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Initial Final

Date / time
Draft reading Port Stb Mean Port Stb Mean
Forward 1.05 1.05 1.05 4.60 4.60 4.60
Steam correction 0 0
Corrected 1.05 4.60
Aft 0.55 0.55 0.55 5.10 5.10 5.10
Stern Corrtd. 0 0
Corrected 0.55 5.10
Mean fwd & Aft 0.80 4.85
Midship 0.00 0.00 0.000 0.000 0.000 0.000
Midship Correction 0.000 0.000
Corrected 0.000 0.000
Mean of Means 0.400 2.425
Quarter Mean 0.200 1.213

Cooresponding Displacement 1340.67 9761.301


Trim by head / Stern -0.50 16.061 0.50 -11.798
Trim correction
Displacement corrected for trim 1356.731 9749.503
Observed Density 1.018 1.018
Density correction -9.265 -66.582
Displacement corrtd of Density 1347.466 9682.921
Total consumable store & Balast 0 0
Net Displacement 1347.466 9682.921

TOTAL CARGO LOADED / DISCHARGED 8,335.456 MT


Initial Final
Date / time
Draft reading Port Stb Mean Port Stb Mean
Forward 8.280 8.280 8.280 14.870 14.870 14.870
Steam correction 0.008 -0.001
Corrected 8.272 14.869
Aft 10.350 10.350 10.350 15.077 15.077 15.077
Stern Corrtd. 0.012 0.009
Corrected 10.362 15.086
Mean fwd & Aft 9.3170 14.9775
Midship 9.390 9.400 9.395 15.084 15.084 15.084
Midship Correction 0.000 0.000
Corrected 9.395 15.084
Mean of Means 9.35600 15.03075
Quarter Mean 9.375500 15.057375

Cooresponding Displacement 42841 86092


Trim by head / Stern 2.58 -478 0.55 42
Trim correction
Displacement corrtd for trim 42363.000 86134.000
Observed Density 1.022 1.021
Density correction -123.989 -336.133
Displacement corrtd of Density 42239.011 85797.867
Total consumable store & Balast 24583 2337
Net Displacement 17656 -1686 83461

TOTAL CARGO LOADED / DISCHARGED 65,805 MT


INSTRUKSI KERJA LABORATORIUM TANAH MERAH ( TMCT)

HARI TANGGAL

NO OPERATOR JOB SAMPLE ID SAMPLE PARAMETER

PREPARED BY,

JAHRANI A.S.AGI
Supervisor lab
Proximate Analysis
Moisture In Analysis Sample
Dish No. 1 2
Wt. of Sample+Lid+Dish before Heating 145950 129891 5102 1700
Weight of Lid+Dish 135949 119887 -140848 -128191
Wt. of Sample+Lid+Dish After Heating 144607 128560
IM = (W2-W3) * 100%
13.429 13.305
(W2-W1)
0.12
Mean 13.37
Ash Content
Dish No. 1 2 db
Wt. of Dish + Coal 178146 161107
Wt. of Dish before heating 168146 151102
Wt. of Dish + Residue 168912 151520
Wt. of Dish after heating 168146 151102
% Ash = ( C-D ) * 100
7.660 4.178 3.48
( B-A )
Mean 5.92 6.83
Volatile Matter
Crus No. 1 2 db daf
Wt. of Crucible+lid+Sample before heating 777654 578354
677679 478364
758414 558946 .
% VM = ( X-Z ) *100 (a)
19.245 19.410
( X-Y )
Mean 19.328
% VM = a - IM 5.96 6.88 7.38
%Fixed Carbon = 100-IM-A-VM 74.75
417
151519

3.48

19154 19308
-758500 -559046

-0.17

39.4
19.7

38.63 12.85
51.480
FREE MOISTURE (TWO STAGE)
( Volume 3B, Method No. : P-007 and P-008 )

Job No : 07/S.278 Menthod :ASTM


Date : 06./11/09 Work shift :(Day)/(night)

Lab Sample Weight of Weight of Weight of % Loss of


ID Tray Tray+Sample Sample Weight
TM.5299. 1607.5 2623.4 1015.9
9 2594.8 987.3 2.82

