You are on page 1of 41

इंटरनेट

मानक

Disclosure to Promote the Right To Information
Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
“जान1 का अ+धकार, जी1 का अ+धकार”

“प0रा1 को छोड न' 5 तरफ”

“The Right to Information, The Right to Live”

“Step Out From the Old to the New”

Mazdoor Kisan Shakti Sangathan

Jawaharlal Nehru

IS 8229 (1986): Specification for Oil-well Cement [CED 2:
Cement and Concrete]

“!ान $ एक न' भारत का +नम-ण”
Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह”
है”

Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

IS : 8229 - 1986
( Reaffirmed 2008)

Indian Standard
SPECIFICATION FOR OIL-WELL CEMENT

(First Revision)
First Reprint JANUARY 2001

UDC 606 946 7 622 24

© Copyright 1987

BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG

NEW DELHI 110002

Gr 7

July 1987

VIBVB:8VARAYA National Council for Cement and BUilding Materials.s D. K. New Delhi Alternate) Central Water Comrrusaron.I["ngatlon Department. Lucknow DR H. Hyderabad JOIN~ DIRECTOR ( A/lerna/I) Central Soil and DIRECTOB Materra ls Research Staaron.RASOR ( AiJerllale ) DE~IONS ) Canreal Pubhc Work. GUANEKAU Structural Engmcermg Research Centre (CSIR). Calcutta K. Bombay MALANI ( AlleFul.1986 Indian Standard SPECIFICATION FOR OIL-WELL CEMENT ( First Revision) Cement and Concrete Sectional Committee. New Delhi DZPUTY Dm ec-ron \ C &. Larsen and Toubro Limited. ( SaRI J. BANERJEE SHRI S. MIGLANJ ( Alternate) ( Conhflued on. New Delhi EXECUTIVE ENGINEH:R (D)-III (Allemate) CHIltll' ENGlNEER ~ RESEARCH).NDARDS protected under the Indum CetpyrJght Atl (XIV of 1917) and reproduction in who j e or in part by an. partment. V. BDC 2 Representang Chmrmtln C. C BD ) Bhakra Be-as Management Doar d. Designs and Standards Orgamaanon ( MintUry of Raifways ). ) SBBI K P. . Roorkee Development Com rms-uone r for Cement Industrv SHIll A.U OF INDIAN STA. (B & S ) DEPUTY DIRECTOR ST AJ'rlD ARDS ( 8&S ) ( AI".' means except w n h wr-rt t e n per nussron of 1111 publisher shaH be deemed to be an Infringement of cupyrlght under the saad Act.. New Del ht ADDITIONAL DIRECTOR STA"NDABD8 Research.-DIRECTOR RESEARCH OFFICER ( CIINCRETE TECHNOLOGY) (Alt~rI1aJe) CHIEF ENGINEER ( A. DIRECTOR P Eogmeenng Leboratcrres. MDD-I ) (AlZotrnate) SHRI V.a'. ) SURf HARISH N National Test House. BANERJEE elllEI' ENGINEER.18 I 8229 . page 2 ) © This pubhcation 13 COPYright 1987 BUREA. Nangal Townshrp . GOKAK CHIEF RESEARCH OFFI( En ( DIRECTOR ( C&MDD·I) ( MiDl3try of Industry 1 8BRr S S. Government of Punjab CU.

Bombay SHU S. N. Army Headquarters 51£( HhT.AKARAN GliPTA SHILl A. Bombay Roads Wing ( Mimstry of Transport). Roy ( Alle'male) SllRI T. New Deihl MOHAN RAJ Roorkee Da S. New Delhi Alte'fllJt. REDDI ( Alternate) DR M. Hvderabad The Assoc rared Cement Companies Ltd.INTENDING of Orissa Cement Limited. SAXENA.1986 ( Cont. LADA The Institution of Engineers ( India L Calcutta SHIH B T. R Boa rd New Delhi EN o J NEE R ( Dssmxs ) EXECU1!VE and Power.) H S.IS I 8229 . S. SUliBA RAO Gammon India Limited.) Cement Corporation of India. New Delhi DB A V Drrec tor ate General of Supplies and Dasposals .TT\{)-[AIt"\'YA SJlHJ L IrrigatIon Alternattt) SAXENA { SUPFH. New Delhi Indian Roads Congress.) Hindusean Prefab Limited. V CHALAPATHI RAO Geological Survey of India. RAMAIAB Structural Engmeer-ing Research Centre (CSIR). R KOTNIS ( Alternate ) SHRI Engfneer-In-Cbfefvs Branch. SURI R. R. GOPINA'l'H J.. MADRAVA RAO RIJH~lNGHANI U SHIll C S SHARMA ( (Allornal. PAL SHRI BIMAN DABGUPTA ( PASRICHA. Central Budding Research Lnafrtute (CSIR). SUUl Y R PHULL nab. Dastur and Company Private Limited.J AGUS DR A. SURI H. New Delhi (Alienwte) 2 . G.\MANA DB K C NARANO ( Aiternate ) Slll!I G R \MllM'l ~1I1{1 Dalmia Cemr nt ( Bharat ) Limited.\Jty De ntra J SHRI K. Calcutta SaRI S.seniffJ/: The India Cements Lrmife d. Madras ::-'HN GUPTA Dn A. Government of Tamil Nadu ENOINEEk (SMD DI\ I:SION ) ( Alternate ) ~WAR{)OP ~I1UI H HIl".mud fr om pag. Madl'811 (Alterrrate) Hvderabad Industries Limited. K. K MULLIflK National Council for Cement aod Butldmg Mate- SnRI S. I Mem6ns SHRI S SHRI T TAMU. A. K SnRI P Repr. Calcutta Alterntlt. L. (Alternate) SBRI S K. CUATTERJEE SURI N. G SlIlU A. Bombay (Alternate) Indian Hume Pipes Co Limited. N. N('w Delhi M. New Defhr R Sunt } RAO (Alternale) SHIll R. New DeJhJ J08Hl KAPOOI~ SHIll R K.O"d Central Road Research Institute (CSIR " New Delhi Central Road M. N. New Delhl. Pubhc Works Department. S RElIbI ( Alternate ) A V R. UNWALLA ( Altlf'f1tJle) Dn A. Departmeet of Surface Transport. New DelhI National BUIldmgs OrgaDlsallon. CHATTERJEE (Allema Ie ) SHRI n« Research In statute (CSIR). SATYANARAYANA SHIn V.

!-'mHeJ at :'IOeu 111\11<1 Pllllllll~ l-'rL:l~ !o'I. 1 JUNE 1989 TO IS : 8229 . However.A.1986 SPECIFICATION FOR OIL-WELL CEMENT ( FIrst Revision ) ( Page 12.uncr contarrun g 1 000 kg or more net mass of cement 'ihdlJ be considered a s bulk supply of cement Suppi re s of cement may also be made In intermediate c ontame rs.3. clause 9. the average net mass of cement In a sample shall be equal to or more than 15 kg • ( Page 12.J .• The number of bags In a sample taken for weighment showing a mInUS error greater than 2 percent of the specified net mass shall be not more than 5 percent of the bags In the sample. Also the rnmus error In none of such bags In the sample shall exceed 4 percent of tbe specified net mass of cement m the bag. clause 9.2 and renumber the exisnng clause 9.4: '9.2 ) .AMENDMENT NO.4 ) - Insert the followmg NOTE below the clause' 'NOTE -..l lnJI. single bag or cont.• and packed In suitable bags as agreed to between the purchaser and the manu fact urer. (or ex mapl e . drums of 200 kg.3 The average net mass of cement per bag may also be 25 kg subject to tolerances as grven In 9. by agreement bef ween the purchaser and the manufacturer' r eoc 2.] as 9. 9.3 .hUllo.Insert the following after 9.

3. packing of cement may be done In bags other than those given in 9.AMENDMENT NO.4. 9.4.3.3.1 JUNE 1991 TO IS 8229: 1986 SPECIFICATION FOR OIL-WELL CEMENT ( Flr.3 with an average net mass of cement per bag as agreed to between the purchaser and the manufacturer.Insert the following new clauses after 9.1 and 9.t Revtston ) ( Page 12.4.S· "9.4.4 When cement is intended for export and if the purchaser so requires.1 except the average net mass which shall be equal 10 or more than the quantuy In 9. clause 9.1 (see als» Amendment No.4 The tolerance requirements for the mas> of cement packed in bags shall be as given m 9..4 .3 The pack ing material shall be as agreed to between the supplier and the purchaser 9.1 For this purpose.1 The words 'FOR EXPORT' and the average net mass of cement per bag shall be clearly marked in mdehble ink on each bag 9.4 as 9. r)] . the permissron of the certifying authority shall he obtained m advance for each export order 9. (CED 2 ) .1 and renumber the existing clause 9.

