Manual 6650SP

OPERATING INSTRUCTIONS FOR
MODEL 6650SP-XD
UV Fluorescence Analyzer
P/N:M6650SP-A
8/25/15
DANGER
Toxic gases and or flammable liquids may be present in this monitoring system.
Personal protective equipment may be required when servicing this instrument.
Hazardous voltages exist on certain components internally which may persist for a
time even after the power is turned off and disconnected.
Only authorized personnel should conduct maintenance and/or servicing. Before
conducting any maintenance or servicing, consult with authorized
supervisor/manager.
Teledyne Analytical Instruments

P/N M
04/19/2011
Model 6650SP-XD
Copyright 2015 Teledyne Analytical Instruments

All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed,
stored in a retrieval system, or translated into any other language or computer language in
whole or in part, in any form or by any means, whether it be electronic, mechanical,
magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne
Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 91748.
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us free from
defects of material and of construction, and that our liability shall be limited to replacing or
repairing at our factory (without charge, except for transportation), or at customer plant at
our option, any material or construction in which defects become apparent within one year
from the date of shipment, except in cases where quotations or acknowledgements provide
for a shorter period. Components manufactured by others bear the warranty of their
manufacturer. This warranty does not cover defects caused by wear, accident, misuse,
neglect or repairs other than those performed by Teledyne or an authorized service center.
We assume no liability for direct or indirect damages of any kind and the purchaser by the
acceptance of the equipment will assume all liability for any damage which may result from
its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus,
and to make any alterations in the dimensions, shape or weight of any parts, in so far as
such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which
valuable data can be gathered. The information provided by the instrument may assist the user
in eliminating potential hazards caused by his process; however, it is essential that all
personnel involved in the use of the instrument or its interface, with the process being
measured, be properly trained in the process itself, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process
conditions. While this instrument may be able to provide early warning of imminent danger,
it has no control over process conditions, and it can be misused. In particular, any alarm or
control systems installed must be tested and understood, both as to how they operate and as
to how they can be defeated. Any safeguards required such as locks, labels, or redundancy,
must be provided by the user or specifically requested of Teledyne at the time the order is
placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser
is responsible for the training of personnel, for providing hazard warning methods and
instrumentation per the appropriate standards, and for ensuring that hazard warning devices
and instrumentation are maintained and operated properly.
Teledyne Analytical Instruments, the manufacturer of this instrument, cannot accept
responsibility for conditions beyond its knowledge and control. No statement expressed or
implied by this document or any information disseminated by the manufacturer or its
agents, is to be construed as a warranty of adequate safety control under the users process
conditions.
ii
Model 6650SP-XD
Safety Messages
Your safety and the safety of others are very important. We have
provided many important safety messages in this manual. Please read
these messages carefully.
A safety message alerts you to potential hazards that could hurt you
or others. Each safety message is associated with a safety alert symbol.
These symbols are found in the manual and inside the instrument. The
definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the instructions
for details on the specific danger. These cautions warn of
specific procedures which if not followed could cause bodily
Injury and/or damage the instrument.
CAUTION: HOT SURFACE WARNING: This warning is
specific to heated components within the instrument. Failure
to heed the warning could result in serious burns to skin and
underlying tissue.
WARNING: ELECTRICAL SHOCK HAZARD: Dangerous
voltages appear within this instrument. This warning is
specific to an electrical hazard existing at or nearby the
component or procedure under discussion. Failure to heed this
warning could result in injury and/or death from
electrocution.
Technician Symbol: All operations marked with this symbol
are to be performed by qualified maintenance personnel only.
NOTE: (No symbol). Additional information and comments

regarding a specific component or procedure are highlighted
in the form of a note.
CAUTION:
THE ANALYZER SHOULD ONLY BE USED FOR THE

PURPOSE AND IN THE MANNER DESCRIBED IN
THIS MANUAL.
iii
Model 6650SP-XD
IF YOU USE THE ANALYZER IN A MANNER OTHER

THAN THAT FOR WHICH IT WAS INTENDED,
UNPREDICTABLE BEHAVIOR COULD RESULT
POSSIBLY ACCOMPANIED WITH HAZARDOUS
CONSEQUENCES.
This manual provides information designed to guide you through

the installation, calibration and operation of your new analyzer. Please
read this manual and keep it available.
Occasionally, some instruments are customized for a particular
application or features and/or options added per customer requests.
Please check the front of this manual for any additional information in
the form of an Addendum which discusses specific information,
procedures, cautions and warnings that may be peculiar to your
instrument.
Manuals do get lost. Additional manuals can be obtained from
Teledyne at the address given in the Appendix. Some of our manuals are
available in electronic form via the internet. Please visit our website at:
www.teledyne-ai.com.
iv
Model 6650SP-XD
Table of Contents
Safety Messages............................................................................iii
Table of Contents............................................................................
List of Figures..............................................................................viii
List of Tables..................................................................................ix
Introduction.....................................................................................
1.1 Introduction
1.2 Model 6650 Components
1.2.1 PX2 Photometric Transmitter
1.2.2 Control Unit
1.2.3 Xenon UV Source
1.2.4 Flourescence Probe
1.3 Optional Components
1.4 User Interface
1.4.1 Displays
1.4.2 Control Unit Front Panel
1.4.2.1 UP/DOWN Switch
1.4.2.2 ESCAPE/ENTER Switch
1.5 Equipment Interface
1.5.1 Electrical Connector Panel
Theory of Operation......................................................................11
2.1 Fluorimetry
11
2.2 Filter Based Flurometer Description
12
2.3 Model 6650 Theory and Terminology
12
2.3.1 Excitation Filter
13
2.3.2 Emission Filter
14
2.3.3 Measure Detector
14
2.3.4 Source Reference Detector
14
Model 6650SP-XD
2.3.5 Background Fluorescence

2.3.6 Sensitivity
2.3.7 Specificity
2.3.8 Signal-to-Noise Ratio
2.3.9 Signal-to-Background Ratio
2.3.10 Dynamic Range
2.3.11 Linearity
2.3.12 Process Background
14
14
15
15
15
16
16
16
Installation.....................................................................................17
3.1 Unpacking and Mounting the Analyzer
17
3.2 Electrical
19
3.2.1 Primary Input Power
20
3.2.2 Fuse Installation
21
3.2.3 Analog Outputs
21
3.2.4 Alarm Relays
23
3.2.5 Digital Remote Cal Inputs
24
3.2.6 Network I/O
25
3.2.7 RS-485
25
3.3 Fiber Optic Cables
26
3.4 Probe Installation
27
3.5 Sample Handling System
27
3.6 First Time Power Up and Initialization
27
3.7 Calibration
27
Setup & Operation.........................................................................29
4.1 Interface Panel
29
4.2 Control Unit
30
4.2.1 Mode/Function Selection
31
4.2.1.1 CALC Mode
31
4.2.1.2 Setup Mode
31
4.2.2 Data Entry
33
4.2.2.1 ENTER
33
4.2.2.2 ESCAPE
33
vi
Model 6650SP-XD
4.3 CALC (Analyze)

4.4The PWD (Password) Function
4.4.1 Entering the Password
4.4.2 Installing or Changing the Password
4.5 The LOGOUT Function
4.6 The VERSION Screen
4.7 The SELF-TEST Function
4.8 The Zero and Span Functions
4.8.1 Calibration Preparations
4.8.1.1 Equipment Required
4.8.1.2 Calibration Frequency
4.8.1.3 Preparation
4.8.1.4 Calibration Fluid Preparation
4.8.1.5 Calibrating the Control Unit
4.8.2 Zero Calibration
4.8.3 Span Calibration
4.9 The ALARMS Function
4.10 Alarm Test Function
4.11 The RANGE Function
4.12 Show Negative Function
4.13 The 4-20 Test Function
4.14 The STANDBY Function
4.15 Transmitter Interface Panel
34
34
35
36
37
38
38
39
39
39
40
40
40
42
42
43
44
46
47
47
48
48
49
Maintenance & Troubleshooting.................................................51

5.1 Application Engineering
51
5.2 Diagnostic Messages
51
Appendix........................................................................................53
A.1 Specifications
53
A.2 Spare Parts Listing
54
A.3 Reference Drawings
54
vii
Model 6650SP-XD
List of Figures
Figure 1-1: Model 6650SP-XD Components....................................

