Professional Documents
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WHAT IS MEASURABLE
AND MAKE MEASURABLE
THAT WHICH IS NOT
'ALILEO 'ALILEI
AMVn
Automated Microviscometer
Instruction Manual
AMVn
Automated Microviscometer
Nor is any liability assumed for damages resulting from information contained in the document.
Anton Paar GmbH reserves the right to content changes. This also extends to changes to delivery
volumes or any features of delivered parts.
All rights reserved (including translation). This document, or any part of it, may not be reproduced,
changed, copied, or distributed by means of electronic systems in any form (print, photocopy, microfilm
or any other process) without prior written permission by Anton Paar GmbH.
Trademarks, registered trademarks, trade names, etc. may be used in this manual without being marked
as such. They are the property of their respective owner.
E-Mail: rheology@anton-paar.com
Web: www.anton-paar.com
B80IB01 5
7.3 Displaying the Measured Values ........................................................................................... 25
7.4 Printing the Measured Values................................................................................................ 26
7.5 Cleaning the Measuring System............................................................................................ 27
8 AMVn Firmware Update................................................................................................................. 28
8.1 Menu "SETUP Instrument" ................................................................................................. 28
8.1.1 Date and Time ........................................................................................................ 28
8.1.2 Temperature Equilibration ...................................................................................... 29
8.1.2.1 Temperature Equilibration in "constant mode" ........................................ 29
8.1.2.2 Temperature Equilibration in "auto mode"............................................... 29
8.1.3 Default Settings ...................................................................................................... 30
8.1.4 Printer Configuration .............................................................................................. 30
8.1.5 Software Update..................................................................................................... 31
8.1.6 Zero Point Adjustment............................................................................................ 31
8.2 Menu "SETUP Measurement" ............................................................................................ 32
8.2.1 Method ................................................................................................................... 32
8.2.2 Measuring System.................................................................................................. 34
8.3 Menu "Print Configuration" ................................................................................................. 35
9 Calibration of Measuring Systems ............................................................................................... 36
9.1 Calibrated and Uncalibrated Capillaries ................................................................................ 36
9.2 Menu Calibration.................................................................................................................... 36
9.3 Calibrating a New Measuring System.................................................................................... 37
10 Maintenance ................................................................................................................................... 38
10.1 Cleaning the Measuring System............................................................................................ 38
10.2 Cleaning the Filling Adapter................................................................................................... 38
10.3 Cleaning AMVn...................................................................................................................... 39
10.4 Wetted Parts of AMVn ........................................................................................................... 39
10.5 Replacing O-rings in the Filling Adapter ................................................................................ 40
10.5.1 Filling Adapter Without Engraved Marking Ring .................................................... 40
10.5.2 Filling Adapter With Engraved Marking Ring ......................................................... 40
10.5.3 Exchanging the O-rings.......................................................................................... 40
11 Technical Data ................................................................................................................................ 41
Appendix A: Viscosity..................................................................................................................... 42
A.1 Viscosity Standard Fluids .................................................................................... 42
A.2 Calibration Constant K1 ...................................................................................... 43
A.3 Determining the Viscosity.................................................................................... 43
Appendix B: Extension of the Measuring Range.......................................................................... 44
B.1 Quadrupling the Maximum Measuring Range..................................................... 44
B.2 Doubling the Maximum Measuring Range .......................................................... 45
Appendix C: Menu Tree Firmware Structure.............................................................................. 46
6 B80IB01
B80IB01 7
1 About the Instruction Manual
Warning:
This symbol calls attention to the risk of accidental injuries or damage to
goods. Do not proceed until the indicated conditions for averting this threat
are fully understood and met.
Caution:
This symbol calls attention to the risk of instrument damage or
measurement errors. Do not proceed until the indicated conditions for
averting this threat are fully understood and met.
Information:
This symbol calls attention to any additional information of use to the
operator.
8 B80IB01
2 Safety Instructions
2 Safety Instructions
Read the instruction manual at hand before using AMVn.
2.1.1 Liability
The instruction manual at hand does not claim to address all safety issues
associated with the use of the instrument and samples. It is your
responsibility to establish health and safety practices and determine the
applicability of regulatory limitations.
