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experimental results and the agreement is .found to be where x1 and xz are, respectively, the fiber orientation
satisfactory. 0 1996 Elsevier Science Limited and fiber length factors, and the product of x1 and xz,
i.e. x1x2, is the fiber efficiency factor for the strength
Keywords: composites, fiber length distribution, fiber of the composite; a,, and af, are the ultimate strength
orientation distribution, strength of SFRP of the composite and fiber, respectively; V, and V,
denote the volume fraction of the fiber and matrix;
and u, is the matrix stress at the failure of the
1 INTRODUCTION composite. For unidirectional discontinuous compos-
ites x1 = 1 and x2 < 1. If the fiber length is uniform
Short-fiber-reinforced polymers (SFRP) are used
and equals L, then
increasingly as a structural material because they not
only provide superior mechanical properties, but they x2 = Ll(2LJ for L CL, (2)
can also be easily produced by the rapid, low-cost
x2 = 1 - LJ(2L) for L 2 L, (3)
injection molding process. During the injection
process of fiber-reinforced molded articles, the where L,, the critical fiber length, is given by
distributions of fiber length and fiber orientation are L, = rfa,,/ri, where Zi and rf are the interfacial shear
governed by a variety of factors. These include the stress between matix and fibers and the fiber radius,
original length and concentration of fibers, the gate respectively. If the fiber length is not uniform, eqns
design and the processing conditions.- It was pointed (2) and (3) must be modified. Kelly and Tyson** put
out that the mechanical properties of any material forward a model considering the effect of fibers,
1179
1180 S.-Y. Fu, B. Lauke
shorter and longer than the critical fiber length. This distribution with an asymmetric character with a tail at
model can be given by:17 long fiber lengths.5*2~13~27~28
The mechanical properties
of SFRP are undoubtedly related to this distribution.
The fiber length distribution can be described with a
probability density function. Let us define the fiber
length probability density function, f(L), so that
+ C ~fU[l -
L, = L,
Lcl(2Lj)] + VmU, (4) f(L)dL and F(L) are the probability density that the
length of fiber is between L and L + dL and the
The first and second terms take into account the probability that the length of a fiber is less than or
contributions of fibers with sub-critical length shorter equal to L, respectively. Then the relationship of f(L)
than L, and of fibers with super-critical length longer and F(L) is:
than L,, respectively. However, the contribution of
the fiber orientation is not considered. This model is F(L) = lLf(x) & and Imf(x) dx = 1 (6)
modified by the addition of an orientation factor to 0
+ 2yafu,[l -
L,=L,
LI(2Lj)JJ
I
+ J&U, (5) f(L) = (m/n)(L/n)-lexp[ - (L/n)] for L > 0 (7)
The critical damage zone model of Fukuda and where m and n are shape parameters. Another form
Chou was also used to predict the tensile strength of of Weibull distribution, i.e. the so-called Tung
the SFRP.24 This model goes one step further by distribution has been given:
considering the distribution function of both the fiber f(L) = abLbwlexp( - aLb) for L > 0 (8)
length and the fiber orientation. However, the
generalized formulae of both the fiber length where a and b are scale and shape parameters,
distribution function and the fiber orientation respectively. Inserting b = m and a = 12~~into eqn (8),
distribution function are not given, thus the effects of it then becomes the same as eqn (7). Equation (8) has
the fiber length and orientation distributions on the also been used successfully for describing the fiber
strength of SFRP cannot be studied; the dependences length distribution in short-glass-fiber-reinforced
of the ultimate fiber strength and the critical fiber polyamide. 27 In the present study, therefore, we adopt
length on the inclination angle 8, which must be this probability density function and prefer the form
considered,16325,26are not taken into account. of eqn (8) as the fiber length distribution function of
In the present paper two probability density SFRP since it appears simple. The cumulative
functions are used for modelling the fiber length and distribution function, F(L), can be obtained by
orientation distributions respectively, which have been combining eqns (6) and (8):
used with the aim of predicting the elastic properties
of SFRP.12*3,27The strength of SFRP is then derived F(L) = 1 - exp( - aLb) for L > 0 Pa)
as a function of the fiber length and fiber orientation
Therefore, the percentage, (Y, of fibers with lengths
distributions by considering the dependences of the
shorter than L, can be evaluated by:
ultimate fiber strength and the critical fiber length on
the inclination angle and the effect of inclination angle (Y= 1 - exp( - aLb,) (9b)
on the bridging stress of oblique fibers. The effects of
the fiber length distribution and the fiber orientation From eqn (8) we can get the mean fiber length (i.e.