Figure 1-2: PX2 Photometric Module................................................
Figure 1-3: Model 6650SP-XD Control Unit Front Panel..................
Figure 1-4: Fluorescence Probe.......................................................
Figure 1-5: Front Surface Probe Design Features............................
Figure 1-6: Electrical Connector Panel.............................................
Figure 2-1: Molecular Fluorescence Example................................11
Figure 2-2: Operating Principles of the Model 6650.......................13
Figure 3-1: System Component Location and Identification...........18
Figure 3-2: Required Front Door Clearance...................................19
Figure 3-3: Electrical Connector Panel..........................................20
Figure 3-4: Primary Input Power Connections................................21
Figure 3-5: Analog Output Connections..........................................22
Figure 3-6: Types of Relay Contacts...............................................23
Figure 3-7: Optical Cable Installation..............................................26
Figure 3-8: Typical Piping Diagram.................................................28
Figure 4-1: Control Unit Interface....................................................30
Figure 4-2: Hierarchy of Available Functions..................................32
Figure 4-3: UV Transmitter Interface Panel....................................50
viii
Model 6650SP-XD
List of Tables
Table 3-1: Analog Concentration OutputExample.......................22
ix
Model 6650SP-XD
DANGER
FLAMMABLE LIQUID USAGE
WARNING
The analyzer is housed in an explosion proof housing and is

designed for use in a Class 1, Division 1, Group B, C, D
environment. It is the customer's responsibility to ensure
safety especially when flammable liquids are being analyzed
since the potential of leaks always exist.
The customer should ensure that the principles of operating
of this equipment are well understood by the user. Misuse of
this product in any manner, tampering with its components,
or unauthorized substitution of any component may
adversely affect the safety of this instrument.
Since the use of this instrument is beyond the control of
Teledyne, no responsibility by Teledyne, its affiliates, and
agents for damage or injury from misuse or neglect of this
equipment is implied or assumed.
Model 6650SP-XD
Introduction
Introduction
1.1 Introduction
The Model 6650SP-XD UV Fluorescence Analyzer is a
sophisticated instrument designed to measure an oil concentration in
water. It consists of a Control Unit, PX2 Photometric Transmitter, and an
integrated Fluorescence Probe. The Analyzer is housed in an explosion
proof housing with a window providing visual access to the control unit
display. Operational controls are conveniently located on the outer door
of the enclosure so the unit can be operated without having to open the
door.
The PX2 Photometric Transmitter is a dedicated module that
includes a flashed xenon UV light source, detectors and filters plus input
and output connections for the probe. It communicates with the control
unit via a digital RS485 connection. The transmitter is configured at the
factory to produce a highly selective, narrow UV band of radiation to
optically stimulate a target species (the analyate) in a solution. The
excited molecules almost immediately return to a ground state with a
corresponding longer wavelength emission whose signature is
characteristic of the oil species in solution. The Model 6650SP-XD
precisely measures the corresponding fluorescence emission and the
control unit converts signal and displays the concentration in units
convenient to the end user.
The analyzer is equipped with configurable high and low
concentration alarms, a system failure alarm with digital and analog
output signals for process control and measurement. An integral probe
interfaces with the process and transmits optical signals to and from the
sample.
1.2 Model 6650 Components

The Model 6650SP UV Fluorescence Analyzer consists of four
major components:
PX2 Transmitter
Introduction
Control Unit
Integrated Fluorescence Probe
Fiber Optic Cables
A typical Model 6650SP is shown in Figure 1-1. The Model

6650SP Analyzer depicted is a bulkhead mounting instrument designed
to measure a specific component of interest in a solution. The Model
6650SP is a highly configurable system and is often modified for a
particular application. Any non-standard modifications to the instrument
that affect the operation, specifications, maintenance, replacement parts
listing etc. are described in an addendum. Check the front of this manual
for any addendum that may pertain to your instrument.
Figure 1-1: Model 6650SP-XD Components

1.2.1 PX2 Photometric Transmitter
The PX2 Transmitter is the heart of the Model 6650SP-XD. It
houses the measurement and reference detectors, filters, UV light source
and associated electronics for data collection and signal pre-processing
from the incoming radiation from the sample probe. The collected data
is averaged and passed to the control unit for signal processing and
display through the RS-485 port.
Model 6650SP-XD
Introduction
The PX2 Transmitter is carefully configured and tested at the

factory for your specific application. The unit can be reconfigured if
necessary via a USB connection with a remote computer. Contact the
factory for further information on reconfiguring or making changes to
the PX2 setup.
A self-testing routine is installed in the module with multi colored
LEDs indicating status: in test, unit ok, or a fault condition. The
indicators will light up and cycle through a series of colors (blue, red,
green, purple, light green, aqua, and blue) as the unit is supplied with
power. Once the LED has returned to solid blue, the unit is ready for
operation. The PX2 module is shown in Figure 1-2.
The transmitter operates from a dedicated 24VDC power supply
mounted adjacent to the transmitter. See Figure 1-1.
Figure 1-2: PX2 Photometric Module

1.2.2 Control Unit
In addition to acting as the main user interface, the Model 6650SPXD Control Unit is responsible for signal conditioning, display output,
alarm handling, output signal generation, and instrument calibration.
Introduction
The PX2 Transmitter outputs the fluorescence level as a raw signal

which is the average of many readings per second and outputs it to the
controller via the RS-485 port. The control unit takes the raw count
signal from the Transmitter, conditions and linearizes it, then displays
the output in meaningful engineering units such as ppm. It also provides
user functions such as alarm configuration, and calibration control.
Figure 1-3 shows the front panel interface of the Model 6650
Control Unit. The unit is mounted on the front door of the system
enclosure. See Section 4.2 for information on using the interface panel.
Figure 1-3: Model 6650SP-XD Control Unit Front Panel
1.2.3 Xenon UV Source

Unlike many fluorescence units on the market, the Model 6650SPXD utilizes a xenon flash lamp to provide excitation energy in the form
of UV radiation. The lamp, installed inside the PX2 transmitter module,
allows the analyzer to be easily configured to meet the excitation
wavelength requirements for different applications by using appropriate
Model 6650SP-XD
Introduction
filters (also installed within the transmitter) to block all but a narrow
spectral range. The xenon flash lamp also has an extended lifetime
compared to other common UV sources (deuterium, mercury vapor, etc.)
thus reducing the cost of ownership of the analyzer.
1.2.4 Flourescence Probe
The integrated fluorescence probe is shown in Figure 1-4. It uses
fiber optic cables to deliver excitation energy to the sample fluid and to
return the collected fluorescence signal to the UV transmitter.
The probe is configured with a front surface design which has
important advantages over conventional probe design:
No moving parts
Rugged sapphire spherical lens
Constant focal length and sample volume
Delivered optical energy is concentrated via a ball lens

producing a greater excitation energy
Effective sampling of liquids, slurries, powders, pastes and solids
Particle size has minimal effect on optical performance
Figure 1-4: Fluorescence Probe

In addition, the fluorescence probe easily installs in a 1/2 or metric
13 mm tube fitting for sampling in the process fluid. As shown in Figure
Introduction
1-5, the front surface design produces a probe which is unaffected by

solids or solution reabsorption of either excited or emitted wavelengths.
Figure 1-5: Front Surface Probe Design Features
1.3 Optional Components

Although each Model 6650SP is specific to a particular species of
interest, it is a versatile instrument and can readily be modified to suit a
wide variety of environments and applications. Contact TAI Customer
Service with your specific requirements. Some common modifications
and options are listed below:
Z- or X-Purged Enclosure
Ultrasonic Homogenizer
Integrated Sample System with Water/Steam Flush
1.4 User Interface

1.4.1 Displays
Digital Meter Display: The meter display is a LED device that
produces large, bright, 7-segment numbers that are legible in any
lighting. It produces a continuous readout from 0-10,000 ppm and then
switches to a continuous percent readout from 1-25%. It is accurate
across all analysis ranges without the discontinuity inherent in analog
range switching. It is identified as Concentration Display in Figure 1-3.
Alphanumeric Interface Screen: The backlit VFD screen is an
easy-to-use interface from operator to analyzer. It displays values,
Model 6650SP-XD
Introduction
options, and messages that give the operator immediate feedback. It is

identified as Setup Display in Figure 1-3.
1.4.2 Control Unit Front Panel
The operator interacts with the analyzer primarily through the two
switches mounted on the front door of the explosion proof housing. See
Figure 1-3.
1.4.2.1 UP/DOWN SWITCH
Functions: The UP/DOWN switch is used to select the function to

be performed. Choose UP or DOWN to scroll through the following list
of thirteen functions:
Calc
Toggles readout between sensor output and concentration.
PWD
Install a password to protect your analyzer setup.
Logout
Locks Setup Mode.
Version
Displays model and version of analyzer.
Self-Test
Runs internal diagnostic program, displays results.
Span
Span calibrate the analyzer.
Zero
Zero calibrate the analyzer.
Alarms
Set the alarm setpoints and attributes.
Range
Set up the 3 user definable ranges for the instrument.
Negative
Display negative values.
4-20 Test
Routine to test analog output.
Alarm Test
Routine to test concentration alarms.
Standby
Leave analyzer powered, but no outputs or displays.
WARNING:
THE POWER CABLE MUST BE DISCONNECTED TO

FULLY REMOVE POWER FROM THE INSTRUMENT.
Sub functions: Once a function is entered, the UP/DOWN switch

is used to select between any sub functions displayed on the VFD setup
screen.
Introduction
Parameter values: When modifiable values are displayed on the

