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30/CCSUN 4935/00

Sunscreen Softcream (O/W), SPF 43*, water-resistant**, with broad UVA Protection
(UVA/UVB Balance***)
Ingredients

INCI-Name

% w/w

SUPPLIERS

PHASE A
Emulsiphos
(677660)

Potassium Cetyl Phosphate,


Hydrogenated Palm Glycerides

1,500

Symrise GmbH & Co. KG

Cetearyl Alcohol

1,000

Cognis Dtl. GmbH, Germany

C12-15 Alkyl Benzoate

3,000

Degussa-Goldsch midt
AG,Germany

Ethylhexyl Isononanoate

2,000

Symrise GmbH & Co. KG

Dimethicone

2,000

Degussa-Goldsch midt
AG,Germany

Octocrylene

10,000

Symrise GmbH & Co. KG

Homosalate

3,000

Symrise GmbH & Co. KG

Isoamyl p-Methoxycinnamate

3,000

Symrise GmbH & Co. KG

Butyl Methoxydibenzoylmet
hane

5,000

Symrise GmbH & Co. KG

Ethylhexyl Salicylate

5,000

Symrise GmbH & Co. KG

Tocopheryl Acetate

0,500

DSM Nutritional Products, CH

Titanium Dioxide, Alumina,


Simethicone

4,000

Merck KGaA, Germany

Disodium EDTA

0,100

BASF AG, Germany

Bisabolol

0,100

Symrise GmbH & Co. KG

Xanthan Gum

0,200

CP-Kelco, Germany

Carbomer

0,200

Noveon, Belgium

Water (Aqua)

43,400

Sodium Cetearyl Sulfate

0,750

Cognis Dtl. GmbH, Germany

Phenylbenzimidazole Sulfonic
Acid

5,000

Symrise GmbH & Co. KG

Disodium Phenyl
Dibenzimidazole Tetrasulfonate

4,550

Symrise GmbH & Co. KG

WWWWWWWWWWWWWWWWWW

Lanette O
WWWWWWWWWWWWWWWWWW

Tegosoft TN
WWWWWWWWWWWWWWWWWW

Dragoxat 89
(109854)
WWWWWWWWWWWWWWWWWW

Abil 350
WWWWWWWWWWWWWWWWWW

Neo Heliopan 303


(600154)
WWWWWWWWWWWWWWWWWW

Neo Heliopan HMS


(182573)
WWWWWWWWWWWWWWWWWW

Neo Heliopan E 1000


(656083)
WWWWWWWWWWWWWWWWWW

Neo Heliopan 357


(622501)
WWWWWWWWWWWWWWWWWW

Neo Heliopan OS
(131494)
WWWWWWWWWWWWWWWWWW

Vitamin E Acetate
WWWWWWWWWWWWWWWWWW

Eusolex T-2000
WWWWWWWWWWWWWWWWWW

Edeta BD
WWWWWWWWWWWWWWWWWW

(-)-Alpha-Bisabolol Natural
(660338)
WWWWWWWWWWWWWWWWWW

Keltrol RD
WWWWWWWWWWWWWWWWWW

Carbopol ETD 2050


WWWWWWWWWWWWWWWWWW

PHASE B
Water
WWWWWWWWWWWWWWWWWW

Lanette E
WWWWWWWWWWWWWWWWWW

Neo Heliopan Hydro (103089),


used as a 30% aq. solution
neutralized with
Triethanolamine
WWWWWWWWWWWWWWWWWW

Neo Heliopan AP (106796),


used as a 22% solution
Date: 13.11.2006

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30/CCSUN 4935/00
Sunscreen Softcream (O/W), SPF 43*, water-resistant**, with broad UVA Protection
(UVA/UVB Balance***)
neutralized with
triethanolamine
WWWWWWWWWWWWWWWWWW

Glycerin 99,5 P.

