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Abstract
The tensile strength of aggregates is a dynamic property under field conditions and for any
given soil reflects the integration of processes leading to a strengthening and weakening of
failure zones. The objectives of this study were to determine if variation in the tensile strength
of natural aggregates from a red-brown earth could be related to the combined effects of (a)
conditions favouring dispersion of clay and a subsequent increase in strength by cementation on
drying and (b) wettingldrying cycles which would result in a decrease in strength. Aggregates
were collected from the A horizon of different long-term rotations. The seasonal variation
in tensile strength was assessed using data collected in 1988 and unpublished data which
had been collected annually between 1978 and 1981. Trends in tensile strength over 5 years
confirmed the importance of an interaction between climatic conditions which could lead to
increased dispersion of clay and wettingldrying cycles. The extent of weakening of failure
zones by wettingldrying cycles varied with the rotation. The nature of the impact of cropping
history on tensile strength was dependent on antecedent climatic conditions.
Keywords: Soil structure, aggregrate strength, climate.
Introduction
The soil matrix can be considered to be perforated with a three-dimensional
network of failure zones. The zones have a distribution of strengths and determine
the response of soil to stresses as diverse as tillage, raindrop impact and root
growth. Tensile strength is a measure of the strength of the weakest failure
zones (Braunack et al. 1979) and the distribution of strengths has been used as
a measure of soil friability (Utomo and Dexter 1 9 8 1 ~ ) .
Tensile strength is a dynamic property. The strength of failure zones at any given
time relates to the presence of air-filled pores, the occurrence of microcracks and
the strength of intergranular bonds within and between microcracks. Consequently
the tensile strength of soil is related to water content, and processes which change
pore characteristics and/or the cementation between structural units.
Cementing materials which alter the strength of failure zones may be of organic
or inorganic form. Changes in cropping practices can cause changes in the nature
of organic materials present and can cause progressive changes in tensile strength
over several seasons (Kay et al. 1988).
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Methods
Soils
Samples were taken from the C1 permanent rotation trial which was established in 1925 on
a red-brown earth, the Urrbrae fine sandy loam, at the Waite Agricultural Research Institute.
The rotations selected for sampling (Table 1) represented a range in organic carbon contents
and time from last tillage. Dates of sampling are given in Table 4.
Ten samples were collected from a plot at a depth of 0-5 cm, composited, air-dried
and then gently sieved into different sized fractions (19-9.5, 9.5-6.7, 6.74.0, 4.0-2.0,
2.0-1.0, 1.0-0.5, 0-5-0 25, <0.25 mm). Samples for tensile strength measurements alone
were collected from plots 11, 14, 15, 16, and 17 in 1978, 1979, 1980 and 1981. Samples for
tensile strength and dispersible clay measurements were taken from all of the plots in 1988
only. The plots were resampled in 1991 to determine the organic carbon, clay, silt and sand
contents of the 6.7-9.5 and 9.5-19 mm fractions. Organic carbon content was measured
using a LECO carbon analyser (there was no CaC03 in the samples). Particle size analyses
involved dispersion of samples with sodium hexametaphosphate and NaOH, shaking for 18 h,
determining the suspended clay content gravimetrically and removing the clay and silt to
determine the sand content. The silt content was calculated using the clay and total sand
contents.
Dispersible Clay
Air-dry aggregates (9 5-6.7 mm diameter) were wet up slowly with distilled water over a
2 week period on sintered glass funnels in order to minimize slaking. The water supply in the
funnels was maintained at -10.0 kPa. A vial filled with chloroform was taped to the inside
of each funnel in order to minimize microbial activity. After equilibration the aggregates were
carefully transferred to plastic vials with care being taken to minimize mechanical disturbance
of the aggregates. Additional distilled water was added to create water contents in excess
of saturation and the samples were equilibrated for 25 min. The amount of dispersed clay,
hereafter referred to as spontaneously dispersed clay, was then measured. Samples were
subsequently shaken end-over-end for 3.0 min, and the amount of dispersed clay, which will be
referred to as mechanically dispersed clay, was measured. Dispersed clay was measured under
the two conditions in order to distinguish between clay which dispersed by physico-chemical
forces as a consequence of the low electrolyte content (arising from the use of distilled water)
and clay which became dispersed as a consequence of the introduction of mechanical energy.