VFD, the UP/DOWN switch can be used to increment or decrement the
values.
1.4.2.2 ESCAPE/ENTER SWITCH
Data Entry: The ESCAPE/ENTER switch is used to input data,

from the alphanumeric VFD setup screen into the instrument:
Escape
MovesVFDdisplaybacktothepreviousscreenina
series.Ifnoneremains,returnstotheAnalyze
screen.
Withsubfunctionselected,movesVFDback
throughitemsonscreen,tofirstitem,thenmoves
VFDtopreviousdisplay.
Enter
Withasubfunctionselected:MovesVFDontothe
nextscreeninaseries.Ifnoneremains,returnsto
theAnalyzescreen.
Withavalueselected:Entersthevalueintothe
analyzerasdata.AdvancesVFDtonextoperation.
(SeeChapter4fordetails.)
Calibration, alarm indication, alarm setpoints, and range
configuration are other functions performed from this panel. See Section
4.2.
1.5 Equipment Interface

1.5.1 Electrical Connector Panel
The electrical connector panel, shown in Figure 1-6, contains the
electrical connections for external inlets and outlets. The connectors are
described briefly here and in detail in the Installation chapter of this
manual.
CAUTION: The power cable must be disconnected to fully
remove power from the instrument.
Model 6650SP-XD
Introduction
Electrical Connections: The electrical connections on the

electrical connector panel are described briefly here, and in more detail
in chapter 3 Installation.
Figure 1-6: Electrical Connector Panel

PowerConnection
115or230VAC,50or60Hz.
AnalogOutputs
01VDCconcentrationplus01VDC
rangeIDandisolated420mADC
plus420mADCrangeID.
AlarmConnections
2concentrationalarmsand1system
alarm.
USBPort
USBconnectiontoremotecomputer.
RemoteValves
Usedforcontrollingexternal
solenoidvalves,ifdesired.
ProbeConnection
LightsignalsinandoutofPX2
Transmitter.
Introduction
RemoteSpan/Zero
Digitalinputsallowexternalcontrol
ofanalyzercalibration.
CalibrationContact
Tonotifyexternalequipmentthat
instrumentisbeingcalibratedand
readingsarenotmonitoringsample.
RangeIDContacts
Fourseparate,dedicated,rangerelay
contacts.Low,Medium,High,Cal.
NetworkI/O
Serialdigitalcommunicationsfor
localnetworkaccess.
10
Model 6650SP-XD
Theory of Operation
Theory of Operation
2.1 Fluorimetry
The ability to monitor the concentration of an analyte in a process
stream is critical for accurate and reliable process control. There are
many techniques used to determine the analyte concentration of interest.
One of the most sensitive sensing techniques is molecular fluorescence.
Fluorescence occurs when a molecule absorbs light energy, either
ultraviolet or visible, and rapidly emits light, at some longer wavelength.
Fluorescence of this type is referred to as Stokes fluorescence.
Fluorimetry characterizes the excitation and emission properties of the
molecular species. Figure 2-1 shows an example of the excitation and
emission spectrum from a hypothetical fluorophore.
Fluorimetry is concerned with two types of information:
The (spectral) wavelength distribution, which is characteristic of

the electronic properties of the molecule
The intensity of the fluorescence, which is typically correlated to

the concentration of the fluorescent molecule in the solution
Figure 2-1: Molecular Fluorescence Example
11
Theory of Operation
2.2 Filter Based Flurometer Description

The transmitter, as used the Model 6650SP series, is a filter-based
analyzer which measures the ability of an analyte of interest to absorb
light in a narrow spectral region and emit light at a longer wavelength.
The Model 6650SP is a filter-based transmitter, and represents a good
analytical tool to use when quantitative measurements are desired for a
specific analyte in a process. Additionally, the Model 6650SP provides a
relative measurement and can be calibrated with known concentration
standards or correlated to measurements using standard laboratory
methods resulting in a quantitative fluorescence.
The PX2 transmitter in the Model 6650SP uses optical filters to
provide specific excitation or emission wavelengths for molecular
fluorescence. In this instrument the filters are located internal to the
transmitter and are specific to the application. Therefore, the analyzer is
a dedicated instrument for precise measurement of only one specific
analyte of interest. The filter sets used to configure the instrument are
specific to the analyte of interest. In order to monitor a new analyte of
interest, the user must return the instrument to TAI for factory
reconfiguration. The Model 6650SP can be used for both quantitative
measurements (determination of analyte concentration) and control
measurements (switching of valves once a fluorescence level is attained,
for example). In some circumstances, the instrument can monitor other
species of interest that are known to fluoresce within the same spectral
band. This will require a special initialization setup and must be done in
coordination with TAI Customer Service. In all likelihood, without
extensive testing as performed at the factory during initial setup, the
analyzer will not provide a quantitative result for any species other than
the component it was designed to analyze.
2.3 Model 6650 Theory and Terminology

As depicted in Figure 2-2, the Model 6650SP works as follows: The
light source within the PX2 module launches excitation light into a fiber
optic cable. The fiber optic cable transfers the excitation light to the
fluorescence probe mounted in the process. The fluorescence probe
launches light into the process sample, and collects the molecular
fluorescence (emission) from the sample. The emission light is then
transferred from the probe through fiber optic cable back to the
transmitter. The emission light passes through an emission filter in order
to remove any residual excitation energy collected by the fluorescence
12
Model 6650SP-XD
Theory of Operation
probe. The emission light then impinges on a detector which converts

the fluorescence intensity to an electronic signal. The detector output is
passed to the control unit where it is processed and the results displayed
on the control unit display panel.
The dedicated control unit in the Model 6650SP handles
linearization and signal conditioning so that the display indication is in
appropriate units (parts per million, ppm) for the application.
Arbitrary units (counts) can be useful when analyzing a species
whose fluorescence is unknown or the range is unknown. For this
purpose, a detector output count reading is available for selection and
display on the control unit display.
Figure 2-2: Operating Principles of the Model 6650
2.3.1 Excitation Filter

The excitation filter is used to select the range of wavelengths,
often referred to as the pass band, that is used to cause or excite the
molecular fluorescence. Wavelengths not in the pass band are rejected
and ideally never reach the sample. The removal of wavelengths outside
the pass band minimizes the possibly of false fluorescence readings due
13
Theory of Operation
to detection of light from the lamp which mimics the fluorescence

signal.
2.3.2 Emission Filter
The emission filter is used to select the range of wavelengths, the
pass band, to be passed to the measure detector. Wavelengths not in the
pass band are rejected and ideally never reach the sample. It is critical
that the excitation wavelengths never reach the detector, since the
detector will respond to excitation light and produce a false signal. If
excitation light is allowed to reach the measure detector, it will cause
increased residual background levels which reduces the dynamic range,
the signal-to-noise ratio and the signal-to-background ratio.
2.3.3 Measure Detector
The measurement detector is the detector that measures the
intensity of light after it has contacted the sample. The system is
designed in such a way that only absorbing or fluorescing wavelengths
of light are measured by the detector. The light intensity, which is
proportional to the analyte concentration, is registered as a digital
readout.
2.3.4 Source Reference Detector
The reference detector directly measures the intensity of the light
source before exposure to the sample.
2.3.5 Background Fluorescence
Background fluorescence refers to the fluorescence signal due to
the probe/analyzer optical configuration, stray light, and fluorescence
from the background material. The design of the Model 6650SP-XD
minimizes the background fluorescence.
2.3.6 Sensitivity
The sensitivity of the instrument refers to the ability of the analyzer
to detect a given level of analyte based on the molecular fluorescence
from the analyte. The actual limits of detection depend on the properties
of the analyte measured and the process conditions. Parameters such as
pH, temperature, oxygen content, and background solvent, to name but a
few may dramatically alter the fluorescence intensity measured.
Typically, detection of parts-per-million (ppm) and parts-per-billion
14
Model 6650SP-XD
Theory of Operation
(ppb) analyte levels can be detected. In general, fluorescent

measurements are 1,000 to 500,000 times more sensitive than
absorbance based photometric measurements. As used here, sensitivity
means the minimum analyte concentration that can be measured above
background fluorescence in the process.
2.3.7 Specificity
The specificity is the ability of the analyzer to monitor one specific
analyte in a mixture of background materials without interference from
the background materials. In absorbance based photometric
measurements, interference problems are common since many materials
absorb light, making it difficult to isolate the targeted analyte in a
complex mixture. However, transmitters, like the Model 6650SP, are
highly specific and less susceptible to interferences because fewer
materials exhibit molecular fluorescence. Furthermore, if background
materials do absorb and emit light, it is rare that they will emit the same
wavelength of light as the analyte of interest.
2.3.8 Signal-to-Noise Ratio
Signal refers to the emission collected by the fluorescence probe
and monitored by the analyzer using the internal span filter. Noise refers
to the output from the instruments electronics, which is present whether
or not sample is being read plus any collection of errant wavelengths not
removed by the optical filters. Noise is measured by placing the
fluorescence probe in air and in complete darkness (no stray light). For
process monitoring, the signal-to-noise ratio is not as important as the
signal-to background ratio.
2.3.9 Signal-to-Background Ratio
Signal refers to the emission collected from a sample with known
analyte concentration by the fluorescence probe and monitored by the
analyzer. Background refers to the process liquid containing no analyte
of interest and any stray light present in the system. The signal-tobackground ratio should be calculated during the application engineering
phase of the project. Knowing this ratio will help determine when the
stray light level changes and/or the background material fluorescence
properties change. Refer to Appendix 1 for additional details.
15
Theory of Operation
2.3.10 Dynamic Range

