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Tabel 2

Volume tiosulfat (mL) Volume terkoreksi Kadar vitamin C


Bahan
Awal Akhir Terpakai (mL) (mg)
Blanko 20,00 30,30 10,30 - -
Sari Buah 1 20,00 27,30 7,40 3.00 26,40
Sari Buah 2 20,00 25,20 5,20 5,10 44,88
Sari Buah 3 20,00 25,84 5.84 4,46 39,25
Rata -Rata 36,85
Contoh perhitungan :

V terpakai = V akhir – V awal


= 30,30 mL – 27,30 mL
= 7.30 mL
V terkoreksi = V blanko – V terpakai
= 10,30 mL – 7.30 mL
= 3,00 mL
Kadar vit C = V terkoreksi x 8,8 mg/mL
= 3,00 ml x 8,8 mg/mL
= 26,40 mL

Tabel 1 Data hasil penentuan kadar vitamin c tablet


Volume tiosulfat (mL) Volume terkoreksi Kadar vitamin C
Bahan
Awal Akhir Terpakai (mL) (mg)
Blanko 19,00 29.30 10.30 - -
Tablet 1 16,00 22,50 6.50 3.80 33.44
Tablet 2 15.10 19.80 4.70 5.60 49.28
Tablet 3 26.10 31.30 5.20 5.10 44.80
Rata -Rata 42,51
Contoh perhitungan:
Volume terpakai = volume akhir - volume awal
= 19,8 mL – 15,1 mL
= 4,7 mL
Volume terkoreksi = volume terpakai blanko – volume terpakai sampel
= 10,3 mL – 4,7 mL
= 5,6 mL
Kadar vitamin C = volume terkoreksi x 8,8 mg/mL
= 5,6 mL x 8,8 mg/mL
= 49,28 mg/mL
LAMPIRAN

Reaksi
C6H8O6 + I2 C6H6O6 + 2HI
I2 + 2Na2S2O3 2NaI + Na2S4O6
1 mL Tiosulfat = .... ? mg Vitamin C

mmol Na2S2O3 = N X V
= 0,1 N X 1 mL Vit. C
= 0,1 mmol

1
mmol I2 = 2 X mmol Na2S2O3
1
= 2 X 0,1 mmol
= 0,05 mmol

mmol C6H8O6 = mmol I2


= 0,05 mmol

m
mmol C6H8O6 =
Mr
m
0,05 mmol =
176 mg/mmol
m = 8,8 mg