solution. The
lightning mixer must be in operation at all times. Any paper from
the bags that fall into the tank must be removed.
g)
After above solution has mixed for 5 minutes, add 240 ml
of formaldehyde.
h)
With Baume instrument, measure the density of the spray
mixtures. Adjust the consistency of the solution to 35O - 40O
Baume. (Baume may be different from plant to plant depending on
gun distance from mold and other variables. This difference shall
be verified through the Operating Department). If the Baume is too
high, add water slowly and carefully bring down the Baume within
limits. If the Baume is too low, add Fused Silica slowly and
carefully bring up the Baume within limits. Determine the proper
amount of water to add to the mixing tank (in part (a)) in order to
obtain a consistent Baume on the final spray mixture from batch to
batch.

i)

The Baume shall be recorded on the 302s for the molds being sprayed.

38

2.

## Typical Mixes to Obtain 29-33 Baume with 15 Micron Min-U-Sil.

Total Quantities
Gals
GRS
Water
CMC

GRS
Veegum

ML
FORMAL
DEHYDE

10
20
30
40
50

2.0
3.8
5.7
7.6
0.5

4.54
0.09
13.6
18.16
22.70

45.6
91.2
136.8
182.4
228.0

12
24
36
48
60

Gals
GRS
Water
CMC
In
+
tank
1 Gal.
Water
0
4.54
1.8
9.08
3.7
13.62
5.6
18.16
6.5
22.70

60

11.4

27.24

273.6

72

8.4

27.24

70

13.3

31.78

319.2

84

9.3

80

15.2

36.32

364.8

96

11.2

90

17.1

40.86

410.4

108

12.1

15.89
15.89
18.16
18.16
20.43
20.43

100

19.0

45.40

456.0

120

14.0

22.70
22.70

110

20.9

49.94

501.6

132

15.9

24.97
24.97

120

22.8

54.48

547.2

144

17.8

27.24
27.24

130

24.7

59.02

592.8

156

19.7

29.51
29.51

140

26.6

63.56

638.4

168

19.6

150

28.5

68.10

684.0

180

21.5

21.19
21.19
21.19
22.70
22.70
22.70

160

30.4

72.64

729.0

192

23.4

15
Micron
Min U
Sil

24.21
24.21
24.21

GRS
Veegum
+ 1 Gal.
Water

15
Micron
Min-USil

ML
Formal
Dehyde

45.6
91.2
136.8
182.4
114.0
114.0
136.8
136.8
159.6
159.6
182.4
182.4
136.8
136.8
136.8
152.0
152.0
152.0
167.2
167.2
167.2
182.4
182.4
182.4
197.6
197.6
197.6
159.6
159.6
159.6
171.0
171.0
171.0
171.0
182.4
182.4
182.4
182.4

10
20
30
40
50

12
24
36
48
60

60

72

70

84

80

96

90

108

100

120

110

1332

120

144

130

156

140

168

150

180

160

192

D. MIXING EQUIPMENT
1.

Mixer Mixing Equipment Co., Inc., C/o Fuente and Webster, 549 West Randolph
Street, Chicago, Illinois.
Model S-1,1/3 H.P. Lightning Mixer 110 Volt with 36 long # 304 stainless shaft
and two # 304 stainless steel 4 3 blade propellers.
39

2.

## Mixer Tank and Fixtures. Chicago Carb-O-Tank Co.,

746 West Fullerton, Chicago, Illinois
1 60 gallon type H

## 304 stainless steel tank complete with three 16 legs

1 female outlet
1 figure 11 brass N.P. faucet
1 SS bracket (Portable agitator bracket for use with Lightning S-1 ,Mixer)
1 SS cover slotted for Lightning S-1 1/3 H.P. Mixer
3.

Blender Mixer. Master Elect Service Co., 835 West Washington Blvd., Chicago,
Illinois
Warning Mixer 1 gallon size, Part 004180 Alternate 3 gallon mixing bucket
Griffin Drawing E-606. 3-1, Detail-D

40

## Heat treatment of axle:

The process involving heating&cooling to egt the desired properties suitable for
serviceby changing the structure,composition etc.
Stages of heat treament:
1. Heating to the required temperature
2. Holding(Soaking) at this temperature for a period of time to attain
uniform temperature throughout the section.
3. Cooling the steel at specified rate.

Normalizing

Existing
structure and
properties of

properties of

steel

steel

Quenching

Tempering

## Principle of heat treatment

Air
cooling

Normalizing:
It is the process of heating the steel to above the upper critical temperature followed by cooling in
air.
Normalizing
Austenite
910

Temperature
O

723

Ferrite +
Pearlite

Pearlite +
Cemintite
0.8

C% wt
Purpose:
1. To relieve the internal stress
2. To refine the grain structure
41

## 3. To improve the machinability

4. To improve strength&toughness

Temperature&time of NF:
Temperature in o C
Required
Set
840 - 860
850
840-870
855
850-880
865

Zones
Pre heating
Main heating
Soaking

## Time in hrs(Cycle time x capacity

of the furnace)
2
2
2

Tempering:
Process of heating the axle to a temperature below lower critical temperature followed by air
cooling.
Purpose:
1.
2.
3.
4.