Dynamic range refers to the range of concentrations an instrument
can read, from the minimum to the maximum detectable. The minimum
detectable concentration is determined by signal-to-noise and signal-tobackground ratios. The maximum detectable concentration is determined
by the compounds chemistry and by factors such as instrument
sensitivity ranges, fluorescence (quantum) efficiency, specificity of
optical filters, etc.
2.3.11 Linearity
Fluorescence intensity is typically directly proportional (linear) to
concentration. There are, however, factors that affect this linear
relationship. For example, variations in temperature, pH, dissolved
oxygen content, stray light, turbidity, variation in the chemical
composition of the background, etc. can dramatically affect the linearity
of the fluorescence response. Practically, the linearity of the
measurement is determined during the application engineering phase of
the project. Refer to Appendix 1 for details.
2.3.12 Process Background
The liquid solution used to transport or sustain the analyte of
interest in the process is referred to as the process background. This
solution has all the chemical constituents found in the process except the
analyte of interest.
16
Model 6650SP-XD
Installation
Installation
Installation of the Model 6650SP analyzer includes:
1. Unpacking and mounting the analyzer.
2. Making AC power, alarm, and output signal electrical
connections.
3. Optical connection and installing the probe.
4. First time power up and initialization
5. Calibration.
Please follow the outlined sections below as a guideline to
installing the Model 6650SP-XD in your plant environment.
3.1 Unpacking and Mounting the Analyzer

The analyzer is shipped with all the materials you need to install
and prepare the system for operation. Carefully unpack the unit and
inspect it for damage. Immediately report any damage to the shipping
agent.
The Model 6650SP-XD is housed in an explosion proof NEMA-7
steel enclosure with a viewing window for visual access to the
instrument display. It is designed for bulkhead mounting in hazardous
environments. There are four mounting lugsone in each corner of the
enclosure, as shown in Figure 3-1. The outline drawing, at the back of
this manual, gives the mounting hole size and spacing. The drawing also
contains the overall dimensions. Do not forget to allow an extra 1-3/8"
for the hinges.
Be sure to allow enough space in front of the enclosure to swing the
door opena 16-1/4" radius, as shown in Figure 3-2.
All electrical connections are made via cables which enter the
explosion-proof housing through ports in its side. No conduit fittings are
supplied. The installer must provide two 3/4" NPT and two 1" NPT
adapters and the appropriate sealing conduit.
Installation
The transmitter, control unit, power supply, interconnection

terminal block, power switch/fuse housing have all been installed and
tested at the factory, however you should check to make sure that all
components remain secured and that no fasteners, cables or fittings have
become loose during shipping. Figure 3-1 identifies the major external
components of the analyzer and Figure 3-2 identifies the internal
components.
Figure 3-1: System Component Location and Identification
Model 6650SP-XD
Installation
Figure 3-2: Required Front Door Clearance

In addition to the physical, optical, and electrical installation
requirements of the Model 6650SP-XD it is recommended that the unit
be placed in a clean, dry area of the facility. If the area where the
electronics are mounted exceeds 115F (46C), it is recommended that
the transmitter be moved or purged with plant air to cool the enclosure.
Typically, the fiber optic cables are shipped separately and must be
connected by the user. See Section 3.3.
3.2 Electrical
The Model 6650SP-XD is configured to operate from a standard
110 or 220 VAC 50/60 Hz power source depending on the installation
location. Use the dedicated 3/4 and 1 NPTF feedthroughs for bringing
AC power, signal and alarm connections in and out of the enclosure.
Refer to the Interconnection Diagram in the Appendix for terminal
connections.
Figure 3-3 shows the Electrical Connector Panel. There are
terminal blocks for connecting power, communications, and both digital
and analog concentration outputs.
Installation
Figure 3-3: Electrical Connector Panel

For safe connections, ensure that no uninsulated wire extends
outside of the connectors they are attached to. Stripped wire ends must
insert completely into terminal blocks. No uninsulated wiring should be
able to come in contact with fingers, tools or clothing during normal
operation.
3.2.1 Primary Input Power
The universal power supply requires a 115 or 230 VAC, 50 or 60 Hz
power source. The actual input voltage used must show in the window
Model 6650SP-XD
Installation
of the VOLTAGE SELECTOR switch before the power source is

connected. See Figure 3-4 for detailed connections.
DANGER: Power is applied to the instrument's circuitry as
long as the instrument is connected to the power
source. The Standby function switches power on
or off to the displays and outputs only.
Figure 3-4: Primary Input Power Connections

3.2.2 Fuse Installation
The fuse holders accept 5 x 20 mm, 1.6 A, T type (slow blow)
fuses. Fuses are not installed at the factory. Be sure to install the proper
fuse as part of installation. (See Fuse Replacement in Chapter 5,
maintenance.)
3.2.3 Analog Outputs
There are eight DC output signal connectors on the ANALOG
OUTPUTS connector block. There are two connectors per output with
the polarity noted. See Figure 3-5.
Installation
Figure 3-5: Analog Output Connections

The outputs are:
01 VDC % of Range: Voltage rises linearly with increasing oil
concentration, from 0 V at 0 ppm to 1 V at full
scale. (Full scale = 100% of programmable
range.)
420 mA DC % Range: (-M Option) Current increases linearly with
increasing oil concentration, from 4 mA at 0 %
to 20 mA at full scale. (Full scale = 100% of
programmable range.)
The signal output for concentration is linear over the analysis
range. For example, if the analyzer is set on a range that was defined as
010 ppm oil, then the output would be as shown in Table 3-1.
Table 3-1: Analog Concentration OutputExample
OilConc.
(ppm)
0
1
2
3
4
5
6
7
8
VoltageSignal
Output(VDC)
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
CurrentSignal
Output(mADC)
4.0
5.6
7.2
8.8
10.4
12.0
13.6
15.2
16.8
Model 6650SP-XD
9
10
Installation
0.9
1.0
18.4
20.0
3.2.4 Alarm Relays

There are three alarm-circuit connectors on the alarm relays block
(under RELAY OUTPUTS) for making connections to internal alarm
relay contacts. Each provides a set of Form C contacts for each type of
alarm. Each has both normally open and normally closed contact
connections. The contact connections are indicated by diagrams on the
connector panel. They are capable of switching up to 3 amperes at
250 V ac into a resistive load. See Figure 3-6.
Figure 3-6: Types of Relay Contacts
The connectors are:

Threshold Alarm 1:
Can be configured as high (actuates when concentration is above

threshold), or low (actuates when concentration is below
threshold).
Can be configured as failsafe or non-failsafe.
Can be configured as latching or non-latching.
Can be configured out (defeated).
Threshold Alarm 2:
Can be configured as high (actuates when concentration is above

threshold), or low (actuates when concentration is below
threshold).
Installation
Can be configured as failsafe or non-failsafe.
Can be configured as latching or non-latching.
Can be configured out (defeated).
System Alarm:
Actuates when DC power supplied to circuits is unacceptable in

one or more parameters.
Permanently configured as failsafe and latching. Cannot be

defeated.
Actuates if self test fails.
To reset a System Alarm during installation, disconnect power to

the instrument and then reconnect it.
Further detail can be found in Chapter 4, Section 4-5.

3.2.5 Digital Remote Cal Inputs
Remote Zero and Span Inputs: The REMOTE SPAN and
REMOTE ZERO inputs are on the DIGITAL INPUT terminal block.
They accept 0 V (OFF) or 24 VDC (ON) for remote control of
calibration. (See Remote Calibration Protocol below.)
ZERO:
Floating input. 5 to 24 V input across the + and

terminals puts the analyzer into the Zero mode. Either
side may be grounded at the source of the signal. 0 to 1
volt across the terminals allows Zero mode to terminate
when done. A synchronous signal must open and close
the external zero valve appropriately. See 3.3.9 Remote
Sensor and Solenoid Valves. (With the C option, the
internal valves automatically operate synchronously.)
SPAN:
Floating input. 5 to 24 V input across the + and

terminals puts the analyzer into the Span mode. Either
side may be grounded at the source of the signal. 0 to 1
volt across the terminals allows Span mode to terminate
when done. A synchronous signal must open and close
the external span valve appropriately. See 3.3.9 Remote
Sensor and Solenoid Valves. (With the C option, the
internal valves automatically operate synchronously.)
Cal Contact: This relay contact is closed while analyzer is

spanning and/or zeroing. (See Remote Calibration Protocol below.)
Model 6650SP-XD
Installation
Remote Calibration Protocol: To properly time the Digital