Glycerin

4,000

Phenoxyethanol,
Methylparaben, Ethylparaben,
Butylparaben, Propylparaben,
Isobutylparaben

0,800

Triethanolamine

0,500

Parfum

0,400

WWWWWWWWWWWWWWWWWW

Dragocide Liquid
(660079)
WWWWWWWWWWWWWWWWWW

Triethanolamine 99 %

Symrise GmbH & Co. KG

WWWWWWWWWWWWWWWWWW

PHASE C
Fragrance

Symrise GmbH & Co. KG

WWWWWWWWWWWWWWWWWW

Production Method
Production in a Becomix Mini Lab RW 2,5:
Part A:
Heat up to 85C (without Keltrol, Carbopol and Titanium Dioxide) until all ingredients completely dissolved.
Transfer into the preheated Becomix, add Keltrol, Carbopol and Titanium Dioxide and homogenise.
(Heating 85 C, Stirrer 1 m/S, Homogeniser 10m/s; 4 min, Vacuum -0,8 bar)
Part B:
Heat on a hotplate to 85C. Add part B to part A via the funnel. Stir for 10 min at 85C. Then cool down to
65C and homogenise for 5 min.
(Heating 85 C, Stirrer 1 m/S, Vacuum -0,8 bar; Homogeniser 10m/s; 5 min)
Cool down to ambient temperature.
Part C:
At ambient temperature add part C and homogenise. Ventilate and remove the product with homogenising.
(Stirrer 1 m/S, Vacuum -0,8 bar, Homogeniser 10 m/s; 5 min, Homogeniser 2 m/s; 3 min).
The pH value of the finished product should be approx. 7.3 to 7.5 and has to be checked.
Preparation of the 30 % Neo Heliopan Hydro solution:
52.25 % Water, demineralised
17.75 % Triethanolamine
30.00 % Neo Heliopan Hydro (103089)
Dissolve two thirds of triethanolamine in water. Then add with stirring Neo Heliopan Hydro. Add the rest of
triethanolamine until the solution becomes clear. The pH value of the finished Neo Heliopan Hydro solution
should be 7.5 - 8.0 and has to be checked. For longer time of storage it is advisable to add preservatives (eg
Parabens) to the solution.
(For example: 6,67% of the 30 % Neo Heliopan Hydro solution neutralised with triethanolamine equals 2%
active.)
Preparation of the 22% Neo Heliopan AP solution:
Date: 13.11.2006

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30/CCSUN 4935/00
Sunscreen Softcream (O/W), SPF 43*, water-resistant**, with broad UVA Protection
(UVA/UVB Balance***)

67.50% Water, demineralised


22.00% Neo Heliopan AP (106796)
approx. 10.50% Triethanolamine
Dissolve two thirds of triethanolamine in water. Then add with stirring Neo Heliopan AP. Slowly add the rest
of triethanolamine until the solution becomes clear. The pH value of the finished Neo Heliopan AP solution
should be 7.0 - 8.0 and has to be checked. If you don't need all triethanolamine complete to 100% with
water. For longer time of storage it is advisable to add preservatives (eg Parabens) to the solution.
(For example: 10% of the 22 % Neo Heliopan AP solution neutralised with triethanolamine equals 2,2%
active.)
*The SPF 43 was determined on a six-subject panel test based on the recommendation of the COLIPA
TASK FORCE "Sun Protection Measurement" (December 2005).
The product should be labelled SPF 40 (Colipa Recommendation No. 11 - SPF Classification / upper limlt,
COLIPA, June 2002)
**Water-Resistance:
An SPF of 27 was found after immersion using the method described by K. and A. Schrader: Akt. Dermatol.
20, 130-134, 1994.
*** UVA/UVB Balance according to DIN 67502: 42

Specifications:

pH :
Viscosity :

7,5
0,001 1/s - eta= 4547 Pas
5 1/s - eta= 15 Pas

Rheology-Instrument:
Haake RS1, sensor: PP 60/Ti, gap= 1,500 mm, T= 20C, Controlled
Stress

All information herein provided is to the best of our knowledge. Nevertheless we accept no responsibility for any
incorrectness or inaccuracy. You are requested in your own interest and sole responsibility to test the suitability,
compatibility and stability of preparations made on the basis of such information provided to you and also to ensure
that these preparations do not infringe third party rights, such as patents or other intellectual property rights.
Date: 13.11.2006

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