Pressure Measurements Notes

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Pressure Measurements Notes

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Pressure measurement

6.1 Introduction

Pressure is represented as a force per unit area and has the same units as parameter discussed previously in

lecture No.4 as stress,

F

A

The new aspect of the same parameter which will be discussed in this lecture is the force exerted by a fluid per

unit area on a containing wall. The pressure measurement devices for fluid are usually measure pressure in three

different forms: absolute pressure, vacuum and gage pressure.

Absolute pressure is the absolute value of the force per unit area exerted on the containing wall by a fluid.

Gage pressure is the positive difference between the absolute pressure and the local atmospheric pressure.

Vacuum is the negative difference between the local atmospheric pressure and the absolute pressure.

From these definitions in Fig. 1 we see that:

1. The absolute pressure is usually positive.

2. The gage pressure may be positive or negative (vacuum)

3. The vacuum is usually smaller than the local atmospheric pressure.

Because a fluid pressure is result of a momentum exchange between the molecules of the fluid and containing

wall, it depends on the total number of molecules striking the wall per unit time and on the average velocity v of

the molecules.

For an ideal gas the pressure is:

1

1

m2

N

(1)

p nmv 2 [ 3 kg

] [ 2 ] Pascal

2

3

m

sec

m

where n is molecular density, molecules/unit volume; m is molecular mass and velocity v is root mean square

velocity:

v12 v22 v32 .......vn2

3kT

(2)

n

m

where T 0 K is the absolute temperature of the gas, k =1.3803 1023 J /K is Boltzmanns constant, molecular

mass, velocity is:

J K

J

Nm kgmm

m2

[

m / sec]

K kg kg kg sec 2 kg sec 2

v vrms

Since the pressure depends on collisions between the molecules, it should be dependent on the average

distance passed by a molecule of radius r between collisions. The mean free path in an ideal gas is

2

2 m3

[

(3)

m]

8 r 2 n m 2

More n smaller is the mean free path. For air the Eq. (3) reduced to

T

2.27 105 [m]

(4)

p

Where T 0 K and pressure p must be in Pascal [ N / m 2 ].The mean free path decreases with increase in the gas

pressure p (or the density n) and with decrease in temperature T. The typical examples of mean free path in air at

20 C were calculated using Eq.(4):

1atm 6.564 108 m

1atm

= 1.0132x 105 Pa

1torr

1 m

= 133.32 Pa

1 m 0.04989m

= 0.13332 Pa

0.01 m 4.989m

0.01 m = 1.332 103 Pa

At a standard conditions (p=1 atm) is quit small (about 0.1A), while in vacuum it reaches several meters

length.

Low absolute pressure or vacuum is used in many practical operations: the manufacture of computer chips

and laser crystals, for example, are completed in vacuum. Vacuum is measured in torr which is defined as 1/760

of the standard atmosphere. Since the standard atmosphere is 760 mm Hg, 1 torr is 1 mmHg. Usual definitions for

the ranges of vacuum are:

1atm 6.564 108 m

Low vacuum

760 to 25 torr

Medium vacuum

25

to 103 torr

High vacuum

103

to 106 torr

1 m 0.04989m

0.01 m 4.989m

Very high vacuum

106 to 109 torr

Ultrahigh vacuum

below 109 torr

Since the length in vacuum is large this is used in a series of gages for measuring vacuum which have

electrical output.

The vacuum gages contain all components of the measuring device shown in Fig. 1*. ) 3) ( 2)

6.2.1 Pirani gage

3

In gage shown in Fig. 2 a measured parameter (1) is vacuum. A sensing element (2) is heated filament ( )

which is located at the center of a chamber connected to the vacuum source. The variation in filament temperature

(electrical resistance) is mechanical reaction (3). Temperature depends on heat loss to the wall. Heat loss in torn,

dependent on the thermal conductivity ( ) of the gas. When the pressure within a chamber is low the

length is large and the heat transfer from a filament to the walls is strongly sensitive to the variations in

pressure:

q C T f Tw Pvac

where T f is the filament temperature, Tw is the chamber wall temperature. Coefficient C depends on the gas in

the chamber, the wall temperature, the geometry of the chamber, and the filament surface area. The lower is the

pressure, the lower the thermal conductivity and, consequently, the higher the filament temperature (resistance)

for a given electric-energy input. Since the filament is part of electrical bridge circuit (4), the variations in

temperature of the filament causes variation in the filament resistance (tangsten) which affects the resulted output

(( ) 5).