Measurements of spontaneously dispersed clay would be expected to be most relevant after
rainfall events when the ionic strength of the pore fluid has been reduced but there has been
little mechanical energy applied. Measurements of mechanically dispersed clay, on the other
hand, would be most relevant to the dispersion of clay by processes such as raindrop impact.
The two measurements of dispersible clay are not necessarily correlated. The amounts of
spontaneously and mechanically dispersed clay were measured using turbidimetric techniques
and were expressed as a per cent of the oven-dry (105OC) weight of the original aggregates.
Equilibration of the aggregates to a given water pontential and dispersion of the clay took place
in constant temperature rooms maintained at 20HC. Additional details on the prewetting
procedure and the determination of dispersible clay are provided in Kay and Dexter (1990).
Tensile Strength
The tensile strength of aggregates was calculated from the maximum compressive force
required to fracture air-dry aggregates (1% gravimetric water content) between flat parallel
Grant (1989).
Wheat-fallow
Continuous wheat
2 yr wheat-4 yr
pasture
Continuous pasture
Rotation
wheat
wheat
pasture
pasture
pasture
35
17
11
14
15
16
29
2 yr
1 yr
2 yr
4 yr
Plot
No.
Phase
in 1988
1.02
1.32
2.06
2-15
1-74
2.16
2-87
mm
6.7-9.5
0.96
1.28
1.90
2-18
1-71
2-20
2.58
9.5-19
mm
Organic carbon
13.1
12.2
13.2
12.8
16.6
14.1
14.1
6.7-9.5
mm
12.4
12.3
13.5
13.6
16.0
12.9
17.1
9-5-19
mm
Clay (%)
28.8
33.8
32.9
32.1
29.5
32.2
30.4
6.7-9-5
mm
29.6
33.8
31.8
30-8
30.0
35 7
26-0
9-5-19
mm
Silt (%)
58.0
54.1
53.9
55.1
53-9
53-7
55.5
6.7-9.5
mm
58.0
53.9
54-7
55.5
54.1
51-4
56.9
9.5-19
mm
Sand (%)
Table 1. Cropping history of plots and characteristics of aggregates 6.7-9.5 and 9 5-19 mm diameter
1-6dA
1-61A
1.50A
Bulk density
of clods
(Mg WK3)
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plates (Braunack et al. 1979). A value of 0.58 was used for the proportionality constant
relating maximum compressive stress to the tensile strength at failure. Twenty aggregates
(19-9.5 m m diameter) per sample were employed to determine the mean tensile strength of
aggregates collected between 1978 and 1981, whereas 40 aggregates were used from samples
collected in 1988.
The effect on aggregate tensile strength of wetting aggregates for long enough to permit
spontaneous dispersion of clay followed by air-drying aggregates was determined. Aggregates
(19-9.5 mm) from the 0-5 cm depth from each of the plots sampled in 1988 were wet-up over
a one week period by using the same procedure as outlined for dispersible clay measurements.
Aggregates were then equilibrated at -0.3 kPa water potential for a second week. An
additional set of aggregates from the 0-5 cm depth were equilibrated at -10.0 kPa potential
to determine if differences in the amounts of dispersible clay which had been observed at
these two potentials (Kay and Dexter 1990) influenced aggregate tensile strength on drying.
After equilibration, the sintered glass funnels were drained and the aggregates allowed to dry
slowly over a two week period in the funnels. Tensile strengths were then determined.
Climatological Records
Values of daily precipitation and evaporation were obtained from the weather station
adjacent to the site for each of the years in which sampling was done.