distribution on the tensile strength of composites are the number average fiber length):
discussed in detail. Finally, the present theory is m
applied to existing experimental results. L mean= Lf (L) dL = a -lbr(l/b + 1) (10)
i0
2.2 Fiber orientation distribution (FOD) Differentiating eqn (12) and letting the resultant
During extrusion compounding and injection molding equation be zero we get:
processes, progressive and continuous changes in fiber
orientation throughout the molded components take 8 mod= arctan{[(2p - 1)/(2q - l)]} (13)
place. The changes are related in a complex way to
the size and concentration of fibers, the flow behavior Equation (13) represents the most probable fiber
of melted polymer matrix, the mold cavity and the orientation angle. When p = q = 1, emod = x/4; when
processing conditions. An orientation distribution p = 1 and q > 1, then ornod> n/4; when p 11 and
generally requires a three-dimensional description. q = 1, then emmod > ~14; when p = l/2, ornod= 0; when
However, when investigating the effect of the fiber q = l/2, then emod= ~12; when p = q = l/2, then there
orientation angle on the strength of short-fiber is no emmodand the fibers distribute randomly; the
composites, only the angle, 8, between the fiber axis corresponding fiber orientation distribution curves are
and the loading direction needs to be shown in Fig. 1. When p = l/2, large q (e.g. 100)
considered.19v24*29For example, the loading direction indicates that fibers have a major preferential
can be placed in the direction parallel to the mold fill alignment parallel to the 8 = 0 direction; when
direction, then this fiber orientation angle is the q = l/2, large p (e.g. 100) expresses that fibers have a
inclination angle or the out-of-plane angle, as defined major preferential orientation normal to the 8 = 0
previously,3C32 respectively. A fiber orientation direction; this is shown in Table 2. So, all the cases of
distribution function representing the inclination angle fiber orientation distribution are included in eqn (12).
must have the property such that the variation of its Thus eqn (12) is a suitable probability density function
functions shape parameters is able to describe a for describing the fiber orientation distribution and
change from a unidirectional distribution to a random will be used in the present study.
distribution. The mean fiber orientation, e,,,,, can be derived
Let us define a fiber orientation density function from eqn (12) as follows:
f(e) such that f(6)de is the probability density that
%ax
the orientation of fiber is between 8 and 8 + de. With
this assumption, Xia et ~1.~ proposed a two-parameter
exponential function to describe the fiber orientation
e IlEa
=
I@nun
e(e) de (14)
distribution in the injection molded specimens. Similar The fiber orientation coefficient, fe, can be definied
to this definition, the fiber orientation distribution as follows:16,29
function is given as follows:
{sin(f3)}2p-1{c0s(e)}2~~1 fe = 2&s(s)cos(e) de - i (15)
g(e) = TBmu* (12)
J
e,,,, {sin(f3))2~-1{c0s(e))2q- de
When fe = - 1, all fibers lie perpendicular to the
where p and q are the shape parameters which can be loading direction; fe = 0 corresponds to a random
used to determine the shape of the distribution curve, distribution in the angle 6; fe = 1 implies all fibers are
and p 1 l/2 and q 2 l/2. Also, 0 I emin5 8 I t3,,, 5 aligned parallel to the loading direction.
7ri2. The cumulative distribution function of fiber
orientation is then given by:
c(e) = Ie g(e) de
I.41 1 i %U.
1.2.
e
l- {sin(e)}2~-1{c0s(e)}2q--I de
I
0.8. = %I,
%a (16)
0.6. {sin( e)}2P-1{cos( e)}2q-1 de
0.4. I%,
0.2.
