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Process specification
for
09-T-0005
Purge gas scrubber
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Lake Charles Methanol, LLC
Lake Charles Methanol Project
Document ID
5000 STPD grade AA Methanol Unit S-06030 P58005-T 0
Job no. Doc. no. Rev.
Page Item no.
Purge gas scrubber
2 of 4
09-T-0005
Operating data
Design case EOR design case
Fluid description Purge gas/Distilled water
Vapor inlet Design
Temperature 110 F
Pressure 62 psig
Gas flow 31377 lb/h
Gas density 0.16 lb/ft
Gas viscosity 0.016 cP
Gas molecular weight 12.52 lb/lbmol
Liquid inlet Design
Temperature 109 F
Pressure 60 psig
Liquid flow 12419 lb/h
Liquid density 61.89 lb/ft
Liquid viscosity 0.622 cP
Liquid surface tension 69.31 dyn/cm
Vapor outlet Design
Temperature 113 F
Pressure 60 psig
Gas flow 30393 lb/h
Gas density 0.15 lb/ft
Gas viscosity 0.016 cP
Gas molecular weight 12.19 lb/lbmol
Liquid outlet Design
Temperature 111 F
Pressure 62 psig
Liquid flow 13403 lb/h
Liquid density 59.97 lb/ft
Liquid viscosity 0.592 cP
Liquid surface tension 59 dyn/cm
Mechanical data
Location Outdoor
Design temperature (min.) 14 F Construction code ASME Sec. VIII
Design temperature (max.) 220 F Stress relieving According to code
Design pressure (min.) psig Construction material SS304L
Design pressure (max.) 150 psig Corrosion allowance 0 in
Insulation purpose None
Inner diameter 2) 40 in Top head type Ellipsoidal
Tangent to tangent distance 2) 312 in Bottom head type Ellipsoidal
Elevation in
Demister
Type York mesh type 709 or similar
Effective diameter 38 in Capacity constant 1417 ft/h
Thickness 6 in Construction material SS316
Demister top to TL distance 10 in Mounting Doughnut ring
Design of demister support must ensure a negligible flow restriction as per Topsoe standard 4-1323/U.
Design requirements
Construction material requirements
Design H2 partial pressure 113 psia
Nozzle data
Ref. No. Size Description Details
A1 1 2" Wash water inlet Liquid feed pipe
A2 1 16" Purge gas inlet
B1 1 16" Washed purge gas outlet
B2 1 2" Wash water outlet Vortex breaker
H1 1 6" Handhole
L1-8 8 2" Level instrument
M1-2 2 Full size flange Manhole
P1-2 2 2" Pressure differential transmitter
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Lake Charles Methanol, LLC
Lake Charles Methanol Project
Document ID
5000 STPD grade AA Methanol Unit S-06030 P58005-T 0
Job no. Doc. no. Rev.
Page Item no.
Purge gas scrubber
3 of 4
09-T-0005
Liquid feed pipe details (nozzle A1)
Length in
Koch-Glitsch type 119 or equivalent
Remarks
1 Column has been designed with 20% extra liquid flow. Operating data shown without this margin.
2 Column ID and tagent to tangent length are indicative only, shall be specified by packing vendor. Selected design shall be
verified by Topsoe.
3 Estimated approach to flooding is 62%. To be confirmed by packing vendor.
4 If full diameter structured packing layer is installed then vendor shall put another flanged connection beneath the inlet
distributor.
5 Specified bed height corresponds to 15 layers of Flexipac HC 350Y, material SS304. Total bed height should
correspond to approximately 6 equilibrium stages. To be verified by packing vendor.
40
B1
T.L.
16
38 M1
50
A1 P1
312
159
M2
P2
A2
Maximum level L1 L3 L5 L7
High level
87
Low level
42
Minimum level
36
L2 L4 L6 L8
26
H1
20
T.L.
B2