Weight of Weight of Weight of % ADL % Loss of weight


JAM KE Tray Tray + Sample Sample dr. timb.sblmnya dr. timb. Awal
1 3200.4 5265.2 2064.8 -
5 5150.1 1949.7 5.57 5.570
6 5133.5 1933.1 6.38 0.850 0.80
7 5122.3 1921.9 6.92 0.580 0.54
8 5111.4 1911.0 7.45 0.570 0.53
9 5102.3 1901.9 7.89 0.480 0.44
10 5098.1 1897.7 8.09 0.220 0.20
11 5103 1902.6 7.86 -0.260 -0.24
12 5106.4 1906.0 7.69 -0.180 -0.16
13 5106.4 1906.0 7.69 0.000 0.00
14 5110.2 1909.8 7.51 -0.200 -0.18
15 5112.0 1911.6 7.42 -0.090 -0.09
16 5113.3 1912.9 7.36 -0.070 -0.06
17 5112.3 1911.9 7.41 0.050 0.05
18 0.0 100.00 100.000 92.59

Equalize 4927.3 1726.9 16.36


-3200.4

% FM TWO STAGE 18.71

Job No : 07/S.278 Menthod :ASTM


Date : 06./11/09 Work shift :(Day)/(night)

Lab Sample Weight of Weight of Weight of % Loss of


ID Tray Tray+Sample Sample Weight
TM.5298. 1607.5 2623.4 1015.9
9 2594.8 987.3 2.82

Weight of Weight of Weight of % ADL % Loss of weight


JAM KE Tray Tray + Sample Sample dr. timb.sblmnya dr. timb. Awal
1 3235.4 5226.9 2026.5 -
5 5165.9 1965.5 4.81 3.010
6 5148 1947.6 5.68 0.910 0.87
7 5134.8 1934.4 6.32 0.680 0.64
8 5120.9 1920.5 6.99 0.720 0.67
9 5110.2 1909.8 7.51 0.560 0.52
10 5099.9 1899.5 8.01 0.540 0.50
11 5096.4 1896.0 8.18 0.180 0.17
12 5102.1 1901.7 7.90 -0.300 -0.28
13 5105.4 1905.0 7.74 -0.170 -0.16
14 5108.4 1908.0 7.59 -0.160 -0.15
15 5111.1 1910.7 7.46 -0.140 -0.13
16 5113.3 1912.9 7.36 -0.120 -0.11
17 5112.3 1911.9 7.41 0.050 0.05
18 0.0 100.00 100.000 92.59

Equalize 4927.3 1726.9 16.36


-3200.4

% FM TWO STAGE 18.71

Job No : 07/S.278 Menthod :ASTM


Date : 06./11/09 Work shift :(Day)/(night)

Lab Sample Weight of Weight of Weight of % Loss of


ID Tray Tray+Sample Sample Weight
TM.5300. 1607.5 2623.4 1015.9
9 2594.8 987.3 2.82
Weight of Weight of Weight of % ADL % Loss of weight
JAM KE Tray Tray + Sample Sample dr. timb.sblmnya dr. timb. Awal
1 3219 5236.7 2017.7 -
5 5127.4 1908.2 7.58 5.430
6 5112.4 1893.4 8.30 0.780 0.72
7 5075.6 1856.6 10.08 1.940 1.78
8 5044.6 1825.6 11.58 1.670 1.50
9 5018.5 1799.5 12.85 1.430 1.26
10 4999.9 1780.9 13.75 1.030 0.90
11 4986.3 1767.3 14.41 0.760 0.66
12 4977.2 1758.3 14.84 0.510 0.44
13 4970.4 1751.4 15.18 0.390 0.33
14 4964.2 1745.2 15.48 0.350 0.30
15 4958.2 1739.2 15.77 0.340 0.29
16 4951.8 1732.8 16.08 0.370 0.31
17 4957.8 1738.8 15.79 -0.350 -0.29
18 4958.1 1739.1 15.77 -0.020 -0.01