Jntha .hlll].WELL CEMENT ( First Revision .)l New IndIa Pnu/mg Pres-s Jl. (C£D2) Pruned . (Page 28. clause n-l~) - Substitute 'up to 25 tonnes' for '0[20 to 25 tonnes" .AMENDMENT NO.3 NOVEMBER 1991 TO IS 8229: 1986 SPECIFICATION FOR OIL.<t.

4 NOVEMBER 1993 TO IS 8229: 1986 SPECIFICATION FOR OIL-WELL CEMENT ( First Revision) [ Page 12.4 The tolerance requirements for tbe mass of cement packed in bags/drum shall be as given in 9. packmg of cement may be done in bags or In drums WIth an average net mass of cement per bag or drum as agreed to between the purchaser and the manufacturer. 9. '.AMENDMENT NO.4 When cement is intended for export and If the purchaser so requrres.4: .1 and 2 »).4.1 For this purpose the permrssron of the certifying authonty sball be obtained in advance for each export order. clause 9.4 (see also Amendments No.4. '.3.2 The words 'FOR EXPORT' and the average nel mass of cement per bag/drum sball be clearly marked m mdelible ink on each bag/drum.Substitute the following for the existing matter: '9.3 The paclung material shall be as agreed to between tbe manufacturer and the purchaser.4. '.4.1 except tbe average net mass whicb sball be equal to or more tban the quanuty (CEO 2) 1ft 9.

'average net mass' wherever II appears in tbe (CED2) Prmred .: Press Kluma lndm .rr New InJId PrllltlllJ.AMENDMENT NO. 5 APRIL 2000 TO IS 8229: 1986 SPECIFICATION FOR OIL-WELL CEMENT ( First Revision} Substitute 'net mass' [or standard.

6 JUNE 2006 TO IS 8229: 1986 SPECIFICAnON FOR OIL-WELL CEMENT ( First Revision) ( First cover page) Indian Standard Insert the following above the English 1I11e of the ~rrRCfi itR *~31T ~ ~~ P'l~I~ (WfffT~) (CED 2) Reprography Urut. SIS.AMENDMENT NO. New Deihl. India .

'Thrs standard cove-rs the requirements of oil-well cement required for the Indian Oil Industry which IS expanding at a rapid pace.4 Mass of cement packed in bags and the tolerance requirements for the mass of cement packed In bags ~hall be HI accorda'nce With the r eh-va nt provisions of the Standards of Welghls and Measures ( Packaged Commodities ) Rules.un either gas or water that is flowmq into oil-bear inq formations At present a small quantitv of oil-wr-Il cement is being produced 10 the country . after the draft finalized by the Cement and Concrete Sectional Committee had been approved by the Civil Engineering Division Council.2 ('e! Appendix B for mformauon j Anv modification in these rules.1 ThIS Indian Standard (First Revision) was adopted by the Indian Standards Institution on 12 November I ~86. in response to a proposal received from the Department of Industrial Development. 3 . 0. and is intended to provide guidance to the cement producers for the manufacture of this cement. IS used by the petroleum industry for cementing gas ~ and oil-wells at high temperatures and pressures.2 Oil-well cement a sufficient length of time and then harden fairly rapidly The two principal uses of oil-well cement are to cement the steel casing to the walls of the well and to seal the porous formations which cont. FOR E W 0 R D 0. In tl ris revision four new classes of oil-well cement A.md appreciable quantitic s arc imported.3 This standard was published as an emergency standard in 1976 to meet the immediate needs of the country. 0. 1977 and 8-1. B. C and D have also been incorporated and special class cement has been deleted. The Cement and Concrete Sectional Committ ee subsequently decided to regularize thrs standard and this revision was taken up WIth this purpose and also to incorporate a few modifications found necessary In the hght of experience ~ained in ilS use. Slurries of such cement have to remain pumpable at these elevated temperatures and presosures for 0. Government 01 India.IS : 8229 • 1986 Indian Standard SPECIFICATION FOR OIL·WELL CEMENT ( First Revision I O. In respect of tol ernrice on mass 01 c e-rne nt "\\ ou hl apply automatrca llv to this vtandard .

1. d) Class D .IS : 8229 • 1986 0. c) Class C . when conditions require moderate to high sulphate resistant type of the cement under extremely high temperatures and pressures. due werghtage has been given to the VIeWS of manufactures.1 This standard covers nine classes of oil-well cement used for the purpose of securing oil-well pipe casing with the surrounding earth and rocks. when condition> require ordinary tc hig~ sulphate resistant type of the cement and high early strength.5 In the preparation of this standard. June 1984.intended for use from surface to I 830 m depth. g) Class G . when conditions require moderate to high sulphate resistant tj p" of the cement and can be used with accelerators and ---- • Rules for roundmg off numerical values ( . when special properties are not required. The number of significant places retained in the rounded off value should be the same as that of the specified value III this standard.intended for use from 3050 to 4 270 m depth. 2•.intended for use from 3 050 to 4 880 m depth.1 The cement shall be classified as follows: a) Class A . b) Class B . second edition. e) Class E . the final value.intended for use from surface to I 830 m depth. when coriditrons require moderate to high SUlphate resistant type of the cement.6 For the purpose of deciding whether a particular requirement of this standard is complied with. expressing the result of a test. SCOPE 1. so all be rounded off in accordance with IS : 2-1960·. f) Class F . published by the American Petroleum Institute 0.intended for use from I 830 to 3 050 m depth. when conditions require moderate to high SUlphate resistant type of the cement under high temperatures and pressures.ttJlStd ) 4 .tended for use from surface to I 830 m depth. users and technologists.intended for use as a basic ce-ment from surface to 2 440 m. when conditions require moderate to high sulphate resistant type of the cement under moderately high temperatures and pressures. observed or calculated. CLASSES 2.ir. and considerable assistance has been derived from API Spec 10 Specification for rnaterrals and testing for well cements.

III orl-well . retarders to cover a wide range of well depth. shall comply with the chemical requirements given in Table I. barite and fly ash may be used as admixtures cement. j) ClaJJ J . C and H. shall be interground or blended with clinker during manufacture. E. shall be manufactured by gr indmg chnker consisting essentially of hydraulic calcium silicates. when conditions require moderate sulphate resistant type and can be used WIth accelerators and retarders to cover a wide range of well depths and temperatures. B. D.kcr or blended With the ground chnker during manufacture of the cement However.1 The oil-well cement shall conform to the physical requirements given III Table 2.. 3. MANUFACTURE 3.1 Bentonite. No additions other than calcium sulphate or water or both. 4032-19115".1 Oil-well cement of classes A. when tested in accordance with IhL methods gIven 1D IS . D.on ). 6. C and H. C.ts 18229· I . 5. No additions other than calcium sulphate or water or both. E. hardened cement and causes no 4. F. B. CHEMICAL REQUIREMENTS 4. C.intended for use as manufactured from 3 660 to 4 IlIlO m depth. shall be interground or blended with the clinker during manufacture. Class J cement shall be manufactured 10 conform to the physical requirements given in Table 2. ADMIXTURES 6. No additions other than calcium sulphate or water or both. suitable set-modifying agents ( se« Note) may be interground or blended during manufacture of classes D. F. No material other than one or more forms of calcnim sulphate shall be mterground WIth the clu. PHYSICAL REQUIREMENTS 5.intended for use as a basic cement from surface to 2 440 m. NOTE - A surtableset-modrfving agent shall be defined as the one which haa no deleterrous effect on the durability of the retrogression ID strength. E and F cement.1 Oil-well cement of classes A. h) CIMs H . when conditions require moderate to high sulphate reststant type under extremely high temperatures and pressures and can be used with accelerators and retarders to cover a wide range of well depths and temperatures. • Method of chemical analysrs of hydraulic cement (ji. shall be interground or blended with the clinker during manufacture.sl nVlJ. and temperatures.