Only use AMVn for the purpose described in this instruction manual. Anton
Paar GmbH is not liable for damages caused by incorrect use of AMVn.
Do not use any accessories or wearing parts other than those supplied or
approved by Anton Paar GmbH.
Make sure all operators are trained to use the instrument safely and correctly
before starting any applicable operations.
Check AMVn for chemical resistance to the samples and cleaning agents.
The results delivered by AMVn not only depend on the correct function of the
instrument, but also on various other factors. We therefore recommend to
have the results checked (e.g. plausibility tested) by skilled personnel before
consequential actions are taken based on the results.
B80IB01 9
2 Safety Instructions
2.1.4 Disposal
2.1.5 Returns
For repairs send the cleaned AMVn instrument to your Anton Paar
representative. Only return the instrument together with the filled out
"Maintenance/Error Report" and the "Standard Maintenance Contract". Find
the applicable forms on the Anton Paar homepage (www.anton-paar.com).
Observe and adhere to your national safety regulations for handling the
measured samples (e.g. use of safety goggles, gloves, respiratory protection
etc.).
Only store the minimum required amount of sample, cleaning agents and
other inflammable materials near the AMVn.
Make sure that the setup location is sufficiently ventilated. The environment
of AMVn must be kept free of inflammable gases and vapors.
Connect AMVn to the mains via a safety switch located at a safe distance
from the instrument. In an emergency, turn off the power using this switch
instead of the power switch on AMVn.
10 B80IB01
2 Safety Instructions
When handling caustic fluids, acids, easily inflammable fluids etc. use the
required protective clothing (protective gloves, safety goggles). If the samples in
the capillary are heated up to measuring temperatures of over 70 C after filling,
the thermal expansion of the fluid in the glass capillary may result in the
unintentional opening of the capillarys sealing caps.
During the activation of the AMVn instrument, the capillary block moves into the
physical end position (initialization). The capillary block should not be touched
during this movement, in order to avoid possible clamping or displacement of the
zero position. The capillary block should only be moved by hand when the
instrument is inactive.
B80IB01 11
3 AMVn - An Overview
3 AMVn - An Overview
Anton Paar GmbH thanks you for buying AMVn, the global vanguard measuring
instrument for the automatic, high-precision viscosity determination of low viscous
substances. It provides you with measurement solutions of utmost precision in a
very broad viscosity and temperature measurement range.
Choose various measurement methods and systems that accord with your
measurement applications.
You can print and display measurement results with sample names and
measurement system data. Only the most recent measurement result is saved in
the AMVn instrument.
The optionally delivered, fully automatic sample changers of Anton Paar GmbH
automatically fill the AMVn capillaries with samples. Between measurements the
capillaries are automatically cleaned with two cleaning agents, and consecutively
dried in air.
Our trained Anton Paar GmbH personnel always welcome your requests and will
gladly provide you with additional offers.
12 B80IB01
4 Unpacking and Checking the Supplied Items
AMVn was tested and packed carefully before shipment. However, damage may
occur during transport.
Keep the packaging material (box, foam piece, transport protection) for
possible returns and further questions from the transport- and insurance
company.
Compare the supplied parts to those noted in the table to check the delivery
for completion.
If a part is damaged, contact the transport company and your Anton Paar
representative.
The following tables list all supplied items contained in your order. Every
instrument is delivered as a unit.
1 Instruction manual
German or English
1 Mains cable:
Euro- or 52112
GB- or 61865
US- or 52656
PRC 27011
1 Temperature tube 22109
B80IB01 13
4 Unpacking and Checking the Supplied Items
A measuring system set is delivered in a box, including all necessary parts for
a measurement with AMVn. Every measuring system set includes the measuring
system that accords with your order.
Find a listing of all measuring system sets and all parts contained in the box in the
tables below. You can order all registered parts either in a set (Chapter 4.2.2.1)
or separately, in reference to the material number listed on the right (Chapter
4.2.2.2).
