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18/7/2017 the synthesis of urea-calcium phosphate by using ball milling

reaction between calsium phosphate and urea


reaction name : mechanochemistry
ratio between ball milling and sample 20g-1g (double the ratio in
experiment 40:2)
ratio between calsium phosphate and urea is (set 1 is 50 wt%: 50 wt%) and
set 2 is 1(10wt%: 90 wt%)
the parameter is time (5 hours),
radius of ball mining???

ball milling.......clean it with ethanol and after rinse it with ethanol.


.......dry the ball milling in dryer about 15 minutes

Thursday and friday....analyse the sample with XDR and xxx on thursday and friday.
....check new peak on the sample.
....

19/7/2017 1st
for the sample (ratio 50:50%), wash the sample with ethanol to get the rest
of the sample.
analyze it with two samples yesterday.

2nd
identify the which component that change the phase whether urea or
calcium phosphate
the procedure same like the synthesis of urea-calcium phosphate.
Set 1 = Urea and Set 2 = Calcium Phosphate
reaction name : mechanochemistry
ratio between ball milling and sample 20g-1g (double the ratio in
experiment 40:2)
ratio between urea and calcium phosphate is (set 1 is 100 wt%: 0 wt%) and
set 2 is 1(0wt%: 100 wt%)
time : 5 hours
techniques : ball milling
ball milling radius :
result: the phase of both sample does not changed (still in solid)

20/7/2017 1st
RUN 1
the synthesis of urea-calcium phosphate by using ball milling
reaction between calsium phosphate and urea
reaction name : mechanochemistry
ratio between ball milling and sample 20g-1g (double the ratio in
experiment 40:2)
ratio between calsium phosphate and urea is (set 1 is 50 wt%: 50 wt%) and
set 2 is 1(10wt%: 90 wt%)
the parameter is time (2 hours)

2nd
DSC result
samples on (18/7/2017)
Set 1 and Set 2
samples on (19/7/2017)
Set 1 and Set 2

the result will be analyze on monday 24/7/2017


3rd
RUN 3
the synthesis of urea-calcium phosphate by using ball milling
reaction between calsium phosphate and urea
reaction name : mechanochemistry
ratio between ball milling and sample 20g-1g (double the ratio in
experiment 40:2)
ratio between calsium phosphate and urea is set 1 is (1mole : 4mole) and
set 2 is (1mole : 2mole)
the parameter is time (2 hours)