## To reduce the thermal stress

To stabilize the structure of the axle
To reduce the brittleness and
To increase the toughness&ductibility.

Austenite
910

Temperature
O

723
640

Tempering

550

0.8

C% wt

Temperature&time of TF:
Zones
Pre heating
Main heating

Temperature in o C
Required
Set
550-640
610
610-640
610

## Time (Cycle time x capacity of the

furnace)
2 hrs 55 min.
2 hrs 55 min.
42

Soaking

610-640

610

2 hrs 55 min

Quenching:
The process of heating the axles to austenite phase followed by sudden cooling in polymer
quenchant which is echo friendly for about half an hour.
Purpose of hardening followed by tempering :
1.
To develop high hardness, wear resistance and
2.
To improve the strength and toughness

Austenite
Hardnening
910

Temperature
O

723
640
550

0.8

C% wt

43

i.

1.5210 gm

ii.

2.06 mm H2O

iii.

## Measure the Stack temperature(Ts) in kelvin

77 + 273 = 350 oC

velocity:
C
=
Pitet tube constant x Root of h x Ts m/sec. iv.
Select the nozzle (An)
=

## 0.2022x 2.06 x350

5.43 m/sec

Flow rate:
Qm

V x A x 60 x 1000 LPM

## 5.43 x 60x1000 x3.165x10-5

10.31 LPM / Nozzle
5.43 x 60 x 1000 x7.123x10-5
23.21 LPM / 3/8 Nozzle
5.43x60x1000x7.917x10-6
2.58 LPM / 1/8 Nozzle

298
Qn

Qm x

298
LPM

23.21x

350
19.76 LPM

TS
v.

1000
Sampling time

1000
Min. -

Qn
-

19.76
50 Min.

vi.

31+273=304 oK

vii.

Measure the

20 mm Hg

viii.

## Calculate the volume of the sample collected

Vs

ix.

x.

meter pressure mm

## Actual volume of sample collected:

Vsx (750-Pm) x 298
Vn =
760 x Ta
Take the final weight of the thimble
Wt of dust
=Fwt-Iwt
Wt of dust
SPM =
x 106 Mg/Nm3
Vs

19.76x50=988 lit

19.76x(750-20)x298
760 x 304
18.61 x 50=930.5 Litre at STP
1.5413gm
1.5413-1.5210
0.0203 gm
0.0203
x106
930.5
44

21.8121.82 Mg/Nm3

a)

## Take the initial weight of the moisture free filter paper in gm

b)

Place the paper on the air sampler,set the time for 24 hours and switch on.

c)

d)

V

e)

## Take the final weight of the filter paper in gm

Wt of dust
x 106

SPM =

m / m3

Eg)
FWt
IWt

=
=

4.1970 gm
2.8627 gm

Wt of the dust =

1.3343 gm

Flow rate

1.435 m3 / min.

Tsampling

24 x 60 Min.

1.435 x 24 x 60 M3

1.3343
SPM

x 106
1.435 x 24 x 60

SPM

645.71 m / m3

45

Manufacturing of Wheel:
Furnace used:
High power basic direct electric arc furnace.The charge is melted by the heat produced by the arc
by passing high power electric current through the graphite electrodes.The charge is loaded as
heavy,medium&light scraps in bottom,middle&top of the furnace respectively.
Charge:
The raw material contains axle end cuts, risers, wheel cuts, medium scraps like sleeper, steel
plate,rods,buffes,spikes,keys etc.,borings,shereded scraps etc.The weight od each in the buckect
is as follows.
Sl.No.

Type of scraps

Number of magnets

1
2
3
4
5
6
7

## Axle end cuts

Wheel risers
Wheel cuts
Medium scraps
Borings
Shredded scraps
Lime stone / Calcined lime

2
3
3
5-7
2-3
2
--

Weight
in
approximately
2.5
4 4.5
6
4
2
2
1.7 / 1.25

MT

Melting:
The scrap is melted under a basic oxidizing slag consisting of lime stone and mill scales
providing cutting os scrap / collapses of bridges by O2 lancing..Consequently the Si,Mn&P
present are observed in to the basic oxidizing slag(Black) and when the process is completed,the
slag is completely removed without drain of steel melt.Take sample and send to spectro for
analysis. The oxidation reaction reactions are:

2FeO

Si

SiO2

FeO

Mn

MnO

FeO

SiO2

FeO.SiO2

MnO

SiO2

MnO.SiO2

5FeO

2P

5Fe

3FeO

P 2 O5

(FeO)3.P2O5

(FeO)3.P2O5

3CaO =

3FeO +

2Fe

P2O5

(CaO)3 . P2O5

In the next stage new slag is formed by adding reducing slag mixture to deoxidize the bath.
Deozidation occurs due to the unoxidized Mn left during the first stage.Lime reacts with C to
form CaS which will further deoxidize and fix the S as CaS.The reactions are:
FeO