Statistical Analyses
Statistical analyses of the data were carried out using the computer software package SAS
(SAS Institute Inc. 1985). The significance level at which all analyses were evaluated was
P 5 0.05.
Soil Characteristics
The organic carbon and textural analyses are given in Table 1. The influence
of aggregate size on these properties was small and not significant. Larger
variations were noted, however, between the rotations. Organic carbon declined
in the sequence: continuous pasture, wheat/pasture, continuous wheat and wheat
fallow. These trends have been noted by other investigators working on the same
plots (e.g. Tisdall and Oades 1980). Small differences in textural characteristics
were also noted between the plots, with the highest clay content occuring on the
plots with most organic carbon and lowest where organic carbon was lowest.
Table 2. Spontaneously dispersible clay, Ms, mechanically dispersible clay, Mm, % of total
clay dispersible, M m f , and antecedent gravimetric water content, 8, of aggregates from different
rotations (samples collected in 1988)
Measurements were on 6.7-9.5 mm diameter aggregates equilibrated at -0.10 kPa water
potential. Rotations with the same superscript are not significantly different
Plot number
Ms (%)
Mm (%)
Mmf
(%)
(w/w)
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Dispersible Clay
Mechanically and spontaneously dispersible clay contents were measured on
aggregates 9.5-6.7 mm diameter (Table 2). The mechanically dispersed clay
content was about 50 times larger in magnitude than the spontaneously dispersed
clay content. A simple visual examination would have suggested the soils has no
spontaneously dispersible clay. The exchangeable sodium content (expressed as a
percentage of the total exchangeable cations present) of soil from the 0-5 cm depth
of plot 17 is 1% (Emerson 1968) and accounts for the relatively small amount
of spontaneously dispersible clay. The variation in spontaneously dispersible clay
with rotation may be due to variations in the exchangeable sodium content but is
more likely due to the role of organic matter in moderating the forces developed
in the electrical double layer.
The mechanically, M,, spontaneously, M,, dispersible clay contents we're
linearly correlated and described by the relation
The intercept was not significantly different from zero. A much stronger correlation
was obtained between these two variables than was obtained by Kay and Dexter
(1990) and is to be expected since aggregate size fraction was a constant in this
study, whereas aggregate size was a variable in the study conducted by Kay and
Dexter (M,, would be expected to be strongly dependent on aggregate size).
Values of M, and mechanically dispersible clay expressed as a percentage of
total clay, M,f, were strongly correlated with organic carbon content.
Table 3. Tensile strength of 19-9.5 mrn diameter aggregates from different rotations, before
and after wetting to - 0 . 3 kPa water potential and then drying (samples collected in 1988)
Plots with the same superscript are not significantly different (comparisons within columns)
Plot number
29
11
14
15
16
17
35
Mean
41bC
62"
43bC
67"
65"
35C
48b
52
Tensile Strength
The tensile strengths of aggregates 19-9.5 mm in diameter are summarized
in Table 3. Significant differences existed between plots. A stepwise multiple
regression did not indicate, however, that the coefficients for independent variables
such as organic carbon or total clay content had a significant influence on tensile
strength.
The tensile strength of aggregates from the different plots did not show a
large increase in tensile strength after being wet-up under conditions which would
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enhance the spontaneous dispersion of clay followed by slow drying (Table 3).
Only plots 29, 14 and 35 showed a significant increase in strength. A significant
difference between the different plots persisted after the wettingldrying treatment.
No difference in the tensile strengths of aggregates were observed when they
had been wet to -10kPa as compared with wetting to - 0 . 3 kPa prior to
air-drying. There obviously was not enough clay which spontaneously dispersed,
or cementing materials dissolved at either potential to cause a large increase in
strength on drying. Under field conditions, rainfall may mechanically disperse
more clay at the soil surface, thereby increasing the strength on drying. This
would, however, have to compensate for greater slaking than would have occurred
under the wetting conditions used in the laboratory.