0, 2.3 Bridging stress of fibers
When an applied load is exerted on a short-fiber-
reinforced polymer, the interfacial shear stress
0 between fibers and matrix will increase with the
Fig. 1. Fiber orientation distribution curves for: (a) applied stress.33 In order to estimate the force
p = q = 1; (b) p = 1, q = 2; (c) p = 2, q = 1; (d) p = l/2, required to break the composite at some random
q = 2; (e) p = 2, q = l/2; (f) p = q = 112. cross-section, the bridging stress of fibers across the
1182 S.-Y. Fu, B. Lauke
failure plane needs to be evaluated16 and the single reduced significantly and decreases with the increase
fiber bridging case will be considered first. of inclination angle. So the introduction of the
When a fiber crosses the crack plane and the fiber inclined tensile strength of fibers can undoubtedly
orients parallel to the normal of the crack plane or the help to predict better the mechanical behavior of
applied load, F (see Fig. 2(a)), then the bridging short-fiber composites. If the fibers are brittle (e.g.
stress, af, of the fiber across the crack is given by: glass fibers, etc.), then crfUecan be expressed using the
(Tf= L,27wfzil(n$) = 2L,Zi/rf for L, < LJ2 (17a) following formula:6~25
(4 Fibre Matrix and the effect of the crack diversion for the very short
I I I r I
I
1
embedded segment case which was considered by
l--L Piggott.16
I I I 1:
II_lL___iI
Secondly, we consider composites with the fibers
r I I II oriented obliquely at an angle 0 with the crack plane,
a part of which is shown schematically in Fig. 3(b).
Similar to the above derivation, we get the average
bridging stress of fibers crossing the crack plane as
follows:
gf0 = (L/4)2Krfriexp(p@)/(Z$)
= af,Lexp(kf3)/(2L,) for L < LCB (28)
gfe = {(L,,/L)(Lc,/4)2RrfzeXP(~~)
+ (I- LfJL)~fuddl/(ti)
=
af,,(l - Ll(2L)) for L 2 LB (29)
When 0 equals zero, eqns (28) and (29) are the same
as eqns (2) and (3).
Substituting eqns (20), (22), (28) and (29) into eqn respect to the loading direction on the c axis (i.e.
(33), we get the strength of SFRP: loading direction) is:
L,= k0qe) (40)
Thus the average number of fibers of length from L to
L + dL and an angle from 8 to 8 + de, which cross an
%m Lmx
x exp(@) dLd6J +
I I
%ul &ll
f(Lk(~)(LILl-M)
arbitrary section in the specimen, can be given by:
NC= NiLp/c (41)
X (+r,(l -A tan(e))(l - L,(l -A tan(e))
where N, is the number of fibers of length from L to
L + dL and an angle from 8 to 0 + de as that given by
/(2Lexp(@))) dLd6J f v,,,Vm (34) eqn (30). Then the composite strength can be
I
obtained:
Equation (34) can be rewritten in the following form:
b: L, = 0. 4 mm
IC: L, = 0. 8 mm
.
40%
s
f 20%
ii
It
0%
0 0.1 0.2 0.3 0.4 0.5 0.6
0 2 4 8 8 10
Mean fibre length, L,,,, [mm] Critical fibre length, L, [mm]
Fig. 6. Variation of the percentage, (Y,of fibers with L CL,
Fig. 4. Variation of the percentage, LX,of fibers with L -CL, as critical fiber length, L,, varies (L,,,, = 0.4 mm,
as mean fiber length, L,,,, varies for the cases of different L _, = 0.213 mm, Lmin= 0 mm and L,,,= m mm).
LC (kIlod = 0.2 mm, L_ = 0 mm and L,,,= m mm).
1. 2
0. 2 1 J
0 2 4 6 8 10 0 0.1 0.2 0.3 0.4 0.5 0.6
4 150%
Table 1. Parameters b and a, mean fiber length, mode
V
A fiber length, critical fiber length, the content of fibers with
2 120% a subcritical fiber length and fiber length factor, ,yz
B
b l-5 1.5 1.5 1.5 1.5
!! 90% a 3.390 1.846 1.199 0.858 0.653
a-
E L ITlCi 0.4 0.6 0.8 1 .O 1.2
z L mod 0.213 0.320 0.426 0.533 0,639
d 60%
LC 0.2 0.3 0.4. 0.5 0.6
& % of L < L, 26.2 26.2 26.2 26.2 26.2
30% x2 0.766 0.766 0.766 0.766 0.766
i!