Remote Cal Inputs to the Model 6650SP controller, the customer's
controller must monitor the CAL CONTACT relay.
When the contact is OPEN, the analyzer is analyzing, the Remote
Cal Inputs are being polled, and a zero or span command can be sent.
When the contact is CLOSED, the analyzer is already calibrating. It
will ignore your request to calibrate, and it will not remember that
request.
Once a zero or span command is sent, and acknowledged (contact
closes), release it. If the command is continued until after the zero or
span is complete, the calibration will repeat and the Cal Relay Contact
(CRC) will close again.
For example:
1. Test the CRC. When the CRC is open, Send a zero command
until the CRC closes (The CRC will quickly close.)
2. When the CRC closes, remove the zero command.
3. When CRC opens again, send a span command until the CRC
closes. (The CRC will quickly close.)
4. When the CRC closes, remove the span command.
When CRC opens again, zero and span are done, and the sample is
being analyzed.
3.2.6 Network I/O
A serial digital input/output for local network protocol. At this
printing, this port is not yet functional. It is to be used in future versions
of the instrument.
3.2.7 RS-485
The Model 6650SP-XD uses a RS-485 protocol for communication
between the PX2 transmitter and the control unit. Connections between
the transmitter and the PX2 Interface Input terminal section on the user
interface board have been made at the factory.
Installation
3.3 Fiber Optic Cables

Typically, the probe and fiber optic cables are shipped as separate
items and must be installed before using the analyzer. The probe is
shipped as a complete assembly with a bifurcated fiber optic cable
attached.
To install the optical cable:
1. Thread the bifurcated fiber optic cable through the 1-3/4 fitting
on the bottom of the enclosure.
2. Insert the optic cables into the sockets at the bottom of the
transmitter. Both the cable end connectors and sockets are
labeled. Make sure the connectors are inserted into the correct
socket. See Figure 3-7.
Hand-tighten the liquid-tight connectors 1 nut at the bottom
of the NEMA-4 housing.
Figure 3-7: Optical Cable Installation
Model 6650SP-XD
Installation
3.4 Probe Installation

The probe is fabricated with a 1/2 dia. tube (13 mm) for
interfacing with the process fluid using a standard slip-fit tube fitting.
It is important that all oil in the process fluid over 20 mg/l be totally
representative of the process and homogenized as an emulsion. The oil
should be uniformly dispersed otherwise erroneous readings can occur.
An optional ultrasonic homogenizer can be installed in the analyzer to
create a uniform dispersion of oil in water.
3.5 Sample Handling System

The standard Model 6650 is shipped with an integral probe and it is
the customers responsibility to ensure an adequate and representative
sample is available to the probe. The standard unit is not configured with
a sample handling system.
Depending on the nature of the application, safe and accurate
analysis may require special sample handling considerations. Teledyne
often supplies the analyzer with an integral sample system. Contact
Customer Service for specific sample conditioning and handling
requirements for your application.
If a sample system is required, TAI recommends a piping system as
shown in Figure 3-8. This system is equipped with pressure and flow
controls, sample conditioning and extraction capability, probe and piping
water/steam flush lines, plus appropriate valves for switching between
calibration and sample delivery.
3.6 First Time Power Up and Initialization

The power up and initialization of the unit is discussed in Chapter
4. It requires familiarity with the interface panels and operational details.
Refer to Chapter 4.
3.7 Calibration
Prior to using the analyzer, the unit must be calibrated. The
calibration procedure is discussed in Sections 4.6 and 5.6. Calibration
requires a familiarity with the operating interfaces of the transmitter and
control unit. Please read Chapter 4 prior to calibrating this instrument.
Installation
Figure 3-8: Typical Piping Diagram
Setup & Operation

The Model 6650SP-XD Oil in Water Analyzer is designed to
monitor the fluorescence signal from a laboratory or process stream.
Under most conditions the fluorescence range of the sample is well
defined and can be verified with standard reference materials such as
zero and span solutions of know concentrations.
Note: For some applications this may not be the case and
measuring a sample whose fluorescence is not
characterized but is known to fall in the instrument range is
required. A special mode has been built in to this
instrument for this purpose. Please contact Customer
Service if an uncharacterized sample must be measured.
The PX2 Transmitter has been configured at the factory for your
particular application. It should not require any additional input from the
user. A special configuration mode has been built in to the transmitter for
reconfiguring the transmitter via a remote computer however it is not
recommended to do so unless requested by TAI Customer Service.
Setting up the instrument involves calibration of the analyzer
using known standards.
This section describes how to set up and calibrate the control unit.
See also Sections 5.5 and 5.6 which contains additional information for
recalibrating the 4-20 output signal and linearizing the output for your
application.
4.1 Interface Panel

The operator controls of the control unit for setting up and
configuring the analyzer are located on the front door of the explosion
proof housing. Once set up and calibrated, the control unit becomes the
main interface during analysis. The interface panel is shown in Figure
4.1
.
Setup & Operation
4.2 Control Unit

The control unit used in the Model 6650SP contains the main
interface panel for operating the analyzer. See Figure 4-1. This section
and sub sections describe how to operate the control unit.
Figure 4-1: Control Unit Interface

To get the proper response from these controls, turn the control
toward the desired action (ESCAPE or ENTERDOWN or UP), and
then release it. Turn-and-release once for each action. For example, turnand-release twice toward UP to move the VFD screen two selections
upwards on the list of options (menu).
The item that is between arrows on the screen is the item that is
currently selectable by choosing ENTER (turn-and-release toward
ENTER with the ESCAPE/ENTER control).
In these instructions, to ENTER means to turn-and-release toward
ENTER, and To ESCAPE means to turn-and-release towards ESCAPE.
To scroll UP (or scroll DOWN) means to turn-and-release toward UP (or
DOWN) as many times as necessary to reach the required menu item.
4.2.1 Mode/Function Selection
When the analyzer is first powered up, and has completed its
initialization and self diagnostics, ESCAPE toggles the instrument
Model 6650SP-XD
Setup & Operation
between the ANALYZE screen (Analysis Mode) and the MAIN MENU
screen (Setup Mode). The ANALYZE screen is the only screen of the
Analysis Mode.
The MAIN MENU screen is the top level in a series of screens used
in the Setup Mode to configure the analyzer for the specific application.
The DOWN/UP commands scroll through the options displayed on the
VFD screen. The selectable option appears between arrows. When you
reach the desired option by scrolling, ENTER the selection as described
below.
ESCAPE takes you back up the hierarchy of screens until you reach
the MAIN MENU again. ESCAPING any further just toggles between
the MAIN MENU and the ANALYZE screen.
4.2.1.1 CALC MODE
CALC (or Analyze) Mode is the normal operating mode. The

analyzer monitors and displays either the oil content of the sample or the
raw output of the detector. Using the UP or DOWN switch when in this
mode toggles between SENSOR: YES (raw output) or SENSOR: NO
(actual oil concentration) .
Activating either ENTER or ESCAPE on the control switch will
place the analyzer in Setup Mode. Setup Mode switches back to
Analyze Mode if no controls are used for more than five seconds.
4.2.1.2 SETUP MODE
The MAIN MENU consists of 12 functions you can use to

customize and check the operation of the analyzer. Figure 4-2 shows the
functions available with the 6650SP-XD. They are listed here with brief
descriptions:
1. PWD: Used to establish password protection or change the
existing password.
2. LOGOUT: Logging out prevents unauthorized tampering with
the analyzer settings.
3. VERSION: Displays Manufacturer, Model, and Software
version of the instrument.
Setup & Operation
4. SELF-TEST: The instrument performs a self-diagnostic routine

to check the integrity of the power supply, output boards and
amplifiers.
5. ZERO: start a zero calibration.
6. SPAN: Set up and/or start a span calibration.
7. ALARMS: Used to set the alarm setpoints and determine
whether each alarm will be active or defeated, HI or LO acting,
latching or not, and failsafe or not.
8. RANGE: Used to set the analysis range.
9. SHOW NEGATIVE: Allows the display to indicate negative
values (useful when using an offset to zero).
10. 4-20 TEST: A test screen that allows the user to test the analog
output at selected points between 4 and 20 mA.
11. ALARM TEST: A test screen that allows the user to test the
concentration alarm circuit.
12. STANDBY: Remove power to outputs and displays, but
maintain power to internal circuitry.
Figure 4-2: Hierarchy of Available Functions