Table 4. Characteristics of tensile strength and climatic conditions preceding sampling in
different years
Description
Date/Value
Tensile strength
5 Nov. 17 Oct. 14 Apr. 23 Nov.
1981
1980
1978
1979
49 9
58-9
69.4
63.3
52.8
9 Dec.
1988
59.3
66.5
Climatic conditions
Characteristics of wet periodA
Starting date (day number)
Duration (days)
Total precipitation (mm)
Total precipitation minus
evaporation (mm)
Maximum daily precipitation (mm)
Characteristics of largest daily precipitationB
Date (day number)
Precipitation (mm)
Number of wetting events between
sampling and antecedentC
wet period
Largest daily precipitation event
5 Aug. 3 Sept.
1978
1979
(217)
(246)
6
11
57.6
83.2
51.2
20.4
74.6
30.6
6 July
1978
(187)
28.4
6 Sept.
1979
(249)
30.6
12
17
7
7
4 June
1988
(156)
7
75.0
3 Sept.
1979
(246)
11
83.2
2 July
1981
(183)
5
59.2
6 Sept.
1979
(249)
30.6
23 June 23 May
1981
1988
(174)
(144)
22.8
41.2
A First period dating backwards from time of sampling in which the total precipitation minus
evaporation is equal to or greater than 40 mm and daily values greater than 0 mm.
In auntumn, winter or spring (rainy season) preceding sampling date.
Daily precipitation is equal to or greater than 4 rnm. Successive days in which precipitation
minus evaporation is greater than zero counted as single event.
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300
Julian day
Fig. 1. Daily precipitation and cumulative precipitation minus evaporation for 1979 and
early 1980.
the tensile strength data for plots 11, 14, 15 and 16 were pooled for comparison
with plot 17 for each of the five sampling years (Table 4).
Meteorological data, from the weather station adjacent to the site, were obtained
for each of the years in which sampling was done. Daily precipitation and
cumulative precipitation minus pan evaporation for 1979 and early 1980 are given
in Fig. 1 and illustrate climatic conditions at the site. There is an annual moisture
deficit and a large number of precipitation events during the winter rainy season.
Often the precipitation events are of sufficient magnitude and daily frequency
as to result in positive values of daiIy precipitation minus evaporation persisting
over several successive days. Such conditions would accentuate opportunity for
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spontaneous dispersion of clay due to the high water content and low electrolyte
content in the pore fluid. An extended wet period also makes clay in exposed
surface soils particularly susceptible to mechanical dispersion by raindrop impact
during storms. Frequent drying conditions and small intermittent rainfall provide
opportunity for wetting and drying cycles.
Analysis of the precipitation and cumulative precipitation minus evaporation
data was based on the premise that the tensile strength at any time is a
result of the number of wettingldrying cycles between the date of sampling and
the last date on which dispersion of clay and cementation was maximal. Two
criteria were used to identify the latest date of maximum dispersion of clay.
First, precipitation data were analysed to determine the date and amount of
the largest daily precipitation prior to sampling during the rainy season, thereby
indicating when mechanically dispersed clay may have been greatest. Second,
data on precipitation minus evaporation were analysed to determine the date
and characteristics of the last wet period prior to sampling, thus indicating when
spontaneous dispersion of clay would have been maximum. A wet period was
arbitrarily defined as a period in which the daily values of precipitation minus
evaporation were zero or positive and the cumulative values over the period were
equal to or greater than the total amount of water which would exist in the
top 10 cm of the profile when fully saturated. This value was taken as 40 mm
and was based on an average bulk density across the different rotations of 1.6
Mg m-3 (Table 1). The characteristics of the wet period and the largest daily
precipitation are given in Table 4. In two of the five years, the maximum daily
precipitation occurred within the wet period. The duration of the wet period
varied from 5 to 11 days ,total precipitation varied from 58 to 83 mm, and total
precipitation minus evaporation varied from 51 to 75 mm.