Mn

Fe

MnO
46

3C
+
3FeO +
3MnO +

CaO =
CaC2 =
CaC2 =

CaC2 +
3Fe
+
3Mn +

CO
CaO
CaO

+
+

2CO
2CO

## Sulphur present in the steel as FeS&MnS.and eliminated in the following way.

3FeS
3MnS
FeS
MnS

+
+
+
+

CaC2
CaC2
C
C

+
+
+
+

2CaO
2 CaO
CaO
CaO

=
=
=
=

3Fe
3Mn
Fe
Mn

+
+
+
+

2CO
2CO
CO
CO

+
+
+
+

3CaS
3CaS
CaS
CaS

CaS is insoluble in steel and will join with slag(White) and CO will maintain reducing
atmosphere in the furnace.Add Fe-Mn/Si-Mn to pick up the Mn containt in the bath(0.35 0.45%).Decarboration/recorporation may done by O2 lancing/by adding graphite powder as per
the spectr sample result.Stir the bath and maintain the temperature as 1640 1650 oC and take the
pre tap sample.After stirring the bath again take the 2nd pretap sample within 2 -3 minutes.Raise
the temperature to 1680 - 1740 and tap the metal bath by opening the tap hole through the spout
in to the pre heated ladle containing calculated quantity of Graphite powder,Ferro-Silicon,FerroManganese/Silico-Manganese as per the spectro sample result.
Transfer the ladle with the molten metal in to the slaggoff station and remove the slag from the
center by slag coated metallic rabble through the lip of the ladle.Take slagoff sample for spectro
analysis and transfer the mladle in to John-mohr pressure pit.Measure the temperature by the TC
tip and when the temperature is 1620 oC add Al star of weight 450 gms each in to the bottom of
the ladle with the help of metallic rod to kill the steel.Take samples for ladle anslysis & H2&N2
measurement by spectro&Leco gas determinater respectively.
Casting:
Start the casting at 1610 - 1520 oC by bottom pressure pouring technique after closing the
pressure pit by the lid containing preheated ceramic pouring tube at its center by using graphite
mould(Assembled Cope&Drag moulds).When the molten metal touch the probe inserted in one
of the riser the pressure will drop and simultaneously the clay graphite stopper head will close the
entrance of the molten metal to prevent the run back. Add sufficient quantity of rice hull to
prevent the dropping of temperature and transfer the mould for solidification.
Splitting:
After calculated time(10-12 Min.)split the mould using the split grain.If dropping of metal is
observed increase the solidification time of reduce the solidification time if the risers are not
fallen during the splitting.Pass the hot wheels through the hot wheel kiln foe further hot
processing.
Sprue Wash:
Wash the protruded sprue by copper cotted electrode of one inch thichickness by using the
current of 1200-1800 Amps and minimum temperature of the sprue wash shall be of 380 oC to
prevent the sprue crack formation.
Number stamping:
Stamp the correct number of the heat on the back hub face by automatic number stamping
maching.
Hub cutting:
Make the hub bore by oxi-acetylene flame by using required pressure.
Heat treatment:
47

The process involving heating&cooling to egt the desired properties suitable for
serviceby changing the structure,composition etc.
Stages of heat treament:
4. Heating to the required temperature
5. Holding(Soaking) at this temperature for a period of time to attain
uniform temperature throughout the section.
6. Cooling the steel at specified rate.

Normalizing

Existing
structure and
properties of

## Existing structure and

properties are wiped
out.Metal is now in a
new structure.

Heat

steel

Quenching

Tempering

## Principle of heat treatment

Hub
cooling

Normalizing:

Air cooling

It is the process of heating the steel to above the upper critical temperature followed by cooling in
air.
Normalizing
Austenite
910

Temperature
O

723

Ferrite +
Pearlite

Pearlite +
Cemintite
0.8

C% wt
Purpose:
5.
6.
7.
8.

## To relieve the internal stress

To refine the grain structure
To improve the machinability
To improve strength&toughness
48

Temperature&time of NF:
Temperature in o C
Required
Set
840 - 860
850
840-870
855
850-880
865

Zones
Pre heating
Main heating
Soaking

## Time in hrs(Cycle time x capacity

of the furnace)
2
2
2

Quenching:
The process of heating the Wheels to austenite phase followed by sudden cooling of rim by
water for about 4 - 4.5 min.
Purpose of hardening followed by tempering :
1. To develop high hardness, wear resistance and
2. To improve the strength and toughness

Austenite
Hardnening
910

Temperature
O

723
640
550

0.8

C% wt

Tempering:
Process of heating the axle to a temperature below lower critical temperature followed by air
cooling.
Purpose:
5.
6.
7.
8.