8 LC 0.8 1.2 1.6 2.0 2.4
t % of L < L, 91.2 91.2 91.2 91.2 91.2
P 0% x2 0.355 0.355 0.355 0.355 0.355
0 0. 1 0.2 0.3 0.4
Table 3. The effect of fiber orientation distribution on the the value of x1x2 and hence the strength of composites
TS of SFRP increases rapidly with the mean fiber length at small
mean fiber lengths (in the vicinity of L,) and
No. p q %lean %lmod fe x1x2 approaches gradually a plateau level at large mean
1 0.5 1 0.571 0.0 0.33 0.549 fiber lengths (greater than about 5LJ. This is the same
2 1 2 0.589 0.524 0.33 0.569 as that for the case of unidirectional composites (see
3 2 4 0.601 0.580 0.33 0.588 Fig. 5).
4 4 8 0.608 0.599 0.33 0.595 Figure 11 represents the effects of the mode fiber
5 0.5 0.5 0.785 0 0.417
6 1 1 0.785 0%5 0 0.416 length and the critical fiber length on the value of
7 2 2 0.785 0.785 0 0.415 x,x2. It shows that the value of x1x2 and hence the
8 4 4 0.785 0.785 0 0.414 composite strength increases with the decrease of
9 8 4 0.962 0,972 -0.33 0.351 critical fiber length; moreover, the value of x1x2 and
10 4 2 0.970 0.991 -0.33 0.330 hence the composite strength decreases slightly with
11 2 1 0.982 1.047 -0.33 0*308
12 1 0.5 0.999 l-57 -0.33 0.290 the increase of mode fiber length. These are the same
as those for the case of unidirectional composites (see
Figs 5, 7 and 9).
Figure 12 shows the effect of the snubbing friction
contrary, when fe < 0, then the value of x1x2 decreases coefficient on xa2, where A = 0.4, Lmin = 0, L,,, = ~0,
with the increase of mean fiber orientation angle. L ,_,,, = 0.4 mm, L, = O-2 mm and Lmod= 0.213 mm,
When fe = 0, there is almost no change in the mean
and p = 0.5 and q = 10 for the fiber orientation
fiber orientation angle and the value of x1x2. No direct
distribution function, respectively. It becomes clear
relationship is found between the value of x1x2 and
that the value of x1x2 increases slightly with the
the most probable fiber orientation angle, ornod.
snubbing friction coefficient, which demonstrates that
When adding the consideration of the fiber
the snubbing friction has only a small effect on the
orientation distribution, since the inclined tensile
strength of composites.
strength and critical fiber length of oblique fibers are
Figure 13 shows the effect of the constant A on the
related to the inclination angle, the effect of the fiber
value of x1x2. It becomes clear that the value of the
length distribution on the TS of SFRP can be studied
fiber efficiency factor, x1x2, decreases with the
based on eqn (36).
increase of the constant, A. This indicates that if the
Figure 10 shows the effects of the mean fiber length
fiber flexural effect on the fracture strength of oblique
on the fiber efficiency factor, x1x2, where p = 0.1,
fibers is smaller, then the composite strength would be
A ~0.4, Lmin=O, L,,,= 00, L,,,=0*2mm and
higher. Otherwise, the composite strength would be
L, = O-2 mm, the parameters a and b are the same as
lower. So the inclined tensile strength of fibers is a
in Figs 4 and 5 for the fiber length distribution
very useful parameter for the development of
function, p = O-5 and q = 10 for the fiber orientation
non-unidirectional SFRP.
distribution function. It can be seen from Fig. 10 that
1. 2
2 0.8 G!
b: L, = 0. 4 mm
s ?z '
c: L, = 0. 8 mm
i0 L"
0
, 0.6 t; 0. 8
,m
e a
6 2 0. 6
b
S 0.4 .s_
G g 0. 4
5
s!
