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Copyright © 2007 by ABCM

**19th International Congress of Mechanical Engineering
**

November 5-9, 2007, Brasília, DF

**DETERMINATION OF THE INTRINSIC PERMEABILITY OF
**

MICROTOMOGRAPHIC IMAGES BY THE LATTICE BOLTZMANN

METHOD

Alysson Nunes Diógenes nunes@lmpt.ufsc.br

Carlos Enrique Pico, capico@lmpt.ufsc.br

Daniel Nalin, nalin@lmpt.ufsc.br

Celso Peres Fernandes, celso@lmpt.ufsc.br

Luís Orlando Emerich dos Santos, emerich@lmpt.ufsc.br

Paulo César Philippi, philippi@lmpt.ufsc.br

Universidade Federal de Santa Catarina

Laboratório de Meios Porosos e Propriedades Termofísicas

Campus Universitário – Trindade

Florianópolis/SC - Brasil - 88040-900

Abstract. The pore scale low Reynolds flow, in a high resolution tomographic image of a sedimentary rock, was

calculated by numerical simulation of the Navier-Stokes equations using the Lattice Boltzmann Method. These results

were used to investigate the influence of sample size on the determination of the intrinsic permeability. The size of the

representative elementary volume as a function of the autocorrelation length was estimated based on the permeabilities

obtained from simulation on several sub-domains. The permeability results of Lattice Boltzmann simulation for the

tomographic image and three dimensional reconstructed media from sections of the same sample were compared with

experimental results.

Keywords: Lattice Boltzmann Method, flow in porous media, Microtomographic Image, REV, Porous Media

Reconstruction

1. INTRODUCTION

Flow in porous media is analyzed in several scales: pore (microscopic), local (macroscopic) and field scales.

Dominant process and governing equations also vary with spatial scales. The latter scale is of more practical interest,

for example, for the problem of water resources and oil recovery. The macroscopic variables, related to the field scale,

e. g. permeability, are commonly defined as volume average of microscopic variables over a Representative Elementary

Volume (REV). The REV is well known concept and it is explained in detail by Bear (1972). The size of the REV is

believed to be large when compared to the pore dimension or solid particle structures, but small compared to the

dimension of the physical domain of interest in macroscopic analysis. Zhang et al. (2000) treated questions about what

is the actual size of a REV and how a REV varies inside a medium. In this work, the medium autocorrelation function

was computed and used as a basis to estimate the size of the REV.

The porous medium structure could be measured using a non-invasive technology, namely X-ray microtomography.

This technology has been successfully applied to rock geometries imaging and has addressed several problems about

REV and medium reconstruction. Specifically, the new technology of high resolution microtomography is able to obtain

three-dimensional images of rocks with a resolution of the order of one micrometer. These images have been also

successfully used in pore scale studies of flow in porous media (Zhang et al., 2000).

In this research we investigate the relation between the REV and the autocorrelation length, calculating the

permeability using the Lattice Boltzmann method (dos Santos et al. 2005). We also compare the permeability results of

the microtomographic sample with those of tridimensional media, reconstructed using the Truncated Gaussian (Liang et

al., 1998) and Simulated Annealing (Torquato and Kim, 2000) methods.

2. REV DETERMINATION METHODOLOGY

For the REV determination we used a microtomography obtained from a Botucatu sandstone which was measured in

the Petrobrás Research Facility (CENPES). This sample was scanned with a SKYSCAN 1172 X-Ray microtomograph

equipment using a resolution of 3.81μm. The porosity of this sample is 31.16% and its autocorrelation length is 40

voxels, comprising 152.4 μm. The experimental permeability measured was 5.000mD. The scanned microtomography

had 1503 voxels and can be observed in Fig. 1a, with the pore space shown in gray scale. A slice image, extracted

approximately at the middle of the sample, is shown in Fig. 1b.