percent. Mal' Insoluble residue) percent. percent. percent. percent.n Total alkali content.AIIIO a ).).. TABLE I CHEMICAL RE2lJIREMENTli FOR OIL-WELL CEMENT ( Clausd 1 ) g • i . percent. Ma' Sulphur trioxide (SO. Class DE MDderal. Max (2) CHARACTERISTIC I) (I) SL No. Max Tncalcrum a I u m r n ate 1111 ( SCaO. percenta) Max (4) (5) - 300 0'75 15'00 450 - - 6'00 - Ordinary Typ' (6) 8'00 3'00 0'75 3'00 0'75 S'OO 3'00 3'50 3'00 8'00 3'00 0'75 6'00 600 6'00 Class F CI. G Class H 8'00 800 58'00 4800 800 075 0'75 48'00 8'00 sa-oo 800 075 3'00 0'75 3'00 0'75 3'00 0'75 3'00 3'00 3'00 3'00 6'00 \10) 6'00 (9) 6'00 (8) 6'00 (7) CIa. ABC Magnesium oxide (MgO).0'1 xiI) XI) XI I vul) ix ViII vr) v) M. Max Trrcalcium a I u m I Bat e (3CaO AI. expressed as !I0d1Um oxide (Na2. Type 300 0'75 Loss on Ignition.O) equrvalent.. Sulpha I' Resistan. percent.. percent. Max b) Magnesrum oxide ( MgO ) t percent. Mil:< II) (3) 600 IV) REQUIREMENT r---------------~---------------~ Class Class CIa.). percent. Max Tr icalcrum sil rcate (SCaD. Max Insoluble residue.SiD\!.. Max Loss on rgurtron. percent. ..Oa). Max 3'50 SUlphur t r roxrde (SO~).

. percent.Al zO a ) .aJe - 24'00 3'00 - 3'00 0'75 300 600 - 2400 3'00 - 3'00 0'75 3'00 6'00 0'75 24'00 300 6500 48'00 3'00 075 300 6'00 075 24 00 300 6500 48'00 300 0'75 3'00 6 00 C..'00 X percentage of SIO.A C. Max Magnesium oxide ( MgO ) > percent.. NOTE 2 ~ When the ratio of the percentag-e 01 . the ea >\ content IS zero.( 2 85 x percentas. IS (J 64. Max Sulphur trroxrde ( 50 a).When the trrcalcrum alu mmate content ( expressed as CaA ) of the class A cement 15 8 percent or less. When the AlIDa to Fe. expressed as sodium oxide ( NaaO ) equivalent..Oa ratio IS greater than 0 tJ+. percent. percent: a) Max b) M .SiO.( 1·-13 X percentage of Fe:i':Oa ) . percent.0 3 ) (265 x percentage of AI~U3 I 3'04 X percentage of I e~()1 ( 4'07 X percentage 01 l a~ ) - ( Continued) ~OTE I . Max trrcalctum alummate (3CaO.Al a0 3 ) . Teerecalclum a l u m r n o f e e r r t e (4CaO AI 20. xx) XIX) XV 111) XVII) xvi) xv) XlV) xliii . t' (J I :..! ) . l'Il . 3'00 0'75 - - - 24 00 - 24'00 300 300 - - - 075 3'~) - 3'50 3'00 - - 24'00 3'00 - 3'00 0'75 300 Resistant Type 600 6'00 60U - Hl~h SIl.. tile compounds shall be calculated as follows.axrmum SOa content shall be 3 percent.(6'72 X percentage of o\l~03) .or less. Fe. percent...Jp~. Max percent. I CQ co .AF CaS = ~ = - '\ ['69 X percentage of Fe20a ) I . ).. Max Loss on lgnitron.\I~03 to the percentage of Fe~O. l\1ax Tricalcrum silicate ( 3CaO.. percent... Max Insoluble residue. Total alkali content. the n.Oa) plus twice the Trrca lcium aluminate (3CaO.

O.) + (1'70 X percentage of Fe. ) . ) CaS = ( 4 07 x perceotage of CaO ) .( 4 '48 X percentage of Al. Io'llows: TABLE I + elF) ] i - ~ - . ) The total alkali content (expressed as :'lata equivalent) shall be calculated as follows: NOTE 3 - (2'10 X perceotage of A1. (C.AF When the ratio of AI.0.O. ) .O.eo CHEMICAL REQUIREMENTS FOR OIL-WELL CEMENT .Conld Na20 equivalent = (0-658 X percentage of KID) + ( percentage of Na.O.P.O ) so.F) = . ) .O.( 2'85 X percentage of + C..( 2'86 X percentage of Fe. an Ifon-a1umina-calclum sohd solution [ expressed as S5 C4AF IS formed and (he compounds shall be calculated a.(Li'50 x percentage of S. n leu than 0'64. to Fe.I .

liT Class Class Clas.• " I II .. Max (4) (3) (2) (J) - - - 21 - - 0'8 225 56 (5) C - 3'5 - - - - 3'5 - - - - - 0'8 - 0'8 38 (7) 38 (6) 3'5 - - - - - 2'1 - 1'4 0'8 - 38 ( 10) - - - - - 10-3 10'3 2 I - 1'4 0'8 - 0'8 44 (9) 38 (8) - - = - - - - A-3 A-2 ( Conlm".. METHOD 01' TEST ~ - JII (ll ) Cia" CI.water content of slurry. 3. percent.f! ..d ) - - 5.--...a. _---.iN/rnm l - - - 1'7 - - 14 - - 225 225 Fineness (specific surface) by Blaine) rot/kg. .1 ) TABLE 2 PHYSICAL REQUIREMENTS FOR OIL-WELL CEMENT I'" 10 .2 - 4 ( 12) lS. ~ B CHAa..) Schedule 9 S 31 Schedule 6 5 4) Schedule 8 5 pressure I) 38'C at atmospheric pressure 21 bO'C at atmospherrc at With B-h'Jur cunng (He Note 2) Mill.. ( Cltzu".. Min Soundness (autoclave expansron).. Clasa Clasa E D F G H J _________ _ _A -_ _ _ _ _ _ _ _ _ _ _ ~ REQUIBEKE:J. RUTOCL No. Clasa CI...--..cTBBJSTIC A SL No. Compressive strength.....'" 0'8 0'8 Free .) III) •. Max il) - 46 46 of Water.4()311968· (13) - Note 1 dix A Appea- IN . percent by mass cement i ) percent by volume.1 dnd 5.vl .

..:.. 1968" (13) It '"IS: 4()31-. Note 2) I) Scbedule 8 S CHAR. CI. - - - - - - - - - - - 90 90 90 - - 90 - - - - - 100 - - 154 100 - 190 100 - - - 90 6'9 - 6'9 - (8) - 138 6'9 - (7) - 6'9 13'8 (6) 13'8 ~ - - - - - - (10) AppendlxA '\-4 (121 <0 N CD N II> - .. H F E G D J (5) - - 90 90 - - - 10'3 - 12'4 (4) (3) CI . CIa..o) (120 Ma.. r----~- 180 180 6'9 3'~' ( 11) 90 90 (120M.) - - (9) Cl.----------------""'-- TABLE 2 PHYSICAL REQUIREMENTS FOR OIL. atmospheric (2) b) Witb 12·bour curing (". METHOD 01' TEST... minutes. Class Clan A B C REQVJRBN'UT . 5and7) .CTEBISTIQ d I Schedule 6 S e) Schedule 8 S f) Schedule 9 S a I Schedule t S h) Schedule 4 S c) Schedule 5 S em Note 6) 6) Schedule lOS vi) Tbickemug time (maximum consietencv during 15 to 30 minutes strrrrng penod: 30 Be.. Min ( see Notes 2 4.. (1) SL No. Clas.WELL CEMENT -C••td .. c) 2) 3) 4) 5) Schedule 4 S Schedule 6 S Scbedule 8 S Schedule 9 S pt'~S5ure With 24·hour curiag (JII Note 2) I) 38"C a. ::• RZTTO CLNo.l. Clau Cia....