Wetting and drying events were arbitrarily defined as those in which the daily
precipitation was equal to or greater than 4 mm. When such days were followed
by days in which precipitation minus evaporation was greater than zero the data
were considered to represent a single event. The number of wettingldrying events
was then calculated, dating backwards from the time of sampling to either the
first wet period or the largest daily precipitation event during the preceding rainy
season. The numbers of cycles calculated by the two methods were very similar
for four of the five years and ranged from 7 to 19 (Table 4). The dates of both
the latest wet period and the largest daily precipitation in 1980 coincide with the
dates in 1979. This situation arose because of the date of sampling in 1980 and
the limited precipitation between the two sampling dates (Fig. 1). Consequently,
changes in tensile strength between 12 Oct. 1979 and 14 Apr. 1980 must relate
to the number of wetting and drying cycles which occurred between the sampling
dates.
Regression of tensile strength with numbers of wettingldrying cycles showed
that tensile strengths were negatively correlated with both the number of wetting
and drying cycles dating from sampling back to the most recent wet period, and
also the number of cycles dating back to the date of maximum daily precipitation.
The correlation with tensile strength was slightly higher when wetting and drying
cycles were calculated dating from sampling back to the most recent wet period,
the relation between these variables is illustrated in Fig. 2 for plot 17 and the
pooled values of plots 11, 14, 15 and 16.
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r Plot 17
o Mean plot 1 1 , 14,15,I6
5
10
15
20
Number of wetting events after wet period
Fig. 2.
Relation between the number of wetting events after the last wet period prior to
sampling and the tensile strength of aggregates from the 2 yr wheat-4yr pasture rotation
(plots 11, 14, 15 and 16) and the continuous wheat rotation (plot 17).
The intercepts of the two lines in Fig. 2 were significantly different, with
the highest tensile strength at zero wetting events after the wet period being
associated with plot 17. Plot 17 had significantly more mechanically dispersible
clay than either plots 11, 14, 15 or 16. The relation between these two intercepts
is compatible with the observation that the strength of a moulded red-brown
earth after air-drying increases with dispersible clay content (Shanmuganathan
and Oades 1982). The process of moulding at water contents close to the plastic
limit would create a uniform distribution of failure zones in the soil in the moist
state and therefore differences in strength on drying must be due to the cementing
action of different amounts of dispersible clay.
The slopes of the lines in Fig. 2 indicate that the creation or weakening
of failure zones by differential swelling or shrinking during wetting or drying,
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Conclusions
Two important conclusions arise from this study:
Significant trends in tensile strength over five years could be discerned by
applying a relatively simple analysis to precipitation and evaporation data.
The analysis confirmed the importance of climatic conditions which could
lead to increased dispersion of clay thereby resulting in an increase in
tensile strength on drying, and wetting and drying cycles which could lead
to a decrease in tensile strength. The analysis was unable to distinguish
between extended wet periods which would maximize the spontaneous
dispersion of clay and high precipitation events which woiild maximize
the mechanical dispersion of clay as causes of increasing tensile strength.
(ii) The extent of strengthening of failure zones by cementation and the
extent of weakening of failure zones by wetting and drying cycles varies
with the rotation. Conversely, the impact of rotation on tensile strength
varies with antecedent climatic conditions. The relation between tensile
strength and dispersible clay may vary with antecedent wettirig/drying
conditions.
The degree to which these conclusions apply to other soils with similar
climatic conditions would be expected to relate to the amounts of dispersible clay,
opportunities for this clay to function as a cement in microcracks on drying and
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Acknowledgments
Travel funds were provided to B. D. Kay by the University of Adelaide and the
Natural Sciences and Engineering Research Council of Canada to support this
collaborative research project. Assistance with statistical analyses was provided
by Dr V. Rasiah. Soil characterization was completed by Dr C. D. Grant.
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