Equalize 4963.5 1763.1 14.61


-3200.4

% FM TWO STAGE 17.01


bts
Total Sulphur And Calorific Value

TM : 18.36
IM : 19.10
Ash : 2.35
Total Sulphur
Mass of Coal 0.5000 0.5007 db daf
Vol.of 0.025 M Na2B4O7.10H2O used in Test (V1) 0.7600 0.7200
Vol.of 0.025 M Na2B4O7.10H2O used in Blank (V2) 0.0500 0.0400
% TS = 0.0802*(V1-V2)
0.114 0.109
W
Mean 0.11 0.14 0.14

Calorific Value
Heat Value (Mj/Kg) 21.8089 21.8436 db daf
Mean 21.8263
Total Sulphur 0.08
Corection Sulphur 0.0075
Gross CV (MJ/Kg) 21.8188
Gross CV (Cal/g) 5211 6442 6634
0.0050 0.0850

ml mb
-0.0347 18.81 19.49 5255.416
Job No. :
Date :
Lab. Sample ID :

Tray No Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of


Tray Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl
jam ke 1 5 6 7
1606.9 4031.6 2424.7 3980 2373.1 3961.4 3947.6

1620.1 4019 2398.9 3947 2326.9 3924.2 3904.7

1611.6 4074.7 2463.1 4007.3 2395.7 3991.1 3973.9

1620.1 4045 2424.9 3977.8 2357.7 3950.2 3935.4

TOTAL 6458.7 16170.3 9711.6 15912.1 9453.4 15826.9 9368.2 15761.6


% Loss of Weight 2.66 0.90 0.70
% Free Moisture 2.66 3.54 4.21
Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of
Sample Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample
8 9 10 11
3937.7 3923.5 3910 3898.7

3887.2 3876.4 3868.1 3859.6

3959.7 3949.7 3940.3 3924.8

3922.3 3911.5 3901.4 3895.7

9302.9 15706.9 9248.2 15661.1 9202.4 15619.8 9161.1 15578.8 9120.1


0.59 0.50 0.45 0.45
4.77 5.24 5.67 6.09
Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of Weight of
Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample Tray+Smpl Sample
12 13 14 15 16
3887.6 3877.2 3874.6 3872.9 3869.3

3851.4 3843.1 3838.3 3833 3829.4

3911.7 3899.7 3894.9 3891.9 3887.1

3889.5 3883.3 3876.5 3871.9 3866.6

15540.2 9081.5 15503.3 9044.6 15484.3 9025.6 15469.7 9011 15452.4 8993.7
0.42 0.41 0.21 0.16 0.19
6.49 6.87 7.06 7.21 7.39
Weight of Weight of Weight of Weight of Equalize
Tray+Smpl Sample Tray+Smpl Sample 3 jam
17 18
3864.3 3861.9 3866.1

3817.1 3812.3 3818.6

3884.4 3878.8 3884.6

3862 3855.1 3861.9

15427.8 8969.1 15408.1 8949.4 15431.2 8972.5


0.27 0.22
7.65 7.85 7.61
Dish No. 1 2 1
Wt. of Sample+Lid+Dish before Heating 138554 138614 137527
Weight of Lid+Dish 128557 128611 127534
Wt. of Sample+Lid+Dish After Heating 136908 136970 135719
IM = (W2-W3) * 100%
(W2-W1)
16.465 16.435 18.093
0.03
Mean 16.45 18.10

Dish No. 1 2
Wt. of Sample+Lid+Dish before Heating 135726 134022
Weight of Lid+Dish 125719 124017
Wt. of Sample+Lid+Dish After Heating 134496 132799
IM = (W2-W3) * 100%
(W2-W1)
12.2910 12.2240
0.07
Mean 12.26
2
125865
115860
124054
18.101
-0.01
18.10
50 7860 3.68 3.68
-50 + 31.5 17890 8.37 8.37
-31.5 + 16 37970 17.77 17.77
-16 + 8 46320 21.68 21.68
-8 + 2 7600.5 46.19 22.40 22.40
-2 26.10
100.00
(A) 110040 51.50 7600.5 46.19 22.40
(B) 103630 48.50 8793.5 53.44 25.92
sample used(C') 213670 100.00 16456.3 100.00
Loss (D) - 0 62.3 0.38 0.18
B+D 48.50 26.10
F 0.4850 0.261
12.05
29.82
51.50
73.90
100.00