The procedure

The reference chamber is sealed and evacuated. Since both gages are connected in series and exposed to

the same environment, variations in the ambient conditions are compensated. A balance condition initially

adjusted through resistance R2 and then the test gage is exposed to the vacuum. Since the change in environment

temperature is compensated, all deflection of the bridge from the null position shows the vacuum.

Advantages

1. An overall range of this gage is about 0.1 to 100 Pa (from 1 m to about 1 torr) medium vacuum.

2. Electric output allows automation.

Disadvantages

1. The establishment of thermal equilibrium is rather slow and the transient response is several minutes.

2. Preliminary calibration of each pressure gage is required.

6.2.2 The ionization gage

The arrangement shown in Fig. 3 is similar to the ordinary triode vacuum tube when the heated cathode

emits electrons, which are accelerated by the positively charged grid.

The electrons move toward the grid and produce ionization of the gas molecules through collisions. The plate is

maintained at a negative potential, so that the positive ions are collected there, producing the plate current i p .

The electrons and negative ions are collected by the grid, producing the grid current ig . The number and

effectiveness of the collisions effect the ratio of plate current to grid current. This ratio is sensitive part of the gage

which is proportional to the pressure of the gas (or vacuum):

1 ip

p

S ig

where the constant S is called the gage sensitivity which should be determined by calibration.

4

Advantages

1. An overall range is between 1.0 to 10 5 m Hg (0.13 1.3 106 Pa ) - high vacuum, while special types of

ionization gages can be used for very high and ultra high vacuum up to 1012 torr (1.13nPa ) .

2. Due to linear output current these gage can be used for automation purpose.

Disadvantage

Danger of burning out of the cathodes due to a high sensitivity to a pressure change.

The several types of traditional pressure measuring devises that have no electrical output still deserve

mention. The U-manometers and the bourdon gages enable a pressure to be read quickly and reliably while the

MacLeod gage and the dead-weight tester are used for calibration. None are suitable for dynamic measurements

and automation and composed of only three first components (1) (3) of the schematics shown in Fig.1*. The

fluid U-tube manometer shown in Fig. 4 is used for measurements of fluid pressure and vacuum under laboratory

conditions. It consists of a U-shaped transparent glass or plastic tube partially filled with a liquid. The sensing

lines of the pressures to be sensed are connected to the tubes as shown in Fig. 4. The U-tube manometer is used

readily for measurement of differential pressure (A) (the difference in pressure at two points in a system) or

gage pressure (B). In the last case one sensing lines is opened to atmospheric pressure. Hence the input parameter

for this type of the measuring device is pressure, ( ) - (2) the measuring liquid and mechanical reply

(3) . The U-tube manometer is used either for gases or for liquids. When the fluid being sensed

is a liquid, then the manometer fluid must be both denser than the sensed fluid and be immiscible with it. The

fluids should also have different colors so the interface (meniscus) is readily visible. The pressure difference at

the top of the manometer can be computed from:

P P1 P2 hg ( m s ) Rg ( m s )

where h is the difference in levels of the two interfaces (given the symbol R), m is the manometer liquid

density, s is the density of the sensed fluid and g is the acceleration of gravity.

Fig. 4 U-tube manometer for measurement of differential pressure (a) the difference in pressure at two points A

and B or gage pressure (b) in point A.

For gases, since s m , P Rg m and the result of P / g , known as reading R has the unit of a fluid

column height:

3 2

P

N

kgmm s

m

2

2 2

g m g s m kgm

If we use the density of water, the pressure can be expressed as feet of water or inches of water, atmospheric

pressure is usually expressed as 30 in Hg or 760 mm Hg. The accuracy of fluid U-tube manometer depends on the

scale and on the manometer fluid density m . A new term: specific gravity, S ( ) specifying the ratio

of the fluid density to the density of water at a specified temperature (usually 4C).

Example 1*

Given

U-tube manometer uses the mercury which is 13.6 times denser then water. g=9.8 m / sec 2

The density of water at 4 C is 1000 kg / m3

Objectives

1. Define specific gravity, S of the mercury.

2. Determine the reading of the manometer or the difference in levels of the two interfaces (given the symbol R)

when it measures pressure difference P 4 atm.

