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MILL TEST CERTIFICATE Number: Page:

83474978.0.1 1/5
Date: August 15, 2013
Customer: MID STATES SUPPLY % WOMBLE INDUSTRIAL ROAD, HOUSTON, Customers Order Item: Customers Reference: Manufacturers Works Order N:
TX, 77015 31078146/SO/10 B081313BS3 N/A
Manufacturing Process: Product Type: Surface:
HFW Line Pipe Bare

Standard or Specification: Steel Grade: Ends:


API 5L X52M PSL 2 Plain End Bevelled

Dimensions: Schedule: Length: Quantity: 36 PCS Nominal Weight:


8.625 x 0.322 in N/A Double Random 1533 FT 44384 LB 28.58 LB/FT

TENSILE TEST
Specimen condition Specimen dimensions Test Y.S. U.T.S. Elongation
Heat N Sample N Zone Lot N temp .5% EUL Req.
Ls Sc Type Ori Size Min: 52 200 Min: 66 700 Lo Min. Obt.
Max: 76 900 Max: 110 200
in F psi psi in % %
233396 3579644 E1 233396 B AM Ss T 1.500 RT 68 100 74 200 2.0 27.0 40.2

AM: As manufactured Ls: Location of sample Ori: Orientation Ss: Strip specimen
B: Body Max: Maximum Req: Required T: Transversal
E1 / E2: Ends of Sampling Min: Minimum RT: Room temperature U.T.S: Ultimate tensile strength
Lo: Initial length Obt: Obtained Sc: Specimen condition Y.S: Yield strength

Specimen condition Specimen dimensions Test U.T.S.


Heat N Sample N Zone Lot N temp Req.
Ls Sc Type Ori Size Min: 66 700
Max: -
in F psi
233396 3579644 E1 233396 W AM Ss T 1.500 RT 78 710

AM: As manufactured Min: Minimum Sc: Specimen condition W: Weld


E1 / E2: Ends of Sampling Ori: Orientation Ss: Strip specimen
Ls: Location of sample Req: Required T: Transversal
Max: Maximum RT: Room temperature U.T.S: Ultimate tensile strength

This certificate is issued by a computerized system and it is valid with electronic signature. On the original certificate the trade-mark green colored
"Tenaris" is stamped. In case the owner of the original certificate would release a copy of it, he must attest its conformity to the original one taking
upon himself the responsibility for any unlawful or not allowed use. Any alteration and/or falsification will be subjected to the law.

FOR03171
MILL TEST CERTIFICATE Number: Page:

83474978.0.1 2/5
Date: August 15, 2013
Customer: MID STATES SUPPLY % WOMBLE INDUSTRIAL ROAD, HOUSTON, Customers Order Item: Customers Reference: Manufacturers Works Order N:
TX, 77015 31078146/SO/10 B081313BS3 N/A
Manufacturing Process: Product Type: Surface:
HFW Line Pipe Bare

Standard or Specification: Steel Grade: Ends:


API 5L X52M PSL 2 Plain End Bevelled

Dimensions: Schedule: Length: Quantity: 36 PCS Nominal Weight:


8.625 x 0.322 in N/A Double Random 1533 FT 44384 LB 28.58 LB/FT

CHEMICAL COMPOSITION
Composition %
X1

C Mn P S Si Cu Ni Cr Mo Al Sn Nb V Ti Ca B N CE-Pcm

H Max 0.22 1.4 0.025 0.015 0.45 0.5 0.3 0.3 0.15 -- -- -- -- -- -- 0.001 -- --
Min -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --
Heat N Sample N Lot N Ls P Max 0.22 1.4 0.025 0.015 0.45 0.5 0.3 0.3 0.15 -- -- -- -- -- -- 0.001 -- --
Min -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --
233396 3569965 233396 B.M. H 0.04 1.05 0.01 0.001 0.18 0.14 0.05 0.05 0.01 0.03 0.01 0.034 0.001 0.01 0.002 0 0.008 0.11
233396 3573117 233396 B.M. P 0.045 1.08 0.011 0.002 0.21 0.14 0.05 0.05 0.01 0.035 0.01 0.03 0.002 0.014 0.002 0.001 0.006 0.117
233396 3573137 233396 B.M. P 0.044 1.08 0.011 0.002 0.22 0.15 0.05 0.05 0.01 0.035 0.01 0.031 0.002 0.014 0.002 0 0.008 0.117

B.M: Base metal H: Heat Max: Maximum P: Product


CE-Pcm: CE-Pcm Ls: Location of sample Min: Minimum

THROUGH WALL HARDNESS


Required values Individuals Average Hardness type:HRBW
Min: - Max: - Var: -- Min: -- Max: -- Var: --
Heat N Sample N Lot N Specimen condition Scale Avg.
Ls Sc
233396 3579644 233396 B AM HRBW 84.5

AM: As manufactured B: Body Max: Maximum Sc: Specimen condition


Avg: Average Ls: Location of sample Min: Minimum Var: Variation

This certificate is issued by a computerized system and it is valid with electronic signature. On the original certificate the trade-mark green colored
"Tenaris" is stamped. In case the owner of the original certificate would release a copy of it, he must attest its conformity to the original one taking
upon himself the responsibility for any unlawful or not allowed use. Any alteration and/or falsification will be subjected to the law.