## To reduce the thermal stress

To stabilize the structure of the axle
To reduce the brittleness and
To increase the toughness&ductibility.

49

Austenite
910

Temperature
O

723
640

Tempering

550

0.8

C% wt

Temperature&time of TF:
Zones
Pre heating
Main heating
Soaking

Temperature in o C
Required
Set
550-640
610
610-640
610
610-640
610

## Time (Cycle time x capacity of the

furnace)
2 hrs 55 min.
2 hrs 55 min.
2 hrs 55 min

Hub cooling:
Cool the hub by the mixture of air&water for about 2.5 minutes.
Air cooling:
After complition of the heat treatment allow the wheels to air cool.
Apex gring;
Remove pins on the apex of the wheel by apex grinding machine about one full rotation.
Steel shot blasting;
Remove oil,crease,dirt,sand grains,spray particles and othe inclusions by steel shot blasting in a
closed chamber.
Magnaglow:
Do visual inspection followed by spraying the magnaglow bath on the magnetized wheel and
inspect und UV lamp.If free from any defects stock the wheel as first line stock otherwise send
the wheel containing defects to the grinding line and reinspect.
Ultrasonic testing:
Evaluate the quality of the rim portion of the wheel by detecting the discontinuities which are
harmful to service by automatic immersion technique in a water tank by radially & axially by
using 5&2 MHz convergent beam probes of six numbers respectively(3 for axile&other 3 for
radial).The wheel containg 3.2 diameter flaw ore shall be the cause for rejection.
50

## Brinel Hardness testing:

Remove the scale on the front rim by automatic grinding machine and measure the BHN by
giving indentation by 10 mm hardened steel ball with the load 30000 kgs.
Warpage:
Check the warpage of the wheel on the drag side to prevent the derailment of the wheel.
Wheel peening:
Peen the wheel in a closed chamber by steel shots of SAE-550 grade or equivalent to improve the
fatigue strength of the wheel,to weldup the HLCs on the surface,distribute the locked up strees
uniformely through the wheel.
Hub bore:
Make the hub bore to the required diameter by Hub borer.
Final inspection:
Measure all dimensions of the wheels,rotundity,circumference and others by using suitable
measuring gauges and record the weight of the stocked wheel also.

## Heat treatment of wheel:

The process involving heating&cooling to egt the desired properties suitable for
serviceby changing the structure,composition etc.
Stages of heat treament:
7. Heating to the required temperature
8. Holding(Soaking) at this temperature for a period of time to attain
uniform temperature throughout the section.
9. Cooling the steel at specified rate.

Normalizing

Existing
structure and
properties of

steel

Heat

## Existing structure and

properties are wiped
out.Metal is now in a
new structure.
Quenching

Tempering

## Principle of heat treatment

Normalizing:

Hub
cooling

Air cooling

51

It is the process of heating the steel to above the upper critical temperature followed by cooling in
air.
Normalizing
Austenite
910

Temperature
O

723

Ferrite +
Pearlite

Pearlite +
Cemintite
0.8

C% wt
Purpose:
9. To relieve the internal stress
10. To refine the grain structure
11. To improve the machinability
12. To improve strength&toughness

Temperature&time of NF:
Temperature in o C
Required
Set
840 - 860
850
840-870
855
850-880
865

Zones
Pre heating
Main heating
Soaking

## Time in hrs(Cycle time x capacity

of the furnace)
2
2
2

Quenching:
The process of heating the Wheels to austenite phase followed by sudden cooling of rim by
water for about 4 - 4.5 min.
Purpose of hardening followed by tempering :
3. To develop high hardness, wear resistance and
4. To improve the strength and toughness

Austenite
Hardnening
910

Temperature
52

723
640
550

0.8

C% wt

Tempering:
Process of heating the axle to a temperature below lower critical temperature followed by air
cooling.
Purpose:
9.
10.
11.
12.

## To reduce the thermal stress

To stabilize the structure of the axle
To reduce the brittleness and
To increase the toughness&ductibility.

Austenite
910

Temperature
O

723
640

Tempering

550

0.8

C% wt

Temperature&time of TF:
Zones
Pre heating
Main heating
Soaking

Temperature in o C
Required
Set
550-640
610
610-640
610
610-640
610

## Time (Cycle time x capacity of the

furnace)
2 hrs 55 min.
2 hrs 55 min.
2 hrs 55 min

53

Hub cooling:
Cool the hub by the mixture of air&water for about 2.5 minutes.
Air cooling:
After complition of the heat treatment allow the wheels to air cool.