14 B80IB01
4 Unpacking and Checking the Supplied Items
5 Syringe, 5 mL 63130
1 Funnel
for 1.5 mm balls or 20743
for 2.5 mm and 3.0 mm balls 20742
1 Filling adapter incl. O-rings 63390
4 Replacement-O-rings Viton
(Chapter 10.5)
O-ring viton 6.4x1.9 mm FPM 75 23726
(for filling adapter with engraved
marking ring)
oder
O-ring viton 6.5x1.5 mm FPM 80 65555
(for filling adapter without engraved
marking ring)
1 O-ring tool 24943
B80IB01 15
4 Unpacking and Checking the Supplied Items
1 Ball dispenser
for 1.5 mm balls or 63604
for 2.5 mm and 3.0 mm balls 63605
10 Tungsten carbide-cobalt balls 3.0 mm 70116
for the viscosity measuring range
extension of the 4.0 mm capillary
1 Uncalibrated capillary:
1.6 mm 67605
1.8 mm 63180
3.0 mm 63181
4.0 mm 63182
Disposable syringes:
1 1 mL Luer 68015
100 2 mL Luer 6771
100 5 mL Luer 6772
1 VisioLab Windows software 5034
16 B80IB01
5 Functional Components
5 Functional Components
Information:
The interfaces COM 1, COM 3, PC and S-Bus are only necessary if the
VisioLab Windows software is used.
Density meters are connected to COM 1.
Sample changers are either connected to COM 3 (SPV and SP3-V) or to
the S-BUS interface (SP-1m and SP-3m).
B80IB01 17
5 Functional Components
E
D A ... Sealing cap
B ... Capillary
C C ... Glass knob
D ... Filling adapter
E ... Plug
B F ... 8-digit serial number of capillary
F G ... Ball
G
A
Fig. 5. 3 Measuring system set
Keyboard use:
The keyboards function keys (F1 F5) accord with the function keys of AMVn.
Use these to choose the menu and/or input field you wish to access. An external
keyboard enables a much faster and easier input.
18 B80IB01
6 Putting AMVn into Operation
1. Set up AMVn on the lab desk and level it off with the adjustable feet and the
built-in bubble level. Make sure all four feet touch the lab desk.
Caution:
Before activating the AMVn instrument make sure that the correct line voltage
is applied (85 V to 264 V, 50 Hz to 60 Hz). If large voltage fluctuations are to
be expected, we recommend using a constant-voltage source (UPS).
2. Connect the power inlet of the AMVn instrument to the mains using the
delivered power cord.
3. Activate AMVn with the power switch located on its rear side. The green
display light signals that the power is on.
Warning:
After its activation, AMVn independently runs through the coil- and zero
position initialization. In the course of this the capillary block first moves to its
final position before it remains in its home position leaning backwards at
20 . The capillary block should not be touched during this movement, in order
to avoid possible clamping or displacement of the zero position. The capillary
block should only be moved by hand when the power of the instrument is
switched off.
4. After the successful initialization you will see the following reading on the
display:
"actual SETTINGS" displays the settings of the last measurement. Browse with
F3 or the down button to check the following:
Sample: sample name, remark, temperature, density
Method: the last method used
Meas. system: the measuring system used for the last measurement
Instr. Settings: instrument constant K2, temperature equilibration mode
B80IB01 19
6 Putting AMVn into Operation
Before starting a measurement, fill the capillary and mount the measuring system
in the capillary block.
1. Hold the capillary (B) vertically and place the funnel (A) on
the capillary opening (Fig. 6. 1).
2. Use the delivered plastic tweezers to introduce a ball into the
funnel.
(B)
Information:
Never touch the balls with your fingers, as these need to be completely
clean to function correctly. Only use clean capillaries and clean or new
balls.
You can also use an optionally available ball dispenser to introduce the
ball.
20 B80IB01
6 Putting AMVn into Operation
Warning:
When handling caustic fluids, acids, easily inflammable fluids etc., use the
required protective clothing (protective gloves, safety goggles).
Always mount the temperature tube and the protective cap (Chapter 6.2.6) before
you start a measurement.
1 ... Temperature
tube
2 ... Protective cap
Screw the temperature tube on to the rear side of the capillary block. For
functionality reasons it should always stay attached to the capillary block and
should only be unscrewed for cleaning.
B80IB01 21
6 Putting AMVn into Operation
Before mounting the filled capillary, you need to activate AMVn and wait until the
self-test is concluded (Chapter 6.1).