3. How long this device should be?

Solution

1. Specific gravity of the mercury is S=13.6

2.1atm= 105 Pa 105 N / m 2 105 kgm / sec2 m 2

5

3 2

P

P

4 10 kg m m sec

R

3m

m g water gS m21000kg sec 2 13.6 9.8m

More simple solution is: 4atm x 760 torr = 3040mm

Example 2

We have to measure absolute pressure P 0.4atm by U-tube manometer which scale is 1mm/div. Manometer is

filled by oil with specific gravity, S =0.9. To define the reading and to compare a reading accuracy for the two Utube manometers: one filled by Hg and another filled by oil/?

Given.

U-tube manometer with scale 1mm/div is filled by oil.

Oil specific gravity is S =0.9.

Hg specific gravity is 13.6

An absolute pressure which has to be measured is P 0.4atm.

Solution.

A. Reading

For Hg manometer

R Hg P 0.4atm=0.4 x 760torr=304torr

For oil manometer

S Hg

13.6

15.1

0.9

S

Oil

R 15.1 x 304torr=4.59m

oil

6

B. Reading accuracy:

For oil manometer reference error is:

R (0.5 / 4590) 100% 0.01%.

For Hg manometer reference error is:

R (0.5 / 304) 100% 0.16%.

0.16/0.01=16

Accuracy of the oil reading is 16 times of this for Hg.

Simple estimate was already obtained previously as ration of Hg to Oil specific gravities:

S Hg 13.6

15.1 .

S

0.9

Oil

6.3.1 An inclined manometer

The minimum pressure measured by U manometer (of 0.5 in. of water 1mmHg ) can be reduced to 0.1 in.

(0.19mmHg) by the use an inclined manometer.

A small change in a fluid height causes larger displacement in the transparent tube when it is inclined to the angle

and filled by oil. A reading formula for gases is:

p h g R sin g

Example

An inclined manometer with a resolution of the sloping scale of 0.05 in has to measure a gas pressure 3 in.

of water with a resolution of 0.01 in. What is the angle and how long is the inclined tube of manometer which

is filled with water?

Solution

In order to choose the angle one should remember that the minimum pressure level to be measured has to be

equal to requested value of the resolution 0.01in H 2O . At the same time this resolution must be equal to reading

R of single division on the inclined scale of the manometer. Hence

p h g R sin g

h 0.01

sin

0.2 Hence 11.5.

=

R 0.05

Since the total rise of a water column is 3 in. one can obtain:

sin 3 / L 0.2 , L=15in 38.1cm.

To read the locations of the two interfaces of U-manometer is rather inconvenient. To overcome this

problem, on can use the well with the cross-sectional area larger then the area of the transparent tube. When a

pressure is applied, the change in surface elevation of the well is extremely small and only one reading is

required:

P P1 P2 hg ( m s ) Rg ( m s )

Since for gases- s m , P Rg m

Example

A gas pressure applied to the well port of a well-type manometer results in a reading R= 47.5 cm. To

define the applied pressure if the manometer fluid has a specific gravity of 2.0.

Solution

3

3

m 2 1000 kg / m 2000 kg / m

g 9.8 m / s

Pa=N/ m 2 = kgm / s 2 m 2 kg / ms 2

Finally we have P 9.31kPa .

A well-type manometer is also used for measure absolute atmospheric pressure.

For this purpose one leg is evacuated and the well is exposed to atmospheric pressure. The top of the

column contains saturated mercury vapor at the local temperature. However in comparison to atmospheric

pressure this saturated pressure is negligible

The height R is thus a measure of the absolute atmospheric pressure read directly in inches (or mm of mercury).

8

A small temperature correction has to account for the vapor pressure of mercury and differential thermal

expansion of the mercury and the measuring scale.

When pressure measuring devices indicates gage pressure, the absolute pressure is:

P(absolute)=p (gage)+ p atm

A common mistake is to take as the local atmospheric pressure p atm the value given by the local weather bureau

pZ .The value stated by the weather bureau is usually corrected to the see level, using the altitude at the weather

station Z:

5.26

BZ

p z p0 1

T0

Z= altitude, m or ft

T0 518.690 R 288.16 K 150 C

B=0.003566 0 R / ft =0.00650K/m

When the problem is to specify P(absolute), the local atmospheric pressure must be measured near the

place where the gage pressure is measured.

Example

Calculate the standard atmospheric pressure in mmHg at the altitude 7000ft (2133.6m).