NOTE 7 . the NOTE 3 . NOTE 1 - ~ -I ~ rn .og 15 t o 30 mrnures stirrJng period may be Irmrred to 20 Be lor Class G cement by mutual agreement between the purchaser and the manufacturer. Petroleum Instrture. Non 2 .The thickening time requirements are cased on 75 percent values or the total cementing times observed in survey plus a ail-eety factor of 25 percent. The maximum thickening ume requrreme nt for Schedule 5 S NOTB 5 - NOTE 6 - ca~nDg IS 120 minutes.Test schedule. . NOTE4 . These schedules correspond to those given In API Specification 10-1984 "Specrficancn for materlall and reltlng for well cements'.-- Water as recommended by the manufacturer 'Be' is the Bearden unit of alurry consistency.The compressive strength after 7 da)'s shall be not less than the Schedule Hl S. 24-hour compressive strength for -Methods of physical test for hydrauhc cement. June 1984 Issued by the Amencan.Maxunum consistency dUrl.blckeDIDg time are given in Tables 6 and 7.. for compressive strength are glveA ID Table S aDd for .

·Specification for ordinary and low beat PortiaDd cement (third .3 Supplies of cement in bulk may be made by arrangement between the purchaser and the supplier ( manufacturer or stockist ). 9. double hessian bituminized ( CRI type) multi-ply paper. TESTS AND REJECTION 7. under which a licence fOT the use of the Standard Mark may be granted to manufacturera 01' processcrs. and if requested. woven polypropylene or any other approved composite bags] bearing the manufacturer's name or his registered trade-mark. 9.1 Requirements in respect of storage. .'Dinon ). telting and quality control which iJ deviled and IUpPTvUed by BIS and operated by the producer. STORAGE. Standard marked products are also contmuoualy checked by BIS for conformhy to that seanderd at • further aaft:'guard. sampling.. Details of coDditioDS.1 The manufacturer shall satisfy himself that the cement conforms to the requirements of this standard.for ordinary Portland cement.1 The bags or packages may also be marked with the Standard Mark. lightWeight ( CRr type) jute. Tbe Standard MarJr on products covered by AD Indiaa ~tanda.1976.1.1 The cement shall be packed in bags [jute sacking bags conforming to IS : 2580-1982 'Specification for jute sacking bags for packing cement (second Ftvision)'. MANUFACTURER'S CERTIFICATE 8. may be obtained.2 The average net mass of cement per bag shall be 50 kg (see Appen- dix B). 1986 and the Rules aDd Regulations made thereunder. from the Bureau of Indian Standardl.1916 7. within ten days of despatch of the cement. 9. shall furnish a certificate to this effect to the purchaser or his representative. jf any. NOTE - The use of the Standard Matk u goverm d by the provisions oflbe Bureau of Indian Standard!! Act. the assurance that tbey have been produced to comply with the requirements of tbat nandan! UDder a well-defined system of Inspecajon. woven HDPE. polyethylene lined ( CRr type) jute. The words 'Oil-Well Cement' and the number of bags to a tonne or the approximate net mass shall be marked legibly and indelibly on each bag.IS : 8229 . The bags shall be in good condition at the time of Inspection. SAMPLING.d convey. 8. DELIVERY 9. 9. tests and rejection of oil-well cement shall be as laid down in IS : 269.

2 W. the indicated weights shall conform to the requirements given in A-I. The variation in volume shall not exceed ± 0·2 percent. except that the new weights shall be accurate within one-half of these tolerances. except that for new scales the tolerances on accuracy shall be one-half of these values.I Apparatus A-I.The indicated load on the scales shall be accurate within a tolerance of ± 2 g for loads of 2 000 g or more. and within ± 0·1 percent of the indicated load for loads smaller than 2 000 g. the required volume of mixing water at 27 ± 2°e.The weights shall be accurate within the tolerance shown in Table 3.I.I.I.I. The sensibility reciprocal shall be not greater than twice the permi· ssible tolerance on scales accuracy. NOTE - red to move the posrtion of equ il ibr ium ( rest A-I. PREPARATION OF SLURRY A.The graduated glass cylinders shall be large enough to measure and deliver.1. The graduations shall be sub-divided to at Ieast 13 .WELL CEMENT A-I.ights ..I Stales . On beam-type scales.I. TABLE 3 PERMISSIBLE VARIATION IN WEIGHTS WEIGHT VARIATION (I) g (2) g 1000 0'>0 035 030 020 0·L5 0'10 ± 500 300 200 100 50 A-l. The sennbility reciprocal iJ obtained by determining the weight requi.IS I 8m • 1986 APPENDIX A ( Table 2 ) METHODS OF TEST FOR OIL. where the "eights are on the beam. In a single operation.3 Graduated Glass Cyllflders . POIDC ) of the balance pointer by one division of the eca le.

graduation lines shall be in complete circles. and a notation made as to its chnracre risncs. and a large multiple-speed propeller-type mixer of 4 000 ml capacity.2 Pro<:edure A-I.The mixing device.The addition of bentonite to cement requ rr es that the amount of water be mer-eased..>0 14 . For example Class E cement slurry having a watar-cement ratio oro 38 to which IS added 3 percent ben.1985-. It lS recommended. capable of rotating at 4 000 rev/min or greater at no load at 'slow' speed. and shall be intermediate graduations shall extend around a minimum the circumference. A-1.For reference tests.The percentage of water by mass to be added for each class of cement shall conform to the values given in Table 4.The sample of cement to be tested shall be passed through an 850'micron sieve conforming to IS : 460 ( Part I ). any potable water may be employed. wrl I TcqUItC' an increase in water-cement ratio 10 0". freshly distilled water or dislllled water ""'ol. the mass recorded as percent of the tota] r r mc-nt sieved. for tesung purposes. mal wator-c ement ra no oro 38 and wicg hted to 2-20 glm l by adduron of GO percent barth'. and the smallest gr aduauon s shall a minimum of one-seventh of the circumference of the A-t. that 5'3 percent water be added for each I percent benron rt e in all classes of cement. and 14 000 rev] min or greater at no load at 'high' speed..2.2. A-I. The materials retained on the screen shall be weighed.1 Screening ." Percentage if Water .all\' free of carbon droxide shall be used For routine tests. etc. for preparation of cement slurr res shall be small two-speed propeller. in order to break Ilf' lumps and remove foreign materials.2. for testing purposes. capable of rotating at 6 000 rev/min or greater at no load at 'slow' speed. The mixing containers shan be constructed of either corrosion-resistant metal or glass. It is recommended. No water shall be added to compensate for evaporation. a cement slurry having a nor.IS I 8229 • 1986 5 ml The mam numbered The of one-fifth of extend around rylinder.~ Devices . A-I. type mixer of I 000 ml capacity. The rmxing water shall bemeasured in a graduated glass cylinder or weighed by means of scales and weights. The propeller blades shall be constructed of corrosion-resistant metal. and 10000 rev/min or greater at no load at 'high' speed. These materials shall then he discarded. NOTE 1 . tonne: Will require an mer ease in water-cement ratio to 0 539.3 Temperature af Wa/(T and Cement . A-l. wetting. NO'l'E 2 - The addition of bante to cement generally requires that the amount of water be increased.VI lIfu:zn.The temperature of water and cement prior to mixing shall be 27 ± 2°C.2 lI[l\l1Ig lVater . that 0'2 percent wate-r be added for each 1 percent bas-ito FOT example.2.

