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Hydroxycitric acid is obtained by aconitic acid with oxidation, which is obtained by citric acid
with dehydration.
The optimum conditions of aconitic acid and hydroxycitric acid are studied separately.
- mol citric acid reacts with 56% sulfuric 270 ml to obtain aconitic acid after 7 - hour reflux in
140°C. Its' m. p. is 186°C.
Because waste acid and unreacted citric acid are used cyclically, reclaimed citric acid is 28% and
reclaimed sulfuric acid is 65%.
The optimum condition for hydroxycitric acid is that 2 mol oxidant reacts with 1 mol aconitic
acid in 50 for 7-hour, and obtains hydroxycitric acid, whose yield is about 80%.