## Preparation of coated sand:

54

Poring rate:
Fast pouring rate:
The flow of molten metal from the ladle in to the clay graphite head through ceramic pouring
tube is cast fast pouring rate.
Controlled pouring rate:
The flow of molten metal from the clay graphite stopper head through the wheel profile in to the
probe sensor in the riser is called as controlled flow rate.
The Pouring rate is given by the formula
Time
Pouring rate

## Sec / PSI and can be read from the Anger-Gein chart

Pressure
plotted by time in second in Y axis and pressure in PSI in X axis.The X axis is calibrated as one
division is one PSI and the time in Y axis is 2.5 minutes.It shall be 2.25 1.25 Sec / PSI.
Eg)
The graph for the following values of time&pressure is as follows.
Time in seconds
2.5
5
7.5
10

1.6
3.2
4.8
6

10
Pouring rate

=
6
=

12
10
8
Time in Sec.6
4
2
0
1.6

3.2

4.8

Pressure in PSI

55

## Effect of pouring rate during wheel casting:

High pouring rate:
Porosity,gas holes,pin holes,cavity may form in the rim and below sprue portions
If the temperature is low flow rate may sufficiently increase to prevent the cold defects
Low pouring rate:
Low pouring rate may leads to cold defects like LAP
If the pouring temperature is high then low pouring rate is pemitted
If the bath temperature is low pouring rate may lead to cold defects.

## Use of graphite moulds for wheel casting:

It has sufficient permeability
It has high thermal shock
It is easly machinable
It may re use after casting of one wheel for further casting
It has low thermal expansion
It has low linearity of coefficient
It has low ash content
It is less volatile
The chemical reaction between it and the molten metal bath is negligible
After casting easily cleanable without damage for further use
This is non-destructive mould
Less heat / thermal loss
The spray solution will easily adhere on the surface
It has sufficient strength.
It has high electric resistance
Repairable by machining

Sand testing:
GFN determination:
Take 100 gms of washed,dried and any other foreign material free sand and poured in the top of
the clean pre weighed test sieve series contains 600,425,300,212,150,106,75,53 micron sieves
and pan from top to bottom.Shake well for about 5 minutes by the sieve shaker motor and take
the final weight.Findout the % of the retention in each sieves and find out the GFN of the sand as
follows

Sieve size

600
425
300
212
150
100

Initial
Final
Weight of % of the Factor
weight of weight of the
retention
the sieve
the seieve
retention
20
30
40
50
70
100

Product

56

75
53
Pan

140
200
270
Total
Weight of the product

GFN

AFS.
Retention

## Stick point determination(SP):

Spred thin layer of coated sand using metal feeder on the stick point apparatus.After one minute
brush out the un-sticking sand by camel hair brush to the point where sand has stuck to the bar
from the lower gradient side.Immediately measure the temperature by using the thermocouple at
the point where the sand has stuck.
Determination of CTS:
Make the test samples by pouring the coated sand on the brequtte shape on the bottom of the
heater at 232+/- 5 oC using aluminium scoop.flatten immediately and place the top heater on the
leveled surface.Soak for four minutes and remove the heater.After air cooling find out the CTS
value from the outermost scale(with the help of the movable magnet).Average of six samples will
be the CTS value of the coated sand.
Determination of HTS:
Pour the sample on the slot of brequtte shape of the bottom of the heater,flatten and immediately
place the heater overit.Bake 4 mintes and apply the load and read out the HTS value after
breaking the sample in hot condition.Average of the two samples will be the HTS value of the
coated sand.

57

## Estimation of SiO2(Ram. mass):

Take 0.5 gm of dry sample in a beaker add 50 ml of 1:1 HCL and bake. It completelyExtract with
1;1 Hcl and wash thoroughly.Warm,cool and filter through 41 No. fiter paper.Take the ppt in a Pt
crucible ,chara and heat to 950 oC for about 30 minutes.9Filterate for the determination of
CaO&MgO)
Cool,moisten with conc.H2SO4 and add sufficient quantity of HF and evaporate on a hot
plate.Heat to 950 o c for 15 min,cool and weigh.

Wt before HFT

After HFT

SiO2 =

x 100
Wt of the sample taken

Estimation of CaO:
Makeup the above filterate in to 250 ml in a SM flak.Pipette out 25 ml in a conical flask,add 10
ml NaOH(10 N).Make up the volume in to 50 ml,add 0.2 - 0.4 gm of P&R indicator & titrate Vs
0.02M EDTA soltion(7.44 gms in one litre of water).The end point is the appearance of the violet
blue colour.Note the volume of EDTA.

## Vol. of EDTA consumed x 0.11216

CaO

=
Wt of the aliquot taken

Estimation of MgO:
Pipette out 25 ml in a conical flask,add 30 of water and 25ml of buffer(68 gm of NH4Cl+570 ml
of Conc. NH in 1 litre) solution and few drops of EPT(0.5 gm EPTand 5 gm Hydroxlamine Hcl I
1 litre) indicator.Titrate Vs 0.02M EDTA till the colour changes from wine-red to blue.Note the
volume of EDTA consumed.
Vol. of EDTA consumed - Vol. of EDTA consumed for CaO
MgO =