FOR03171
MILL TEST CERTIFICATE Number: Page:

83474978.0.1 3/5
Date: August 15, 2013
Customer: MID STATES SUPPLY % WOMBLE INDUSTRIAL ROAD, HOUSTON, Customers Order Item: Customers Reference: Manufacturers Works Order N:
TX, 77015 31078146/SO/10 B081313BS3 N/A
Manufacturing Process: Product Type: Surface:
HFW Line Pipe Bare

Standard or Specification: Steel Grade: Ends:


API 5L X52M PSL 2 Plain End Bevelled

Dimensions: Schedule: Length: Quantity: 36 PCS Nominal Weight:


8.625 x 0.322 in N/A Double Random 1533 FT 44384 LB 28.58 LB/FT

IMPACT TEST
Type: Charpy V Orientation: T Unit: FT-LBS Shear area %
Position: Temp: 32 Unit: F Ind.Min.Req: 10 Req.Min.Avg: 13 Ind.Min.Req: - Req.Min.Avg: -
Heat N Sample N Lot N T.T Size Results Results
Ls Sc F - 1 2 3 Avg. 1 2 3 Avg.
233396 3579644 233396 B AM -22 2/3 176.6 180.1 175.8 177.5 100 100 100 100

AM: As manufactured Ind. Min. Req: Individual Minimum Required Sc: Specimen condition
Avg: Average Ls: Location of sample T.T: Test temperature
B: Body Req. Min. Avg: Required minimum average Temp: Temperature

FLATTENING TEST
Standard:
Heat N Lot N Sample N Result

233396 233396 3579644 Good

This certificate is issued by a computerized system and it is valid with electronic signature. On the original certificate the trade-mark green colored
"Tenaris" is stamped. In case the owner of the original certificate would release a copy of it, he must attest its conformity to the original one taking
upon himself the responsibility for any unlawful or not allowed use. Any alteration and/or falsification will be subjected to the law.

FOR03171
MILL TEST CERTIFICATE Number: Page:

83474978.0.1 4/5
Date: August 15, 2013
Customer: MID STATES SUPPLY % WOMBLE INDUSTRIAL ROAD, HOUSTON, Customers Order Item: Customers Reference: Manufacturers Works Order N:
TX, 77015 31078146/SO/10 B081313BS3 N/A
Manufacturing Process: Product Type: Surface:
HFW Line Pipe Bare

Standard or Specification: Steel Grade: Ends:


API 5L X52M PSL 2 Plain End Bevelled

Dimensions: Schedule: Length: Quantity: 36 PCS Nominal Weight:


8.625 x 0.322 in N/A Double Random 1533 FT 44384 LB 28.58 LB/FT

HYDROSTATIC TEST
Pressure Time Results

Unit Value Seconds

psi 2,920 5 Satisfactory

SUPPLEMENTARY INFORMATION
Supplementary Information Supplementary Information

This material has been manufactured, sampled, tested and inspected in accordance with this NDT OK UT with ID/OD N-10 Notches verified by 1/8" FDH
specification and has been found to meet the requirements called for by the above order. COMPLIANT TO ASTM A53 GRADE B AND ASME SA53 GRADE B
This product is silicon and/or aluminum fully killed.

Heat Treatment

The minimum weld seam heat treatment temperature is 1650F.

Steel Vendor Name and Manufactured

233396,NUCOR STEEL HICKMAN,ARMOREL,AR,Melted and Manufactured in USA

This certificate is issued by a computerized system and it is valid with electronic signature. On the original certificate the trade-mark green colored
"Tenaris" is stamped. In case the owner of the original certificate would release a copy of it, he must attest its conformity to the original one taking
upon himself the responsibility for any unlawful or not allowed use. Any alteration and/or falsification will be subjected to the law.
FOR03171
MILL TEST CERTIFICATE Number: Page:

83474978.0.1 5/5
Date: August 15, 2013
Customer: MID STATES SUPPLY % WOMBLE INDUSTRIAL ROAD, HOUSTON, Customers Order Item: Customers Reference: Manufacturers Works Order N:
TX, 77015 31078146/SO/10 B081313BS3 N/A
Manufacturing Process: Product Type: Surface:
HFW Line Pipe Bare

Standard or Specification: Steel Grade: Ends:


API 5L X52M PSL 2 Plain End Bevelled

Dimensions: Schedule: Length: Quantity: 36 PCS Nominal Weight:


8.625 x 0.322 in N/A Double Random 1533 FT 44384 LB 28.58 LB/FT

SUMMARY REPORT
Heat N Quantity Length Weight

(Pieces) FT LB
233396 36 1,533.701 44,384.784

This is to certify that the product described here has been manufactured, sampled, tested, and inspected in accordance with
purchaser order requirements. This certificate is not a declaration of origin nor may it be used as a declaration of origin.

CUSTOMER . THIRD PARTY TENARIS QUALITY DEPARTMENT SIGNATURE


INSPECTION COMPANY
COMPAA DE INSPECCIN

Company Name: N/A


Employee Name: N/A QUALITY CERTIFICATION DEPT. CHIEF OF QUALITY CERTIFICATION DEPT.

Robert Semmel Emilio Fernandez

This certificate is issued by a computerized system and it is valid with electronic signature. On the original certificate the trade-mark green colored
"Tenaris" is stamped. In case the owner of the original certificate would release a copy of it, he must attest its conformity to the original one taking
upon himself the responsibility for any unlawful or not allowed use. Any alteration and/or falsification will be subjected to the law.
FOR03171