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LAMPIRAN

1. Pembuatan larutan
- NaOH 6M 250 ml - Na2CO3 2M 100 ml
𝑀.𝑀𝑟.𝑉 𝑀.𝑀𝑟.𝑉
Massa= Massa =
1000 1000
6.60.250 2.106.100
= =
1000 1000

= 60 gram = 21,2 gram
- H2SO4 3M 100 ml 98% - HNO3 2M 100ml 65%
𝜌.10.% 𝜌.10.%
M = M =
𝑀𝑟 𝑀𝑟
1,8 .10.98 1,4.10.65
= = 18 M = = 12,64 M
98 72

V1.M1 = V2.M2 V1.M1 = V2.M2
3M. 100ml= 18M. V2 2M. 100ml= 12,64 M. V2
V2= 16,67 ml V2= 15,82 ml

2. Pembuatan larutan induk Fe(NO3)3 pada spektrofotometri
1000 ppm
𝑚𝑔
ppm= 𝐿
𝑚𝑔
1000 ppm = 0,025𝐿

mg= 25 mg
𝑀𝑟𝐹𝑒(𝑁𝑂3)3.9𝐻2𝑂
massa yang harus ditimbang= 𝑥 𝑔𝑟𝑎𝑚 𝑝𝑝𝑚
𝐴𝑟𝐹𝑒
403,9
= 55,85x 0,025 g = 0,18079 gram

3. Pengenceran larutan standar
- Fe(NO3)3 100 ppm 25 ml - Fe(NO3)3 25 ppm 25 ml
ppm. V1= ppm. V2 ppm. V1= ppm. V2
100 𝑝𝑝𝑚 .25 𝑚𝑙 25 𝑝𝑝𝑚 .25 𝑚𝑙
V1= = 2,5 ml V1= = 12,50 ml
1000 𝑝𝑝𝑚 50 𝑝𝑝𝑚

- Fe(NO3)3 75 ppm 25 ml - Fe(NO3)3 10 ppm 25 ml
ppm. V1= ppm. V2 ppm. V1= ppm. V2
75 𝑝𝑝𝑚 .25 𝑚𝑙 10 𝑝𝑝𝑚 .25 𝑚𝑙
V1= = 18,75 ml V1= = 10 ml
100 𝑝𝑝𝑚 25 𝑝𝑝𝑚

- Fe(NO3)3 50 ppm 25 ml
ppm. V1= ppm. V2

25 0.218= 0.35 y = 0.25 𝑚𝑙 V1= = 16. Penentuan kadar Fe dalam water glass Hukum Lambert Beer 0.9739 0.26 ppm 5.0027x + 0.05 0 0 20 40 60 80 100 120 y = 0.0000 = 55.3 R² = 0. Pemisahan dan pemurnian NaCl .0002−2.2 y 0. pemakaian AgNO3= 10. Penambahan dengan HNO3 𝑚𝑎𝑠𝑠𝑎 𝑎𝑤𝑎𝑙 – 𝑚𝑎𝑠𝑠𝑎 𝑠𝑒𝑡𝑒𝑙𝑎ℎ 𝑝𝑒𝑚𝑎𝑛𝑎𝑠𝑎𝑛 %Fe hilang = x 100% 𝑚𝑎𝑠𝑠𝑎 𝑎𝑤𝑎𝑙 7.0000−3.0027x + 0.1 0. Penambahan dengan aquadest 𝑚𝑎𝑠𝑠𝑎 𝑎𝑤𝑎𝑙 – 𝑚𝑎𝑠𝑠𝑎 𝑠𝑒𝑡𝑒𝑙𝑎ℎ 𝑝𝑒𝑚𝑎𝑛𝑎𝑠𝑎𝑛 %NaCl hilang = x 100% 𝑚𝑎𝑠𝑠𝑎 𝑎𝑤𝑎𝑙 7.15 Linear (y) 0. Standarisasi larutan AgNO3 V.3% 6.0499 0. NaCl= 0.1292 = 𝑥 100% 7.1942 = 𝑥 100% 7.0499 0.8 ml V.0499 X= 62.67 ml 75 𝑝𝑝𝑚 4. 50 𝑝𝑝𝑚 .0027x + 0.1 N .66% . Penentuan kadar NaCl dalam sampel campuran .0002 = 63.

125 gram massa Cl Kadar (%) Cl sampel= × 100% massa sampel 0.092 M atau 0. 0.025 gram V.0076 L = 0.8 ml.V titrasi = 0.5% 1.V1. 1= M2.labu ukur 50 ml massa Cl sampel = massa Cl × = 0.pipet 10ml = 0.1 M .=[AgNO3].0926 M.= mol Cl.5 g/mol =0.125 gram = × 100 % =12..0007 mol .ek1=M2.0007 mol Massa Cl. Kadar NaCl Mol Cl.V2.ek2 0.1M.025 × V.1 M2= 0. Ar. 10 ml. 10. M1. Cl- = 0.0000 gram Dokumentasi Praktikum Filtrasi water glass Cawan+sampel campuran Cawan kosong . 35.

Pemanasan filtrat Pendinginan Hasil pendinginan Evaporasi water glass Penyaringan1:sampel+aquadest Penyaringan2 .