0.003566 7000 5.26

p 760[1

]

586mmHg

518.69

The relative error in atmospheric pressure is: p

760 586

760

0.23 23%

Advantage of U-manometers

1. Simple, inexpensive and based on clear principles.

2. With light oils differential pressures as low as 0.5 - 0.1 in. of water can be measured with a resolution of the

order of 0.02 in (0.5mm).

Disadvantage

Limited pressure range (due to the length restriction).

The densest fluid normally available in manometers of this type is mercury, with a density 13.6 times that of

water. To measure a pressure difference about 4 atm, for example, a device height is about 10 ft 3m and a ladder

is required to read it.

This is another type of a simple device which is used for readings of fluid pressure with visual control.

In this device a sensing element is curved, flattened tube (bourdon tube) which attempts to straighten out when

subject to internal pressure. The end of the tube is linked to a rotary dial indicator.

Advantages

Relatively inexpensive and used for a wide range of pressures, from low vacuum up to 20,000psi (1350bar), error

of 5% of full scale.

The most expensive gages with a mirror scale (about 2000-3000$) have an accuracy about 0.5% of full scale.

Disadvantages

1. If not protected, easily destroyed by high overpressure.

2. Are mostly suited for a steady state measurements.

3. After the year of application can change its characteristics due to repair or other reasons.

After the some period of time since

production

(usually

several

years)

the

manufacturers' specifications can not be further

taken at face value of the measuring accuracy. To be

sure of the validity of the measurements in this case

we have to make a calibration before accepting the

reading of an instrument. The term calibration

means to check the instrument against a standard

and thus, to reduce the measurement errors. The

term static indicates that the pressure change during

calibration is slow and the device is allowed to

come to equilibrium prior to taking a reading. Usual

calibration procedure involves a comparison of the

particular instrument with one of the following:

(1) primary standard;

(2) known input source;

10

than that of the instrument to be calibrated,

11

(1) comparing it with a standard pressure-measurement facility of the National Bureau of Standards (is very

expensive).

(2) direct calibration with a primary source of a known force applied normally over a full cross section area of the

pressure gage (rather complex).

(3) comparing it with a secondary standard (another gage of known accuracy). The term "known accuracy" means

here a gage which accuracy was specified by a reputable source.

Since first two possibilities are too expensive or complex, many instrument manufacturers use only third option

shown schematically in Fig.9. Calibrated gage and gage of known accuracy (secondary standard) connected to the

same pressure chamber. Since both

Gages are subject to equal pressure, the output of the secondary standard serves as measure of applied pressure,

which value is referred to the calibrated gage reply. A standardized procedure regulated by the document

ANSI/ISA (1979) note that the values of the applied pressure must cover the intended range of use of the pressure

gage to be calibrated. In the first step, using a fine pressure valve the pressure values are incrementally increased

from the low end of the range to the top end of the range. The pressure values are then incrementally reduced to

the low end of the range and this process is repeated several times (cycles). A final result is a set of the data which

include calibrated gage outputs as a function of the output of the secondary standard. A graphical presentation of

these data is known as the calibration curve which in most cases is correlated using a mathematical function using

the process of curve fitting. When correlating function is a straight line this results in a single value of the gage

sensitivity "s", for example [mv/Pa]. When correlating function is a parabola or a higher-order polynomial, the

obtained correlating function is used to convert the calibrated gage output to the pressure in real experiment. In

this procedure, the accuracy statement effectively combines system's contribution to the overall errors due to

nonlinearity, hysteresis and nonrepeatability.

6.4.1 Secondary standards

Calibration philosophy prefers the secondary standard (gage or measuring system) which are based on

simple and clear physical principles. This ensures the experimenter that calibration accuracy is really maintained.

Such simple and clear physical principle is base of McLeod gage, which used as a secondary standard for

calibrating vacuum measuring devices. In this gage a large volume of the low-pressure gas is firstly compressed

into a much smaller volume and then its pressure is measured as shown in Fig.10.

12

Initially, when the gage is connected to the vacuum source, the mercury is below point A, as shown on Fig.9a.