Any function can be selected at any time. Just scroll through the
MAIN MENU with the DOWN/UP control to the appropriate function,
and ENTER it. The analyzer will immediately start that function, unless
Model 6650SP-XD
Setup & Operation
password restrictions have been assigned. (Password assignment is

explained further on.)
All of these functions are described in greater detail in the
procedures starting in section 4.3. The VFD screen texts used to
illustrate the procedures are reproduced in a Arial Narrow Bold type style.
4.2.2 Data Entry
4.2.2.1 ENTER
When the selected option is a function on the Main Menu screen,

the function name appears between the arrows on the screen. You
activate the function by turning the ESCAPE/ENTER control to
ENTER.
When the selected option is a function or subfunction, ENTER
moves the display to the VFD screen for that function or subfunction.
When the selected option is a modifiable item, the DOWN/UP
control can be used to increment or decrement that modifiable item to
the value or action you want. Then you ENTER the item, which also
puts you into the next field to continue programming.
When the last field is entered, ENTER takes you to the next screen
in the process, or if the process is completed, ENTER takes you back to
the ANALYZE screen.
4.2.2.2 ESCAPE
A turn-and-release toward ESCAPE moves the blinking to the next

field on the left. When you are on the leftmost field, another ESCAPE
takes you back to the previous screen.
If you do not wish to continue a function, you can abort the session
by escaping to the leftmost field, and then issuing another ESCAPE.
Escaping a function takes the analyzer back to the previous screen, or to
the ANALYZE Function, depending on the function escaped.
4.3 CALC (Analyze)

The Model 6650SP-XD can display either the raw output from the
PX2 transmitter or process the output, calculate and then display the oil
concentration in parts per million (ppm). The CALC screen (referred to
as the Analyze screen) allows the user to toggle between either display.
Setup & Operation
The Analyze mode is the default mode of the instrument and is shown
below:
67.4 ppm Anlz
Range 0 - 100
To change the display activate the ENTER switch. The following

screen will display:
Data Analysis in
Sensor:
Yes
Yes indicates that the displayed value is the raw output of the PX2
transmitter, No indicates the display is ppm oil.
To switch the display from one to the other, activate the UP/DOWN
switch to toggle between Yes and No. When finished, use the ENTER
switch to save the result and the screen will change to the desired output.
When the analyzer is turned on, the display will inform the user
that a zero calibration must be performed. The user has the option of
retaining the previous calibration settings.
4.4The PWD (Password) Function

Security can be established by choosing a 5 digit password from the
standard ASCII character set. If you decide NOT to employ password
security, use the default password TETAI. This password will be
displayed automatically by the microprocessor. The operator just
ENTERs it to be allowed total access to the instruments features.
Once a unique password is assigned and activated, the operator
MUST enter the UNIQUE password to gain access to any of the set-up
functions (except to enter the password). However, the instrument will
continue to analyze sample gas and report on alarm conditions without
entering the password.
Only one password can be defined.
After a password is assigned, the operator must log out to

activate it. Until then, anyone can continue to operate the
instrument without entering the new password.
To defeat the security after a unique password is activated, the

password must be changed back to TETAI.
Note: If you use password security, it is advisable to keep a copy
Model 6650SP-XD
Setup & Operation
of the password in a separate, safe location.

4.4.1 Entering the Password
To install a new password or change a previously installed
password, you must key in and enter the old password first. If the default
password is in effect, issuing the ENTER command will enter the
default TETAI password for you.
Scroll to PWD, and ENTER to select the password function. Either
the TETAI default password or AAAAA place-holder password for an
existing password will appear on screen depending on whether or not a
password has been previously installed.
TETAI
Enter PWD
or
AAAAA
Enter PWD
The screen prompts you to enter the current password. If you are
not using password protection, ENTER to accept TETAI as the default
password. If a password has been previously installed, enter the
password using ENTER to scroll through the letters, and the DOWN/UP
keys to change the letters to the proper password. The last ENTER
enters the password.
If the password is accepted, the screen will indicate that the password
restrictions have been removed and you have clearance to proceed.
PWD Restrictions
Removed
In a few seconds, if you do not ESCAPE, you will be given the

opportunity to change this password or keep it and go on.
Change Password?
<ENT>=Yes <ESC>=No
ESCAPE to move on, or proceed as in Changing the Password,

below.
Setup & Operation
4.4.2 Installing or Changing the Password

If you want to change the existing password: Proceed as above in
Entering the Password, until you are given the opportunity to change the
password:
Change Password?
<ENT>=Yes <ESC>=No
ENTER to change the password (to change either the default TETAI
or the previously assigned password), or ESCAPE to keep the existing
password and move on.
If you choose ENTER to change the password, the password
assignment screen appears.
TETAI
<ENT> To Proceed
or
AAAAA
<ENT> To Proceed
Enter the password using ENTER to scroll through the existing

password letters, and DOWN/UP to change the letters to the new
password. The full set of 94 characters available for password use are
shown in the table below.
Characters Available for Password Definition:
A
K
U
_
i
s
}
)
3
=
B
L
V
^
`
j
t
*
4
<
>
C
M
W
D
N
X
E
O
Y
F
P
Z
G
Q
[
H
R
I
S
]
J
T
a
k
u
!
+
5
b
l
v
"
'
6
c
m
w
#
7
d
n
x
$
.
8
e
o
y
%
/
9
f
p
z
&
0
:
g
q
{
'
1
;
h
r
|
(
2
When you have finished typing the new password, the last ENTER
enters it. A verification screen appears. The screen will prompt you to
retype your password for verification.
Model 6650SP-XD
Setup & Operation
AAAAA
Retype PWD To Verify
Wait a moment for the entry (<ENT>) screen. You will be given
clearance to proceed.
AAAAA
<ENT> TO Proceed
ENTER the letters of your new password. Your password will be

stored in the microprocessor and the system will immediately switch to
the ANALYZE screen, and you now have access to all instrument
functions.
If all alarms are defeated, the ANALYZE screen appears as:
67.4
ppm Anlz
Range: 0 100
If an alarm is tripped, the second line will change to show which

alarm it is:
67.4
ppm Anlz
AL1
Note: If you log off the system using the LOGOUT function in the
MAIN MENU, you will now be required to re-enter the
password to gain access to any of the functions except
password (PWD).
4.5 The LOGOUT Function

By entering LOGOUT, you effectively log off the instrument,
leaving the system protected against tampering until the password is
reentered. To log out, scroll to place the LOGOUT function between the
arrows, and ENTER to log out. The screen will display the message:
Protected Until
Password Reentered
Setup & Operation
4.6 The VERSION Screen

Scroll through the MAIN MENU to VERSION, and ENTER. The
screen displays the manufacturer, model, and software version
information.
4.7 The SELF-TEST Function

The Model 6650SP-XD has a built-in self-testing diagnostic
routine. Preprogrammed signals are sent through the power supply,
output board and sensor circuit. The return signal is analyzed, and at the
end of the test the status of each function is displayed on the screen,
either as OK or as a number between 1 and 3. (See System Self
Diagnostic Test in chapter 5 for number code.)
The self diagnostics are run automatically by the analyzer whenever
the instrument is turned on, but the test can also be run by the operator at
will. To initiate SELF-TEST during operation:
Use the DOWN/UP control to scroll through the MAIN MENU to
SELF-TEST. The screen will follow the running of the diagnostic.
RUNNING DIAGNOSTIC
Testing 15V Power
Then:
RUNNING DIAGNOSTIC
Testing Analog Out
When the testing is complete, the results are displayed.

Power: OK Analog: OK
The module is functioning properly if it is followed by OK. A

number indicates a problem in a specific area of the instrument. Refer to
Chapter 5 Maintenance for number-code information. The results screen
alternates for a time with:
Press Any Key
To Continue...
Then the analyzer returns to the ANALYZE screen.
Model 6650SP-XD
Setup & Operation
4.8 The Zero and Span Functions

Calibration is necessary for attaining the published accuracy
specification of this instrument. The analyzer must be calibrated at both
zero and span using known calibration solutions.
Note: A zero calibration must be performed first followed by a
span calibration. If you attempt to perform a span
calibration without first calibrating the zero, the display will
indicate that you must perform the zero calibration first and
will not let you proceed to the span calibration function.
Calibrating the Model 6650SP-XD involves:
Preparing suitable calibration solutions such as zero (oil-free

water), plus full span and 1/2 span solutions.
Setting the zero on the control unit
Span calibration of the control unit
4.8.1 Calibration Preparations

4.8.1.1 EQUIPMENT REQUIRED
Digital Multimeter: (DMM) to read DC current output
Teledyne Calibration Kit P/N A48715
Blender: A Waring model 1120 (or suitable equivalent)

laboratory type blender. (typically 18,000 RPM, low/high speed.
Micro-liter Syringe: Use an adjustable pipette suitable for the

range of calibration.
Graduated Cylinders: A 500 and a 100 milliliter (ml)

graduated cylinder to measure the water for preparing span and
span fluids.
Erlenmyer Flask: A 500ml Erlenmeyer flask to prepare the

span fluids.
Deionized Water: In a suitable large container for zeroing the

analyzer. This may be substituted with tap (potable), utility or
zero prepared sample water from the customer process line.
Setup & Operation
Plastic Waste Collection Jug: To collect the oil/water mixture

as it leaves the analyzer.
Tubing: Plastic inch tubing about 5 feet long to introduce the

calibration fluids to the analyzers calibration reservoir by
gravity feed.
Calibration Oil: Use the application specific oil, otherwise, use