x 0.08062
Wt of the aliquot taken

Determination of Fe2O3:
Pipette out 50 ml of the filtrate obtained after filtration of Silica.Add 5 gm of NH4Cl,2 drops of
methyl orange(0.5gm in 1 litre) in
and add NH4OH till the colour changes to
yellow.Warm&cool the solution and filtrate through 41 No. filter paper. Wash the ppt with hot
water and dissolve it in 50 ml of 1:1 Hcl and boil the solution.Add staneous chloride(6gm in
40ml Conc.Hcl&60ml dis.water,add few pieces of granulated tin and stored in amber coloured
bottle). till the soloution become colourless.Cool rapidely to room temperature.Add 10 ml of
stauraed mercuric chloride till the formation of silky white ppt.Add 20 ml of acid
mixture(Conc.Phosphoric acid&75ml Conc.Sulphuric acis in 350ml water),2-3 drops of BDAS
indicator(0.2-0.3gm in 100ml dis.water&stored in amber coloured bottle) and titrate Vs 0.01 N
Potassium dichromate solution(0.49gm in 1 litre) till the appearance of violet colour.

## Vol. Of K2Cr2O7 consumed

Fe2O3%

x 7.984
Wt of the aliquot taken
58

## Determination of Al2O3 in HA70% bricks:

Take 0.2-0.3gm sample and fuse with the fusion mixture at 950 deg. C & extract with 1:1
Hcl..Fllter through 41 No. filter paper and make it in to 250 ml in a SM flask.Transfer 25ml of
the aliquot and add sufficient amount of 0.01M EDTA (1 ml = 1.25gm of alumina)Add 2-3
drops of methyl orange and dilute with NH4OH(1:10) drop wise till the colour change to
yellow.Add 5ml acetate sodium acetate buffer(2ml acetic acid&21.5gm sodium acetate in 1 litre
of dis. Water-PH 5.2),25ml water and heat toboilingfor 5 minutes.Cool and add 5-6 ml of xynol
orange indicator(0.1gm in 100ml dis. Water with 2 drops of 1:1 HCl) and titrate against standard
Zinc Acetate solution till the colour changes from yellow to orange or pink.Add 10ml of
ammonium fluoride solution and heat to boiling for 5 minutes.Cool and add 5ml buffer and 5-6
drops of zylenol orange indicator and titrate against standard Zinc Acetate solution till the colour
changes from yellow to pink.

## Vol. of ZnAc consumed x 1.25

Al2O3

x 100
Wt of aliquot

Alumina in Fe-Si:
Take 2.5gm in a Pt crucible and dissolve in 1:2 HF + HNO3 acid mixture till the samples
dsolved.Add 5ml of 50% Conc.HCl & fume till dense fumes evolved.Extract with 50ml of water
and again boil till faint smell of NH3 persists.Filter through 41 No. filter paper,wash with hot
water and transfer the ppt in to 250ml beaker.Add 15ml conc.HNO3 +15ml conc.perchloric
acid.Fume to syrupy state with beaker covered with watch glass.Cool,add a drop of hcl,dilute to
20ml,boil and add50_60ml of 10% NaOH solution,boil on low heat,cool,filter through 41 filter
paper.Wash with hot water,collect the filtrate in to beaker,Add xynol orange indicator.Add hcl till
it turns from blue to yellow.Cool,make upto 250ml.Take an aloquot of 100ml,add 20ml of
0.01MEDTA,neutralize with 5% NaOH.Then add 5-10ml of acetate buffer.Boilfor
10minutes,cool,add xynol orange buffer and titrate against 0.01 M Zinc sulphate.
Carryout the blank with the same amount of EDTA and other reagents used above.

## (Vol. of Zn Ac consumed for blank-Vol. of Zn Ac consumed for sample)

Al%

x 0.027
Wt of sample in the aliquot

## Estimation of Silicon in Fe-Mn:

Take 1gm sample and dissolve in 30% conc.Nitric acid in a hot plate.Dry&bake for 1 hr at 100110 deg.C.Redissolve the baked mass in 40ml conc.Hcl by warming and dilute to 150ml with hot
water.Allow to settle and filter through 40 filter paper,wash 10-12 times alternatively with hot
1:20 Hcl and hot water.Ignite the ppt at 950 deg. C for about 30 minutes,cool and weigh.

59

Wt of silica obtained
Si

x 46.72
Wt of sample taken in gm.

Estimation of Mn:Take the filtrate obtained after removal of silica in a 500 ml conical flask and
treat with 10ml conc.Sulphuric acid and evaporate to fumes.Cool&dilute in to 100m.Boil until all
salts get dissolved.Make up in to 500ml.Pipetted out 25ml,add small amount of Zinc Oxide
emulsion till the liquid suddenly coagulates.Dilute to 200ml,boil and add 2-3 drops of conc.nitric
acid and titrate vs 0.1 N KmnO4 solution in hot condition itself.Agitate the contents in a conical
flask after each addition of 0.1 N KmnO4 and allow the ppt to settle and continue to titrate till the
supernatent liquid shows pink tinge.Take two such piolet readings so that in the 3rd titration all
permanganate required can be added rapidly and the end point is noted.