Caution:
Make sure that the self-test is concluded and no measurement program has
started, so that the capillary block does not start any surprising movements.
Do not push too hard when mounting the capillary, because the glass could
break. Do not use excessive force!
1. Carefully insert the capillary into the capillary block, starting from the front.
2. Turn the capillary so that the glass knob easily slips into the corresponding
recess of the capillary block opening.
As soon as the glass knob has slid into the opening, completely insert the capillary
into the capillary block until the red silicone O-ring of the adapter is no longer
visible and you meet a resistance.
1. After mounting a capillary, attach the protective cap (2, Fig. 6. 4) in a straight
position in the front of the capillary block.
2. Fix the protective cap by turning it clockwise.
Leave the protective cap on the capillary block during the measurement and only
remove it once you change the capillary.
Hot surface:
When attaching or removing the temperature tube and the protective cap at
high measuring temperatures you might be operating in the direct vicinity of
hot surfaces. Therefore only touch the capillary block and the capillary with
adequate protective gloves (Chapter 2.2) or wait until the capillary block has
cooled down.
Warning:
If the samples in the capillary are heated up to measuring temperatures up to
135 C, the thermal expansion of the fluid in the glass capillary may result in
the unintentional opening of the capillarys sealing caps. It is imperative to use
the temperature tube and the protective cap.
22 B80IB01
7 Measurement
7 Measurement
Before starting a measurement, set up AMVn according to your wishes.
Scroll through all items with the F3 <down button> and make sure all settings
always listed on the right are correct before starting the measurement:
Information:
A new method or measuring system can only be entered in the submenu
"Setup Measurement" in "MENU".
Individual settings of the temperature equilibration mode are only possible
in the submenu "Setup Instrument" - "Temperature equilibration" .
Keep in mind that only measuring systems that apply to the chosen
method are displayed.
B80IB01 23
7 Measurement
*** Start *** starts the measurement, for this option press F5 <ENTER>.
If the set temperature ("set T:") does not accord with the actual temperature ("act
T:"), the instrument holds up the temperature equilibration of the sample until the
display reading "!Temp. diff >!" disappears. This occurs at differences smaller
than 0.05 C.
The sample thermostatting takes place immediately after the thermostatting of the
capillary block. You can find settings for this in Chapter 8.1.2.
Every start and stop signal is accompanied by a beeping sound. After the second
measurement the actual and desired deviation ("var Coef:") is displayed. After a
successful temperature equilibration, the measuring instrument starts the actual
measurement.
24 B80IB01
7 Measurement
The display shows the actual measuring angle, the current number of actual
repetition, and, from the third measurement onwards, the determined viscosity.
RUN 11:25:12
Time (s) set T : 20.00C
to Start: 2.65 act T : 20.00C
Runtime : 11.34 set ang.: 70
to End : 0.63 act ang.: 70.0
Visc. : 1.002 mPa.s rep :
Stop Show Strtd
Information:
Always enter an even number of repetitions, because viscosity is always
determined from two repetitions.
For the viscosity calculation a maximum of 20 repetition periods is used. If you
want more than 20 repetitions, you have the further option of connecting
AMVn to a PC. The AMVn Visiolab Windows software allows a nearly
unlimited amount of repetitions, which is only one of its many benefits.
EVALUATION 11:23:56
Sample:Sample1 Testlauf1
dyn. Visco Mean : 1.0019 mPa.s
kin. Visco Time : 11.35 s
Infos St.Dev :0.00006 mPa.s
Rep.times Var.Co : 0.01 %
ESC Print
B80IB01 25
7 Measurement
Sample: Water
Remark:
Method: Standard 1.6
Angle: 70 deg Repetitions: 4
CapSys: 1.6/1.500 mm
Density : 0.9982 g/cm3
act. Temp: 20.00 C
MeasSystem: 15844194-70A
K1 : 0.984e-02
26 B80IB01
7 Measurement
Caution:
Do not leave any samples in the measuring system after you have
finished the measurement.
Rinse the measuring system with a suitable cleaning agent.
Only use cleaning agents that are compatible with the materials (Chapter
10.4).
