HACH ANALYSIS PROCEDURE

NO

NAME

Iron Ferrozine

Total iron

Total iron TPTZ

Phosphorus,reactive
( Orthophosphate )

Total Chlorine
F & T PP

Free Chlorine
F & T PP

Chloride

Silica (LR)

Silica (HR)

10

Ca & Mg Hardness

11
12

Total Hardness
Hydrazine

13

Sulfate

PROCEDURE
Blank(sample 10 ml)
Sample 25ml + Ferrozine iron reagent solution pillow ( 5")
( Jika timer habis tuang ke cuvet 10ml )
Blank(sample 10 ml)
Sample 10ml + FerroVer iron reagent powder pillow ( 3")
Blank(demin 10 ml) + TPTZ iron reagent powder pillow ( 3")
Sample 10ml + TPTZ iron reagent powder pillow ( 3")
Sebelum jalankan timer aduk dulu 30 detik.
Blank(sample 10 ml)
*Sample 10ml + phosVer 3 phosphate powder pillow ( 2")
jika pakai acid persulfate digestion tunggu 10"
*Sample 10ml + phosVer 3 phosphate accuVac ampul ( 2")
aduk 30 detik dulu
Blank(sample 10 ml)
Sample 10ml + DPD Total Chlorine powder pillow ( 3")
sebelum timer aduk dulu 20 detik
Blank(sample 10 ml)
Sample 10ml + DPD Free Chlorine powder pillow
Aduk dulu 20 detik,langsung read
Blank(demin 10 ml) + Mercuric Thiocyanate solution 0,8ml
+ Ferric ion solution 0,4ml ( 2")
Sample 10ml + Mercuric Thiocyanate solution 0,8ml
+ Ferric ion solution 0,4ml ( 2")
Blank(sample 10 ml) + Molybdate 3 reagent (14 tetes)(4")
+ Citric Acid reagent powder pillow ( 1")
Sample 10ml + Molybdate 3 reagent (14 tetes)(4")
+ Citric Acid reagent powder pillow ( 1")
+ Amino Acid F reagent powder pillow ( 2")
Blank(sample 1oml)
Sample 10ml + Molybdate reagent powder pillow for HR silica
+ Acid reagent powder pillow for HR silica ( 10")
+ Citric acid powder pillow ( 2")
1.Sample 100ml + Calcium & Magnesium indikator solution ( 1ml )
+ Alkali solution for Calcium & Magnesium ( 1ml )
2.Tuang dalam 3 cuvet 10ml ( masing-masing 10ml )
3.Ambil 1 u/ blank,tambahkan 1 M EDTA solution (1 tetes )
4.Ambil 1 u/ magnesium sample,tambahkan EGTA solution(1 tetes)
langsung cek ketemu Mg,jangan dikeluarkan dulu tapi keluar
menuju program Ca tekan Zero.
5.Masukkan cuvet ke-3 tanpa tambahan reagent lagi,tekan Read
ketemu hasil Ca.
Total Hardness = Ca + Mg
Blank(demin) 10ml + HydraVer 2 Hydrazine (0,5ml)(12")
Sample 10 ml + HydraVer 2 Hydrazine (0,5ml)(12")
Blank(sample) 10ml
Sample 10ml + SulfaVer 4 Reagent powder pillow ( 5")

P.GEL

RANGE

562

0.09 s/d 1.400 ppm

510

0.02 s/d 3.00 ppm

590

0.012 s/d 1.800 ppm

880

0.02 s/d 2.50 ppm

530

0.02 s/d 2.00 ppm

530

0.02 s/d 2.00 ppm

455

0,1 S/D 25.0 ppm

815

0.010 s/d 1.600 ppm

452

1 s/d 100 ppm

522

0.05 s/d 4.00 ppm

455

4 s/d 600 ppb

450

2 s/d 70 ppm