.d A·I. A-I.6 MIxing of Cement and Water .Mixing of the cement and the requisite percentage of water at the given temperature shall be done in accordance WIth the following procedure: The required quantity of water shall be placed in the mixing container. 2. For the large size mixer. After all of the cement has been arlded to the water.A. A-I.The volume of slurry in the small mixer shall be 600 m\. the volume of slurry shall be :2 000 ml. L r ~ L ( J I 1 (2) ml 600 2000 3000 4000 (3) (4) Large MaD 30 45 55 (6) g 355 1 183 \ 775 2367 (7) g 772 2572 3859 5 145 58 56 56 56 383 I 276 1 915 2553 684 2279 3419 4559 600 2000 3 000 4000 Large Large 35 30 45 55 600 2000 3 000 4 000 SmalJ Large Large Large 35 30 45 55 38 38 38 38 327 1090 1634 2 179 860 2868 430\ 5735 600 2000 3000 4 000 Small Large Large Large 35 30 45 55 H 44 44 44 349 I 162 I 743 2324 7q2 2640 3961 5281 600 2 000 3 000 4 {)()(J Small Large Cement (5) percent 46 46 46 46 • 35 Small Large Large Amount of Amount of 'HIGH' SPEED (I) 8229 • 1986 REQUIREMENTS FOR PREPARATION OF SLURRY ( C/a.2. the cove r shall be replaced on the mixing container and surrmg contrnued at 'high' speed In accordance wuh Table 4.2A. the mixer turned on to operate at 'slow' speed._-_-_. and the cement sample added in not more than 15 seconds.2.IS TABLE .. 3 000 ml or + 000 m\.A-----~ ~ Water ___.". 15 . E.2 5 a..5 Volume and Composuion of Slurry in Mixer . F and H G ~ l ( ~... Percentage by mass of cement A and B r ~ l ( C D. A-I.6 ) CLASS CEIlENT I Small Large 35 1 30' 45 ~ o5) Large Large As recommended by the manufacturer A·1. VOLUIIIll MIXBR OF OF SLURRY SIZE MIXING COMPOSITION OJ' SLUBBY TiKI!: AT r-------.. The composition of slurry for these volumes shall be as given in Table 4.

1 Apparata. "'-2.2 Il1Jervlll Count" - A stopwatch is suitable.1.. DETERMINATION OF FREE WATER CONTENT OF 8LUI\RY A-2. base board and carrying case ( see Fig.IS I 1221 • 1986 A-2.DDLE Fill. thermoregulator. I ).1.L ATMOSPUBRIC PRESSURE CONSISTO!tBTER 16 .1 AtmospWe Pressur« Consistomeler - Furnished complete with motor. switches. 1 TyPIC.t.. A-2.. 'ORQUE ORUN LID DRIVING PIN FILL LEYEL INDICATING GAOOvE SLlJRRV CONTAINER P.

I.S Preparation of Apparatus A-2. For this reason. The slurry-container assembly shall rotate at a speed of 150 rev/min.2 Water·Batk . such surfaces (particularly the outside edges of paddles) shall be cleaned and brushed with a brass cement mould brush.2 The slurry shall be stirred at 27°C for a period of 20 minutes. A. and the torqueindicator cord passed around the torque drum and looped over the pin.IS I 8229 • 1986 A-2.•. Surfaces which come in contact with the slurry shall he given a thin coating of waterproof grease or light oil before each test.e proper 611 level which is indicated by a groove around the inside of the container. The paddle shall be inserted and the lid placed in position by engagin g the pin located in the torque shaft of the lid.2.Water shall always be used as the bath liquid. The index of the torque-indicator mechanism shall point to zero when the pendulum hangs free. It shan then be remixed for an additional 35 seconds at 'high' speed in a mixer of I 000 ml capacity ( see A-I. the viscosity-temperature relationship of which is known over a range of 5 to 100 Be. The assembly shall then be placed in the bath." Procedure A-2.2 Calibration . ( Paratone shall be discarded after the use because of possible contamination during calibration.The slurry prepared according to A.:f. the quadrant seals shall be adjusted.I shall be quickly poured into the slurry container to tl.Care shall be taken to ensure that all surfaces which come in contact with the cement slurry are clean.l Filling oj Apparatus . all exposed steel parts shall be kept clean and lightly oiled or greased.3. The apparatus shall be recalibrated at least once each year. The ball bearings in the top of the cylinder and those in the mechanism shall be kept clean by frequent washings in kerosene and shall be oiled with a light grade of lubricating oil.2. The motor shall be started. The water-bath shall always be filled with water before turning on the heater. and used to fiU a 250 ml graduated glass cylinder. gears engaged. with the slotted paddle shaft." ). If It does not. A·2. A-2. After each test.f.1 Cleaning and Lubricating . The 0-250 ml graduated portion of the cylinder shall J7 . ) A-2.3. also whenever wear of any metallic part in contact with cement slurry becomes noticeable or when such part is replaced.The apparatus shall be calibrated with Paratone calibration oil.3 Assembly . A. Care shall be taken to ensure that the cord is properly aligned on the 45·mm drums of both the torque-indicator ring and the torque drum in order to preserve a constant radius of pull.The slurry-container mechanism shall be assembled and the paddle rotated by hand to ensure that none of the parts scrapes.

tMethods or physical tests for hydraulic ceme at . NOTE .18 I 8229 . 25 mm thick. The vessel shall have sufficient heating capacity to raise the temperature uniformly from 27 to 174°C in 75 minutes.Plate glass or non-corroding metalplates having a minimum thickness of 6 mm. The supernatant water developed after standing quiescent for 2 hours shall he removed by either pipetting or decanting and measured in a graduated glass cylin. The cylinder shall be sealed to prevent evaporation.1.1 Apparatus A-3.2 Spmmen Moulds - IS sieve [see IS: 460 ( Part I )-1985" ].S Cooling Bath . It may be either of the following two types: a) A non-pressure vessel suitable for curing specimens at a temperature of 82°C or less.A curing bath or tank having dimensions suitable for the complete immersion of compressive strength moulds in water. ·Specification for 'e.3.3.1." Water CU71ng Both . TEST FOR COMPRESSIVE STRENGTH A-3. The steel plate and the pad shall be approximately 200 X 300 mm.1986 neither be Iess than 232 rnm nor more than 248 mm in length.1. It shall be expressed in millilitres and designated as C free water content' .1 SinJe - 8~r-micron A-3. and having a suitable ~gitator or circulating system to ensure a uniform bath temperature. 18 .2 of IS: 4031-1968t.1 Thermomtter (for non-pressur« Iype vessel) with smallest scale divisions not exceeding 2'C.der of proper size.I. The cylinder shall then be set on a 6-mm steel plate which is supported by a 25 mm foam-rubber pad.1. range 0 to 104°C.1. A-3. operable within ± 2°C of the prescribed test temperatures. A.6 Temperature Indicator A-3. b) A pressure vessel suitable for curing specimens at temperatures up to and inc1ud Ing 193°C and a t pressures that can he controlled between zero and 20 700 kPa. A-3. Conforming to 9.st saeves : Part] Wire cloth test ereves (th"d "~l-lJltm ).1I.6.1.3 Base and Cover Plates . A-3.The foam-rubber pad shaH be upholsterer's medium density flatstock foam rubber.Such that the specimen to be cooled from the curing temperature can be completely submerged in water maintained at 27 ± 2°C. A.

--------.of glass or non-corroding metal.. A-3. wuh smallest scale divisions not exceeding 3°C. Schedule 4S 10 ± 3 400 kPa lOS NOTE 2 . cahbrated to accuracy of ± I percent..The interior faces of the moulds and the contact surfaces of the plates shall be thmly covered wrth grease The contact surfaces of the halves of each mould shall also be coated with grea.The final temperature grven m col 13 shall be mamtarned wuhlD ± 2°C throughout tbe remainder of the cunng perrod A-3.4...1 Preparation 'if Moulds .7 Puddling Rod .4. A-3.1.. A 3.4 ) SeD£:- TEMPERATURE ~T EL~. Excess grease shall be removed 19 .d A-3.3..--------------~.2 PYlOmtler (fur pT<SSUrt I]pt u-ssd) - range 0 to 210°C..2.1. TABLE 5 WELL-SIMULATION TEST SCHEDULES FOR CURING STRENGTH TEST SPECIMENS (Clau.BKa (I) (2) m 4S 6S 8S 95 lOS ---.. I 830 3050 4270 4880 5490 (3) kPa 20700 20700 20700 20700 20700 30 45 60 mID mID (4) °C 47 56 67 73 82 (5) °C 49 64.8. ...2..1.. 8229 • 1986 A-3.[ 68 99 120 136 72 103 123 150 G8 96 128 147 167 72 77 103 136 110 143 160 153 172 177 NOTE 1 The test pressure shall be applied as soon a! thE! specimens are placed m the pressure vessel.2..1..IS . and mamrarned wuhm the followmg va nations for the duranon of the ell rmg pertod.1.. (b) good adhesive properties to prevent leakage. A-3.Any grease which is noncorrosive in the temperature range of 27 to 21 O'C and which when subjected to test temperatures and pressures specified in Table 5 has: (a) a consistency to permit ease of application.0 mID min min mrn mm mID mID (6) 'C (7) 'C 53 (8) 'C 55 75 106 127 153 (9) (10) °C °C 59 64 82 89 113 121 133 140 157 162 min ( II) (12) ( 11) 'C 'C 'C . approximately 200 mm long and 6 rnrn in diameter.6. A·3.2 Prucedllre A.. 87 97 108 75 90 120 150 180 210 24.e to make the Joint watertight when assembled..PSED TIME (FROM' FIRST D:n>TB PRESSURE DULE ApPLICATION OF HEAT AliID PRJ!8BURE ) 011' Nu..8 Grease 10 Seat Spmmen Moulds ..2 4. and (c) water resistance.2 d..