The autocorrelation graphic and its autocorrelation length corresponding to the microtomography can be seen in the

Fig 2.

the particle distribution function. comprising 603. based in a special discretization of the Boltzmann transport equation. 1003.81μm resolution. defined in specific sites of a regular lattice. – Correlation – Corr. (2005). (1). Botucatu sandstone microtomography with 3. . evolves following the Lattice Boltzmann Equation with the Bhatnagar-Gross-Krook collision model. The procedure started subdividing the microtomography sample in smaller media. The Lattice Boltzmann Method (LBM) is a relatively new scheme for the simulation of the hydrodynamics of nearly incompressible fluids. Autocorrelation function (R[u]) and autocorrelation length (Integral[u]) from the microtomographic sample shown in Fig 1. f i ( x . For each one of these samples we calculated the permeability using the Lattice Boltzmann method described in dos Santos et al. 803. Lenght R(u) Integral (u) Displacement (um) Figure 2. Eq. 3D (a) and binarized 2D views (b) with edge size of 150 voxels. In the particular G implementation of this numerical method used in this work. t ) . 1203 and the complete 1503.(a) (b) Figure 1.

( ρ . t ) + . with a simple slice domain decomposition method in one direction. i G (2) G ρu = ∑ f i c i . t + δt ) = f i ( x . and the parameter τ is the relaxation time. u ). Brasília. 3 was used. t ) G G G f i ( x + ci δt . These choices simplify the Eq. linked by a set of velocity vectors ci . ρ = ∑ fi . DF G eq f i − f i ( x. The relaxation time was set as and a body force field was used to drive the flow. The three dimensional lattice with nineteen velocities used in the simulations. ρ 2 2 where p = ρc s and ν = cs (τ − 1 / 2) . (4) Figure 3. X is the body force and the mean velocity was calculated as the average value of the momentum of all fluid sites . 2007. (5) where φ is the porosity. (1) τ G G where x indicates vertices of a regular lattice. The permeability values were determined according to the Darcy law as τ =1 u = kφ ν X. a parallel version of the lattice Boltzmann method was written. δt denotes the time step. G The velocity u and density ρ are defined as macroscopic moments of the distribution function. (3) i A Chapman-Enskog multiscale analysis of the Lattice Boltzmann Equation gives the continuity and the NavierStokes equation for incompressible flows 1 ∂ t uα + u β ∂ β (uα ) = − ∂ α p + ν∂ β ∂ β (uα ) . (1) and allows the use of only G four real numbers. The explicit and local nature of the algorithm provides its straightforward implementation in parallel computers. usually called 3DQ19 lattice. to represent the state of a site. Using the MPI communication library. For all cases the 3D lattice with nineteen velocities presented in Fig.Proceedings of COBEM 2007 Copyright © 2007 by ABCM 19th International Congress of Mechanical Engineering November 5-9.

Table 1.500mD value. suggested also by previous simulation in reconstructed media. The microstructure size is 1203 and the resolution is the same as the microtomography. This medium does not retain the autocorrelation function. Figure 3 exposes a Truncated Gaussian reconstruction result. The sub-sample permeability results are given in Tab 1. For example. the three values are closed showing the isotropy of the Botucatu sandstone. however. Note that the method does not retain the pore sizes from the original microtomography. COMPARISON WITH RECONSTRUCTION METHODS We used two methods to reconstruct tridimensional structures from slices of the original tomographic sample. Results from permeability calculated in the microtomography slices.. 2000). Figure 3. We used the Truncated Gaussian method (Liang et al.62μm resolution is shown in Fig 4. which is very near to the experimental one. 3. a conservative estimative of the REV size. but it represents better the pore sizes as can be noted when the slice Fig.u = ∑ ρu x ∑ρ . A larger microtomographic sample. with sizes equal or greater than twice the autocorrelation length. as determined in the previous section. is necessary for a final conclusion. This problem is circumvented when the spatial resolution is reduced during the reconstruction process. Truncated Gaussian simulation with 1203 voxels. as its autocorrelation length is greater than the original one. 1b. to verify the reconstruction methods and the conclusions about the REV. . for the 803 sample the values are 3917. indicating that the slice should have. 4b is compared to Fig. twice the autocorrelation length to perform a valid simulation. 4520 and 4223 mD. 1998) and the Simulated Annealing method (Torquato and Kim. the intrinsic permeability k was calculated in the three orthogonal orientations and the mean value was taken as the representative value for each size. The instrinsic permeability of this reconstruction. This would also discard the first processed slice as a valid simulation. Nevertheless. at least. has the order of twice the autocorrelation length. Size in voxels Permeability k (mD) 60 5937 80 4220 100 4296 120 4961 150 4533 The permeability results exposed in the Tab. (6) x For every sub-sample. optimizing the autocorrelation and the linear chord functions. A reconstruction result with 7. Generally. 1 shows a stability tendency around the 4.