## Vol.Std KmnO4 consumed x Nor. Of KmnO4

Mn%

x 1.666
Wt in gm of the sample in the aliquot.

Estimation of Mn in Al star:
Dissolve 1gm sample in 3ml of acid mixture(Con.Sil.acid90ml +Conc.Nitric acid 50ml + Conc.
Phopouric acid 95ml + Dis. Water 765ml).Dissolve an accurately weighed sample of std steel
containing a known conc. Of Mn in 30ml of acid miture.Boil,cool and dilute to 100ml with
boiling water.Add 10ml of silver nitate solution and 30ml of 10% ammo.per-sulphate
solution.Heat till permanganic acid colour is obtained.Cool the solution to room temperature add
10ml of NaCl solution to pptAgCl.Titrate quickly the permanganic acid with std. Sod.Arsenite
solution until the pink colour disappears.

## Vol. of std. Sodium Arsenite solution consumed

Mn%

x (A x B) / C
Wt. Of the sample taken

Where,
A
B
C

=
=
=

## % of Mn in std steel sample

Wt of saple taken and
Vol. of std arsenite solution used for titration.

Settling test:
Fused silica poeder in water with the suspensions CMC&Veegum
Weigh 315gm of fused silic powder,0.315gm of CMC(0.1% of FSP)&1.575gm of
veegum(1% of FSP) in 2 pockects each containing 1.575gm
Dissolve CMC in 53ml distilled water& stir with mechanical stirrer for about 4 minutes
Repeat the same for both the pockets of veegum in a seprate beakers.
60

Take 432ml of distilled water in 1 litre measuring jar and add CMC& stir 4 minutes.
Repeat the same for the two pockets of vegum.
Add 315gm of FSP and stir for 4 minutes.
Keep it for 24 hrs and oserve any sttling take plac e or not.

## Specific gravity of FSP:

Take the empty wt of clean,dry pyknometerw1
Fill with water and weigh-w2
Pour out the water and filled with 1/ of FSP&weigh-w2
Fill with water and weigh-w4

(w3-w1)
Specific gravity =
(w3-w1)-(w4-w2)

61

Cope side:-

Flange
Front rim

Sprue

## Front hub face

Hub bore
Front hub fillet
Front plate
Front rim fillet

Drag side:Flange
Back rim
Back of flange or
Flange fillet of
Back rim fillet

## Back hub face

Hub bore
Back hub fillet
Back plate
Back rim

62

Fracture toughness:
Eventhough the charpy&Impact tests have certain importants they are not considering
for engineering design.LEFM is used for the design problems.Fracture toughness is
one of the material properties like yield strees and used in designs.It is defnied as the
resistance of the material to resists fracture starting from the preexisting crack /
defect.
Testing of fracture toughness:
Sample preparation:There are so many sample preparation method and one of the method for the
preparation of the sample as per ASTM,Philadelphiya STP 381133/1965 is as
follows.

## Pin hole for apply load

Crack
L(4w)

Slot
2C or W / 3

Crack

The length of the specimen is 4 times of the width and the length of slot&crack is 1/3
of the width.Load is applying through the pins in which the sample is inserted.
Procedure:Do the preliminary adjustments for the Fracture Toughnes machine and insert the
specimen in to the pins.Apply the load and the material will fracture under plain
strain condition.Note the maximum load(pm ) for the calculation.

Pm
Fracture Toughness (Kic)

=
wxt

tan
(1- 2 )

Mpa a
w

Where,
Pm

63

w
t

=
=
=
=
=

width
thickness
poison ratio
3.14 and
half of the crack length.

The material having higher Kic value will undergo brittle fracture at lesser load and
the material having higher Kic value will undergo ductile fracture.

Time

Temp. Deg. C
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20

100
200
300
300
300
300
400
500
600
700
800
900
1000
1100
1200
1200
1200
1200
1200
1200

64

Time

Temp. Deg. C
1

100

200

300

400

500

600

600

600

600

10

600

11

700

12

800

13

800

14

800

15

800

16

800

17

850

18

900

19

950

20

1000

21

1000

22

1000

23

1000

24

1000

25

1025

26

1050

27

1075

28

1100

29

1125

30

1150

31

1175

32

1200

65

## Ladle lining well type with mullite castable.

115

32

50
230
7
Top of molten metal

6
HA 70 230x115x76/70 &
HA 70 230x115x76/65
5
1698
(1650)
4

1588
(1540)

1870
3

Steel shell
1

460

HA 70 Mortar
40

25

Mullite castable

110

282

66

67

## Defect analysis of axle.

Billet cutting:
Working pressure:
DA
O2

0.8 - 1 bar
10 bars

Nozzle life

1200 billets

## Nozzle getting blocked due to back-firing,over used,poor quality etc

Conveyors should not move during cutting
Cleen the nozzle at the beginning of each and immediately in case of
back firingReplace the slag bins and never allow bins to overflow
Ensure proper seating of nozzle to torch
Cutting of correct billet length
Select proper billet to be cut as per the specification of R-16&43.