3. A-3. A-3.18 I 822. The curing penod ends when specimens are tested for strength. A-3. 49. Specimens m moulds which show evidence of leaking shall be discarded A greased cover plate shall be placed on top of the mould. the curing period starts when specimens are initially placed in the curing bath. 9S and lOS given in Table 5.2 Placement rif Slw ry In Moulds .3 Curl1lg Period .The curing penod is the elapsed time from subjecting the spec.3 The recommended curing periods for test specimens are 8 and 24 hours. in case of Class J cement the curing periods are 12 and 24 hours. the remaining.4 Curl1lg Temperatures and Pressures A-3. not less than three specimens shall be employed. For one determination. the moulds filled to over-flowing. additional tests may be necessary.3.slurry shall be stirred 10 eliminate segregation.2.2. In some cases where waiting-on cement time data and other information are wanted. 60. After puddling. . Schedule 48 given in Table 5. the curing period starts WIth the initial application of pressure and temperature. the excess slurry shall be struck off even with the top of the mould.4.2. 8S.The slurry prepared in accordance with A·l shall be placed in the prepared moulds in a layer of thickness equal to one-half of the mould depth and puddled 25 times per specimen with a puddling rod. are recommended. A-3.3. c sealed in the curing vessel.1 For specimens cured at atmospheric. It is necessary that grease be applied to the exterior contact line of the mould and the base plate. Additional test at 7 days may be necessary for Class J cement. one or more of the Schedules. 20 . and puddled as for the first layer. However. immediately after slurry has been placed in the moulds.1 Cunng at temperatures below 82°C .2. 6S. 38.2.19841 from the interior faces of the assembled mould" giving particular attention to the corners.2. The moulds shall be placed on a thinly greased plate.4. is recommended. A-3.men to temperature m the curing vessel to testing the specimen for strength.For curing at atmospheric pressure and temperature of 82°C or less. The slurry shall be placed in all the specimen compartments before commencing the puddling operation After puddling the layer. FOT curing at pressures above atmospheric and temperature of noe or less. 71 and 82°e are recommended. A-3.2 For specimens cured at pressures above atmospheric. using a straight edge. A-3. one or more of the temperatures of27. The curing period ends when specimens are tested for s trength.2. to be apphed immediately after specimens a.2. pressure.2 Curing at temperatures above 82°C - For curing at tempera- jures above 82°C.

2.. immediately after mouldmg and covering. per minute is recommended. A hydraulic testing machine shaU be used and a rate of loading in the range of 6 900 to 27 600 kPa per minute shall be employed (see Note) When the ulimate strength is approached.2. Heat and pressure shall be applied in accordance WIth the appropriate schedule as recommended m A-:J.5 Tesung of specimens .2.4. at which time they shall be transferred to a water-bath and maintained at 27 ± 2°e for approximately 35 minutes. A-3.IS I 8229 • 19M A-3. For specimens of low errengfb ( 3 4. a loading rate of 27600 kP. at which time heating shall be discontinued.For curing pressures greater than atmospheric.Cube specimens shall be tested immediately after removalfrom the cooling-bath water.4.Z. they shall be removed from the curing bath approximately 45 minutes before the age at which they are to be tested. they shall be removed from the curing bath 20 to 23 hours after the cement slurry is initially mixed. NOTE -For normal strength specimens. the test specimens.1 and A-1. Where specimens are to be tested at ages of less than 24 hours.t.t.3 Curing at atmospheric pressure . shall be Immersed in water at 27 ± zoe in the pressure vessel.2. Where specimens are to be tested at ages of 24 hours or more. At 45 minutes prior to the age at which specimens are to be tested.2..00 kPa or less ). 21 . A-:J. The maximum schedule temperature and pressure shall be mamrained as given in Notes I and 2 in Table 5 till 105 mmutes prior to the age at which the specimens are to be tested. and returned to the curing bath.For curing at atmospheric pressure. a rate of 690C to 13 BOO kPa per minute is suggested. transferred to ~ water-bath and maintained at 27 ± 2°C for approximately 35 minutes.4. the pressure then remaining shall be released gradually (to avoid damage tc the specimens) and the specimens removed from moulds. immediately after being placed in moulds and covered. no readjustment in the machine control shall be made to maintain the rate ofloading selected. Immediately removed from their moulds. and placed in a water-bath maintained at 27 ± 2°e for approximately 35 minutes. the temperature shall be decreased to 93°e or less without release of the pressure other than that caused by thermal contraction.4 CuTtng at pressures above atmospheric . the test specimens. Immediately removed from their moulds. During the next 60 minutes. shall be immersed in a water-bath maintained at the curing temperature. They shan remain in the curing bath till approximately 45 minutes prior to the age at which they are to be tested.

l.In the calculation of compressive strength. 2 ). The space between the slurry container and the walls of the pressure container shall be completely filled wiih white mineral oil..3 CalculatioD aDd Reporting of Results .Operating instructions as furnished by the manufacturer shall be followed. provided devIations of I '6 mm or more from the specified linear drrnension of 50 mm (see IS: 4031-1968·) arc reported. and thus serves as a method of comparing various cements.-nR Instructions ..2 Flillng of Apparatus . A heating element capable of rarsing the temperature of this oil-bath at the rate of at least 3°C per minute IS provided Thermocouples are provided for determining the temperature of the oil-bath and also that of the cement slurry.l. Grade 95 N}' ( National Formulary) or equivalent..Pressurized consistometer ( Sit Fig.2. indrcated by the amount of d-forrnation of a standardized corl-sprurg connecting the stirring paddle and a stationary head.1 Operal.O Thickening time test is designed to determine the length of time a given cement slurry remains 10 fhnd state under given laboratory conditions. variations from the specified cross-sectional area ( 2 500 mm! ) shall be disregarded. A-f.. The compressive strength of all acceptable test specImens made from the same sample and tested for the same period shall be averaged and reported to the nearest 70 kf'a..3 Procedure A. the slurry shall be lightly stirr ed to prevent segregation.3.1 Thukemng Tune Tester Unit .I ApparatDs A-f.The slurry prepared m accordance with A-I shall be quickly poured into the inver ted slurry container. ·Methods of phvsrca l tell! for hydraulic cement.2 Calibration of Thickening Time Tester Unit .'l Stop Watch A-4. 22 ..3.IS : 8229 • 19116 A-3. The thermocouples shall be calibrated at frequent intervals to ensure the accuracy of temperature measu rernents A.. The apparatus consists essentially of a rotating cylindrical slurry container equipped with a stationary paddle assembly. The stirr Illg paddle and all metal parts of the slurry container exposed to the slurry are made of corrosion-resistant alloys A-f. A-f.. The consistency of the cement slurry i. TEST FOR THICKENING TIME A.Calibration of the potentiometer mechanism of the pressurized consistometer shall be done as prescribed far atmospheric pressure consistorneter in A-2. During this fillin!( operation.f. A-4. all enclosed in a pressure chamber capable of withstanding the pressures and temperatures prescribed in Table 7.