Before you dry the capillary with compressed air, remove the ball.
B80IB01 27
8 AMVn Firmware Update
In "Setup Instrument" you can view or change all settings concerning AMVn.
With F5 <Enter> you can access each of the following submenus, with F1 <Back
or <ESC> you return to the menu.
"Date" Date
"Time" Time
"Zero adjust" Zero adjustment
"Temperature equilibration" Temperature equilibration
"Instrument Constant K2" Instrument constant: preset
"Default Settings" Default settings
"Configuration Printer" Printer configuration
"Info" Information on Firmware Version, serial number of AMVn and your
Anton Paar GmbH contact address
"Service Utilities" password-protected service menu for authorized
service personnel of Anton Paar GmbH
"Software Update" Update instrument software
Change date and time with the arrow keys and confirm the entry with <Enter>.
ESC
28 B80IB01
8 AMVn Firmware Update
You can choose between two different modes: constant oder auto mode. The
active mode is highlit and marked with an asterisk (*).
Choose "constant mode" if you know how long your sample will take to reach
measuring temperature.
F2, F3, F4 arrow keys: adjust waiting periods until measurement start
F5 <Enter>: accept changes
F1 <ESC>: discard changes
ESC Edit
B80IB01 29
8 AMVn Firmware Update
In the submenu "Default Settings" you can reset user-defined settings to factory
default values.
In the submenu "Configuration Printer" you can change your printer settings.
ESC
Press F4 :
Delays are necessary for printers without a receive buffer. In case characters are
missing in your printout, increase the delay times.
The parameters of the printer interface on the AMVn instrument are pre-adjusted
and cannot be changed:
baudrate 9600, 7 data bits, even parity, 1 stop bit, no handshake
30 B80IB01
8 AMVn Firmware Update
In the submenu "Software Update" you can install new instrument software
versions. Further information will be included with your update.
Whenever applicable, contact your local Anton Paar representative for possible
firmware updates.
AMVn is already delivered pre-adjusted. In case you observe evident run time
differences between even and uneven repetitions, you can compensate these
with the zero point adjustment.
Before starting a zero point adjustment, make sure that the instrument is placed
on a level, stable surface. If necessary, level AMVn using the adjustable feet and
the built-in bubble level.
F3 <Meas>: starts the zero point adjustment with the method "Zero Adjust"
F5 <Edit>: changes the zero point adjustment method
After the selected angle is measured, AMVn automatically raises the angle by 1
degree and starts a new run. This second run substantially raises the accuracy of
the zero point adjustment.
B80IB01 31
8 AMVn Firmware Update
Menu Print
With F4 <Print> you can print the content of the highlit menu.
8.2.1 Method
A method involves the measuring angle, the number of repetitions, and the
measuring system used for a measurement.
Information:
When using more than one method it is advisable to assign slightly different
names. This might prove helpful later in matching them to the applications.
32 B80IB01
8 AMVn Firmware Update
The option F5 <Overw.> (Overwrite) is only available after you edited a previously
existing method.
B80IB01 33
8 AMVn Firmware Update
The option F5 <Overw.> (Overwrite) is only available after you edited a previously
existing measuring system.
34 B80IB01
8 AMVn Firmware Update
In the third submenu of "MENU" "Print Configuration", you can print the
configuration of AMVn.
ESC
You can find the settings for the printer interface in Chapter 8.1.4.
Example of a printout
(numbers and values are different on every instrument):
AMVn Microviscometer
SW-Version V1.70
Date: 2006-06-10, Time: 09:12:05
Serial Number: 409247
Zero adjust: 27592
Runtime-Limit: 250 s
Instrument-Constant: 1.000
ADC : A = 0.9928
Pt100-factors: KA= 0. 0568
KB= 0.0035
Coil 1: Ampl= 25, Phase= 37, U= 138
Coil 2: Ampl= 21, Phase= 33, U= 152
Printer on COM2
DelayChar/Char: OFF; Line/Line: 1.0s
Settings: 9600 / 7 / even / 1
B80IB01 35
9 Calibration of Measuring Systems
There are calibrated and uncalibrated measuring system sets (Chapter 4.2.2) and
calibrated and uncalibrated capillaries:
When using a new or alternative ball set the calibration constant only needs to
be redefined in case the measuring deviation is above tolerance limit (0.3 %) and/
or the ball set features a different batch number. Read the batch number on the
sticker attached to your ball set.