Reconstructed medium with 1203 voxels using Truncated Gaussian method with a half resolution of the original image. as it can optimize more parameters and represent better the original medium. The autocorrelation functions for the three media are shown in the Fig. DF The Fig. the reconstructed media by the Truncated Gaussian method underestimate considerably the permeability values. Reconstruction Method Size in voxels Permeability k (mD) Truncated Gaussian 80 676 Truncated Gaussian 120 722 Truncated Gaussian 150 677 Simulated Annealing 80 2. is more flexible. The latter method. (a) (b) Figure 4. Although the optimized functions were better fitted than the Truncated Gaussian method. As was predicted by the qualitative criteria of pore size comparison. The Truncated Gaussian method with decreased resolution provided the best results. Brasília. 2007. 2. we can see some non connected porosity scattered around the reconstructed medium. The black pixels are solid. 6. however. (a) 3D view (b) Transversal section. The Truncated Gaussian with half resolution and Simulated Annealing reconstructions also has lower values of the permeability.291 Truncated Gaussian with decreased resolution 120 3. This feature will be exploited in future works. The Lattice Boltzmann simulation results for permeability are shown in Tab. Table 2.512 . Permeability results for the reconstructed media.Proceedings of COBEM 2007 Copyright © 2007 by ABCM 19th International Congress of Mechanical Engineering November 5-9. This method is also remarkably faster than the Simulated Annealing method. showing that the reconstructed medium with the Truncated Gaussian does not retain the autocorrelation function. 5 shows the reconstruction result for the Simulated Annealing method.

. Autocorrelation functions from the microtomography and all the reconstructed media used in this research. The black pixels are solid. Annealing – Botucatu R(u) Displacement (um) Figure 6. (a) 3D view (b) Transversal section. do not represent the porous structure of the sandstone properly.(a) (b) Figure 5. – Red. particularly the pore size distribution. Because the strong dependency between the porous media structure details and the intrinsic permeability. are in progress. Truncated Gaussian and Simulated Annealing methods. these method was unable to furnish reliable values of the intrinsic permeability in this kind of porous media independently of the size of the sample. CONCLUSION AND DISCUSSION As was strongly suggested by the lattice Boltzmann simulations of nearly incompressible fluid flow in microtomographic reconstructed media from Botucatu sandstone. Results for more detailed microtomographic images and different sandstones as well as others three-dimensional reconstruction methods. Simulated Annealing reconstruction result with 803 voxels optimizing autocorrelation and the linear chord functions. 4. a conservative estimative of the size of the representative elementary volume is twice the autocorrelation length. Truncated Gaussian – Truncated Gaussian – Sim. The two reconstruction techniques used here.

Dover Publ. L. and diffusion coefficient of digitized composite media via first-passage-time equations. and statistical REV”. ACKNOWLEDGEMENTS Authors are greatly indebted with ANP (Agencia Nacional do Petroleo).. dos Santos. Liang. A reconstruction technique for three-dimensional porous media using image analysis and Fourier Transform. Kim. S. et al..O.E. “Prediction Of Intrinsic Permeabilities With Lattice Boltzmann Method”. CNPq (Conselho Nacional de Desenvolvimento Científico e Tecnológico ) and Finep (Fundação Nacional de Estudos e Pesquisas) for the financial support and to the CENPES-Petrobrás for providing the microtomographic samples used in this research. pp 1195-1198..Proceedings of COBEM 2007 Copyright © 2007 by ABCM 19th International Congress of Mechanical Engineering November 5-9. Zhang. REV. 7.. 85 (1999) 1560. Dynamics of Fluids in Porous Media. Brasília.C. Vol 27. “Pore scale study of flow in porous media: Scale dependency. Nº 8. et al. 1999. Chen.R. DF 5.. 1998. 21. Effective conductivity.. Soll. W.. D.. Geophysical Research Letters. 6. S.. New York. RESPONSIBILITY NOTICE The authors are the only responsible for the printed material included in this paper. Z. dielectric constant. 2000. 273-283. 2007. . R. J. Proceedings of the XVIII Brazilian Congress of Mechanical Engineering..E. Torquato. Zhang. Journal of Applied Physics. I.. REFERENCES Bear. 1972. Journal of Petroleum Science. 2005.

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