....TaRa J[ 5?RINQ CONTACT PIN POT:::NTIOMETER MECHA~ PROTECTIVE SHiElD -..::: SLURRY CUP SM COMPLETE .......T C0N~ISTOMETE.R 23 . ~~i~!L=~~~ ~~ CYliNDER COOL....l>.AI R-PRESSURE CCltiN£(TIClN PRESSURE~CYLINDER COMPLETE THERI'-40COUPlE TUBULAR HEATER -.. /' CUP (I1APHR'AGM---. 198$ / -CH ~JDE"R 5E... "lc. <.INO ~ CO L ~I)\l PI=lESSU~E CONN£CTJON \EAR REDUCER MITRE GEARS~ W~~~I..Is 8229.J I<'IG 2 TYPl0AL PRES~URIZLD CURRI-... RING // Mf:ASURING POTENr laME TE~ .

are given in Table 7. the slurry container set rotating and the oil-pressure pump started. Band C IS and 4S Class D ·IS and 6S Class E oS and BS Class F 6S and 95 Classes G and H 55 Class J 65 and 9S A_4. The operation of filling and sealing the slurry container. any air in the top of the cha mber shall be vented through the top vent. and the pressure in the slurry container shall be increased in accordance With the relevant schedule ( see A-f.3.IS : 8229 .2 The desired thickening time for any particular well will depend on the history and conditions of the well and 11 IS possible to effect certain suitable modifications in the thickening times for Schedules 58.3. the container placed in the pressure chamber and the chamber filled with the bath 011.. B. sealing and venting the pressure chamber and placing the apparatus III operation shall be completed within 5 minutes after completion of the mixing period. A. the temperature of the cement slurry.. E. placing the container in the pressure chamber. it IS not necessary to conduct tests in accordance WIth all of the specified schedules for Classes A. A-f.3. WIth the pump in operation..1 If only hrmted data are required.4.4.4 Test Schedules . The thickening lime for different classes of oil-well cement shall be determined in accordance with the following schedules' Test Schedule(s) Classes A. 85 and 95 if the local conditions so demand but this will not have any bearing on the acceptance of a particular type of consignment. The head assembly of the pressure chamber shall then be Screwed in place. C. and Pressure Control . 24 . 6S.1986 When the slurry container is completely filled. D.3 Tempe".3. The centre plug shall then be screwed tightly..3. care being taken to ensure that all air is excluded. F and ]. determined with the thermocouple in position in the centre of slurry container.Thickening time test schedules representing casing cementmg conditions assumed as in Table 6.f). the bottom shall he screwed in.. A..tur.Durmg the test period.

. mud densitres and depths shown rn the table.Bottom hole pressures have been calculat ed from the corresponding surface pressures.IS I 8229 • 1986 A-. ed on a.BOTTOM" TIME TO HOLE RZACB HOLE PRESSURE BOTTOM CIRCULA'l'INO TEMPERATUF.E (1) (2) kg/L(kPa/m) IS 305 1-2 (0-120 ) 48 1 830 1-2 (0-120) 58 2 HO 1"2 (0 (20) (3) (~) (7) (8) °C kPa min 27 7000 7 (5) (6) °C kPa 27 3400 27 5200 45 26700 20 27 6 "00 52 35 600 28 6S 31150 11(0114) 27 n GOO 6° 51 600 36 85 4270 I·~ 27 12 100 97 92300 52 95 <Ie 27 13 800 120 III 300 60 880 NOTE I NOTE 2 - (0-192) 2 0 (0-204) Mud densines have been obtained from a review of field data. Surface pressures have been obtamed from a review of field data... Record of Results -. survey of field oper-ation. It is permissible to stop the test at a consistency of approximately 70 Be and to extrapolate the 100 Be value by plotting the results.5 - Tjme to seacb. TABLE 6 BASIS FOR THICKENING TIME TEST SCHEDULE ( Clouse 1\-4 3 4 ) :)CHEDDLE DEPTH MUD Dfl:NSITY NUMBER SUR'B'ACIil SURFACE TKlY:PRESSURE PERA1'llRE BOTTOM.Bottom-hole crrculatmg t ernperatures have been averaged from actual field tests Tun at various depths NOTE 4 ... NOl E..The elapsed time between the starting of the apparatus and the occurrence of a consistency of 100 Bc shall be reported as the thickening time for the cement under test for the particular schedule followed in the test. 2S . bottom. For the schedules Involving higher temperatures. NOTE 3 . lS ba. and reflects condrnons as severe as 75 percent of the jobs surveyed.

dule 88 (12) 'C Schedule 68 (11 ) TDPEBATURB Schedule Schedule Schedule Schedule Schedule Schedule Schedule Scbe.Schedule dule 8S 98 48 5S 4S 58 6S IS IS . 12 100 15200 kP.d A·4..a- N r---. ClI " GIl . 6900 9000 kP.4 ) TABLE 7 THI<lKENING TIME TEST &<lHEDULE I - ~.3. _ _ _ _ _ _ _ _ _ _ •• """"'I r-------~ 42700 46200 40000 42 700 30300 32 400 27600 - - - - - - - 20 22 24 26 28 30 26700 - 35200 37200 39300 42 100 44 100 29600 31 700 33800 35600 - 58600 46200 49000 52400 55200 62700 49600 53 100 55800 59300 40000 36500 27600 23400 25500 22100 24800 - 16 18 14 33 100 36500 30300 33800 22800 25500 19300 21400 17900 20000 - 30300 27600 20700 12 17300 15900 - 7000 26900 ID 8 17900 2 4 6 15200 20000 23400 18 000 21 400 24 100 13 100 15900 II 000 l3 100 9700 11 700 4100 5500 6200 0 13800 kPa 13800 17200 n..1 a. Schedule 9S ( 13) 39 36 34 32 35 37 41 43 41 39 39 36 34 31 33 34 29 28 30 32 27 29 27 27 31 32 'C 'C 'C 27 28 Sch ._________ .A. 5200 7600 kP.6) (7) (3) (4) (5) (8) (9) ( 10) (2) ( I) TIllE PR'B88lJRE ( Clauses A·4 1. 3400 mIn - - - - -- - - 27 27 27 27 27 'C - - 50 52 56 48 51 52 54 67 56 59 62 64 46 - 48 - 70 73 61 64 67 58 54 51 53 44 47 43 44 52 48 42 45 46 48 43 46 38 42 41 40 37 37 39 36 30 33 27 'C -. 8600 II 000 kP.

N .. ~ Ij 5j .. - - - - 52 5..The final temperature and pressure should be held Constant within n ll completion of the test... - ~ - - - - - - - - - - - - - 42 44 46 48 5(1 4il 3B 32 34 36 - - - 114 117 120 108 III 92 95 98 101 104 89 86 77 79 B3 respectively ~ - - 97 83 86 88 91 94 81 78 70 72 75 ± lClC and ± iOO kPa - - - - - - - - - - 58 60 62 - - - I '00 .. 56 58 60 - - - - - - - - -- - - - - - 46900 49000 51600 -- - - - 92300 77 200 80 000 82700 86200 88900 73800 71000 61400 64800 0600 104800 108 200 III 300 986UO 101 400 82 000 85500 88300 91 iOO 95 100 78600 75 BOO 65500 68900 72 400 - - - - - - - - - - - - - - - - - - NOTE ..

B·1. NOTE - The matter given in B·l and B-l.1 The number of bags in a sample showing a minus error greater than 2 percent of the specified net mass ( 50 kg ) shall be not more than 5 percent of the bags in the sample and the minus error in none of such bags in the sample shall exceed 4 percent of the specified net mass of the bag.l are extracts based on the Standard of Weigh IS 3Qd Measures ( Packaged Commodun.1. the overall tolerance on net mass of cement shall be 0 to +0·5 percent. tbe mass of a double hessjan bu umrruz ed (CRI type) bag to hold 50 kg of cement is 630 g. .e 100 to 150 151 to 280 281 to 500 SOl to 1 200 I 201 to 3 200 3 201 and over 20 32 50 80 125 200 The bags In a sample shan be selected at random (see IS : 4905-1968·). NOTE . The number of bags in a sample shall be as given below: Batch Si{e Sample Si<.4 and 9.2 In case of a wagon-truck load of 20 to 25 tonnes.IS J 8229 • 1986 APPENDIX B ( Clauses 0. conformmg to IS : 25BO-1982t to hold 50. the mass of a 6-ply paper bag to hold 50 kg or cement IS approximately 400 g and the man of a polye-thylene hned (eRI type) jute bag to bold 50 kg of cement IS approximately 480 g *Methods for random sampling. 1977 to which reference shall be made for full details Any modrficatron made In these Rules and other related Acts and Rules would apply automatically.The maas of a jute eackmg bag. The average net mass of cement packed in bags at the plant in a sample shall be equal to or more than 50 kg.s ) Rules. B. tSpeCificahon for jute aac krng bags for packing cement ( second 28 reVISIOn ).2 ) TOLERANCE REQUIREMENTS FOR THE MASS OF CEMENT PACKED IN BAGS 8-1.kg of cement is 531 g.