F2, F3: browse all stored measuring systems and check all values
F4 <New>: calibrate a new measuring system
F5 <Enter>: choose the measuring system you wish to recalibrate
1/05: the first of five stored measuring systems is displayed
36 B80IB01
9 Calibration of Measuring Systems
1. Press F4 <New>.
2. Enter all values:
3. Fill the capillary with the suitable viscosity standard fluid (Chapter A.1).
4. Press F5 <Start> to start the calibration.
The calibration procedure runs automatically.
5. After measurement conclusion press:
F2, F3: view the detailed evaluations
F5 <Print>: print the result
F4 <Save>: save to use the calibration constant in measurements.
Information:
If you do not save the calibration constant K1, you lose all calibration results.
B80IB01 37
10 Maintenance
10 Maintenance
Clean AMVn and its accessories regularly.
Caution:
Do not leave any samples in the measuring system after finishing the
measurement.
Rinse the measuring system with a suitable cleaning agent.
Only use cleaning agents that are compatible with the materials (Chapter
10.4).
Before you dry the capillary with compressed air, remove the ball.
Clean the filling adapter regularly to avoid clotting or the ball getting stuck.
1. Detach the filling adapter from the capillary with gentle turns. Do not use
excessive force as this could break the capillary.
2. Rinse the filling adapter with a cleaning agent.
3. Rinse the filling adapter with a volatile solvent, e.g. highly concentrated
alcohol, to accelerate the drying procedure after cleaning.
4. Afterwards dry the filling adapter, e.g. with compressed air (max. 0.5 bar).
38 B80IB01
10 Maintenance
Use a soft cloth and warm water to clean the casing and display.
Check the capillary block for pollution and clean it regularly, especially at the
thermostat and protective cap fixations.
Never remove the warning signs on the capillary block. If these come loose,
they need to be attached again.
The following items have contact to the measured samples and cleaning agents:
Item Material
Capillary Borosilicate glass
Ball Steel 1.4125 (AISI 440C)
Filling adapter PCTFE
O-ring Viton
O-ring Kalrez
LUER cap PCTFE
LUER plug PCTFE
B80IB01 39
10 Maintenance
The filling adapter already contains the O-rings at delivery. Always replace both
interior O-rings at the same time.
Viton
Silicone
Fig. 10. 5 O-rings for the filling adapter without engraved marking ring
The O-rings on the inside are made of viton and have the dimension
6.5 x 1.5 mm FPM 80. They have contact to the sample and have a sealing
function.
Viton or
Kalrez
O-rings
Engraved
marking ring
Silicon e
Fig. 10. 6 O-rings for the filling adapter with engraved marking ring
The filling adapter with engraved marking ring contains O-rings of the dimension
6.4 x 1.9 mm FPM 75. In this filling adapter with engraved marking ring O-rings
made of viton and made of Kalrez can be used.
Caution:
The filling adapter without engraved marking ring and the filling adapter with
engraved marking ring are NOT compatible.
The O-rings have another dimension (see Chapter 4.2.2 and Chapter 4.2.3).
The red, outer O-ring is made of silicone and does not usually need to be
exchanged. The inner O-rings are sealing rings. If the O-rings need to be
replaced, first remove them from the adapter using the O-ring tool. Then carefully
insert the new O-rings.
40 B80IB01
11 Technical Data
Time measuring range: 0 - 250 s (999 s *)
Resolution: 0.001 sec
Accuracy: <0.002 sec
Weight: 15 kg (150 N)
Ambient temperature: 15 to 35 C
***) typical value for the range, where the calibration constant was determined
41 B80IB01
Appendix A: Viscosity
Appendix A: Viscosity
For a precise viscosity determination, a suitable calibration standard fluid is
required for the calibration of the capillaries. A calibration constant needs to be
determined and/or entered for every capillary (Chapter 9).
Information:
The calibration procedure has to be repeated periodically, depending on the
specific accuracy requirements of your laboratory.