EPA #2 Reference Oil.
4.8.1.2 CALIBRATION FREQUENCY
The Model 6650SP-XD is designed to work continuously and

requires four hours or more to warm up after power is applied. If the
system is used seldom, say once a month, calibration should be
completed every time the system is used.
4.8.1.3 PREPARATION
1. Be sure the analyzer is warmed up and the zero drift is not

more than 1% per hour. (Allow 1 hour minimum if a cold
start is done).
Connect the voltmeter to the 6650SP-XD control unit analog output
connections. Make sure that the meter is set to read current on a suitable
mA scale.
2. If your instrument is equipped with a TAI sample system, use
the inch tubing to run deionized water into the analyzer via
the Steam/Water Wash port and run it until the analyzers
output stabilizes.
3. Prepare and use known span and zero fluids as described in
Section 4.8.4 Calibration Fluid Preparation then proceed to
Section 4.8.5 Calibrating the Control Unit.
4.8.1.4 CALIBRATION FLUID PREPARATION
Calibration of the control unit will require at a minimum, a zero

fluid (usually deionized water) and two span solutions, a full span
(100% of instrument range) and a half span (50% of instrument range).
Generally, this will be sufficient for most applications although using
more span fluids at different concentrations will enhance the precision of
Model 6650SP-XD
Setup & Operation
the instruments linearity. Up to nine span fluid concentrations can be

entered during calibration.
4. Measure 500ml of deionized water into a 500ml graduated
cylinder and pour it into a blender without spilling any.
5. Select a microliter syringe and draw up the required volume
of oil or EPA # 2 Reference Oil for a known concentration.
For example if the analyzer is configured with a maximum
range of 200 ppm oil, use a 100 l volume as specified in
Table 4-2 to prepare a full span solution (200 ppm). Use 100
l volume to prepare a half span solution (100 ppm).
Table 4-2: Span and Half Span Preparation
Analyzer Span
or Half Span
Volume of
Oil
10 ppm
5 micro liters (l)
20 ppm
10 l
50 ppm
25 l
100 ppm
50 l
200 ppm
100 l
6. Wipe any excess oil off the outside of the syringe with a
lintless tissue. Be careful not to allow the tissue to wick any
oil out of the syringe.
7. Place the lid on the blender and switch it on to its highest
setting. Lift the lid enough to inject the contents of the
syringe into the water midway between the center of the
vortex and the wall of the blender. Make sure oil injection
happens under water or some of the oil may be thrown
against the wall of the blender
8. Place the lid back on the blender and homogenize for exactly
2 minutes.
9. Discard the contents of the blender into the waste jug. The
blender is now stabilized for accurate preparation of the span
fluid. Repeat steps 2 through 5 and the calibration span fluid
is now ready.
Setup & Operation
4.8.1.5 CALIBRATING THE CONTROL UNIT
The control unit uses the non-linear 4-20 mA output signal from the
transmitter to report the oil concentration. Control unit calibration
establishes an accurate, linearized correspondence between transmitter
counts and the unit of measure configured at the factory (typically ppm).
It requires setting the control unit zero, half and full span points to the
known concentration of the calibration fluids while the probe is
immersed in the calibration fluid.
4.8.2 Zero Calibration

From the analyze screen activate the ENTER switch to display the
main setup menu. Scroll though the functions using the UP/DOWN
switch until Zero appears on the display. This function is used to enter
the zero calibration information and to start the calibration.
Make sure the probe is immersed into the zero solution and the
control unit is set to display concentration (ppm) and not the raw output
of the transmitter. See Section 4.3.
CAUTION:
IF THE PROBE IS NOT IMMERSED IN A SOLUTION A

SYSTEM ALARM WILL TRIGGER AND THE LEDS ON
THE PX2 TRANSMITTER WILL TURN RED. A
BROKEN LIGHT PATH MESSAGE WILL APPEAR ON
THE DISPLAY. IF THIS OCCURS, YOU WILL NOT BE
ALLOWED TO PROCEED UNTIL THE PROBE IS
IMMERSED INTO THE FLUID OR THE LIGHT PATH
INTERRUPTION IS IDENTIFIED AND REPAIRED.
With the Zero function appearing on the display, activate the

ENTER switch to enter the zero function. The following screen will
appear:
Apply Zero and
Press Enter Key
Activate the ENTER switch once more to display the next screen:
Getting Zero Values
Please wait . .
Model 6650SP-XD
Setup & Operation
After approximately 30 seconds, the analyzer will cycle through

from sample 1 to sample 10 and then present the following screen:
Zero Calib complete
Please perform Span
This message will time out in 30 seconds and return to the Analyze
screen or you can use the ENTER switch to immediately return to the
Analyze screen.
At this point the control unit has stored the zero calibration
information and the zero calibration is complete.
4.8.3 Span Calibration

The SPAN function is used to span calibrate the analyzer. Span
calibration is performed using a prepared solution of known
concentration. The user enters the concentration into the display and
immerses the probe into the span solution. Then when the span function
is activated an internal algorithm compares multiple consecutive
readings from the sensor to determine when the output matches the span
gas concentration at which point the span calibration process will end.
After span calibration, the unit will be calibrated and ready for use.
To perform a span calibration:
With the probe immersed into the known span fluid, navigate to the
SPAN function using the UP/DOWN switch and then activate ENTER.
The following screen will appear:
Apply SPAN and
Press Enter Key
Use the ENTER switch again to display the next screen where you
enter the known span concentration:
Span Val: 00060.00
UP/DN Mod <ENT> Done
Setup & Operation
The current span value will be blinking. Use the UP/DOWN switch
to modify the value if desired. Then activate the ENTER switch to store
the value in memory. The following screen will display:
Getting Span Values
Please wait . .
After approximately 30 seconds, the analyzer will cycle through

from sample 1 to sample 10 and then present the following screen:
Device Calibrated
Use the ENTER switch to save the calibration and return to the
Analyze screen.
67.4
ppm Anlz
Range: 0 100
4.9 The ALARMS Function

The Model 6650SP-XD is equipped with 2 fully adjustable
concentration alarms and a system failure alarm. Each alarm has a relay
with a set of form C" contacts rated for 3 amperes resistive load at 250
VAC. See Figures 3.3 and 3.6 in Chapter 3, Installation and/or the
Interconnection Diagram included at the back of this manual for relay
terminal connections.
The system failure alarm has a fixed configuration described in
chapter 3 Installation.
The concentration alarms can be configured as either high or low
alarms by the operator. The alarm modes can be set as latching or nonlatching, and either failsafe or non-failsafe, or, they can be defeated
altogether. The setpoints for the alarms are also established using this
function.
Decide how your alarms should be configured. The choice will
depend upon your process. Consider the following four points:
1. Which if any of the alarms are to be high alarms, and which if
any are to be low alarms?
Model 6650SP-XD
Setup & Operation
Setting an alarm as HIGH triggers the alarm when the oil

concentration rises above the setpoint. Setting an alarm as LOW
triggers the alarm when the oil concentration falls below the
setpoint.
Decidewhetheryouwantthealarmstobesetas:
Both high (high and high-high) alarms, or
One high and one low alarm, or
Both low (low and low-low) alarms.
2. Are either or both of the alarms to be configured as failsafe?
In failsafe mode, the alarm relay de-energizes in an alarm
condition. For non-failsafe operation, the relay is energized in an
alarm condition. You can set either or both of the concentration
alarms to operate in failsafe or non-failsafe mode.
3. Are either of the alarms to be latching?
In latching mode, once the alarm or alarms trigger, they will
remain in the alarm mode even if process conditions revert back
to non-alarm conditions. This mode requires an alarm to be
recognized before it can be reset. In the non-latching mode, the
alarm status will terminate when process conditions revert to
non-alarm conditions.
4. Are either of the alarms to be defeated?
The defeat alarm mode is incorporated into the alarm circuit so
that maintenance can be performed under conditions which
would normally activate the alarms.
The defeat function can also be used to reset a latched alarm.
(See procedures, below.)
If you are using password protection, you will need to enter your
password to access the alarm functions. Follow the instructions in
Section 4.4 to enter your password. Once you have clearance to proceed,
ENTER the ALARM function.
AL1 AL2
Choose Alarm
Setup & Operation
Use the DOWN/UPcontrol to blink your choice of alarm, AL-1 or

AL-2. Then ENTER to move to the next screen.
AL1 1000 ppm HI
DftN FsN LtchN
Five parameters can be changed on this screen.