.o 0. 2
Pe! 02.
ii
0
ii
0 L J
0 0. 1 0. 2 0. 3 0. 4
0 2 4 6 a 10
Mode fibre length, L,,,,,,,[mm]
Mean fibre length, L,,,, [mm]
Fig. 10. Effect of mean fiber length, L,,,,, on fiber Fig. 11. Effects of mode fiber length, Lmod,and critical fiber
efficiency factor, x1x2, for the case of non-unidirectional length, L,, on fiber efficiency factor, x1x2, for the case of
composites (p = 0.1, A = 0.4, L, = 0.2 mm, L,, = 0.2 mm, non-unidirectional composites (p = 0.1, A = 0.4, L,,, =
Lmin= 0 mm, L,,, = CCmm, p = 0.5 and q = 10 (@,,,,, = 0.4 mm, L,, = 0 mm, L,, = 30mm, p = 0.5 and q = 10
0.179 rad)). ( kl,,, = 0.179 rad)).
1188 S.-Y. Fu. B. Lauke
2
2 5 CONCLUSIONS
i 0. 6
0 The effects of the fiber length distribution and the
ti
J! fiber orientation distribution on the strength have
6 0. 4 been studied in detail for SFRP. The results show that
f the strength of SFRP increases rapidly with the
'G
increase of the mean fiber length at small mean fiber
f
g! 0. 2 lengths (in the vicinity of the critical fiber length, L,)
P and approaches a plateau level as the mean fiber
ii
length increases for the cases of large mean fiber
0 lengths ( > 5LJ. And the composite strength increases
0 0. 4 0. 8 1. 2 1. 6 2 with the decrease of critical fiber length and hence
with the increase of interfacial adhesion strength and
Constant A
slightly with the decrease of the mode fiber length.
Fig. 13. Ef f e c t of constant A on fiber efficiency factor, x1x2 When the ratios of L,,,,/L, and L,,/L, are the same
(p = O-1, L,,,= 0.4mm, L,= 0. 2 mm, Lmod= 0.213 mm,
L,,=O mm, L,,,= ~0mm, p = O-5 and q = 10 (@,,_,, = for a given fiber/matrix system, the strength of SFRP
0.179 rad)). will be the same no matter how large L,,,,, Lmod and
Effects offiber distributions on the strength of SFRP 1189
Table 4. Comparison of the present theory with the existing experimental resdts9
ID a b P 4 f A (XI& (X1X*)1
L, are. In general the strength of composites increases properties and fiber orientation. Polym. Comp., 10
with the increase of fiber orientation coefficient, fe, (1989) 454-461.
4. von Turkovich, R. & Erwin, L. Fiber fracture in
and the decrease of mean fiber orientation angle; reinforced thermoplastic processing. Polym. Engng Sci.,
however, when the fiber orientation coefficients are 23 (1983) 743-749.
the same, the strength of composites increases with 5. Gupta, V. B., Mittal, R. K. & Sharma, P. K. Some
the increase of mean fiber orientation angle for fe > 0 studies on glass-fibre-reinforced polypropylene: I.
and increases with the decrease of mean fiber length Reduction in fibre length during processing. Polym.
Comp., 10 (1989) 8-15.
for fe < 0. No direct relationship is found between the 6. Lauke, B., Schultrich, B. & Pompe, W. Theoretical
strength of SFRP and the most probable fiber considerations of toughness of short-fibre reinforced
orientation angle. The effect of the snubbing friction thermoplastics. Polym. Plast. Technol. Engng, 29 (1990)
between fiber and matrix on the strength of SFRP is 607-806.
small. The inclined tensile strength of fibers has a 7. Vu-Khanh, T., Denault, J., Habib, P. & Low, A. The
effects of injection molding on the mechanical behavior
great effect on the strength of composites. The present of long-fiber reinforced PBT/PET blends. Comp. Sci.
theory is successfully applied to the existing Technol., 40 (1991) 423-435.
experimental results. 8. Cox, H. L. The elasticity and strength of paper and
other fibrous materials. Brit. .I. Appl. Phys, 3 (1952) 72.
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ACKNOWLEDGEMENT Pulp Paper Mug. Can., 61 (1960) 230-240.
10. Schulgasser, K. Fibre orientation in machine-made
The authors would like to thank the Alexander von paper. J. Mater. Sci., 20 (1985) 859-866.
Humboldt foundation for financially supporting this 11. Hine, P. J., Davidson, N., Duckett, R. A. & Ward, I. M.
work. Measuring the fibre orientation and modelling the
elastic properties of injection-molded long-fibre-
reinforced nylon. Comp. Sci. Technol., 53 (1995)
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