Thus, the gage is filled entirely with gas under a low pressure p. Next, the plunger is pushed downward until the

mercury rises to the level h2 in capillary tube 2. If the volume of the capillary per unit length is a, then, the

volume of the gas which contained within the length y of the capillary1 is

Vc ay

(1)

The volume of the capillary, bulb, and tube down to the point A is V. If we assume that the gas initially occupies a

volume V is further compressed isothermally in the capillary 1 to volume Vc , we have

since pc Vc p V

V

hence pc p

(2)

Vc

In the mode of operation in Fig. 9b, the level of h2 is the same as the top of capillary tube 1. Now, the

pressure indicated by the capillary is

pc p y

(3)

Using (2) one can obtain

pV

p c c

(4)

V

Since usually pc p , Eq.(3) becomes pc y which result in

y ay ay 2

p

ky 2

V

V

Note that parameter k a / V is characteristics of the manometer and the scale of capillary reads directly the units

of torr.

13

Advantages

2. The capillaries are calibrated directly in micrometers and any additional calibration of the gage is requested.

Disadvantages

1. Available for dry gases only that not condense when compressed into the capillary tube.

2. Experiments with large capacity of Hg are dangerous.

Example

A McLeod gage has V=100 cm 3 and a capillary diameter 1mm. Calculate the pressure indicated by a reading of

y 3.00cm. Calculate the error resulted by assumption that pc p

Solution.

Vc ay

(1mm )

2

30 mm 23.56 mm

4

3

V 100cm 105 mm3

y Vc 30mm 23.56mm3

7.068 m Hg

V

105 mm3

1mm Hg = 133.3Pa

3

3

7.068 10 133.3 942.16 10 Pa 0.94 Pa

p

V

23.56mm3

The fraction error resulted by assumption that pc p is c

2.36104 negligible small value.

5

3

V

10 mm

6.4.2 Dead-weight tester

The dead-weight tester shown in Fig. 11 is another example of mechanical device which based on a simple and

clear principle and used for calibration purposes. A sensitive element of this device is a fluid pressure within the

chamber. When balanced with a known weight this pressure used as a secondary standard for static calibration of

pressure gages.

Calibrated pressure gage G is connected to the chamber when the valve V is closed. To fill the tester with a clean

oils the plunger first moving to its most forward position. Withdraw the plunger slowly the oil is poured in

through the opening for the piston.

14

When the valve V is open the known pressure exerted on the fluid by the piston is now transmitted to the

calibrated gage. This pressure may be varied or by adding weights to the piston or by using different pistoncylinder combinations of varying areas.

Advantages

1. Wide range of the application: from1 to 1000 bar

2. Direct calibration by a known standard fluid pressure

Disadvantages

1. The accuracy of dead-weight testers is limited by two factors:

(a) The friction between the cylinder and the piston;

This factor can be reduced by rotation of the piston and use of long enough surfaces to ensure negligible flow of

oil through the annular space between the piston and the cylinder.

(b) The uncertainty in the area upon which the weight force acts.

This is neither the area of the piston nor the area of the cylinder; while it is some effective area which depends on

the clearance spacing and the viscosity of the oil. The smaller the clearance, the closer the effective area will

approximate the cross-sectional area of the piston. The percentage error due to this clearance varies according to

formula:

( p)1/2 b3

Percent error

=0.02 1%

DL

where = oil density; p = pressure differential on the cylinder; b = clearance spacing; = viscosity; D =

piston diameter and L = piston length. It is seen from this formula that at high pressures p when an elastic

deformation of the cylinder increases the clearance spacing, b rises and thereby the error of the tester also

increases. To overcome this disadvantage a pressure supplied by the tester acts simultaneously on calibrated gage

and on the secondary standard gage of known sensitivity as shown in Fig.9. Typical characteristics of several

pressure measuring devises

Device

Dead-weight tester

Range, torr

6

760 -

Relative error, %

0.02 -1.0

Bourdon-tube

1.0

Pirani gages

103 - 1.0

1012 - 1.0

2-7

0.2 - 760

6 - 10

0.02 -1.0

1-3

Ionization gage

U-manometers

McLeod gage

10

10

- 106

5 - 50

Questions to exam

1. Distinguish among gage pressure, absolute pressure and vacuum.

2. What are the advantages of the manometer pressure-measurement device?

3. What is the advantage of a well-type manometer?

4. What are some advantages of the bourdon-tube, diaphragm, and bellows gages?

5. Describe the principle of operation of a McLeod gage.

6. Describe the Pirani gage.

7. Describe the ionization gage.

8. How does ionization gage differ from the Pirani gage? What disadvantages does it have?

9. Describe the principle of operation and main disadvantage of Dead-weight tester.

10. The static calibration what is it means?

11. How many possibilities exist for static calibration of pressure gage?

12 Describe s standardized procedure of the static calibration of pressure gage.

15

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