Due to the different measuring ranges of the capillaries, you need different
viscosity standard fluids. You can order these viscosity standard fluids at Anton
Paar GmbH.
The table below shows general values for the different measuring systems.
The best results are achieved if you calibrate a measuring system at the usual
measuring temperature and in its viscosity range.
(e.g. if you measure approx. 50 mPa.s with a 3.0 measuring system at 100 C,
use e.g. the viscosity standard fluid DKD 10000. At 100 C this standard has
approx. 57 mPa.s).
A custom-tailored calibration is possible. You can use any stable sample with
known dynamic viscosity and density as a viscosity standard fluid.
B80IB01 42
Appendix A: Viscosity
For every measuring angle you plan to use, first determine the calibration
constant K1.
N
K 1 = -----------------------------------
t1(K N )
Information:
The calibration constant is different at every angle and with every
capillary.
A calibration datasheet with pre-determined calibration constants for the
stated angles is enclosed with every calibrated capillary.
If a ball is exchanged, K1 only needs to be readjusted if the measuring
deviation is above the tolerance limit (0.3 %). Readjust the constant if you
use balls with different batch numbers. The batch number is written on the
ball vessel.
The viscosity of the standard fluid should fall within the viscosity range of
the measured samples.
The dynamic viscosity of the sample is calculated from the calibration constant
K1 of the measuring system, the rolling time t1 and the density difference
between ball and sample.
= K1 * (K - P) * t1
The serial number and the ball density of the measuring system are known (steel
ball: K = 7.85 g/cm3, tungsten carbide-cobalt ball: K = 15 g/cm3). The density of
the sample, often a known number, must also be entered.
If there is no information on the density of the sample to be measured, you can
order a manual density meter DMA 35N from Anton Paar GmbH, which measures
the density with an accuracy of +/- 0.001 g/cm3.
Caution:
Choose the angle of your measurement in such a way that the ball rolling
times do not drop below 10 sec. Otherwise turbulence is caused in the
capillary and a seemingly higher viscosity is read.
43 B80IB01
Appendix B: Extension of the Measuring Range
A measuring range extension through an increase in run time from 250 to 999 sec
quadruples the maximum measuring range.
The run time increase can only be defined by means of a "remote" command from
the PC.
Proceed as follows:
AMVn Microviscometer
SNo: 80074021 SW_Ver: V1.70
SW-Version V1.70
Date: 07/21/2006, Time: 11:12:05
Serial Number: 80074021
Zero adjust: 27471
Runtime-Limit: 999 s
Instrument-Constant: 1.000
ADC : A = 0.9928
Pt100-factors: KA= 0. 0568
KB= 0.0035
Coil 1: Ampl= 31, Phase= 39, U= 139
Coil 2: Ampl= 33, Phase= 38, U= 144
Printer on COM2
DelayChar/Char: OFF; Line/Line: 0.5s
Settings: 9600 / 7 / even / 1
B80IB01 44
Appendix B: Extension of the Measuring Range
Before calibrating the measuring system 4.0 with tungsten carbide-cobalt balls,
read Chapter 9 and proceed accordingly.
Proceed as follows:
Save the calculated calibration constant for the measuring system 4.0.
45 B80IB01
Start
B80IB01
Initialization
Method: Name
Angle
F2 F3 Repetitions
Capillary System
Temp. Equi-Mode
F1 F1 F2
Menu Setup Instrument Date
F1 F5 F5 Time
Zero adjust F1
Temperature equilibration Setup Temp. Equilibration
Instrument Constant K2 F5
Default Settings
Configuration Printer
Appendix C: Menu Tree Firmware
Info
Service Utilities
Software Update
46
Appendix C: Menu Tree Firmware Structure
47
F1 F1 F5
Setup Measurement Method Setup: Measure-Method
F5 Print Methods
F4
F1 F5
Measuring System Setup Temp. Equilibration
F2 F3 Print Measuring Systems
F4
F1
Meas. System: Calibrate Setup: Measure-MeasSystem-Calib
F1 F5
Print Configuration
F5
F1
Evaluation Dyn. Visco.: Mean
F4 Time
St.Dev.
Var. Co.
Appendix C: Menu Tree Firmware Structure
B80IB01