-. ( RESERcn) -CUM" DIRECTOR RESEARCH O:rFICEll.j. Bom.lJido Mmalur ) Director ( Oi v Engg ) Sur.. RESEARCH SKftI ( B&S-\ ) (Alltrna. Director General..varaya) On ( SliT) S. New Delhi All"""t.NDYOPADHYAY Deputy Director (Civ Engg }.t of Surface TraDiport. MIGL ANI ( AllenDI. I( MeLLICK Alt. New Delhi The Hrndusran Construction Co Lt4..rlfJln.. KAPOOR SHEr R.IIIinud . KHANNA SKRt SHBI SHin S.inry of Transporl ) Depart.YA..bay Directorate General of Technical DevelopmeDt.rs DB A. GlJHA THAKl1RTA Gannon Dunkerley &. N. Bombay Altnnal.) R.pr. SANKAHUARA. Calcutta Cement Manufactuee ra Aesocaetron.. JAGUS DR A.( C••lintdd Fom PDgt 2 ) M~mbt' s R. C. BOC 2 1 C.attS 10 Dr H.) SHRI A V. New Delhi DB H. DANERJEE SIlRI SOMNATII IlANEHJICE CBIEI' ENGINEER.ioa. L. N.. Lucknow DEPUTY DIRECTOR.nt3n g Snnr S. CHATTEUJII:E ( JOINT DIRECTOR. New Delbi DnUTY DIRECTOR ( C&MDD ) ( Alltl.. Bombay SHSI S. ) ( C.n National Council for Cement and BUilding Matetrials.) (B&S) Research. VlSVE8VARAYA M6mb. RESEARCH The Associated Cement Companies Ltd. HIS (Ex-. Government or PUDJab CT) ( Alternate ) Maharaahtea Engrneer mg Research NaJlk Alternate ) C&MDD ) Central Water Com minion. ) SHnI P. C. DATTA (Alltr. R..'a.alt) W.at. GOKAK Development Commsseroner for Cement IndulIlry ( Minilltry of Industey ) RESEARCH Oll'lI'lCEB ( DIREOTOR ( SIIRI S S. 30 ) . 29 ~. LAXMl SIIBI S K. KARODE S. ( DIRECTOR National Test House. Co Ltd. rombay Irrrgauun Departmenr. GSOSH ( Roads WI~ng ( Mn. Deergns aud Standards OrgaDiz:&1. BIS SKRt Cement Subcommittee. K. P.. K. C. K.. Vbve. 8A.NAN (AIUrrrale) SUR] G RAI4AN. K. K.s.

d~) SHRI A. Central Road New Delhi P. BhJlal Robtal Indultne.) Sam S. R.1WII /JIJg' 29 ) Memlurs lupr.TTAJU ( Altern. New Delhi D.. K.m6. K... A.t.01." DR ( S• . New Delhi SII]II J. PATEL (0411<'.NEER (D) Public Works Department. Rtt!>!>l DR S. AlterrED") Dalmia Cement ( Bharat ) Ltd.ltC'rn. K. Army Headquarters ( Altlf'lUIt... CHATTBRJEE 5B. Vadodara SRnlJ. MOHIDEEN SHRt Y R. K..i Steel Plant." ) SUPERiNTENDING ENGJ. R... D.. (Alt""at#) SaRI C.. S.rs K.. 1 S.t d. Roorkee DB. RAO SBKI N. Bombay Central Budding Research Institute (CSIR l.. K.I."0 ( AII. LA"'" National Council for Cement and Building Matenab l New Delhi M. H. RSBB' Gall1mon IndIa Ltd. ) DR A. S. ARORA DB A.nl..u ) SaRI L. C. Sa" GUPTA ( 041'''/1111' ) • LT·CoL V.) SHUI V M WAD WORKS M ..8RAD MA800D (A. 1R. V. Ltd.:NAGltR ( Cl!KI!:1'o'T) Bbih.Chief'.. SOMANI Shree DJgvijay Cement Co Ltd.m18229· I!NI& ( C•• .. Branch..uULL Saar M. K. Dalmianagar Adhoc Panel for Regularization of IS : 8229E·1976 01. Government of Tamil Nadu S1I::NIOa DEPUTY CBIU::I' ElfOllOl:ll:I1.&JI. New Delhi Salt..a. U.. New Delhi SURI K. BS ..s'nIJ"g Cenrra l Warehousing Corporation. G. THATTB Gujarat Engineering Reteareb lost it ute." OB and Natural Gas Commission.. N & • . V. Sw. Bombay 30 .i. P. New Delhi SeRt K. Bombay SaRI R.. RAO National Buildings Organiaatinn.arch Institute (CSIR)...oOP Oriaa Cement Ltd..d j.6 ( R . Debra DUD The Auoeiated CementCcmpames Ltd.. GALANDB Engineer·ia.§. K. RIJH81NGHANI Cement Corporation of India I.1. R CHATTERJEIC SaRI A. TTACBARY. ( G""aBAL) ( o4l'mu.

Sahlbabad Industrial Area.-lWw: Manak Bhavan.cond Floor. COIMBATORE 641037 550 13 48 83949 S5 55 40 :!1 40 36 :!7 21 01 41 Piol No 43. MUMBAI 400007 27 10 iSales Offioe IS at 'F Block. InCla . R G Barua Road. GHAZIABAD 201001 53/5 Ward No 29.BUREAU OF INDIAN STANDARDS HMdq. CHANDIGARH 160022 Soulhern CIT Campus. 670 AVlnashl Road. P 0 Pnncep Street. Khuqa.Tumkur Road. 5th By-lane. NEW DELHI 110002 "Eastern 1/14 CIT Scheme VII M. 1332 ShlVajl Nagar. SIIe IV. MUMBAI 400093 32376 17 33786 sa 60 38 43 23523 15 8329295 Branch Offlces: 'Pushpak'.jnltng Press. BANGALORE 560002 es 309 65 :!8 222 39 71 Pnnted at NeYJ India Pr. Ganga Nagar BHUBANESHWAR 751001 Kallllkathlr BUIldings. ty BUildIng. IV Cross Road. ~1 11 3239382 Telegrams Manaksanstha (Common to all Offices) Central Laboretory: Plot No 2019. AHMEDABAD 380001 tPeenya Industrial Area.. Sector 34-A. SAHIBABAD 201010 Telepholle 8-77 00 32 Reg/one! Offlces: Central Manak Bhavan. Andhen (East). HYDERABAD 500001 20 1083 E-52. 116 G T Road. Naval Krshore Road. CHENNAI 600113 tWestern Manakalaya. BHOPAL 462003 Plot No 62-63. 2nd Floor. Nurmohamed Shlllkh Marg. 9 Bahadur Shah Zalar Marg. NEW SELHI 110002 Tslephones 3230131. Behind Leela Cinema. 91 11 3239399. Umt VI. NAG PUR 440010 52 51 71 Insbtubon 01 Engn_s ( India) BUIlding. Bangalore . Narashlmaraja Square. E9 Behind Marol TelephOfle Exchange. Grant Road. CALCUTIA 700072 tSales on. 9 Bahadur Shah zalar Marg. Manlktola. ChltaranJan Marg. VI P Road. CALCUTTA 700054 Northern SCO 335-336. Sarvooaya Nagar. Sector 16 A. LUCKNOW 226001 23 89 Patllpulra Induslrlal Estate. BANGALORE 560058 ': Gangetrl Complex 51h Floor Bhadbhada Road. PUNE 411005 323635 ·Sales Olllee IS at 5 Chownnghee Approach. JAI PUR 302001 37 29 :!5 117(418 S. c-Scneme. S. University P 0 Palayam. KANPUR 208005 zt 68 76 Seth Shawan. FARIDABAD 121001 8-28 88 Ql savun 8-71 19 96 Complex. THIRUVANANTHAPURAM 695034 ~3 621 17 NIT Building. T T Nagar.oe IS at Novelty Chambers. U.3239402 Fax 91 11 3234062. PATNA 800013 26 23 05 T C No 1411421. Khanpur. GUWAHATI 781003 54 11 37 5-8-58C L N Gupta Marg. Malhura Road.3233375. Nampally Station Road. 1st Stage. Gokulpat Market.