Forging:
LAP:
Improper corner breaking
Indexing problem during forging
Improper conditioning of the bloom surface

Ensure:
Correct corner breaking during forging
Correct 90o during corner breaking and during handover
Defect free surface on bloom and in case surface conditioning is done on
bloom the width of conditioning should be 10 times the depth(8 mm ) of
the conditioning.

Piping:
Insufficient material on forged ends leading to formation of hole in the
journal end face
Uneven distribution of material on both ends of ournal during forging.
Poor gripping marking on jaws / work piece jerking during during
marking
Improper setting / adjustment before cutting in axle cutting machine
Lack of material due to excess scale formation
Ensure
Correct length of billet loaded to RHw
GFM programme for forging is made considering equal distribution of
material for both ends
GFM chuck jaws are welded properly with grip marks to avoid jerking
during forging.
Maintain correct indicator point to point distance as indicated in work
instruction.Maintain 100 to 150 mm of minimum fish end length

## Ensure no ove saking of billects in RHF.In case of prolonged break

downs put off PHZ and reduced temperature to 1000 deg. C in SZ-I&II

## Misfunction during forging:

Catastriphic failure of electrical or mechanical components/failure of
regular power supply leading to in complete forging
Ensure
Ensure machine condition with maint. Staff after PMS or after attending
to breakings.
Idle cycle(without work piece) is checked in auto sequence and check
whether all the blocks in t forging programme is correctly
executed.Ensure that the programme is correct and then recall the work
piece.
The case of failure is to be analyzed and is best when analyzed separately
depending on the case.
In case of power interruption or failure consult MRS for regular supply
of power before starting of forging.Allow 5 minutes for supply to
stabilize.

69

## AXLE FLOW CHART

Blooms from
ASP,Musco&Others.
Billet cutting
Billet heating in RHF of capacity
80 axles
Forging by LFM
End cutting
Number stamping

## Cooling through ICB of

capacity 30 axles.
Normalizing in NF of capacity 80
axles
Polimer quenching in quenching
tank of capacity 80,000 litres.

## Cooling through ICB of capacity

42 axles.
Tempering
Stock
Sampling for Physical
Chemical,Micro,Macro
and Charpy tests at

70

M.Lab.

## End milling,cup turning and

centering at Stn - 1

UT

## Rough turning at Stns 2

Semi finish of J,D/g&W/s at
Stns - 3
Body finish at Stns - 4
Drilling&Tapping at Stns - 5
Finisf of Stns - 3
W/s furnishing at Stns 7.
J&D/g grinding(Centerless
Grinding) at Stns - 8
MPT at Stns - 9
W/s of axle
Measuring (Automatic)
Wheel hub boring(Wheels from
Wheel shop stock yard)
Wheel set assembly
71

Inspection
Painding&Packing

Despatch

72

Body
W/s fillet
Wheel seat
Journal
CTA

LCB
Body

Body
W/s

Journal
CTA
Face
LCB

OW/s Flt-N.end
IW/s Flt-N.end
IW/s Flt-F.end
OW/s Flt.F.end
Journal Farend
CTA-Far end

74

75

## Manfacturing of BG Loco axles.

Billet cutting:
Cut the fillet of 300/340 RCS of R-43/1992 bloom in to required length by Saw/Gas
cutting.
Charging in to RHF:
Charge the cut billets in to RHF and soak them at 150 1200 deg. C for about 8 hours.
Forging:
Forge the red hot billet at 900 1100 deg. C by 6 minutes by GFM long forging
machine.
End cutting:
Remove sufficient discards by gas cut.
Number stamping:
Stamp the serial number of the axle on wheal seat by hot number stamping maching.
Intermediate cooling:
Cool the axle through the intermediate cooling bed till the surface temperature becomes
200 250 deg. C.
Heat treatment:
Normalizing:
Charge the axles into NF and soak at 860 880 deg. C for about 8 hours.
Hardening;
Quench the normalized hot axles by the polymer quenchant for half an hour.
Tempering:
Charge the quenched axles in to the TF through the intermediate cooling bed and soak
at 610 660 for about 11.45 hours.
Air cooling;
Allow the tempered axles in to air cooling for about 36 hours.
Laboratory testing:
Take the lab. sample Each cast wise from the mid radius of wheel seat/journal and
conduct all the required testing .
Machining in AMS:
End milling, centering and LCB:
I f the lab test is ok load the axles in to station-1 in AMS and do the above operations at
station-1 with the surface finishing of 0.8 micron.
Ultrasonic testing:
Do visual examination and carryout the ultrasonic testing and if the axles are passed
stamp the UT punch mark.
Rough turning of axle:
Do the rough of the axle in station-2 as per the dimensions mentioned in the drawing.