5. Value of the alarm setpoint: AL1 ####
ppm (oil)
6. Out-of-range direction: HI or LO
7. Defeated? (Yes/No): DftY/N
8. Failsafe? (Yes/No): FsY/N
9. Latching? (Yes/No): LtchY/N.
To define the setpoint, use ENTER to blink AL1 ####, if not

already blinking. Then use the DOWN/UP control to change the
number. Holding the control on the DOWN or UP position,
while the number changes, speeds up the incrementing or
decrementing. (Remember, the setpoint units are always ppm
oil.)
To set the other parameters use ENTER to blink the desired

parameter. Then use DOWN/UP to change the parameter.
Once the parameters for the alarm have been set, ENTER the
ALARM function again, and repeat this procedure for next alarm.
To reset a latched alarm:

Go to Dft and then assert either DOWN two times or UP
two times. (Toggle it to Y and then back to N.)
OR
Go to Ltch and then assert either DOWN two times or
UP two times. (Toggle it to N and back to Y.)
Note: In this screen, ENTER moves you through the fields and
ESCAPE takes you back to the previous screen.
4.10 Alarm Test Function

The alarm test function allows the user to test the alarm circuitry for
both concentration alarms.
Model 6650SP-XD
Setup & Operation
Alarm Test
Upon selecting this function, you are given the choice to test alarm 1 or
alarm 2.
Select Alarm: AL1
Use the UP/DOWN switch to toggle between alarms. When the

desired alarm appears on the display, use the ENTER control to activate
the alarm. The contacts on the alarm relay will change state, i.e. move to
the alarm position.
Use the ESCAPE switch to return to the previous menu.
4.11 The RANGE Function

The RANGE function allows the operator to program the
concentration range to the specific application and have it correlate with
the DC analog output. If no range is defined by the user, the instrument
defaults to 0100 ppm.
Since this is a single range instrument, the Model 6650DP-XD
does not support auto-ranging.
4.12 Show Negative Function

The Model 6650SP-XD can be set to display negative readings
when the instrument is set to display concentration. This can be useful to
determine if PX2 detector output has drifted below zero since the last
zero calibration was performed.
To show negative oxygen readings on the display:
Scroll to the NEGATIVE screen using the UP/DOWN switch and
use the ENTER switch when the screen indicates NEGATIVE is the
selectable function.
Range
Negative
Enter the function by activating the ENTER switch.
Setup & Operation
Show Negative Yes
Use the UP/DOWN switch to toggle between YES or NO then use

the ENTER switch to save the setting.
This preference is stored in non-volatile memory, so this
configuration is remembered after a power shutdown. If the instrument
is cold started, it will go back to default (not showing negative oil
readings).
4.13 The 4-20 Test Function

The 4-20 test function can be used to test the analog output of the
control unit. To use this function you will need to connect a millivolt test
meter to the analog output terminals on the electrical connection panel.
See Figure 3-3.
With the meter connected, scroll to the 4-20 Test function using the
UP/DOWN switch.
Negative
4-20 Test
Enter the function by activating the ENTER switch.

Select Test :
This function will send the appropriate signal to the output

terminals on the connection panel. Using the UP/DOWN switch you can
select whether 4 mA, 8 mA, 12 mA, 16 mA, or 20 mA signal is sent to
the connection panel terminals. When the appropriate test is selected,
use the ENTER control to send the signal.
When finished, use the ESCAPE switch to return to the main menu.
4.14 The STANDBY Function

In STANDBY, the analyzers internal circuits are powered, but
there are no displays or outputs from the analyzer.
WARNING:
THE POWER CABLE MUST BE UNPLUGGED TO

FULLY DISCONNECT POWER FROM THE
INSTRUMENT. WHEN THE ACCESS DOOR IS OPEN
AND THE POWER CABLE IS CONNECTED, EXTRA
Model 6650SP-XD
Setup & Operation
CARE IS REQUIRED TO AVOID CONTACT WITH LIVE

ELECTRICAL CIRCUITS.
CAUTION: If you disconnect the primary power source from

the analyzer, then on re-energizing, you will be
required to choose to keep the configuration you
previously programmed into your instrument in
the Setup Mode by pressing the Enter key, or
by pressing the Escape key to reset to factory
defaults. Of you press neither key, the
instrument will time out and take your previous
configuration.
4.15 Transmitter Interface Panel

The transmitter has internal software available that allows the user
to reconfigure the transmitter for a different application or to fine tune
the existing settings. Measurement modes, light source, integration time,
detector gain, and other parameters can be changed. Teledyne
recommends that you contact Customer Service before attempting to
download and install the software and change any of the parameters that
have been set up at the factory for your application. Figure 4-3 is a
screen shot of the PX2 Control Panel software.
Connection from a remote computer to the PX2 module is via the
USB port as shown in Figure 1-6.
Contact TAI Customer Service for the download link and additional
information.
Setup & Operation
Figure 4-3: UV Transmitter Interface Panel
Maintenance & Troubleshooting

This section describes procedures for reconfiguring the transmitter
and other maintenance procedures for continued maximum performance
of your Model 6650SP analyzer.
5.1 Application Engineering

All units supplied by TAI have been configured for specific
applications. This instrument cannot be used as is for a different
application without first establishing a relationship between the new
sample and the fluorescence response from the instrument. Rarely will
this be possible without extensive modification to the transmitter
including new filters specifically tailored to the fluorescence spectra
involved. At a minimum, you will need to develop a compound specific
calibration curve, determine the limit of detect ability, and dynamic
range. The instrument must be reconfigured for the new application.
There are features built in to this analyzer that will, under certain
circumstances, support in-field application changes. Contact TAI
Customer Service before attempting to use this analyzer to measure a
sample other than the original sample and background specified at the
time of purchase.
5.2 Diagnostic Messages

There are two diagnostic messages that may appear on screen
relating to the light source and path. In addition to messages, the
transmitter face has a series of multicolored LEDs in the shape of the
Teledyne logo that change color to indicate the transmitter status: power
ing up, ready, or fault.
If there has been a major change in the probe installation or process
piping, very likely, there will be a stray light leak into the system. Verify
that the monitoring location is in complete darkness. If both the
reference detector and measure detector are not exposed to a light signal
a Broken Light Path message will appear on the VFD display and the
Maintenance & Troubleshooting
LEDs that make up the Teledyne logo on the transmitter will turn from
blue to red.
When the Broken Light Path message appears on the display, the
display will not report concentration or allow passage to any other
function until the probe is returned to darkness or the broken path is
corrected.
A second fault message is possible and occurs when the
measurement detector sees a low signal while the reference detector
signal is normal. This will cause a Light Source Failed message to occur
onscreen and the LEDs on the PX2 to flash red. When this occurs, the
display will not report concentration or allow passage to any other
function until the light path is restored and functioning correctly.
Appendix
A.1 Specifications
Appendix
A.2 Spare Parts Listing

C91743-A
Motherboard for RS485
A.3 Reference Drawings

D92638
C92639
Outline Diagram
Interconnection Diagram

Manual 6650SP

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OPERATING INSTRUCTIONS FOR

Teledyne Analytical Instruments

Copyright 2015 Teledyne Analytical Instruments

Teledyne Analytical Instruments

NOTE: (No symbol). Additional information and comments

THE ANALYZER SHOULD ONLY BE USED FOR THE

Teledyne Analytical Instruments

IF YOU USE THE ANALYZER IN A MANNER OTHER

This manual provides information designed to guide you through

Teledyne Analytical Instruments

2.3.5 Background Fluorescence

4.3 CALC (Analyze)

Maintenance & Troubleshooting.................................................51

Teledyne Analytical Instruments

Figure 1-1: Model 6650SP-XD Components....................................

Teledyne Analytical Instruments

Teledyne Analytical Instruments

The analyzer is housed in an explosion proof housing and is

Teledyne Analytical Instruments

1.2 Model 6650 Components

Integrated Fluorescence Probe

Fiber Optic Cables

A typical Model 6650SP is shown in Figure 1-1. The Model

Figure 1-1: Model 6650SP-XD Components

Teledyne Analytical Instruments

The PX2 Transmitter is carefully configured and tested at the

Figure 1-2: PX2 Photometric Module

Teledyne Analytical Instruments

The PX2 Transmitter outputs the fluorescence level as a raw signal

Figure 1-3: Model 6650SP-XD Control Unit Front Panel

1.2.3 Xenon UV Source

Rugged sapphire spherical lens

Constant focal length and sample volume

Delivered optical energy is concentrated via a ball lens

Effective sampling of liquids, slurries, powders, pastes and solids

Particle size has minimal effect on optical performance

Figure 1-4: Fluorescence Probe

Teledyne Analytical Instruments

1-5, the front surface design produces a probe which is unaffected by

Figure 1-5: Front Surface Probe Design Features

1.3 Optional Components

Integrated Sample System with Water/Steam Flush

1.4 User Interface

Teledyne Analytical Instruments

options, and messages that give the operator immediate feedback. It is

Functions: The UP/DOWN switch is used to select the function to

Toggles readout between sensor output and concentration.

Install a password to protect your analyzer setup.

Locks Setup Mode.

Displays model and version of analyzer.

Runs internal diagnostic program, displays results.

Span calibrate the analyzer.

Zero calibrate the analyzer.

Set the alarm setpoints and attributes.

Set up the 3 user definable ranges for the instrument.

Display negative values.

Routine to test analog output.

Routine to test concentration alarms.

Leave analyzer powered, but no outputs or displays.

THE POWER CABLE MUST BE DISCONNECTED TO

Sub functions: Once a function is entered, the UP/DOWN switch

Teledyne Analytical Instruments

Parameter values: When modifiable values are displayed on the

Data Entry: The ESCAPE/ENTER switch is used to input data,